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Determination of trace elements [[electronic resource] /] / edited by Zeev B. Alfassi
Determination of trace elements [[electronic resource] /] / edited by Zeev B. Alfassi
Pubbl/distr/stampa Rehovot, Israel, : Balaban Publishers
Descrizione fisica 1 online resource (623 p.)
Disciplina 543
Altri autori (Persone) AlfassiZeev B
Soggetto topico Trace elements - Analysis
Trace elements - Speciation
Soggetto genere / forma Electronic books.
ISBN 1-281-75877-9
9786611758776
3-527-61577-6
3-527-61576-8
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Determination of Trace Elements; Contents; 1. Systematic errors in trace analysis; 1.1 Introduction; 1.1.1 General aspects of extreme trace analysis; 1.1.2 Direct instrumental determination methods; 1.1.3 Multi-stage procedures; 1.1.4 Further general important statements; 1.2 Systematic errors and their avoidance; 1.2.1 Volatilization; 1.2.2 Adsorption; 1.2.3 Blanks from vessels, vessel materials and working tools; 1.2.4 Blanks from the reagents; 1.2.5 Blanks from airborne dust; 1.2.6 Contamination by sample handling; 1.2.7 Problems due to changes of the valency state
1.3 Systematic errors during the analytical procedure1.3.1 Sampling, sample storage and Pretreatment; 1.3.2 Decomposition; 1.3.3 Separation; 1.4 Basic rules for the recognition and elimination of systematic errors; 1.5 Conclusion; 2. Limits of detection and accuracy in trace elements analysis; 2.1 Introduction; 2.2 Errors in analytical results; 2.3 Accuracy; 2.4 Measuring trace concentrations; 2.5 The problem of detection; 2.5.1 Random error of blank responses; 2.5.2 Errors of the first kind - the critical level (a posteriori detection)
2.5.3 Errors of the second kind - the limit of detection (a priori detection)2 5.4 Limits to the use of the definitions of Lc atid LD; 2 5.5 Regression theory approaches to the problem of detection; 2.6 Practical applications; 2.7 Reporting results at small concentrations; 2.8 Conclusions and recommendations; Sampling and sample preparation; 3.1 Introduction; 3.2 Changes in trace element composition; 3.2.1 Element specific changes; 3.2.2 Sample specific changes; 3.3 Pre-sampling considerations; 3.4 Aspects of sampling; 3.4.1 Establishment of analytical control
3.4.2 Sampling error in a test portion3.4.3 Uniformity of laboratory samples; 3.4.4 Uniformity of subsamples; 3.4.5 The gross sample; 3.5 Sample decomposition; 4. Separation and preconcentration of trace elements; 4.1 Separation and preconcentration of trace elements by coprecipitation; 4.1.1 Introduction; 4.1.2 Mechanism; 4.1.3 Coprecipitation with inorganic precipitants; 4.1.4 Coprecipitation with organic collectors; 4.2 Separation and preconcentration of trace elements by flotation; 4.2.1 Introduction; 4.2.2 Principle; 4.2.3 General procedures
4.3 Preconcentration and separation of trace elements by solvent extraction4.3.1 Introduction; 4.3.2 Extraction of trace elements; 4.4 Separation and preconcentration of trace elements by ion-exchange; 4.4.1 Introduction; 4.4.2 Ion-exchange resins; 4.4.3 Equilibrium and selectivity; 4.4.4 Practical column operation; 4.4.5 Preconcentration; 4.4.6 Ion chromatography; 4.5 Separation and preconcentration by sorption; 4.5.1 Introduction; 4.5.2 Activated carbon; 4.5.3 Porous polymers; 4.5.4 Complex-forming adsorbents; 4.5.5 Natural polymers
5. Determination of trace elements by atomic absorption spectrometry
Record Nr. UNINA-9910143972003321
Rehovot, Israel, : Balaban Publishers
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Determination of trace elements [[electronic resource] /] / edited by Zeev B. Alfassi
Determination of trace elements [[electronic resource] /] / edited by Zeev B. Alfassi
Pubbl/distr/stampa Rehovot, Israel, : Balaban Publishers
Descrizione fisica 1 online resource (623 p.)
Disciplina 543
Altri autori (Persone) AlfassiZeev B
Soggetto topico Trace elements - Analysis
Trace elements - Speciation
ISBN 1-281-75877-9
9786611758776
3-527-61577-6
3-527-61576-8
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Determination of Trace Elements; Contents; 1. Systematic errors in trace analysis; 1.1 Introduction; 1.1.1 General aspects of extreme trace analysis; 1.1.2 Direct instrumental determination methods; 1.1.3 Multi-stage procedures; 1.1.4 Further general important statements; 1.2 Systematic errors and their avoidance; 1.2.1 Volatilization; 1.2.2 Adsorption; 1.2.3 Blanks from vessels, vessel materials and working tools; 1.2.4 Blanks from the reagents; 1.2.5 Blanks from airborne dust; 1.2.6 Contamination by sample handling; 1.2.7 Problems due to changes of the valency state
1.3 Systematic errors during the analytical procedure1.3.1 Sampling, sample storage and Pretreatment; 1.3.2 Decomposition; 1.3.3 Separation; 1.4 Basic rules for the recognition and elimination of systematic errors; 1.5 Conclusion; 2. Limits of detection and accuracy in trace elements analysis; 2.1 Introduction; 2.2 Errors in analytical results; 2.3 Accuracy; 2.4 Measuring trace concentrations; 2.5 The problem of detection; 2.5.1 Random error of blank responses; 2.5.2 Errors of the first kind - the critical level (a posteriori detection)
2.5.3 Errors of the second kind - the limit of detection (a priori detection)2 5.4 Limits to the use of the definitions of Lc atid LD; 2 5.5 Regression theory approaches to the problem of detection; 2.6 Practical applications; 2.7 Reporting results at small concentrations; 2.8 Conclusions and recommendations; Sampling and sample preparation; 3.1 Introduction; 3.2 Changes in trace element composition; 3.2.1 Element specific changes; 3.2.2 Sample specific changes; 3.3 Pre-sampling considerations; 3.4 Aspects of sampling; 3.4.1 Establishment of analytical control
3.4.2 Sampling error in a test portion3.4.3 Uniformity of laboratory samples; 3.4.4 Uniformity of subsamples; 3.4.5 The gross sample; 3.5 Sample decomposition; 4. Separation and preconcentration of trace elements; 4.1 Separation and preconcentration of trace elements by coprecipitation; 4.1.1 Introduction; 4.1.2 Mechanism; 4.1.3 Coprecipitation with inorganic precipitants; 4.1.4 Coprecipitation with organic collectors; 4.2 Separation and preconcentration of trace elements by flotation; 4.2.1 Introduction; 4.2.2 Principle; 4.2.3 General procedures
4.3 Preconcentration and separation of trace elements by solvent extraction4.3.1 Introduction; 4.3.2 Extraction of trace elements; 4.4 Separation and preconcentration of trace elements by ion-exchange; 4.4.1 Introduction; 4.4.2 Ion-exchange resins; 4.4.3 Equilibrium and selectivity; 4.4.4 Practical column operation; 4.4.5 Preconcentration; 4.4.6 Ion chromatography; 4.5 Separation and preconcentration by sorption; 4.5.1 Introduction; 4.5.2 Activated carbon; 4.5.3 Porous polymers; 4.5.4 Complex-forming adsorbents; 4.5.5 Natural polymers
5. Determination of trace elements by atomic absorption spectrometry
Record Nr. UNISA-996205357603316
Rehovot, Israel, : Balaban Publishers
Materiale a stampa
Lo trovi qui: Univ. di Salerno
Opac: Controlla la disponibilità qui
Determination of trace elements [[electronic resource] /] / edited by Zeev B. Alfassi
Determination of trace elements [[electronic resource] /] / edited by Zeev B. Alfassi
Pubbl/distr/stampa Rehovot, Israel, : Balaban Publishers
Descrizione fisica 1 online resource (623 p.)
Disciplina 543
Altri autori (Persone) AlfassiZeev B
Soggetto topico Trace elements - Analysis
Trace elements - Speciation
ISBN 1-281-75877-9
9786611758776
3-527-61577-6
3-527-61576-8
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Determination of Trace Elements; Contents; 1. Systematic errors in trace analysis; 1.1 Introduction; 1.1.1 General aspects of extreme trace analysis; 1.1.2 Direct instrumental determination methods; 1.1.3 Multi-stage procedures; 1.1.4 Further general important statements; 1.2 Systematic errors and their avoidance; 1.2.1 Volatilization; 1.2.2 Adsorption; 1.2.3 Blanks from vessels, vessel materials and working tools; 1.2.4 Blanks from the reagents; 1.2.5 Blanks from airborne dust; 1.2.6 Contamination by sample handling; 1.2.7 Problems due to changes of the valency state
1.3 Systematic errors during the analytical procedure1.3.1 Sampling, sample storage and Pretreatment; 1.3.2 Decomposition; 1.3.3 Separation; 1.4 Basic rules for the recognition and elimination of systematic errors; 1.5 Conclusion; 2. Limits of detection and accuracy in trace elements analysis; 2.1 Introduction; 2.2 Errors in analytical results; 2.3 Accuracy; 2.4 Measuring trace concentrations; 2.5 The problem of detection; 2.5.1 Random error of blank responses; 2.5.2 Errors of the first kind - the critical level (a posteriori detection)
2.5.3 Errors of the second kind - the limit of detection (a priori detection)2 5.4 Limits to the use of the definitions of Lc atid LD; 2 5.5 Regression theory approaches to the problem of detection; 2.6 Practical applications; 2.7 Reporting results at small concentrations; 2.8 Conclusions and recommendations; Sampling and sample preparation; 3.1 Introduction; 3.2 Changes in trace element composition; 3.2.1 Element specific changes; 3.2.2 Sample specific changes; 3.3 Pre-sampling considerations; 3.4 Aspects of sampling; 3.4.1 Establishment of analytical control
3.4.2 Sampling error in a test portion3.4.3 Uniformity of laboratory samples; 3.4.4 Uniformity of subsamples; 3.4.5 The gross sample; 3.5 Sample decomposition; 4. Separation and preconcentration of trace elements; 4.1 Separation and preconcentration of trace elements by coprecipitation; 4.1.1 Introduction; 4.1.2 Mechanism; 4.1.3 Coprecipitation with inorganic precipitants; 4.1.4 Coprecipitation with organic collectors; 4.2 Separation and preconcentration of trace elements by flotation; 4.2.1 Introduction; 4.2.2 Principle; 4.2.3 General procedures
4.3 Preconcentration and separation of trace elements by solvent extraction4.3.1 Introduction; 4.3.2 Extraction of trace elements; 4.4 Separation and preconcentration of trace elements by ion-exchange; 4.4.1 Introduction; 4.4.2 Ion-exchange resins; 4.4.3 Equilibrium and selectivity; 4.4.4 Practical column operation; 4.4.5 Preconcentration; 4.4.6 Ion chromatography; 4.5 Separation and preconcentration by sorption; 4.5.1 Introduction; 4.5.2 Activated carbon; 4.5.3 Porous polymers; 4.5.4 Complex-forming adsorbents; 4.5.5 Natural polymers
5. Determination of trace elements by atomic absorption spectrometry
Record Nr. UNINA-9910830125603321
Rehovot, Israel, : Balaban Publishers
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Determination of trace elements / / edited by Zeev B. Alfassi
Determination of trace elements / / edited by Zeev B. Alfassi
Pubbl/distr/stampa Rehovot, Israel, : Balaban Publishers
Descrizione fisica 1 online resource (623 p.)
Disciplina 543
Altri autori (Persone) AlfassiZeev B
Soggetto topico Trace elements - Analysis
Trace elements - Speciation
ISBN 1-281-75877-9
9786611758776
3-527-61577-6
3-527-61576-8
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Determination of Trace Elements; Contents; 1. Systematic errors in trace analysis; 1.1 Introduction; 1.1.1 General aspects of extreme trace analysis; 1.1.2 Direct instrumental determination methods; 1.1.3 Multi-stage procedures; 1.1.4 Further general important statements; 1.2 Systematic errors and their avoidance; 1.2.1 Volatilization; 1.2.2 Adsorption; 1.2.3 Blanks from vessels, vessel materials and working tools; 1.2.4 Blanks from the reagents; 1.2.5 Blanks from airborne dust; 1.2.6 Contamination by sample handling; 1.2.7 Problems due to changes of the valency state
1.3 Systematic errors during the analytical procedure1.3.1 Sampling, sample storage and Pretreatment; 1.3.2 Decomposition; 1.3.3 Separation; 1.4 Basic rules for the recognition and elimination of systematic errors; 1.5 Conclusion; 2. Limits of detection and accuracy in trace elements analysis; 2.1 Introduction; 2.2 Errors in analytical results; 2.3 Accuracy; 2.4 Measuring trace concentrations; 2.5 The problem of detection; 2.5.1 Random error of blank responses; 2.5.2 Errors of the first kind - the critical level (a posteriori detection)
2.5.3 Errors of the second kind - the limit of detection (a priori detection)2 5.4 Limits to the use of the definitions of Lc atid LD; 2 5.5 Regression theory approaches to the problem of detection; 2.6 Practical applications; 2.7 Reporting results at small concentrations; 2.8 Conclusions and recommendations; Sampling and sample preparation; 3.1 Introduction; 3.2 Changes in trace element composition; 3.2.1 Element specific changes; 3.2.2 Sample specific changes; 3.3 Pre-sampling considerations; 3.4 Aspects of sampling; 3.4.1 Establishment of analytical control
3.4.2 Sampling error in a test portion3.4.3 Uniformity of laboratory samples; 3.4.4 Uniformity of subsamples; 3.4.5 The gross sample; 3.5 Sample decomposition; 4. Separation and preconcentration of trace elements; 4.1 Separation and preconcentration of trace elements by coprecipitation; 4.1.1 Introduction; 4.1.2 Mechanism; 4.1.3 Coprecipitation with inorganic precipitants; 4.1.4 Coprecipitation with organic collectors; 4.2 Separation and preconcentration of trace elements by flotation; 4.2.1 Introduction; 4.2.2 Principle; 4.2.3 General procedures
4.3 Preconcentration and separation of trace elements by solvent extraction4.3.1 Introduction; 4.3.2 Extraction of trace elements; 4.4 Separation and preconcentration of trace elements by ion-exchange; 4.4.1 Introduction; 4.4.2 Ion-exchange resins; 4.4.3 Equilibrium and selectivity; 4.4.4 Practical column operation; 4.4.5 Preconcentration; 4.4.6 Ion chromatography; 4.5 Separation and preconcentration by sorption; 4.5.1 Introduction; 4.5.2 Activated carbon; 4.5.3 Porous polymers; 4.5.4 Complex-forming adsorbents; 4.5.5 Natural polymers
5. Determination of trace elements by atomic absorption spectrometry
Record Nr. UNINA-9910877256503321
Rehovot, Israel, : Balaban Publishers
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Development of analytical methods for trace elements and elemental species in foods ... annual report
Development of analytical methods for trace elements and elemental species in foods ... annual report
Pubbl/distr/stampa [Washington, D.C.], : U.S. Dept. of Agriculture, Agricultural Research Service
Descrizione fisica : HTML files
Disciplina 363.19
Soggetto topico Trace elements - Analysis
Trace elements - Speciation
Food - Composition - Analysis - Methodology
Soggetto genere / forma Periodicals.
ISSN 1947-069X
Formato Materiale a stampa
Livello bibliografico Periodico
Lingua di pubblicazione eng
Record Nr. UNINA-9910698687603321
[Washington, D.C.], : U.S. Dept. of Agriculture, Agricultural Research Service
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Elemental speciation in human health risk assessment [[electronic resource] /] / first draft prepared by P. Apostoli ... [et al.]
Elemental speciation in human health risk assessment [[electronic resource] /] / first draft prepared by P. Apostoli ... [et al.]
Pubbl/distr/stampa Geneva, : World Health Organization, 2006
Descrizione fisica 1 online resource (256 p.)
Disciplina 615.9515
Altri autori (Persone) ApostoliP (Pietro)
Collana Environmental health criteria
Soggetto topico Trace elements - Speciation
Health risk assessment
Biological monitoring
Bioavailability
Analytical toxicology
Chemical elements - Physiological effect
Soggetto genere / forma Electronic books.
ISBN 1-281-30751-3
9786611307516
92-4-068249-X
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto TITLE; COPYRIGHT; CONTENTS; NOTE TO READERS OF THE CRITERIA MONOGRAPHS; PREAMBLE; WHO TASK GROUP ON ENVIRONMENTAL HEALTH CRITERIA FOR ELEMENTAL SPECIATION IN HUMAN HEALTH RISK ASSESSMENT; ACRONYMS AND ABBREVIATIONS; 1. SUMMARY; 2. DEFINITIONS OF SPECIES AND SPECIATION; 3. STRUCTURAL ASPECTS OF SPECIATION; 4. ANALYTICAL TECHNIQUES AND METHODOLOGY; 5. BIOACCESSIBILITY AND BIOAVAILABILITY; 6. TOXICOKINETICS AND BIOLOGICAL MONITORING; 7. MOLECULAR AND CELLULAR MECHANISMS OF METAL TOXICITY; 8. HEALTH EFFECTS; 9. CONCLUSIONS AND RECOMMENDATIONS; REFERENCES; RESUME; RESUMEN; INDEX OF ELEMENTS;
Record Nr. UNINA-9910454420903321
Geneva, : World Health Organization, 2006
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Elemental speciation in human health risk assessment [[electronic resource] /] / first draft prepared by P. Apostoli ... [et al.]
Elemental speciation in human health risk assessment [[electronic resource] /] / first draft prepared by P. Apostoli ... [et al.]
Pubbl/distr/stampa Geneva, : World Health Organization, 2006
Descrizione fisica 1 online resource (256 p.)
Disciplina 615.9515
Altri autori (Persone) ApostoliP (Pietro)
Collana Environmental health criteria
Soggetto topico Trace elements - Speciation
Health risk assessment
Biological monitoring
Bioavailability
Analytical toxicology
Chemical elements - Physiological effect
ISBN 1-281-30751-3
9786611307516
92-4-068249-X
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto TITLE; COPYRIGHT; CONTENTS; NOTE TO READERS OF THE CRITERIA MONOGRAPHS; PREAMBLE; WHO TASK GROUP ON ENVIRONMENTAL HEALTH CRITERIA FOR ELEMENTAL SPECIATION IN HUMAN HEALTH RISK ASSESSMENT; ACRONYMS AND ABBREVIATIONS; 1. SUMMARY; 2. DEFINITIONS OF SPECIES AND SPECIATION; 3. STRUCTURAL ASPECTS OF SPECIATION; 4. ANALYTICAL TECHNIQUES AND METHODOLOGY; 5. BIOACCESSIBILITY AND BIOAVAILABILITY; 6. TOXICOKINETICS AND BIOLOGICAL MONITORING; 7. MOLECULAR AND CELLULAR MECHANISMS OF METAL TOXICITY; 8. HEALTH EFFECTS; 9. CONCLUSIONS AND RECOMMENDATIONS; REFERENCES; RESUME; RESUMEN; INDEX OF ELEMENTS;
Record Nr. UNINA-9910782697803321
Geneva, : World Health Organization, 2006
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Elemental speciation in human health risk assessment / / first draft prepared by P. Apostoli ... [et al.]
Elemental speciation in human health risk assessment / / first draft prepared by P. Apostoli ... [et al.]
Edizione [1st ed.]
Pubbl/distr/stampa Geneva, : World Health Organization, 2006
Descrizione fisica 1 online resource (256 p.)
Disciplina 615.9515
Altri autori (Persone) ApostoliP (Pietro)
Collana Environmental health criteria
Soggetto topico Trace elements - Speciation
Health risk assessment
Biological monitoring
Bioavailability
Analytical toxicology
Chemical elements - Physiological effect
ISBN 1-281-30751-3
9786611307516
92-4-068249-X
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto TITLE; COPYRIGHT; CONTENTS; NOTE TO READERS OF THE CRITERIA MONOGRAPHS; PREAMBLE; WHO TASK GROUP ON ENVIRONMENTAL HEALTH CRITERIA FOR ELEMENTAL SPECIATION IN HUMAN HEALTH RISK ASSESSMENT; ACRONYMS AND ABBREVIATIONS; 1. SUMMARY; 2. DEFINITIONS OF SPECIES AND SPECIATION; 3. STRUCTURAL ASPECTS OF SPECIATION; 4. ANALYTICAL TECHNIQUES AND METHODOLOGY; 5. BIOACCESSIBILITY AND BIOAVAILABILITY; 6. TOXICOKINETICS AND BIOLOGICAL MONITORING; 7. MOLECULAR AND CELLULAR MECHANISMS OF METAL TOXICITY; 8. HEALTH EFFECTS; 9. CONCLUSIONS AND RECOMMENDATIONS; REFERENCES; RESUME; RESUMEN; INDEX OF ELEMENTS;
Record Nr. UNINA-9910822628703321
Geneva, : World Health Organization, 2006
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Hyphenated techniques in speciation analysis [[electronic resource] /] / Joanna Szpunar, Ryszard ℗Łobi{acute}nski
Hyphenated techniques in speciation analysis [[electronic resource] /] / Joanna Szpunar, Ryszard ℗Łobi{acute}nski
Autore Szpunar Joanna
Pubbl/distr/stampa Cambridge, : Royal Society of Chemistry, c2003
Descrizione fisica 1 online resource (238 p.)
Disciplina 544.92
Altri autori (Persone) ℗Łobi{acute}nskiRyszard
Collana RSC chromatography monographs
Soggetto topico Speciation (Chemistry) - Technique
Metals - Speciation
Trace elements - Speciation
Chromatographic analysis
Soggetto genere / forma Electronic books.
ISBN 1-84755-109-2
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto pt. I. Principles and fundamentals -- pt. II. Applications.
Record Nr. UNINA-9910455116603321
Szpunar Joanna  
Cambridge, : Royal Society of Chemistry, c2003
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Hyphenated techniques in speciation analysis [[electronic resource] /] / Joanna Szpunar, Ryszard ℗Łobi{acute}nski
Hyphenated techniques in speciation analysis [[electronic resource] /] / Joanna Szpunar, Ryszard ℗Łobi{acute}nski
Autore Szpunar Joanna
Pubbl/distr/stampa Cambridge, : Royal Society of Chemistry, c2003
Descrizione fisica 1 online resource (238 p.)
Disciplina 544.92
Altri autori (Persone) ℗Łobi{acute}nskiRyszard
Collana RSC chromatography monographs
Soggetto topico Speciation (Chemistry) - Technique
Metals - Speciation
Trace elements - Speciation
Chromatographic analysis
ISBN 1-84755-109-2
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto pt. I. Principles and fundamentals -- pt. II. Applications.
Record Nr. UNINA-9910778306203321
Szpunar Joanna  
Cambridge, : Royal Society of Chemistry, c2003
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui