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Dynamic studies in biology [[electronic resource] ] : phototriggers, photoswitches and caged biomolecules / / edited by Maurice Goeldner, Richard Givens
Dynamic studies in biology [[electronic resource] ] : phototriggers, photoswitches and caged biomolecules / / edited by Maurice Goeldner, Richard Givens
Pubbl/distr/stampa Weinheim, : Wiley-VCH, c2005
Descrizione fisica 1 online resource (587 p.)
Disciplina 547.2
Altri autori (Persone) GoeldnerMaurice
GivensRichard
Soggetto topico Photobiochemistry
Biomolecules - Separation
Protective groups (Chemistry)
Soggetto genere / forma Electronic books.
ISBN 1-280-52060-4
9786610520602
3-527-60559-2
3-527-60554-1
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Dynamic Studies in Biology Phototriggers, Photoswitches and Caged Biomolecules; Contents; Foreword; Preface; List of Authors; 1 Photoremovable Protecting Groups Used for the Caging of Biomolecules; 1.1 2-Nitrobenzyl and 7-Nitroindoline Derivatives; 1.1.1 Introduction; 1.1.1.1 Preamble and Scope of the Review; 1.1.1.2 Historical Perspective; 1.1.2 Synthetic Considerations; 1.1.3 Survey of Individual Caged Compounds and Caging Groups; 1.1.3.1 2-Nitrobenzyl Cages; 1.1.3.1.1 Mechanistic Aspects of Photocleavage and By-Product Reactions of 2-Nitrobenzyl Cages
1.1.3.1.2 Representative Survey of Nitrobenzyl-Caged Compounds1.1.3.2 7-Nitroindoline Cages; 1.1.3.2.1 Mechanistic and Structural Aspects of Photochemical Cleavage of 1-Acyl-7-nitroindolines; 1.1.3.2.2 Survey of 7-Nitroindoline Caged Compounds; 1.1.4 Conclusion; References; 1.2 Coumarin-4-ylmethyl Phototriggers; 1.2.1 Introduction; 1.2.2 Spectroscopic and Photochemical Properties; 1.2.2.1 Overview; 1.2.2.2 Phototriggers; 1.2.2.2.1 MCM Groups: 7-Alkoxy-Substituted Coumarins; 1.2.2.2.2 DMCM Groups: 6,7-Dialkoxy-Substituted Coumarins; 1.2.2.2.3 Bhc Groups: 6-Bromo-7-alkoxy-Substituted Coumarins
1.2.2.2.4 DEACM Groups: 7-Dialkylamino-Substituted Coumarins1.2.2.3 Target Molecules; 1.2.2.3.1 Phosphates; 1.2.2.3.2 Carboxylates and Sulfates; 1.2.2.3.3 Amines; 1.2.2.3.4 Alcohols and Phenols; 1.2.2.3.5 Carbonyl Compounds; 1.2.3 Synthesis; 1.2.3.1 Synthesis of Precursor Molecules (Caging Agents); 1.2.3.1.1 Phosphates; 1.2.3.1.2 Carboxylates; 1.2.3.1.3 Amines; 1.2.3.1.4 Alcohols and Phenols; 1.2.4 Applications; 1.2.5 Conclusion and Perspective; References; 1.3 p-Hydroxyphenacyl: a Photoremovable Protecting Group for Caging Bioactive Substrates; 1.3.1 Introduction and History
1.3.2 p-Hydroxyphenacyl1.3.2.1 General Physical and Spectroscopic Properties; 1.3.2.2 Synthesis of pHP-Caged Substrates; 1.3.3 Mechanistic Studies; 1.3.3.1 A Triplet "Photo-Favorskii" Rearrangement; 1.3.3.2 Role of the Triplet Phenol; 1.3.3.3 Correlation of the (3)pK(a) with the Quantum Efficiency; 1.3.4 Applications; 1.3.4.1 Neurotransmitter Release; 1.3.4.2 Peptide Release; 1.3.4.3 Nucleotide Release; 1.3.4.4 Enzyme Photoswitches; 1.3.5 Advantages and Limitations; References; 1.4 Caging of ATP and Glutamate: a Comparative Analysis; 1.4.1 Introduction
1.4.2 General Properties for Caging Groups1.4.3 Caged-ATP; 1.4.3.1 Introduction; 1.4.3.2 Syntheses of the P(3)-caged ATP Derivatives; 1.4.3.3 General Properties of the Caged-ATP Molecules; 1.4.3.4 Conclusion; 1.4.4 Caged Glutamate; 1.4.4.1 Introduction; 1.4.4.2 Syntheses of the Caged Glutamate Derivatives; 1.4.4.3 General Properties of the Caged-Glutamate Molecules; 1.4.4.4 Conclusion; Abbreviations; References; 2 Mechanistic Overview of Phototriggers and Cage Release; 2.1 Introduction; 2.2 Major Photoremovable Protecting Groups; 2.2.1 2-Nitrobenzyl (2-NB); 2.2.1.1 The Reactive Excited State
2.2.1.2 The aci-Nitro Intermediate
Record Nr. UNINA-9910143965203321
Weinheim, : Wiley-VCH, c2005
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Dynamic studies in biology [[electronic resource] ] : phototriggers, photoswitches and caged biomolecules / / edited by Maurice Goeldner, Richard Givens
Dynamic studies in biology [[electronic resource] ] : phototriggers, photoswitches and caged biomolecules / / edited by Maurice Goeldner, Richard Givens
Pubbl/distr/stampa Weinheim, : Wiley-VCH, c2005
Descrizione fisica 1 online resource (587 p.)
Disciplina 547.2
Altri autori (Persone) GoeldnerMaurice
GivensRichard
Soggetto topico Photobiochemistry
Biomolecules - Separation
Protective groups (Chemistry)
ISBN 1-280-52060-4
9786610520602
3-527-60559-2
3-527-60554-1
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Dynamic Studies in Biology Phototriggers, Photoswitches and Caged Biomolecules; Contents; Foreword; Preface; List of Authors; 1 Photoremovable Protecting Groups Used for the Caging of Biomolecules; 1.1 2-Nitrobenzyl and 7-Nitroindoline Derivatives; 1.1.1 Introduction; 1.1.1.1 Preamble and Scope of the Review; 1.1.1.2 Historical Perspective; 1.1.2 Synthetic Considerations; 1.1.3 Survey of Individual Caged Compounds and Caging Groups; 1.1.3.1 2-Nitrobenzyl Cages; 1.1.3.1.1 Mechanistic Aspects of Photocleavage and By-Product Reactions of 2-Nitrobenzyl Cages
1.1.3.1.2 Representative Survey of Nitrobenzyl-Caged Compounds1.1.3.2 7-Nitroindoline Cages; 1.1.3.2.1 Mechanistic and Structural Aspects of Photochemical Cleavage of 1-Acyl-7-nitroindolines; 1.1.3.2.2 Survey of 7-Nitroindoline Caged Compounds; 1.1.4 Conclusion; References; 1.2 Coumarin-4-ylmethyl Phototriggers; 1.2.1 Introduction; 1.2.2 Spectroscopic and Photochemical Properties; 1.2.2.1 Overview; 1.2.2.2 Phototriggers; 1.2.2.2.1 MCM Groups: 7-Alkoxy-Substituted Coumarins; 1.2.2.2.2 DMCM Groups: 6,7-Dialkoxy-Substituted Coumarins; 1.2.2.2.3 Bhc Groups: 6-Bromo-7-alkoxy-Substituted Coumarins
1.2.2.2.4 DEACM Groups: 7-Dialkylamino-Substituted Coumarins1.2.2.3 Target Molecules; 1.2.2.3.1 Phosphates; 1.2.2.3.2 Carboxylates and Sulfates; 1.2.2.3.3 Amines; 1.2.2.3.4 Alcohols and Phenols; 1.2.2.3.5 Carbonyl Compounds; 1.2.3 Synthesis; 1.2.3.1 Synthesis of Precursor Molecules (Caging Agents); 1.2.3.1.1 Phosphates; 1.2.3.1.2 Carboxylates; 1.2.3.1.3 Amines; 1.2.3.1.4 Alcohols and Phenols; 1.2.4 Applications; 1.2.5 Conclusion and Perspective; References; 1.3 p-Hydroxyphenacyl: a Photoremovable Protecting Group for Caging Bioactive Substrates; 1.3.1 Introduction and History
1.3.2 p-Hydroxyphenacyl1.3.2.1 General Physical and Spectroscopic Properties; 1.3.2.2 Synthesis of pHP-Caged Substrates; 1.3.3 Mechanistic Studies; 1.3.3.1 A Triplet "Photo-Favorskii" Rearrangement; 1.3.3.2 Role of the Triplet Phenol; 1.3.3.3 Correlation of the (3)pK(a) with the Quantum Efficiency; 1.3.4 Applications; 1.3.4.1 Neurotransmitter Release; 1.3.4.2 Peptide Release; 1.3.4.3 Nucleotide Release; 1.3.4.4 Enzyme Photoswitches; 1.3.5 Advantages and Limitations; References; 1.4 Caging of ATP and Glutamate: a Comparative Analysis; 1.4.1 Introduction
1.4.2 General Properties for Caging Groups1.4.3 Caged-ATP; 1.4.3.1 Introduction; 1.4.3.2 Syntheses of the P(3)-caged ATP Derivatives; 1.4.3.3 General Properties of the Caged-ATP Molecules; 1.4.3.4 Conclusion; 1.4.4 Caged Glutamate; 1.4.4.1 Introduction; 1.4.4.2 Syntheses of the Caged Glutamate Derivatives; 1.4.4.3 General Properties of the Caged-Glutamate Molecules; 1.4.4.4 Conclusion; Abbreviations; References; 2 Mechanistic Overview of Phototriggers and Cage Release; 2.1 Introduction; 2.2 Major Photoremovable Protecting Groups; 2.2.1 2-Nitrobenzyl (2-NB); 2.2.1.1 The Reactive Excited State
2.2.1.2 The aci-Nitro Intermediate
Record Nr. UNINA-9910830086703321
Weinheim, : Wiley-VCH, c2005
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Dynamic studies in biology : phototriggers, photoswitches and caged biomolecules / / edited by Maurice Goeldner, Richard Givens
Dynamic studies in biology : phototriggers, photoswitches and caged biomolecules / / edited by Maurice Goeldner, Richard Givens
Pubbl/distr/stampa Weinheim, : Wiley-VCH, c2005
Descrizione fisica 1 online resource (587 p.)
Disciplina 547.2
Altri autori (Persone) GoeldnerMaurice
GivensRichard
Soggetto topico Photobiochemistry
Biomolecules - Separation
Protective groups (Chemistry)
ISBN 9786610520602
9781280520600
1280520604
9783527605590
3527605592
9783527605545
3527605541
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Dynamic Studies in Biology Phototriggers, Photoswitches and Caged Biomolecules; Contents; Foreword; Preface; List of Authors; 1 Photoremovable Protecting Groups Used for the Caging of Biomolecules; 1.1 2-Nitrobenzyl and 7-Nitroindoline Derivatives; 1.1.1 Introduction; 1.1.1.1 Preamble and Scope of the Review; 1.1.1.2 Historical Perspective; 1.1.2 Synthetic Considerations; 1.1.3 Survey of Individual Caged Compounds and Caging Groups; 1.1.3.1 2-Nitrobenzyl Cages; 1.1.3.1.1 Mechanistic Aspects of Photocleavage and By-Product Reactions of 2-Nitrobenzyl Cages
1.1.3.1.2 Representative Survey of Nitrobenzyl-Caged Compounds1.1.3.2 7-Nitroindoline Cages; 1.1.3.2.1 Mechanistic and Structural Aspects of Photochemical Cleavage of 1-Acyl-7-nitroindolines; 1.1.3.2.2 Survey of 7-Nitroindoline Caged Compounds; 1.1.4 Conclusion; References; 1.2 Coumarin-4-ylmethyl Phototriggers; 1.2.1 Introduction; 1.2.2 Spectroscopic and Photochemical Properties; 1.2.2.1 Overview; 1.2.2.2 Phototriggers; 1.2.2.2.1 MCM Groups: 7-Alkoxy-Substituted Coumarins; 1.2.2.2.2 DMCM Groups: 6,7-Dialkoxy-Substituted Coumarins; 1.2.2.2.3 Bhc Groups: 6-Bromo-7-alkoxy-Substituted Coumarins
1.2.2.2.4 DEACM Groups: 7-Dialkylamino-Substituted Coumarins1.2.2.3 Target Molecules; 1.2.2.3.1 Phosphates; 1.2.2.3.2 Carboxylates and Sulfates; 1.2.2.3.3 Amines; 1.2.2.3.4 Alcohols and Phenols; 1.2.2.3.5 Carbonyl Compounds; 1.2.3 Synthesis; 1.2.3.1 Synthesis of Precursor Molecules (Caging Agents); 1.2.3.1.1 Phosphates; 1.2.3.1.2 Carboxylates; 1.2.3.1.3 Amines; 1.2.3.1.4 Alcohols and Phenols; 1.2.4 Applications; 1.2.5 Conclusion and Perspective; References; 1.3 p-Hydroxyphenacyl: a Photoremovable Protecting Group for Caging Bioactive Substrates; 1.3.1 Introduction and History
1.3.2 p-Hydroxyphenacyl1.3.2.1 General Physical and Spectroscopic Properties; 1.3.2.2 Synthesis of pHP-Caged Substrates; 1.3.3 Mechanistic Studies; 1.3.3.1 A Triplet "Photo-Favorskii" Rearrangement; 1.3.3.2 Role of the Triplet Phenol; 1.3.3.3 Correlation of the (3)pK(a) with the Quantum Efficiency; 1.3.4 Applications; 1.3.4.1 Neurotransmitter Release; 1.3.4.2 Peptide Release; 1.3.4.3 Nucleotide Release; 1.3.4.4 Enzyme Photoswitches; 1.3.5 Advantages and Limitations; References; 1.4 Caging of ATP and Glutamate: a Comparative Analysis; 1.4.1 Introduction
1.4.2 General Properties for Caging Groups1.4.3 Caged-ATP; 1.4.3.1 Introduction; 1.4.3.2 Syntheses of the P(3)-caged ATP Derivatives; 1.4.3.3 General Properties of the Caged-ATP Molecules; 1.4.3.4 Conclusion; 1.4.4 Caged Glutamate; 1.4.4.1 Introduction; 1.4.4.2 Syntheses of the Caged Glutamate Derivatives; 1.4.4.3 General Properties of the Caged-Glutamate Molecules; 1.4.4.4 Conclusion; Abbreviations; References; 2 Mechanistic Overview of Phototriggers and Cage Release; 2.1 Introduction; 2.2 Major Photoremovable Protecting Groups; 2.2.1 2-Nitrobenzyl (2-NB); 2.2.1.1 The Reactive Excited State
2.2.1.2 The aci-Nitro Intermediate
Record Nr. UNINA-9911019423603321
Weinheim, : Wiley-VCH, c2005
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Greene's protective groups in organic synthesis / / Peter G. M. Wuts
Greene's protective groups in organic synthesis / / Peter G. M. Wuts
Autore Wuts Peter G. M.
Edizione [6th ed.]
Pubbl/distr/stampa Hoboken, NJ : , : John Wiley & Sons, Incorporated, , [2025]
Descrizione fisica 1 online resource (1804 pages) : illustrations
Disciplina 547.2
Soggetto topico Protective groups (Chemistry)
Organic compounds - Synthesis
Chemistry, Organic - Methodology
Chemistry Techniques, Synthetic
Organic Chemicals
Chemistry, Organic - methods
ISBN 9781394233182
1394233183
9781394233199
1394233191
9781394233175
1394233175
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Cover -- Volume 1 -- Title Page -- Copyright Page -- Dedication -- Contents -- Preface -- Abbreviations -- Chapter 1 The Role of Protective Groups in Organic Synthesis -- Properties of a Protective Group -- Historical Development -- Development of New Protective Groups -- Selection of a Protective Group from This Book -- Synthesis of Complex Substances. Two Examples (As Used in the Synthesis of Himastatin and Palytoxin) of the Selection, Introduction, and Removal of Protective Groups -- Synthesis of Himastatin -- Synthesis of Palytoxin Carboxylic Acid -- Chapter 2 Protection for the Hydroxyl Group Including 1,2- and 1,3-Diols -- Ethers -- Substituted Methyl Ethers -- Substituted Ethyl Ethers -- Methoxy-Substituted Benzyl Ethers -- Silyl Ethers -- Migration of Silyl Groups -- Cleavage -- Esters -- Proximity Assisted Deprotection for Ester Cleavage -- Miscellaneous Esters -- Sulfonates, Sulfenates and Sulfinates as Protective Groups for Alcohols -- Carbonates -- Carbamate Protection of Alcohols -- Protection for 1,2-and 1,3-Diols -- Monoprotection of Diols -- Cyclic Acetals and Ketals -- Chiral Ketones -- Cyclic Ortho Esters -- Silyl Derivatives -- Cyclic Carbonates -- Cyclic Boronates -- Chapter 3 Protection for Phenols and Catechols -- Protection for Phenols and Catechols -- Ethers -- Silyl Ethers -- Esters -- Carbonates -- Carbamates -- Phosphinates -- Sulfonates -- Protection for Catechols (1,2-Dihydroxybenzenes) -- Cyclic Acetals and Ketals -- Cyclic Esters -- Protection for 2-Hydroxybenzenethiols -- Chapter 4 Protection for the Carbonyl Group -- Acetals and Ketals -- Acyclic Acetals and Ketals -- Cyclic Acetals and Ketals -- Chiral Acetals and Ketals -- Dithio Acetals and Ketals -- Acyclic Dithio Acetals and Ketals -- Cyclic Dithio Acetals and Ketals -- Monothio Acetals and Ketals -- Acyclic Monothio Acetals and Ketals.
Cyclic Monothio Acetals and Ketals -- Miscellaneous Derivatives -- O-Substituted Cyanohydrins -- Substituted Hydrazones -- 1,2-Adducts to Aldehydes and Ketones -- Protection of the Carbonyl Group as an Enolate Anions, Enol Ethers, Enamines, and Imines -- Lithium Diisopropylamide (LDA) -- Monoprotection of Dicarbonyl Compounds -- Selective Protection of -and -Diketones -- Cyclic Ketals, Monothio, and Dithio Ketals -- Chapter 5 Protection for the Carboxyl Group -- Esters -- General Preparations of Esters -- General Cleavage of Esters -- Transesterification -- Enzymatically Cleavable Esters -- Substituted Methyl Esters -- 2-Substituted Ethyl Esters -- Substituted Benzyl Esters -- Silyl Esters -- Activated Esters -- Miscellaneous Derivatives -- Stannyl Esters -- Amides and Hydrazides -- Amides -- Protection of Sulfonic Acids -- Protection of Boronic Acids -- Chapter 6 Protection for the Thiol Group -- Thioethers -- S-Diphenylmethyl, Substituted S-Diphenylmethyl, and S-Triphenylmethyl Thioethers -- 4-Methoxytrityl (Mtt.SR) Thioether -- Substituted S-Methyl Derivatives: Monothio, Dithio, and Aminothio Acetals -- Substituted S-Ethyl Derivatives -- Silyl Thioethers -- Thioesters -- Thiocarbonate Derivatives -- Thiocarbamate Derivatives -- Miscellaneous Derivatives -- Unsymmetrical Disulfides -- Sulfenyl Derivatives -- Protection for Dithiols: Dithio Acetals and Ketals -- Protection for Sulfides -- S-P Derivatives -- Protection for the Amino Thiol Group -- Protection for Selenols -- Volume 2 -- Title Page -- Copyright Page -- Dedication -- Contents -- Preface -- Abbreviations -- Chapter 7 Protection for the Amino Group -- Introduction to Amines -- Carbamates -- Substituted Ethyl Carbamates -- Carbamates Cleaved by a 1,6-Elimination -- Cleavage by -Elimination -- Photolytically Cleaved Carbamates -- Miscellaneous Carbamates -- Urea-Type Derivatives -- Amides.
Transamidation -- Assisted Cleavage of Amides -- Amide Cleavage Induced by Nitro Group Reduction -- Amide Cleavage Induced by Release of an Alcohol -- Amides Cleaved by Other Chemical Reactions -- Bisprotection of Amines -- Special -NH Protective Groups -- N-Alkyl and N-Aryl Amines -- Imine Derivatives -- Enamine Derivatives -- N-Heteroatom Derivatives -- N-Metal Derivatives -- N-N Derivatives -- N-P Derivatives -- N-Si Derivatives -- N-S Derivatives -- N-Sulfenyl Derivatives -- Protection of Amino Alcohols -- Protection for Imidazoles, Pyrroles, Indoles, and Other Aromatic Heterocycles -- N-Sulfonyl Derivatives -- Carbamates -- N-Alkyl and N-Aryl Derivatives -- Amino Acetal Derivatives -- Amides -- Protection for the Amide -NH -- Amides -- Protection for the Sulfonamide -NH -- Chapter 8 Protection for the Alkyne -CH -- Chapter 9 Protection for the Phosphate Group -- Introduction -- Some General Methods for Phosphate Ester Formation -- Removal of Protective Groups from Phosphorus -- Alkyl Phosphates -- Phosphates Cleaved by Cyclodeesterification -- 2-Substituted Ethyl Phosphates -- Haloethyl Phosphates -- Benzyl Phosphates -- Phenyl Phosphates -- Photochemically Cleaved Phosphate Protective Groups -- Amidates -- Miscellaneous Derivatives -- Chapter 10 Protecting Group Effects in Carbohydrate Chemistry -- Introduction -- Early Observations Protecting Group-Induced Reactivity -- Relative Reactivities -- Fraser-Reidfs Concept of Armed and Disarmed -- Examples of How Protecting Groups Arm and Disarm Glycosides -- Aglycone Transfer -- Participating Groups -- Ester at the C-2 Hydroxyl -- Esters at Positions Other Than 2 -- Ethers Primarily at the C-2 Hydroxyl -- Conformational Restriction -- Benzylidene Group and other Acetals -- Directing Effect of Silylene Groups -- Carbonates as Conformational Restrictors -- Orthoester Conformational Restriction.
Silyl Groups: Conformational and Reactivity Effect -- Studies on the Conformational Flip Using Silyl Groups -- Amino Sugar Protection -- Imine Protection -- Protection of the NH2 as An Azide -- Imide Protection -- Oxazolidinones -- Introduction to the Formation of Sialyl Glycosides -- Amides and Their Effects -- Protecting Group Effects in the Glycosylation of 2-Deoxy Sugars -- Furanosides -- Protecting Group Effects on Acceptors -- C-Glycosylation -- Sphingolipids -- Introduction -- Chapter 11 Reactivities, Reagents, and Reactivity Charts -- Reactivities -- Reagents -- Reactivity Charts -- Reactivity Chart 1. Protection for Hydroxyl Group: Ethers -- Reactivity Chart 2. Protection for Hydroxyl Group: Esters -- Reactivity Chart 3. Protection for 1,2-and 1,3-Diols -- Reactivity Chart 4. Protection for Phenols and Catechols -- Reactivity Chart 5. Protection for the Carbonyl Group -- Reactivity Chart 6. Protection for the Carboxyl Group -- Reactivity Chart 7. Protection for the Thiol Group -- Reactivity Chart 8. Protection for the Amino Group: Carbamates -- Reactivity Chart 9. Protection for the Amino Group: Amides -- Reactivity Chart 10. Protection for the Amino Group: Special -NH Protective Groups -- Reactivity Chart 11. Selective Deprotection of Silyl Ethers -- Index -- EULA.
Altri titoli varianti Protective groups in organic synthesis
Record Nr. UNINA-9911019677803321
Wuts Peter G. M.  
Hoboken, NJ : , : John Wiley & Sons, Incorporated, , [2025]
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Greene's protective groups in organic synthesis / / Peter G. M. Wuts
Greene's protective groups in organic synthesis / / Peter G. M. Wuts
Autore Wuts Peter G. M.
Edizione [Fifth edition.]
Pubbl/distr/stampa Hoboken, New Jersey : , : Wiley, , 2014
Descrizione fisica 1 online resource (1399 p.)
Disciplina 547.2
Altri autori (Persone) GreeneTheodora W <1931-2005.> (Theodora Whatmough)
Soggetto topico Organic compounds - Synthesis
Protective groups (Chemistry)
ISBN 1-118-90512-1
1-118-90507-5
1-118-90509-1
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Greene's Protective Groups in Organic Synthesis; Contents; Preface to the Fifth Edition; Preface to the Fourth Edition; Preface to the Third Edition; Preface to the Second Edition; Preface to the First Edition; Abbreviations; 1. The Role of Protective Groups in Organic Synthesis; Properties of a Protective Group; Historical Development; Development of New Protective Groups; Selection of a Protective Group from This Book; Synthesis of Complex Substances: Two Examples (As used in the Synthesis of Himastatin and Palytoxin) of the Selection, Introduction, and Removal of Protective Groups
Synthesis of HimastatinSynthesis of Palytoxin Carboxylic Acid; 2. Protection for the Hydroxyl Group, Including 1,2- and 1,3-Diols; Ethers; Substituted Methyl Ethers; Substituted Ethyl Ethers; Methoxy-Substituted Benzyl Ethers; Silyl Ethers; Esters; Bisfluorous Chain-Type Propanoate (Bfp-OR) Ester; Proximity-Assisted Deprotection for Ester Cleavage; Miscellaneous Esters; Sulfonates, Sulfenates, and Sulfinates as Protective Groups for Alcohols; Carbonates; Carbamates; Protection for 1,2- and 1,3-Diols; Monoprotection of Diols; Cyclic Acetals and Ketals; Chiral Ketones; Cyclic Orthoesters
Silyl DerivativesCyclic Carbonates; Cyclic Boronates; 3. Protection for Phenols and Catechols; Protection for Phenols; Ethers; Silyl Ethers; Esters; Carbonates; Carbamates; Phosphinates; Sulfonates; Protection for Catechols (1,2-Dihydroxybenzenes); Cyclic Acetals and Ketals; Cyclic Esters; Protection for 2-Hydroxybenzenethiols; 4. Protection for the Carbonyl Group; Acetals and Ketals; Acyclic Acetals and Ketals; Cyclic Acetals and Ketals; Chiral Acetals and Ketals; Dithio Acetals and Ketals; Cyclic Dithio Acetals and Ketals; Monothio Acetals and Ketals; Diseleno Acetals and Ketals
Miscellaneous DerivativesO-Substituted Cyanohydrins; Substituted Hydrazones; Oxime Derivatives; 1,2-Adducts to Aldehydes and Ketones; Cyclic Derivatives; Protection of the Carbonyl Group as Enolate Anions, Enol Ethers, Enamines, and Imines; Monoprotection of Dicarbonyl Compounds; Selective Protection of α- and β-Diketones; Cyclic Ketals, Monothio and Dithio Ketals; 5. Protection for the Carboxyl Group; Esters; General Preparation of Esters; General Cleavage of Esters; Transesterification; Enzymatically Cleavable Esters; Substituted Methyl Esters; 2-Substituted Ethyl Esters
2,6-Dialkylphenyl EstersSubstituted Benzyl Esters; Silyl Esters; Activated Esters; Miscellaneous Derivatives; Stannyl Esters; Amides and Hydrazides; Amides; Hydrazides; Protection of Sulfonic Acids; Protection of Boronic Acids; 6. Protection for the Thiol Group; Thioethers; S-Diphenylmethyl, Substituted S-Diphenylmethyl, and S-Triphenylmethyl Thioethers; Substituted S-Methyl Derivatives: Monothio, Dithio, and Aminothio Acetals; Substituted S-Ethyl Derivatives; Silyl Thioethers; Thioesters; Thiocarbonate Derivatives; Thiocarbamate Derivatives; Miscellaneous Derivatives
Unsymmetrical Disulfides
Record Nr. UNINA-9910132164403321
Wuts Peter G. M.  
Hoboken, New Jersey : , : Wiley, , 2014
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Greene's protective groups in organic synthesis / / Peter G. M. Wuts
Greene's protective groups in organic synthesis / / Peter G. M. Wuts
Autore Wuts Peter G. M.
Edizione [Fifth edition.]
Pubbl/distr/stampa Hoboken, New Jersey : , : Wiley, , 2014
Descrizione fisica 1 online resource (1399 p.)
Disciplina 547.2
Altri autori (Persone) GreeneTheodora W <1931-2005.> (Theodora Whatmough)
Soggetto topico Organic compounds - Synthesis
Protective groups (Chemistry)
ISBN 1-118-90512-1
1-118-90507-5
1-118-90509-1
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Greene's Protective Groups in Organic Synthesis; Contents; Preface to the Fifth Edition; Preface to the Fourth Edition; Preface to the Third Edition; Preface to the Second Edition; Preface to the First Edition; Abbreviations; 1. The Role of Protective Groups in Organic Synthesis; Properties of a Protective Group; Historical Development; Development of New Protective Groups; Selection of a Protective Group from This Book; Synthesis of Complex Substances: Two Examples (As used in the Synthesis of Himastatin and Palytoxin) of the Selection, Introduction, and Removal of Protective Groups
Synthesis of HimastatinSynthesis of Palytoxin Carboxylic Acid; 2. Protection for the Hydroxyl Group, Including 1,2- and 1,3-Diols; Ethers; Substituted Methyl Ethers; Substituted Ethyl Ethers; Methoxy-Substituted Benzyl Ethers; Silyl Ethers; Esters; Bisfluorous Chain-Type Propanoate (Bfp-OR) Ester; Proximity-Assisted Deprotection for Ester Cleavage; Miscellaneous Esters; Sulfonates, Sulfenates, and Sulfinates as Protective Groups for Alcohols; Carbonates; Carbamates; Protection for 1,2- and 1,3-Diols; Monoprotection of Diols; Cyclic Acetals and Ketals; Chiral Ketones; Cyclic Orthoesters
Silyl DerivativesCyclic Carbonates; Cyclic Boronates; 3. Protection for Phenols and Catechols; Protection for Phenols; Ethers; Silyl Ethers; Esters; Carbonates; Carbamates; Phosphinates; Sulfonates; Protection for Catechols (1,2-Dihydroxybenzenes); Cyclic Acetals and Ketals; Cyclic Esters; Protection for 2-Hydroxybenzenethiols; 4. Protection for the Carbonyl Group; Acetals and Ketals; Acyclic Acetals and Ketals; Cyclic Acetals and Ketals; Chiral Acetals and Ketals; Dithio Acetals and Ketals; Cyclic Dithio Acetals and Ketals; Monothio Acetals and Ketals; Diseleno Acetals and Ketals
Miscellaneous DerivativesO-Substituted Cyanohydrins; Substituted Hydrazones; Oxime Derivatives; 1,2-Adducts to Aldehydes and Ketones; Cyclic Derivatives; Protection of the Carbonyl Group as Enolate Anions, Enol Ethers, Enamines, and Imines; Monoprotection of Dicarbonyl Compounds; Selective Protection of α- and β-Diketones; Cyclic Ketals, Monothio and Dithio Ketals; 5. Protection for the Carboxyl Group; Esters; General Preparation of Esters; General Cleavage of Esters; Transesterification; Enzymatically Cleavable Esters; Substituted Methyl Esters; 2-Substituted Ethyl Esters
2,6-Dialkylphenyl EstersSubstituted Benzyl Esters; Silyl Esters; Activated Esters; Miscellaneous Derivatives; Stannyl Esters; Amides and Hydrazides; Amides; Hydrazides; Protection of Sulfonic Acids; Protection of Boronic Acids; 6. Protection for the Thiol Group; Thioethers; S-Diphenylmethyl, Substituted S-Diphenylmethyl, and S-Triphenylmethyl Thioethers; Substituted S-Methyl Derivatives: Monothio, Dithio, and Aminothio Acetals; Substituted S-Ethyl Derivatives; Silyl Thioethers; Thioesters; Thiocarbonate Derivatives; Thiocarbamate Derivatives; Miscellaneous Derivatives
Unsymmetrical Disulfides
Record Nr. UNINA-9910822567703321
Wuts Peter G. M.  
Hoboken, New Jersey : , : Wiley, , 2014
Materiale a stampa
Lo trovi qui: Univ. Federico II
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Greene's protective groups in organic synthesis [[electronic resource]]
Greene's protective groups in organic synthesis [[electronic resource]]
Autore Wuts Peter G. M
Edizione [4th ed.]
Pubbl/distr/stampa Hoboken, N.J., : Wiley-Interscience, c2007
Descrizione fisica 1 online resource (1112 p.)
Disciplina 547.2
Altri autori (Persone) GreeneTheodora W <1931-2005.> (Theodora Whatmough)
Soggetto topico Organic compounds - Synthesis
Protective groups (Chemistry)
ISBN 1-280-65448-1
9786610654482
0-470-05348-8
0-470-05347-X
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto The role of protective groups in organic synthesis. -- Protection for the hydroxl group, including 1,2- and 1,3-diols. -- Protection for phenols and catechols. -- Protection for the carbonyl group. -- Protection for the carboxyl group. -- Protection for the thiol group. -- Protection for the amino group. -- Protection for the alkyne - CH. -- Protection for the phosphate group. -- Reactivities, reagents, and reactivity charts.
Record Nr. UNINA-9910143561903321
Wuts Peter G. M  
Hoboken, N.J., : Wiley-Interscience, c2007
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Greene's protective groups in organic synthesis [[electronic resource]]
Greene's protective groups in organic synthesis [[electronic resource]]
Autore Wuts Peter G. M
Edizione [4th ed.]
Pubbl/distr/stampa Hoboken, N.J., : Wiley-Interscience, c2007
Descrizione fisica 1 online resource (1112 p.)
Disciplina 547.2
Altri autori (Persone) GreeneTheodora W <1931-2005.> (Theodora Whatmough)
Soggetto topico Organic compounds - Synthesis
Protective groups (Chemistry)
ISBN 1-280-65448-1
9786610654482
0-470-05348-8
0-470-05347-X
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto The role of protective groups in organic synthesis. -- Protection for the hydroxl group, including 1,2- and 1,3-diols. -- Protection for phenols and catechols. -- Protection for the carbonyl group. -- Protection for the carboxyl group. -- Protection for the thiol group. -- Protection for the amino group. -- Protection for the alkyne - CH. -- Protection for the phosphate group. -- Reactivities, reagents, and reactivity charts.
Record Nr. UNINA-9910830442903321
Wuts Peter G. M  
Hoboken, N.J., : Wiley-Interscience, c2007
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Greene's protective groups in organic synthesis [[electronic resource]]
Greene's protective groups in organic synthesis [[electronic resource]]
Autore Wuts Peter G. M
Edizione [4th ed.]
Pubbl/distr/stampa Hoboken, N.J., : Wiley-Interscience, c2007
Descrizione fisica 1 online resource (1112 p.)
Disciplina 547.2
Altri autori (Persone) GreeneTheodora W <1931-2005.> (Theodora Whatmough)
Soggetto topico Organic compounds - Synthesis
Protective groups (Chemistry)
ISBN 1-280-65448-1
9786610654482
0-470-05348-8
0-470-05347-X
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto The role of protective groups in organic synthesis. -- Protection for the hydroxl group, including 1,2- and 1,3-diols. -- Protection for phenols and catechols. -- Protection for the carbonyl group. -- Protection for the carboxyl group. -- Protection for the thiol group. -- Protection for the amino group. -- Protection for the alkyne - CH. -- Protection for the phosphate group. -- Reactivities, reagents, and reactivity charts.
Record Nr. UNINA-9911019513303321
Wuts Peter G. M  
Hoboken, N.J., : Wiley-Interscience, c2007
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Protecting groups : strategies and applications in carbohydrate chemistry / / edited by Sébastien Vidal
Protecting groups : strategies and applications in carbohydrate chemistry / / edited by Sébastien Vidal
Pubbl/distr/stampa Weinheim, Germany : , : Wiley-VCH, , [2019]
Descrizione fisica 1 online resource (529 pages)
Disciplina 547.78
Soggetto topico Carbohydrates
Protective groups (Chemistry)
ISBN 3-527-69702-0
3-527-69700-4
3-527-69701-2
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Record Nr. UNINA-9910555143403321
Weinheim, Germany : , : Wiley-VCH, , [2019]
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui