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Environmental trace analysis : techniques and applications / / John R. Dean
| Environmental trace analysis : techniques and applications / / John R. Dean |
| Autore | Dean John R. |
| Edizione | [1st ed.] |
| Pubbl/distr/stampa | Chichester, West Sussex, United Kingdom : , : John Wiley & Sons Inc., , 2014 |
| Descrizione fisica | 1 online resource (280 p.) |
| Disciplina | 577.27028/7 |
| Soggetto topico |
Trace analysis - Methodology
Environmental chemistry - Methodology Sampling |
| ISBN |
1-118-68284-X
1-118-68342-0 1-118-68279-3 |
| Classificazione | SCI013040 |
| Formato | Materiale a stampa  |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Environmental Trace Analysis: Techniques and Applications; Contents; About the Author; Preface; Acknowledgements; Acronyms and Abbreviations; 1 Basic Laboratory Procedures; 1.1 Introduction; 1.2 Health and Safety Issues; 1.3 Sample Handling: Solid Samples; 1.4 Sample Handling: Liquid Samples; 1.5 Sample Handling: Gases/Vapour Samples; 1.6 Summary; Further Reading; 2 Investigative Approach for Environmental Analysis; 2.1 Introduction; 2.2 Recording of Practical Results; 2.2.1 Useful Tips on Presenting Data in Tables; 2.2.2 Useful Tips on Presenting Data in Graphical Form
2.2.3 Useful Tips for Templates for Presenting Data in Your Notebook2.3 Significant Figures; 2.4 Units; 2.5 Summary; Appendix; Example Template A: Sample Collection; Example Template B: Sample Treatment; Example Template C: Sample Preparation for Inorganic Analysis; Example Template D: Instrumental Analysis; Example Template E: Sample Preparation for Organic Analysis; Example Template F: Instrumental Analysis; Further Reading; 3 Principles of Quantitative Environmental Analysis; 3.1 Introduction; 3.2 Preparing Solutions for Quantitative Work; 3.3 Calibration Graphs 3.4 Limits of Detection/Quantitation3.5 Calculations: Dilution or Concentration Factors; 3.6 Quality Assurance; 3.6.1 Certified Reference Materials; 3.7 Summary; References; Further Reading; 4 Environmental Sampling; 4.1 Introduction; 4.2 Sampling Soil (and Sediments); 4.3 Sampling Water; 4.4 Sampling Air; 4.5 Summary; Further Reading; 5 Storage of Samples for Analysis; 5.1 Introduction; 5.2 Choice of Storage Container for Liquid Samples; 5.3 Preservation Techniques for Liquid Samples; 5.4 Storage and Preservation of Solid Samples; 5.5 Storage and Preservation of Gaseous Samples; 5.6 Summary Further Reading6 Preparation of Environmental Solid Samples for Inorganic Analysis; 6.1 Introduction; 6.2 Decomposition Techniques; 6.3 Selective Extraction Methods; 6.3.1 Single Extraction Methods; 6.3.2 Sequential Extraction Method; 6.3.3 Chemometric Identification of Substrates and Element Distributions (CISED) Method; 6.4 Physiologically-Based Extraction Test or In Vitro Gastrointestinal Extraction; 6.4.1 Procedure for Gastric Extraction; 6.4.2 Procedure for Gastric + Intestinal Extraction; 6.5 Earthworms; 6.5.1 Procedure for Earthworm Bioaccumulation Studies (Sandoval et al., 2001) 6.6 SummaryAppendix A: Extraction Reagents for Single Extraction Methods; Appendix B: Extraction Reagents for Sequential Extraction Method; Appendix C: Extraction Reagents for In Vitro Gastrointestinal Extraction Using the Unified Bioaccessibility Method (and the FOREhST Method); References; Further Reading; 7 Preparation of Environmental Liquid Samples for Inorganic Analysis; 7.1 Introduction; 7.2 Liquid-Liquid Extraction of Metals; 7.2.1 Procedure for APDC Extraction into MIBK; 7.3 Ion Exchange; 7.3.1 Chelation Ion Exchange; 7.3.2 Procedure for Batch Ion Exchange Extraction 7.4 Co-precipitation |
| Record Nr. | UNINA-9910131929803321 |
Dean John R.
|
||
| Chichester, West Sussex, United Kingdom : , : John Wiley & Sons Inc., , 2014 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Environmental trace analysis : techniques and applications / / John R. Dean
| Environmental trace analysis : techniques and applications / / John R. Dean |
| Autore | Dean John R. |
| Edizione | [1st ed.] |
| Pubbl/distr/stampa | Chichester, West Sussex, United Kingdom : , : John Wiley & Sons Inc., , 2014 |
| Descrizione fisica | 1 online resource (280 p.) |
| Disciplina | 577.27028/7 |
| Soggetto topico |
Trace analysis - Methodology
Environmental chemistry - Methodology Sampling |
| ISBN |
1-118-68284-X
1-118-68342-0 1-118-68279-3 |
| Classificazione | SCI013040 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Environmental Trace Analysis: Techniques and Applications; Contents; About the Author; Preface; Acknowledgements; Acronyms and Abbreviations; 1 Basic Laboratory Procedures; 1.1 Introduction; 1.2 Health and Safety Issues; 1.3 Sample Handling: Solid Samples; 1.4 Sample Handling: Liquid Samples; 1.5 Sample Handling: Gases/Vapour Samples; 1.6 Summary; Further Reading; 2 Investigative Approach for Environmental Analysis; 2.1 Introduction; 2.2 Recording of Practical Results; 2.2.1 Useful Tips on Presenting Data in Tables; 2.2.2 Useful Tips on Presenting Data in Graphical Form
2.2.3 Useful Tips for Templates for Presenting Data in Your Notebook2.3 Significant Figures; 2.4 Units; 2.5 Summary; Appendix; Example Template A: Sample Collection; Example Template B: Sample Treatment; Example Template C: Sample Preparation for Inorganic Analysis; Example Template D: Instrumental Analysis; Example Template E: Sample Preparation for Organic Analysis; Example Template F: Instrumental Analysis; Further Reading; 3 Principles of Quantitative Environmental Analysis; 3.1 Introduction; 3.2 Preparing Solutions for Quantitative Work; 3.3 Calibration Graphs 3.4 Limits of Detection/Quantitation3.5 Calculations: Dilution or Concentration Factors; 3.6 Quality Assurance; 3.6.1 Certified Reference Materials; 3.7 Summary; References; Further Reading; 4 Environmental Sampling; 4.1 Introduction; 4.2 Sampling Soil (and Sediments); 4.3 Sampling Water; 4.4 Sampling Air; 4.5 Summary; Further Reading; 5 Storage of Samples for Analysis; 5.1 Introduction; 5.2 Choice of Storage Container for Liquid Samples; 5.3 Preservation Techniques for Liquid Samples; 5.4 Storage and Preservation of Solid Samples; 5.5 Storage and Preservation of Gaseous Samples; 5.6 Summary Further Reading6 Preparation of Environmental Solid Samples for Inorganic Analysis; 6.1 Introduction; 6.2 Decomposition Techniques; 6.3 Selective Extraction Methods; 6.3.1 Single Extraction Methods; 6.3.2 Sequential Extraction Method; 6.3.3 Chemometric Identification of Substrates and Element Distributions (CISED) Method; 6.4 Physiologically-Based Extraction Test or In Vitro Gastrointestinal Extraction; 6.4.1 Procedure for Gastric Extraction; 6.4.2 Procedure for Gastric + Intestinal Extraction; 6.5 Earthworms; 6.5.1 Procedure for Earthworm Bioaccumulation Studies (Sandoval et al., 2001) 6.6 SummaryAppendix A: Extraction Reagents for Single Extraction Methods; Appendix B: Extraction Reagents for Sequential Extraction Method; Appendix C: Extraction Reagents for In Vitro Gastrointestinal Extraction Using the Unified Bioaccessibility Method (and the FOREhST Method); References; Further Reading; 7 Preparation of Environmental Liquid Samples for Inorganic Analysis; 7.1 Introduction; 7.2 Liquid-Liquid Extraction of Metals; 7.2.1 Procedure for APDC Extraction into MIBK; 7.3 Ion Exchange; 7.3.1 Chelation Ion Exchange; 7.3.2 Procedure for Batch Ion Exchange Extraction 7.4 Co-precipitation |
| Record Nr. | UNINA-9910810814703321 |
|
Dean John R.
|
||
| Chichester, West Sussex, United Kingdom : , : John Wiley & Sons Inc., , 2014 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Environmental trace analysis : techniques and applications / John R. Dean
| Environmental trace analysis : techniques and applications / John R. Dean |
| Autore | Dean, John R. |
| Pubbl/distr/stampa | Chichester, West Sussex, United Kingdom : John Wiley & Sons, 2014 |
| Descrizione fisica | 254 p. : ill.; 23 cm |
| Disciplina | 577.270287 |
| Soggetto topico |
Trace analysis - Methodology
Environmental chemistry - Methodology Sampling |
| ISBN | 9781119962717 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Record Nr. | UNISALENTO-991002456379707536 |
|
Dean, John R.
|
||
| Chichester, West Sussex, United Kingdom : John Wiley & Sons, 2014 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. del Salento | ||
| ||
Handbook of spectroscopy / / edited by Günter Gauglitz and David S. Moore
| Handbook of spectroscopy / / edited by Günter Gauglitz and David S. Moore |
| Edizione | [2nd ed.] |
| Pubbl/distr/stampa | Weinheim, Germany : , : Wiley-VCH Verlag, , 2014 |
| Descrizione fisica | 1 online resource (1951 p.) |
| Disciplina |
543.5
543/.5 |
| Soggetto topico |
Spectrum analysis
Trace analysis - Methodology |
| ISBN |
3-527-65472-0
3-527-65470-4 3-527-65473-9 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto | Volume 1. Sample preparation and sample pretreatment -- Volume 2. Methods 4: Elemental analysis -- Volume 3. Applications 1: Bioanalysis -- Volume 4. Applications 6: Spectroscopy at surfaces. |
| Record Nr. | UNINA-9910139140903321 |
| Weinheim, Germany : , : Wiley-VCH Verlag, , 2014 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Kopplungstechniken zur Elementspeziesanalytik [[electronic resource] /] / Lothar Dunemann, Jutta Begerow
| Kopplungstechniken zur Elementspeziesanalytik [[electronic resource] /] / Lothar Dunemann, Jutta Begerow |
| Autore | Dunemann L (Lothar) |
| Pubbl/distr/stampa | Weinheim, : Wiley-Blackwell, 1995 |
| Descrizione fisica | 1 online resource (240 p.) |
| Disciplina |
543
572.515 |
| Altri autori (Persone) | BegerowJutta |
| Soggetto topico |
Trace elements - Speciation
Trace analysis - Methodology |
| Soggetto genere / forma | Electronic books. |
| ISBN |
1-282-02203-2
9786612022036 3-527-62432-5 3-527-62433-3 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | ger |
| Nota di contenuto | Kopplungstechniken zur Elementspeziesanalytik; Inhalt; 1 Einleitung und Übersicht; 2 Elementspeziesanalytik (ESA); 3 Kopplungstechniken zur Elementspeziesanalytik; 4 Anwendungsgebiete der Kopplungstechniken in der ESA; 5 Zukünftige Entwicklungen; 6 Zusammenfassung und Ausblick; Register |
| Record Nr. | UNINA-9910144394703321 |
|
Dunemann L (Lothar)
|
||
| Weinheim, : Wiley-Blackwell, 1995 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Kopplungstechniken zur Elementspeziesanalytik [[electronic resource] /] / Lothar Dunemann, Jutta Begerow
| Kopplungstechniken zur Elementspeziesanalytik [[electronic resource] /] / Lothar Dunemann, Jutta Begerow |
| Autore | Dunemann L (Lothar) |
| Pubbl/distr/stampa | Weinheim, : Wiley-Blackwell, 1995 |
| Descrizione fisica | 1 online resource (240 p.) |
| Disciplina |
543
572.515 |
| Altri autori (Persone) | BegerowJutta |
| Soggetto topico |
Trace elements - Speciation
Trace analysis - Methodology |
| ISBN |
1-282-02203-2
9786612022036 3-527-62432-5 3-527-62433-3 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | ger |
| Nota di contenuto | Kopplungstechniken zur Elementspeziesanalytik; Inhalt; 1 Einleitung und Übersicht; 2 Elementspeziesanalytik (ESA); 3 Kopplungstechniken zur Elementspeziesanalytik; 4 Anwendungsgebiete der Kopplungstechniken in der ESA; 5 Zukünftige Entwicklungen; 6 Zusammenfassung und Ausblick; Register |
| Record Nr. | UNINA-9910831175703321 |
|
Dunemann L (Lothar)
|
||
| Weinheim, : Wiley-Blackwell, 1995 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Kopplungstechniken zur Elementspeziesanalytik / / Lothar Dunemann, Jutta Begerow
| Kopplungstechniken zur Elementspeziesanalytik / / Lothar Dunemann, Jutta Begerow |
| Autore | Dunemann L (Lothar) |
| Pubbl/distr/stampa | Weinheim, : Wiley-Blackwell, 1995 |
| Descrizione fisica | 1 online resource (240 p.) |
| Disciplina |
543
572.515 |
| Altri autori (Persone) | BegerowJutta |
| Soggetto topico |
Trace elements - Speciation
Trace analysis - Methodology |
| ISBN |
1-282-02203-2
9786612022036 3-527-62432-5 3-527-62433-3 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | ger |
| Nota di contenuto | Kopplungstechniken zur Elementspeziesanalytik; Inhalt; 1 Einleitung und Übersicht; 2 Elementspeziesanalytik (ESA); 3 Kopplungstechniken zur Elementspeziesanalytik; 4 Anwendungsgebiete der Kopplungstechniken in der ESA; 5 Zukünftige Entwicklungen; 6 Zusammenfassung und Ausblick; Register |
| Record Nr. | UNINA-9910877984303321 |
|
Dunemann L (Lothar)
|
||
| Weinheim, : Wiley-Blackwell, 1995 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Methods for environmental trace analysis [[electronic resource] /] / John R. Dean
| Methods for environmental trace analysis [[electronic resource] /] / John R. Dean |
| Autore | Dean John R |
| Pubbl/distr/stampa | Chichester, West Sussex, England ; ; Hoboken, NJ, : Wiley, c2003 |
| Descrizione fisica | 1 online resource (285 p.) |
| Disciplina | 628.5/028/7 |
| Collana | Analytical techniques in the sciences |
| Soggetto topico |
Pollutants - Analysis
Trace analysis - Methodology Environmental chemistry - Methodology Sampling |
| Soggetto genere / forma | Electronic books. |
| ISBN |
1-280-27125-6
0-470-86132-0 9786610271252 0-470-86325-0 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
METHODS FOR ENVIRONMENTAL TRACE ANALYSIS; Contents; Series Preface; Preface; Acronyms, Abbreviations and Symbols; About the Author; 1 Basic Laboratory Skills ; 1.1 Introduction ; 1.2 Safety Aspects ; 1.3 Recording of Practical Results; 1.4 Units ; 1.5 Sample Handling: Liquids ; 1.6 Sample Handling: Solids ; 1.7 Preparing Solutions for Quantitative Work ; 1.8 Presentation of Data: Tables ; 1.9 Presentation of Data: Graphs ; 1.10 Calculations: Dilution Factors ; Further Reading ; 2 Investigative Approach for Sample Preparation ; 2.1 Introduction ; 2.2 Quality Assurance ; References
3 Sampling 3.1 Introduction ; 3.2 Sampling Methods ; 3.3 Number of Samples ; 3.4 Sampling Soil and Sediment ; 3.5 Sampling Water ; 3.6 Sampling Air ; References ; 4 Storage of Samples ; 4.1 Introduction ; 4.2 Methods ; References ; SAMPLE PREPARATION FOR INORGANIC ANALYSIS ; 5 Solids ; 5.1 Introduction ; 5.2 Decomposition Techniques ; 5.3 Dry Ashing ; 5.4 Acid Digestion (including the Use of Microwaves) ; 5.4.1 Microwave Digestion ; 5.4.2 Microwave Digestion Procedure ; 5.4.3 Fusion ; 5.5 Speciation Studies ; 5.6 Selected Examples of Metal Speciation ; 5.6.1 Mercury ; 5.6.2 Tin 5.6.3 Arsenic 5.6.4 Chromium ; 5.7 Selective Extraction Methods ; 5.7.1 Plant Uptake Studies ; 5.7.2 Soil Pollution Studies ; 5.7.3 Single Extraction Procedures ; 5.7.4 Sequential Extraction Procedure ; 5.7.5 Food Studies ; 5.8 Case Studies on Total and Selective Methods of Metal Analysis ; 5.8.1 Example 5.1: Total Metal Analysis of Soil, followed by Flame Atomic Absorption Spectroscopy ; 5.8.2 Example 5.2: Total Metal Analysis of Soil Using X-Ray Fluorescence Spectroscopy - Comparison with Acid Digestion (Method 3050B), followed by Flame Atomic Absorption Spectroscopy 5.8.3 Example 5.3: Sequential Metal Analysis of Soils, followed by Flame Atomic Absorption Spectroscopy References ; 6 Liquids - Natural and Waste Waters ; 6.1 Introduction ; 6.2 Liquid-Liquid Extraction ; 6.3 Ion-Exchange ; 6.4 Co-Precipitation ; References ; SAMPLE PREPARATION FOR ORGANIC ANALYSIS ; 7 Solids ; 7.1 Introduction ; 7.2 Soxhlet Extraction ; 7.2.1 Example 7.1: Soxhlet Extraction of Polycyclic Aromatic Hydrocarbons from Contaminated Soil ; 7.3 Shake-Flask Extraction ; 7.3.1 Example 7.2: Shake-Flask Extraction of Phenols from Contaminated Soil ; 7.4 Ultrasonic Extraction 7.5 Supercritical Fluid Extraction 7.5.1 Instrumentation ; 7.5.2 Example 7.3: Supercritical Fluid Extraction of Organochlorine Pesticides from Contaminated Soil and 'Celite' ; 7.6 Microwave-Assisted Extraction ; 7.6.1 Instrumentation ; 7.6.2 Example 7.4: Atmospheric Microwave-Assisted Extraction of Polycyclic Aromatic Hydrocarbons from Contaminated Soil ; 7.6.3 Example 7.5: Pressurized Microwave-Assisted Extraction of Polycyclic Aromatic Hydrocarbons from Contaminated Soil ; 7.7 Pressurized Fluid Extraction ; 7.7.1 Instrumentation 7.7.2 Example 7.6: Pressurized Fluid Extraction of DDT, DDD and DDE from Contaminated Soil |
| Record Nr. | UNINA-9910145754903321 |
|
Dean John R
|
||
| Chichester, West Sussex, England ; ; Hoboken, NJ, : Wiley, c2003 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Methods for environmental trace analysis [[electronic resource] /] / John R. Dean
| Methods for environmental trace analysis [[electronic resource] /] / John R. Dean |
| Autore | Dean John R |
| Pubbl/distr/stampa | Chichester, West Sussex, England ; ; Hoboken, NJ, : Wiley, c2003 |
| Descrizione fisica | 1 online resource (285 p.) |
| Disciplina | 628.5/028/7 |
| Collana | Analytical techniques in the sciences |
| Soggetto topico |
Pollutants - Analysis
Trace analysis - Methodology Environmental chemistry - Methodology Sampling |
| ISBN |
1-280-27125-6
0-470-86132-0 9786610271252 0-470-86325-0 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
METHODS FOR ENVIRONMENTAL TRACE ANALYSIS; Contents; Series Preface; Preface; Acronyms, Abbreviations and Symbols; About the Author; 1 Basic Laboratory Skills ; 1.1 Introduction ; 1.2 Safety Aspects ; 1.3 Recording of Practical Results; 1.4 Units ; 1.5 Sample Handling: Liquids ; 1.6 Sample Handling: Solids ; 1.7 Preparing Solutions for Quantitative Work ; 1.8 Presentation of Data: Tables ; 1.9 Presentation of Data: Graphs ; 1.10 Calculations: Dilution Factors ; Further Reading ; 2 Investigative Approach for Sample Preparation ; 2.1 Introduction ; 2.2 Quality Assurance ; References
3 Sampling 3.1 Introduction ; 3.2 Sampling Methods ; 3.3 Number of Samples ; 3.4 Sampling Soil and Sediment ; 3.5 Sampling Water ; 3.6 Sampling Air ; References ; 4 Storage of Samples ; 4.1 Introduction ; 4.2 Methods ; References ; SAMPLE PREPARATION FOR INORGANIC ANALYSIS ; 5 Solids ; 5.1 Introduction ; 5.2 Decomposition Techniques ; 5.3 Dry Ashing ; 5.4 Acid Digestion (including the Use of Microwaves) ; 5.4.1 Microwave Digestion ; 5.4.2 Microwave Digestion Procedure ; 5.4.3 Fusion ; 5.5 Speciation Studies ; 5.6 Selected Examples of Metal Speciation ; 5.6.1 Mercury ; 5.6.2 Tin 5.6.3 Arsenic 5.6.4 Chromium ; 5.7 Selective Extraction Methods ; 5.7.1 Plant Uptake Studies ; 5.7.2 Soil Pollution Studies ; 5.7.3 Single Extraction Procedures ; 5.7.4 Sequential Extraction Procedure ; 5.7.5 Food Studies ; 5.8 Case Studies on Total and Selective Methods of Metal Analysis ; 5.8.1 Example 5.1: Total Metal Analysis of Soil, followed by Flame Atomic Absorption Spectroscopy ; 5.8.2 Example 5.2: Total Metal Analysis of Soil Using X-Ray Fluorescence Spectroscopy - Comparison with Acid Digestion (Method 3050B), followed by Flame Atomic Absorption Spectroscopy 5.8.3 Example 5.3: Sequential Metal Analysis of Soils, followed by Flame Atomic Absorption Spectroscopy References ; 6 Liquids - Natural and Waste Waters ; 6.1 Introduction ; 6.2 Liquid-Liquid Extraction ; 6.3 Ion-Exchange ; 6.4 Co-Precipitation ; References ; SAMPLE PREPARATION FOR ORGANIC ANALYSIS ; 7 Solids ; 7.1 Introduction ; 7.2 Soxhlet Extraction ; 7.2.1 Example 7.1: Soxhlet Extraction of Polycyclic Aromatic Hydrocarbons from Contaminated Soil ; 7.3 Shake-Flask Extraction ; 7.3.1 Example 7.2: Shake-Flask Extraction of Phenols from Contaminated Soil ; 7.4 Ultrasonic Extraction 7.5 Supercritical Fluid Extraction 7.5.1 Instrumentation ; 7.5.2 Example 7.3: Supercritical Fluid Extraction of Organochlorine Pesticides from Contaminated Soil and 'Celite' ; 7.6 Microwave-Assisted Extraction ; 7.6.1 Instrumentation ; 7.6.2 Example 7.4: Atmospheric Microwave-Assisted Extraction of Polycyclic Aromatic Hydrocarbons from Contaminated Soil ; 7.6.3 Example 7.5: Pressurized Microwave-Assisted Extraction of Polycyclic Aromatic Hydrocarbons from Contaminated Soil ; 7.7 Pressurized Fluid Extraction ; 7.7.1 Instrumentation 7.7.2 Example 7.6: Pressurized Fluid Extraction of DDT, DDD and DDE from Contaminated Soil |
| Record Nr. | UNINA-9910831025403321 |
|
Dean John R
|
||
| Chichester, West Sussex, England ; ; Hoboken, NJ, : Wiley, c2003 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Methods for environmental trace analysis / / John R. Dean
| Methods for environmental trace analysis / / John R. Dean |
| Autore | Dean John R |
| Pubbl/distr/stampa | Chichester, West Sussex, England ; ; Hoboken, NJ, : Wiley, c2003 |
| Descrizione fisica | 1 online resource (285 p.) |
| Disciplina | 628.5/028/7 |
| Collana | Analytical techniques in the sciences |
| Soggetto topico |
Pollutants - Analysis
Trace analysis - Methodology Environmental chemistry - Methodology Sampling |
| ISBN |
1-280-27125-6
0-470-86132-0 9786610271252 0-470-86325-0 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
METHODS FOR ENVIRONMENTAL TRACE ANALYSIS; Contents; Series Preface; Preface; Acronyms, Abbreviations and Symbols; About the Author; 1 Basic Laboratory Skills ; 1.1 Introduction ; 1.2 Safety Aspects ; 1.3 Recording of Practical Results; 1.4 Units ; 1.5 Sample Handling: Liquids ; 1.6 Sample Handling: Solids ; 1.7 Preparing Solutions for Quantitative Work ; 1.8 Presentation of Data: Tables ; 1.9 Presentation of Data: Graphs ; 1.10 Calculations: Dilution Factors ; Further Reading ; 2 Investigative Approach for Sample Preparation ; 2.1 Introduction ; 2.2 Quality Assurance ; References
3 Sampling 3.1 Introduction ; 3.2 Sampling Methods ; 3.3 Number of Samples ; 3.4 Sampling Soil and Sediment ; 3.5 Sampling Water ; 3.6 Sampling Air ; References ; 4 Storage of Samples ; 4.1 Introduction ; 4.2 Methods ; References ; SAMPLE PREPARATION FOR INORGANIC ANALYSIS ; 5 Solids ; 5.1 Introduction ; 5.2 Decomposition Techniques ; 5.3 Dry Ashing ; 5.4 Acid Digestion (including the Use of Microwaves) ; 5.4.1 Microwave Digestion ; 5.4.2 Microwave Digestion Procedure ; 5.4.3 Fusion ; 5.5 Speciation Studies ; 5.6 Selected Examples of Metal Speciation ; 5.6.1 Mercury ; 5.6.2 Tin 5.6.3 Arsenic 5.6.4 Chromium ; 5.7 Selective Extraction Methods ; 5.7.1 Plant Uptake Studies ; 5.7.2 Soil Pollution Studies ; 5.7.3 Single Extraction Procedures ; 5.7.4 Sequential Extraction Procedure ; 5.7.5 Food Studies ; 5.8 Case Studies on Total and Selective Methods of Metal Analysis ; 5.8.1 Example 5.1: Total Metal Analysis of Soil, followed by Flame Atomic Absorption Spectroscopy ; 5.8.2 Example 5.2: Total Metal Analysis of Soil Using X-Ray Fluorescence Spectroscopy - Comparison with Acid Digestion (Method 3050B), followed by Flame Atomic Absorption Spectroscopy 5.8.3 Example 5.3: Sequential Metal Analysis of Soils, followed by Flame Atomic Absorption Spectroscopy References ; 6 Liquids - Natural and Waste Waters ; 6.1 Introduction ; 6.2 Liquid-Liquid Extraction ; 6.3 Ion-Exchange ; 6.4 Co-Precipitation ; References ; SAMPLE PREPARATION FOR ORGANIC ANALYSIS ; 7 Solids ; 7.1 Introduction ; 7.2 Soxhlet Extraction ; 7.2.1 Example 7.1: Soxhlet Extraction of Polycyclic Aromatic Hydrocarbons from Contaminated Soil ; 7.3 Shake-Flask Extraction ; 7.3.1 Example 7.2: Shake-Flask Extraction of Phenols from Contaminated Soil ; 7.4 Ultrasonic Extraction 7.5 Supercritical Fluid Extraction 7.5.1 Instrumentation ; 7.5.2 Example 7.3: Supercritical Fluid Extraction of Organochlorine Pesticides from Contaminated Soil and 'Celite' ; 7.6 Microwave-Assisted Extraction ; 7.6.1 Instrumentation ; 7.6.2 Example 7.4: Atmospheric Microwave-Assisted Extraction of Polycyclic Aromatic Hydrocarbons from Contaminated Soil ; 7.6.3 Example 7.5: Pressurized Microwave-Assisted Extraction of Polycyclic Aromatic Hydrocarbons from Contaminated Soil ; 7.7 Pressurized Fluid Extraction ; 7.7.1 Instrumentation 7.7.2 Example 7.6: Pressurized Fluid Extraction of DDT, DDD and DDE from Contaminated Soil |
| Record Nr. | UNINA-9910877877103321 |
|
Dean John R
|
||
| Chichester, West Sussex, England ; ; Hoboken, NJ, : Wiley, c2003 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
