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Polymorphism in the pharmaceutical industry [[electronic resource] /] / edited by Rolf Hilfiker
| Polymorphism in the pharmaceutical industry [[electronic resource] /] / edited by Rolf Hilfiker |
| Pubbl/distr/stampa | Weinheim, : Wiley-VCH, c2006 |
| Descrizione fisica | 1 online resource (436 p.) |
| Disciplina | 660.28 |
| Altri autori (Persone) | HilfikerRolf |
| Soggetto topico |
Crystallography
Solid state chemistry Chemical engineering Pharmaceutical chemistry |
| ISBN |
1-280-72340-8
9786610723409 3-527-60788-9 3-527-60772-2 |
| Formato | Materiale a stampa  |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Polymorphism; Contents; Preface; List of Contributors; 1 Relevance of Solid-state Properties for Pharmaceutical Products; 1.1 Introduction; 1.2 Drug Discovery and Development; 1.3 Bioavailability of Solids; 1.4 Phases of Development and Solid-state Research; 1.4.1 Salt Selection; 1.4.2 Polymorph Screening; 1.4.3 Crystallization Process Development; 1.4.4 Formulation; 1.4.5 Method Development; 1.5 Solid-state and Life Cycle Management; 1.6 Conclusions; References; 2 Thermodynamics of Polymorphs; 2.1 Introduction; 2.2 Structural Origin of Polymorphism; 2.3 Thermodynamic Theory of Polymorphism
2.4 Thermodynamic Relationship Between Polymorphs: Enantiotropy and Monotropy2.4.1 Energy-Temperature Diagrams; 2.4.2 Pressure-Temperature Diagrams; 2.4.3 Inversion of Polymorphic Behavior; 2.5 Rules to Predict Thermodynamic Relationships Between Polymorphs; 2.5.1 Heat of Transition Rule; 2.5.2 Heat of Fusion Rule; 2.5.3 Entropy of Fusion Rule; 2.5.4 Heat Capacity Rule; 2.5.5 Density Rule; 2.5.6 Infrared Rule; 2.6 Relative Thermodynamic Stabilities of Polymorphs; 2.7 Crystallization of Polymorphs; 2.7.1 Nucleation of Polymorphs; 2.8 Introduction to Solvates and Hydrates 2.8.1 Thermodynamics of Hydrates2.9 Summary; References; 3 Characterization of Polymorphic Systems Using Thermal Analysis; 3.1 Introduction - Scope of the Chapter; 3.2 Use of Differential Scanning Calorimetry for the Characterization of Polymorphs; 3.2.1 Principles of DSC in the Context of Polymorphism; 3.2.2 Examples of the Uses of DSC: Characterization of Drugs, Excipients and Dosage Forms; 3.2.3 Further Uses of DSC; 3.3 Combined Approaches; 3.3.1 Multi-instrument Approaches; 3.3.2 Thermal and Crystallographic Studies; 3.3.3 Interfaced Techniques 3.4 Additional Thermal Methods for the Study of Polymorphism3.4.1 Thermogravimetric Analysis; 3.4.2 Thermal Microscopy; 3.4.3 Heat of Solution Studies; 3.4.4 Modulated Temperature DSC; 3.4.5 High-speed DSC; 3.4.6 Microthermal Analysis; 3.4.7 Thermally Stimulated Current; 3.5 Conclusions; References; 4 Solid-state NMR Spectroscopy; 4.1 Introduction; 4.1.1 Basics of Solid-state NMR; 4.2 Applications; 4.2.1 Identification; 4.2.2 Selectivity; 4.2.3 Mobility and Dynamics; 4.2.4 Quantitation of Forms; 4.3 Conclusions; References 5 Vibrational Spectroscopic Methods in Pharmaceutical Solid-state Characterization5.1 Introduction; 5.2 Mid-infrared, Raman and THz Spectroscopy: Basic Comparison of Theory, Instrumentation and Sampling; 5.2.1 Basic Theory; 5.2.2 Instrumentation Brief; 5.2.3 Sampling; 5.2.3.1 Raman Sampling [20, 23, 30]; 5.2.3.2 Mid-infrared Sampling [30, 39-41]; 5.2.3.3 THz Spectroscopy Sample Presentation; 5.3 Changes of State and Solid-state Effects on Infrared and Raman Spectra; 5.3.1 Introduction; 5.3.2 Spectra of Gases, Liquids and Solutions; 5.3.3 Hydrogen Bonding 5.3.4 Amine Salts (including Amino Acids) |
| Record Nr. | UNINA-9910144275103321 |
| Weinheim, : Wiley-VCH, c2006 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Polymorphism in the pharmaceutical industry [[electronic resource] /] / edited by Rolf Hilfiker
| Polymorphism in the pharmaceutical industry [[electronic resource] /] / edited by Rolf Hilfiker |
| Pubbl/distr/stampa | Weinheim, : Wiley-VCH, c2006 |
| Descrizione fisica | 1 online resource (436 p.) |
| Disciplina | 660.28 |
| Altri autori (Persone) | HilfikerRolf |
| Soggetto topico |
Crystallography
Solid state chemistry Chemical engineering Pharmaceutical chemistry |
| ISBN |
1-280-72340-8
9786610723409 3-527-60788-9 3-527-60772-2 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Polymorphism; Contents; Preface; List of Contributors; 1 Relevance of Solid-state Properties for Pharmaceutical Products; 1.1 Introduction; 1.2 Drug Discovery and Development; 1.3 Bioavailability of Solids; 1.4 Phases of Development and Solid-state Research; 1.4.1 Salt Selection; 1.4.2 Polymorph Screening; 1.4.3 Crystallization Process Development; 1.4.4 Formulation; 1.4.5 Method Development; 1.5 Solid-state and Life Cycle Management; 1.6 Conclusions; References; 2 Thermodynamics of Polymorphs; 2.1 Introduction; 2.2 Structural Origin of Polymorphism; 2.3 Thermodynamic Theory of Polymorphism
2.4 Thermodynamic Relationship Between Polymorphs: Enantiotropy and Monotropy2.4.1 Energy-Temperature Diagrams; 2.4.2 Pressure-Temperature Diagrams; 2.4.3 Inversion of Polymorphic Behavior; 2.5 Rules to Predict Thermodynamic Relationships Between Polymorphs; 2.5.1 Heat of Transition Rule; 2.5.2 Heat of Fusion Rule; 2.5.3 Entropy of Fusion Rule; 2.5.4 Heat Capacity Rule; 2.5.5 Density Rule; 2.5.6 Infrared Rule; 2.6 Relative Thermodynamic Stabilities of Polymorphs; 2.7 Crystallization of Polymorphs; 2.7.1 Nucleation of Polymorphs; 2.8 Introduction to Solvates and Hydrates 2.8.1 Thermodynamics of Hydrates2.9 Summary; References; 3 Characterization of Polymorphic Systems Using Thermal Analysis; 3.1 Introduction - Scope of the Chapter; 3.2 Use of Differential Scanning Calorimetry for the Characterization of Polymorphs; 3.2.1 Principles of DSC in the Context of Polymorphism; 3.2.2 Examples of the Uses of DSC: Characterization of Drugs, Excipients and Dosage Forms; 3.2.3 Further Uses of DSC; 3.3 Combined Approaches; 3.3.1 Multi-instrument Approaches; 3.3.2 Thermal and Crystallographic Studies; 3.3.3 Interfaced Techniques 3.4 Additional Thermal Methods for the Study of Polymorphism3.4.1 Thermogravimetric Analysis; 3.4.2 Thermal Microscopy; 3.4.3 Heat of Solution Studies; 3.4.4 Modulated Temperature DSC; 3.4.5 High-speed DSC; 3.4.6 Microthermal Analysis; 3.4.7 Thermally Stimulated Current; 3.5 Conclusions; References; 4 Solid-state NMR Spectroscopy; 4.1 Introduction; 4.1.1 Basics of Solid-state NMR; 4.2 Applications; 4.2.1 Identification; 4.2.2 Selectivity; 4.2.3 Mobility and Dynamics; 4.2.4 Quantitation of Forms; 4.3 Conclusions; References 5 Vibrational Spectroscopic Methods in Pharmaceutical Solid-state Characterization5.1 Introduction; 5.2 Mid-infrared, Raman and THz Spectroscopy: Basic Comparison of Theory, Instrumentation and Sampling; 5.2.1 Basic Theory; 5.2.2 Instrumentation Brief; 5.2.3 Sampling; 5.2.3.1 Raman Sampling [20, 23, 30]; 5.2.3.2 Mid-infrared Sampling [30, 39-41]; 5.2.3.3 THz Spectroscopy Sample Presentation; 5.3 Changes of State and Solid-state Effects on Infrared and Raman Spectra; 5.3.1 Introduction; 5.3.2 Spectra of Gases, Liquids and Solutions; 5.3.3 Hydrogen Bonding 5.3.4 Amine Salts (including Amino Acids) |
| Record Nr. | UNINA-9910830721203321 |
| Weinheim, : Wiley-VCH, c2006 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Polymorphism in the pharmaceutical industry [[electronic resource] /] / edited by Rolf Hilfiker
| Polymorphism in the pharmaceutical industry [[electronic resource] /] / edited by Rolf Hilfiker |
| Pubbl/distr/stampa | Weinheim, : Wiley-VCH, c2006 |
| Descrizione fisica | 1 online resource (436 p.) |
| Disciplina | 660.28 |
| Altri autori (Persone) | HilfikerRolf |
| Soggetto topico |
Crystallography
Solid state chemistry Chemical engineering Pharmaceutical chemistry |
| ISBN |
1-280-72340-8
9786610723409 3-527-60788-9 3-527-60772-2 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Polymorphism; Contents; Preface; List of Contributors; 1 Relevance of Solid-state Properties for Pharmaceutical Products; 1.1 Introduction; 1.2 Drug Discovery and Development; 1.3 Bioavailability of Solids; 1.4 Phases of Development and Solid-state Research; 1.4.1 Salt Selection; 1.4.2 Polymorph Screening; 1.4.3 Crystallization Process Development; 1.4.4 Formulation; 1.4.5 Method Development; 1.5 Solid-state and Life Cycle Management; 1.6 Conclusions; References; 2 Thermodynamics of Polymorphs; 2.1 Introduction; 2.2 Structural Origin of Polymorphism; 2.3 Thermodynamic Theory of Polymorphism
2.4 Thermodynamic Relationship Between Polymorphs: Enantiotropy and Monotropy2.4.1 Energy-Temperature Diagrams; 2.4.2 Pressure-Temperature Diagrams; 2.4.3 Inversion of Polymorphic Behavior; 2.5 Rules to Predict Thermodynamic Relationships Between Polymorphs; 2.5.1 Heat of Transition Rule; 2.5.2 Heat of Fusion Rule; 2.5.3 Entropy of Fusion Rule; 2.5.4 Heat Capacity Rule; 2.5.5 Density Rule; 2.5.6 Infrared Rule; 2.6 Relative Thermodynamic Stabilities of Polymorphs; 2.7 Crystallization of Polymorphs; 2.7.1 Nucleation of Polymorphs; 2.8 Introduction to Solvates and Hydrates 2.8.1 Thermodynamics of Hydrates2.9 Summary; References; 3 Characterization of Polymorphic Systems Using Thermal Analysis; 3.1 Introduction - Scope of the Chapter; 3.2 Use of Differential Scanning Calorimetry for the Characterization of Polymorphs; 3.2.1 Principles of DSC in the Context of Polymorphism; 3.2.2 Examples of the Uses of DSC: Characterization of Drugs, Excipients and Dosage Forms; 3.2.3 Further Uses of DSC; 3.3 Combined Approaches; 3.3.1 Multi-instrument Approaches; 3.3.2 Thermal and Crystallographic Studies; 3.3.3 Interfaced Techniques 3.4 Additional Thermal Methods for the Study of Polymorphism3.4.1 Thermogravimetric Analysis; 3.4.2 Thermal Microscopy; 3.4.3 Heat of Solution Studies; 3.4.4 Modulated Temperature DSC; 3.4.5 High-speed DSC; 3.4.6 Microthermal Analysis; 3.4.7 Thermally Stimulated Current; 3.5 Conclusions; References; 4 Solid-state NMR Spectroscopy; 4.1 Introduction; 4.1.1 Basics of Solid-state NMR; 4.2 Applications; 4.2.1 Identification; 4.2.2 Selectivity; 4.2.3 Mobility and Dynamics; 4.2.4 Quantitation of Forms; 4.3 Conclusions; References 5 Vibrational Spectroscopic Methods in Pharmaceutical Solid-state Characterization5.1 Introduction; 5.2 Mid-infrared, Raman and THz Spectroscopy: Basic Comparison of Theory, Instrumentation and Sampling; 5.2.1 Basic Theory; 5.2.2 Instrumentation Brief; 5.2.3 Sampling; 5.2.3.1 Raman Sampling [20, 23, 30]; 5.2.3.2 Mid-infrared Sampling [30, 39-41]; 5.2.3.3 THz Spectroscopy Sample Presentation; 5.3 Changes of State and Solid-state Effects on Infrared and Raman Spectra; 5.3.1 Introduction; 5.3.2 Spectra of Gases, Liquids and Solutions; 5.3.3 Hydrogen Bonding 5.3.4 Amine Salts (including Amino Acids) |
| Record Nr. | UNINA-9910841149603321 |
| Weinheim, : Wiley-VCH, c2006 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
A practical guide to supramolecular chemistry
| A practical guide to supramolecular chemistry |
| Autore | Cragg Peter J |
| Pubbl/distr/stampa | [Place of publication not identified], : John Wiley & Sons, 2005 |
| Disciplina | 541.226 |
| Soggetto topico |
Supramolecular chemistry
Crystallography Chemistry Physical Sciences & Mathematics |
| ISBN |
0-470-86656-X
0-470-86655-1 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Record Nr. | UNINA-9910144711803321 |
Cragg Peter J
|
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| [Place of publication not identified], : John Wiley & Sons, 2005 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
A practical guide to supramolecular chemistry
| A practical guide to supramolecular chemistry |
| Autore | Cragg Peter J |
| Pubbl/distr/stampa | [Place of publication not identified], : John Wiley & Sons, 2005 |
| Disciplina | 541.226 |
| Soggetto topico |
Supramolecular chemistry
Crystallography Chemistry Physical Sciences & Mathematics |
| ISBN |
0-470-86656-X
0-470-86655-1 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Record Nr. | UNISA-996199389703316 |
|
Cragg Peter J
|
||
| [Place of publication not identified], : John Wiley & Sons, 2005 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. di Salerno | ||
| ||
A practical guide to supramolecular chemistry
| A practical guide to supramolecular chemistry |
| Autore | Cragg Peter J |
| Pubbl/distr/stampa | [Place of publication not identified], : John Wiley & Sons, 2005 |
| Disciplina | 541.226 |
| Soggetto topico |
Supramolecular chemistry
Crystallography Chemistry Physical Sciences & Mathematics |
| ISBN |
0-470-86656-X
0-470-86655-1 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Record Nr. | UNINA-9910830083403321 |
|
Cragg Peter J
|
||
| [Place of publication not identified], : John Wiley & Sons, 2005 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
A practical guide to supramolecular chemistry
| A practical guide to supramolecular chemistry |
| Autore | Cragg Peter J |
| Pubbl/distr/stampa | [Place of publication not identified], : John Wiley & Sons, 2005 |
| Disciplina | 541.226 |
| Soggetto topico |
Supramolecular chemistry
Crystallography Chemistry Physical Sciences & Mathematics |
| ISBN |
0-470-86656-X
0-470-86655-1 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Record Nr. | UNINA-9910841514803321 |
|
Cragg Peter J
|
||
| [Place of publication not identified], : John Wiley & Sons, 2005 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Probing Crystal Plasticity at the Nanoscales [[electronic resource] ] : Synchrotron X-ray Microdiffraction / / by Arief Suriadi Budiman
| Probing Crystal Plasticity at the Nanoscales [[electronic resource] ] : Synchrotron X-ray Microdiffraction / / by Arief Suriadi Budiman |
| Autore | Budiman Arief Suriadi |
| Edizione | [1st ed. 2015.] |
| Pubbl/distr/stampa | Singapore : , : Springer Singapore : , : Imprint : Springer, , 2015 |
| Descrizione fisica | 1 online resource (123 p.) |
| Disciplina | 548.842 |
| Collana | SpringerBriefs in Applied Sciences and Technology |
| Soggetto topico |
Materials science
Nanotechnology Crystallography Spectroscopy Microscopy Characterization and Evaluation of Materials Nanotechnology and Microengineering Crystallography and Scattering Methods Spectroscopy and Microscopy |
| ISBN | 981-287-335-X |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto | From the Contents: Introduction -- Synchrotron White-beam X-ray Microdiffraction at the Advanced Light Source, Berkeley Lab -- Electromigration-induced Plasticity in Cu Interconnects: The Length Scale Dependence. |
| Record Nr. | UNINA-9910298618903321 |
|
Budiman Arief Suriadi
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| Singapore : , : Springer Singapore : , : Imprint : Springer, , 2015 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Proceedings of the flat-plate solar array project workshop on crystal growth for high-efficiency silicon solar cells [[electronic resource] ] : December 3 and 4, 1984, at San Diego, California / / [Katherine A. Dumas, editor]
| Proceedings of the flat-plate solar array project workshop on crystal growth for high-efficiency silicon solar cells [[electronic resource] ] : December 3 and 4, 1984, at San Diego, California / / [Katherine A. Dumas, editor] |
| Pubbl/distr/stampa | Pasadena, Calif. : , : Jet Propulsion Laboratory, California Institute of Technology, , [1985] |
| Descrizione fisica | 1 online resource (1 volumes (various pagings)) : digital, PDF file |
| Altri autori (Persone) | DumasKatherine A |
| Soggetto topico |
Cost effectiveness
Crystal growth Crystallography Solar cells Solar collectors Solar generators Solid state devices |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Altri titoli varianti | Proceedings of the flat-plate solar array project workshop on crystal growth for high-efficiency silicon solar cells |
| Record Nr. | UNINA-9910697126603321 |
| Pasadena, Calif. : , : Jet Propulsion Laboratory, California Institute of Technology, , [1985] | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
The prodromus to a dissertation concerning solids naturally contained within solids [[electronic resource] ] : laying a foundation for the rendering a rational accompt both of the frame and the several changes of the masse of the earth : as also of the various productions in the same / / by Nicolavs Steno ; Englished by H.O
| The prodromus to a dissertation concerning solids naturally contained within solids [[electronic resource] ] : laying a foundation for the rendering a rational accompt both of the frame and the several changes of the masse of the earth : as also of the various productions in the same / / by Nicolavs Steno ; Englished by H.O |
| Autore | Steno Nicolaus <1638-1686.> |
| Pubbl/distr/stampa | London, : Printed by J. Winter and are to be sold by Moses Pitt ..., 1671 |
| Descrizione fisica | [16], 112 p. : ill |
| Altri autori (Persone) | OldenburgHenry <1615?-1677.> |
| Soggetto topico |
Geology
Crystallography Paleontology |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Record Nr. | UNISA-996394003503316 |
|
Steno Nicolaus <1638-1686.>
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| London, : Printed by J. Winter and are to be sold by Moses Pitt ..., 1671 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. di Salerno | ||
| ||
Soggetto topico
-
Crystallography
(300)
- Crystallography and Scattering Methods (108)
- Physical Chemistry (28)
- Physical chemistry (28)
- Materials science (26)