top

  Info

  • Utilizzare la checkbox di selezione a fianco di ciascun documento per attivare le funzionalità di stampa, invio email, download nei formati disponibili del (i) record.

  Info

  • Utilizzare questo link per rimuovere la selezione effettuata.

Biblioteca

MARC Lista (tabellare)
Application of IC-MS and IC-ICP-MS in environmental research / / edited by Rajmund Michalski
Application of IC-MS and IC-ICP-MS in environmental research / / edited by Rajmund Michalski
Pubbl/distr/stampa Hoboken, New Jersey : , : Wiley, , 2016
Descrizione fisica 1 online resource (308 p.)
Disciplina 543/.82
Soggetto topico Ion exchange chromatography
Inductively coupled plasma mass spectrometry
Soggetto genere / forma Electronic books.
ISBN 1-119-08548-9
1-119-08547-0
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto TITLE PAGE; COPYRIGHT; TABLE OF CONTENTS; LIST OF CONTRIBUTORS; PREFACE; CHAPTER 1: PRINCIPLES AND APPLICATIONS OF ION CHROMATOGRAPHY; 1.1 PRINCIPLES OF ION CHROMATOGRAPHY; 1.2 ION CHROMATOGRAPHY APPLICATIONS; 1.3 SAMPLE PREPARATION FOR ION CHROMATOGRAPHY; 1.4 SELECTED METHODOLOGICAL ASPECTS OF ION DETERMINATION WITH ION CHROMATOGRAPHY; 1.5 ION CHROMATOGRAPHY DEVELOPMENT PERSPECTIVES; 1.6 REFERENCES; CHAPTER 2: MASS SPECTROMETRIC DETECTORS FOR ENVIRONMENTAL STUDIES; 2.1 INTRODUCTION; 2.2 MASS SPECTROMETRIC DETECTORS; ACKNOWLEDGMENTS; 2.3 REFERENCES
CHAPTER 3: HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY COUPLED TO INDUCTIVELY COUPLED PLASMA MS/ELECTROSPRAY IONIZATION MS3.1 SEPARATION PRINCIPLES; 3.2 DETECTION PRINCIPLES; 3.3 HYPHENATED TECHNIQUES; 3.4 HPLC(IC)-ICP-MS/ESI-MS; 3.5 APPLICATIONS AND CONCLUSION; 3.6 REFERENCES; CHAPTER 4: APPLICATION OF IC-MS IN ORGANIC ENVIRONMENTAL GEOCHEMISTRY; 4.1 INTRODUCTION; 4.2 CARBOXYLIC ACIDS; 4.3 CARBOHYDRATES; 4.4 AMINES AND AMINO ACIDS; 4.5 TRENDS AND PERSPECTIVES; 4.6 REFERENCES; CHAPTER 5: ANALYSIS OF OXYHALIDES AND HALOACETIC ACIDS IN DRINKING WATER USING IC-MS AND IC-ICP-MS; 5.1 INTRODUCTION
5.2 SOURCE OF OXYHALIDES AND HAAS5.3 ANALYSIS OF OXYHALIDES AND HAAS; 5.4 APPLICATION FOR MONITORING OF OXYHALIDES AND HAA IN DRINKING WATER; SUMMARY; 5.5 REFERENCES; CHAPTER 6: ANALYSIS OF VARIOUS ANIONIC METABOLITES IN PLANT AND ANIMAL MATERIAL BY IC-MS; 6.1 INTRODUCTION; 6.2 OPTIMIZATION OF HPIC AND MS SETTINGS; 6.3 APPLICATION OF THE METHOD IN ANALYSIS OF METABOLITES IN PLANT AND ANIMAL MATERIAL; CONCLUSIONS; 6.4 REFERENCES; CHAPTER 7: ANALYSIS OF PERCHLORATE ION IN VARIOUS MATRICES USING ION CHROMATOGRAPHY HYPHENATED WITH MASS SPECTROMETRY; 7.1 INTRODUCTION
7.2 PRECAUTIONS UNIQUE TO ION CHROMATOGRAPHY-MASS SPECTROMETRY7.3 RESULTS AND DISCUSSION; ACKNOWLEDGMENT; 7.4 REFERENCES; CHAPTER 8: SAMPLE PREPARATION TECHNIQUES FOR ION CHROMATOGRAPHY; 8.1 INTRODUCTION; 8.2 WHEN AND WHY IS SAMPLE PREPARATION REQUIRED IN ION CHROMATOGRAPHY?; 8.3 AUTOMATION OF SAMPLE PREPARATION (IN-LINE TECHNIQUES); 8.4 SAMPLE PREPARATION METHODS; 8.5 TRACE ANALYSIS AND PRECONCENTRATION FOR ION CHROMATOGRAPHIC ANALYSIS; 8.6 IN-LINE PRESEPARATIONS USING TWO-DIMENSIONAL ION CHROMATOGRAPHY (2D-IC); 8.7 SAMPLE PREPARATION OF SOLID SAMPLES
8.8 AIR ANALYSIS USING ION CHROMATOGRAPHY - APPLICATION TO GASES AND PARTICULATE MATTER8.9 POSTCOLUMN ELUENT TREATMENT PRIOR TO MS DETECTION; 8.10 CONCLUDING REMARKS; 8.11 REFERENCES; INDEX; END USER LICENSE AGREEMENT
Record Nr. UNINA-9910136757503321
Hoboken, New Jersey : , : Wiley, , 2016
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Application of IC-MS and IC-ICP-MS in environmental research / / edited by Rajmund Michalski
Application of IC-MS and IC-ICP-MS in environmental research / / edited by Rajmund Michalski
Pubbl/distr/stampa Hoboken, New Jersey : , : Wiley, , 2016
Descrizione fisica 1 online resource (308 p.)
Disciplina 543/.82
Soggetto topico Ion exchange chromatography
Inductively coupled plasma mass spectrometry
ISBN 1-119-08548-9
1-119-08547-0
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto TITLE PAGE; COPYRIGHT; TABLE OF CONTENTS; LIST OF CONTRIBUTORS; PREFACE; CHAPTER 1: PRINCIPLES AND APPLICATIONS OF ION CHROMATOGRAPHY; 1.1 PRINCIPLES OF ION CHROMATOGRAPHY; 1.2 ION CHROMATOGRAPHY APPLICATIONS; 1.3 SAMPLE PREPARATION FOR ION CHROMATOGRAPHY; 1.4 SELECTED METHODOLOGICAL ASPECTS OF ION DETERMINATION WITH ION CHROMATOGRAPHY; 1.5 ION CHROMATOGRAPHY DEVELOPMENT PERSPECTIVES; 1.6 REFERENCES; CHAPTER 2: MASS SPECTROMETRIC DETECTORS FOR ENVIRONMENTAL STUDIES; 2.1 INTRODUCTION; 2.2 MASS SPECTROMETRIC DETECTORS; ACKNOWLEDGMENTS; 2.3 REFERENCES
CHAPTER 3: HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY COUPLED TO INDUCTIVELY COUPLED PLASMA MS/ELECTROSPRAY IONIZATION MS3.1 SEPARATION PRINCIPLES; 3.2 DETECTION PRINCIPLES; 3.3 HYPHENATED TECHNIQUES; 3.4 HPLC(IC)-ICP-MS/ESI-MS; 3.5 APPLICATIONS AND CONCLUSION; 3.6 REFERENCES; CHAPTER 4: APPLICATION OF IC-MS IN ORGANIC ENVIRONMENTAL GEOCHEMISTRY; 4.1 INTRODUCTION; 4.2 CARBOXYLIC ACIDS; 4.3 CARBOHYDRATES; 4.4 AMINES AND AMINO ACIDS; 4.5 TRENDS AND PERSPECTIVES; 4.6 REFERENCES; CHAPTER 5: ANALYSIS OF OXYHALIDES AND HALOACETIC ACIDS IN DRINKING WATER USING IC-MS AND IC-ICP-MS; 5.1 INTRODUCTION
5.2 SOURCE OF OXYHALIDES AND HAAS5.3 ANALYSIS OF OXYHALIDES AND HAAS; 5.4 APPLICATION FOR MONITORING OF OXYHALIDES AND HAA IN DRINKING WATER; SUMMARY; 5.5 REFERENCES; CHAPTER 6: ANALYSIS OF VARIOUS ANIONIC METABOLITES IN PLANT AND ANIMAL MATERIAL BY IC-MS; 6.1 INTRODUCTION; 6.2 OPTIMIZATION OF HPIC AND MS SETTINGS; 6.3 APPLICATION OF THE METHOD IN ANALYSIS OF METABOLITES IN PLANT AND ANIMAL MATERIAL; CONCLUSIONS; 6.4 REFERENCES; CHAPTER 7: ANALYSIS OF PERCHLORATE ION IN VARIOUS MATRICES USING ION CHROMATOGRAPHY HYPHENATED WITH MASS SPECTROMETRY; 7.1 INTRODUCTION
7.2 PRECAUTIONS UNIQUE TO ION CHROMATOGRAPHY-MASS SPECTROMETRY7.3 RESULTS AND DISCUSSION; ACKNOWLEDGMENT; 7.4 REFERENCES; CHAPTER 8: SAMPLE PREPARATION TECHNIQUES FOR ION CHROMATOGRAPHY; 8.1 INTRODUCTION; 8.2 WHEN AND WHY IS SAMPLE PREPARATION REQUIRED IN ION CHROMATOGRAPHY?; 8.3 AUTOMATION OF SAMPLE PREPARATION (IN-LINE TECHNIQUES); 8.4 SAMPLE PREPARATION METHODS; 8.5 TRACE ANALYSIS AND PRECONCENTRATION FOR ION CHROMATOGRAPHIC ANALYSIS; 8.6 IN-LINE PRESEPARATIONS USING TWO-DIMENSIONAL ION CHROMATOGRAPHY (2D-IC); 8.7 SAMPLE PREPARATION OF SOLID SAMPLES
8.8 AIR ANALYSIS USING ION CHROMATOGRAPHY - APPLICATION TO GASES AND PARTICULATE MATTER8.9 POSTCOLUMN ELUENT TREATMENT PRIOR TO MS DETECTION; 8.10 CONCLUDING REMARKS; 8.11 REFERENCES; INDEX; END USER LICENSE AGREEMENT
Record Nr. UNINA-9910830631603321
Hoboken, New Jersey : , : Wiley, , 2016
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Applications of ion chromatography for pharmaceutical and biological products / / edited by Lokesh Bhattacharyya, Jeffrey S. Rohrer
Applications of ion chromatography for pharmaceutical and biological products / / edited by Lokesh Bhattacharyya, Jeffrey S. Rohrer
Edizione [1st ed.]
Pubbl/distr/stampa Hoboken, N.J., : John Wiley & Sons, Inc., c2012
Descrizione fisica 1 online resource (477 p.)
Disciplina 660.6/3
Altri autori (Persone) BhattacharyyaLokesh
RohrerJeffrey S
Soggetto topico Ion exchange chromatography
Biological products - Analysis
Pharmaceutical industry - Standards
ISBN 1-280-59061-0
9786613620446
1-118-14699-9
1-118-14700-6
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto APPLICATIONS OF ION CHROMATOGRAPHY FOR PHARMACEUTICAL AND BIOLOGICAL PRODUCTS; CONTENTS; CONTRIBUTORS; PREFACE; PART I PRINCIPLES, MECHANISM,AND INSTRUMENTATION; 1 ION CHROMATOGRAPHY-PRINCIPLES AND APPLICATIONS; 2 RETENTION PROCESSES IN ION-EXCLUSION CHROMATOGRAPHY: A NEW PERSPECTIVE; 3 PULSED ELECTRO-CHEMICAL DETECTION IN ION CHROMATOGRAPHY; 4 SUPPRESSOR DESIGN AND DETECTION FOR ION CHROMATOGRAPHY; 5 MODELLING AND OPTIMIZATION OF ION CHROMATOGRAPHIC SEPARATIONS OF PHARMACEUTICALLY RELEVANT ORGANIC IONS; PART II PHARMACEUTICAL APPLICATIONS; 6 ION CHROMATOGRAPHY IN PHARMACEUTICAL DRUG ANALYSIS
7 ANALYSIS FOR IMPURITIES BY ION CHROMATOGRAPHY 8 ION CHROMATOGRAPHY ANALYSIS OF AMINOGLYCOSIDE ANTIBIOTICS; 9 USE OF CATION-EXCHANGE ION CHROMATOGRAPHY IN THE ANALYSIS OF PHARMACEUTICALS; 10 COMPREHENSIVE APPROACHES FOR MEASUREMENT OF ACTIVE PHARMACEUTICAL INGREDIENTS, COUNTER-IONS,AND EXCIPIENTS USING HPLC WITH CHARGED AEROSOL DETECTION; 11 HIGH PERFORMANCE ION CHROMATOGRAPHIC ANALYSIS OF CHOLINERGIC COMPOUNDS: CARBACHOLAND BETHANECHOL, AND ASSOCIATED DEGRADATION PRODUCTS; 12 ION CHROMATOGRAPHIC ANALYSIS OF PHARMACEUTICALS FOR AUTHENTICITY AND ADULTERATION
13 ION CHROMATOGRAPHY OF DRUG PRODUCT COUNTER-IONS AND OTHER IONS IN DRUG PRODUCTS 14 SAMPLE PREPARATION TECHNIQUES IN ION CHROMATOGRAPHY FOR PHARMACEUTICAL APPLICATIONS; 15 VALIDATION OF ION CHROMATOGRAPHIC METHODS; 16 PHARMACOPEIAL APPLICATIONS OF ION CHROMATOGRAPHY; PART III BIOTECHNOLOGY APPLICATIONS; 17 GLYCAN ANALYSIS BY HIGH PERFORMANCE ANION EXCHANGE CHROMATOGRAPHY WITH PULSED AMPEROMETRIC DETECTION; 18 MONOSACCHARIDE ANALYSIS OF GLYCOPROTEINS BY HIGH-PERFORMANCE ANION-EXCHANGE CHROMATOGRAPHY WITH PULSED AMPEROMETRIC DETECTION
19 TWO-DIMENSIONAL ION CHROMATOGRAPHY FOR SIMULTANEOUS DETERMINATION OF AMINO ACIDS AND CARBOHYDRATES 20 MONITORING PROTEIN N-GLYCOSYLATION CONSISTENCY USING HPAEC-PAD; 21 OLIGOSACCHARIDE ANALYSIS BY HIGH-PERFORMANCE ANION-EXCHANGE CHROMATOGRAPHY HYPHENATED TO INTEGRATED PULSED AMPEROMETRIC DETECTION AND ON-LINE ION-TRAP MASS SPECTROMETRY; PART IV VACCINE APPLICATIONS; 22 APPLICATIONS OF ION CHROMATOGRAPHY IN BIOLOGICAL PRODUCT ANALYSES
23 HIGH PERFORMANCE ANION-EXCHANGE CHROMATOGRAPHY WITH PULSED AMPEROMETRIC DETECTION (HPAEC-PAD)ANALYSIS OF GBS GLYCOCON JUGATE VACCINES:FROM FERMENTATION TO FINAL PRODUCT 24 STABILITY STUDIES AND CHARACTERIZATION OF MENINGOCOCCAL A, C, Y, AND W135 GLYCOCONJUGATE VACCINE; PART V APPENDICES; Appendix 1 DISSOCIATION CONSTANTS (pKa) OF ORGANICACIDS (AT 20?C); Appendix 2 DISSOCIATION CONSTANTS (pKa) OF COMMON SUGARS AND ALCOHOLS; INDEX
Record Nr. UNINA-9910141309403321
Hoboken, N.J., : John Wiley & Sons, Inc., c2012
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Determination of perchlorate in drinking water by ion chromatography with suppressed conductivity and electrospray ionization mass spectrometry [[electronic resource] /] / Elizabeth Hedrick ... [and others]
Determination of perchlorate in drinking water by ion chromatography with suppressed conductivity and electrospray ionization mass spectrometry [[electronic resource] /] / Elizabeth Hedrick ... [and others]
Edizione [Revision 1.0.]
Pubbl/distr/stampa Cincinnati, Ohio : , : National Exposure Research Laboratory, Office of Research and Development, U.S. Environmental Protection Agency, , [2005]
Descrizione fisica 48 pages : digital, PDF file
Altri autori (Persone) HedrickElizabeth
Soggetto topico Drinking water - Analysis
Perchlorates - Toxicology
Ion exchange chromatography
Mass spectrometry
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Altri titoli varianti Method 332.0: Determination of perchlorate in drinking water by ion chromatography with suppressed conductivity and electrospray ionization mass spectrometry
Record Nr. UNINA-9910697922403321
Cincinnati, Ohio : , : National Exposure Research Laboratory, Office of Research and Development, U.S. Environmental Protection Agency, , [2005]
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Handbook of ion chromatography / / Joachim Weiss ; with a foreword by Oleg Shpigun
Handbook of ion chromatography / / Joachim Weiss ; with a foreword by Oleg Shpigun
Autore Weiss Joachim
Edizione [4th ed.]
Pubbl/distr/stampa Weinheim, Germany : , : Wiley-VCH, , 2016
Descrizione fisica 1 online resource (2215 p.)
Disciplina 543.0893
Soggetto topico Ion exchange chromatography
Chromatographic analysis
Soggetto genere / forma Electronic books.
ISBN 3-527-65164-0
3-527-65163-2
3-527-65161-6
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Record Nr. UNINA-9910166638903321
Weiss Joachim  
Weinheim, Germany : , : Wiley-VCH, , 2016
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Handbook of ion chromatography / / Joachim Weiss ; with a foreword by Oleg Shpigun
Handbook of ion chromatography / / Joachim Weiss ; with a foreword by Oleg Shpigun
Autore Weiss Joachim
Edizione [4th ed.]
Pubbl/distr/stampa Weinheim, Germany : , : Wiley-VCH, , 2016
Descrizione fisica 1 online resource (2215 p.)
Disciplina 543.0893
Soggetto topico Ion exchange chromatography
Chromatographic analysis
ISBN 3-527-65164-0
3-527-65163-2
3-527-65161-6
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Record Nr. UNINA-9910830487603321
Weiss Joachim  
Weinheim, Germany : , : Wiley-VCH, , 2016
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
High performance chelation ion chromatography [[electronic resource] /] / Pavel N. Nesterenko, Phil Jones, Brett Paull
High performance chelation ion chromatography [[electronic resource] /] / Pavel N. Nesterenko, Phil Jones, Brett Paull
Autore Nesterenko Pavel N
Pubbl/distr/stampa Cambridge, : Royal Society of Chemistry, c2011
Descrizione fisica 1 online resource (317 p.)
Disciplina 543.82
Altri autori (Persone) JonesP (Phil)
PaullBrett
Collana RSC chromatography monographs
Soggetto topico High performance liquid chromatography
Ion exchange chromatography
Complexometric titration
Chelates
Trace elements - Analysis
Soggetto genere / forma Electronic books.
ISBN 1-84973-231-0
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Record Nr. UNINA-9910459704003321
Nesterenko Pavel N  
Cambridge, : Royal Society of Chemistry, c2011
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
High performance chelation ion chromatography [[electronic resource] /] / Pavel N. Nesterenko, Phil Jones, Brett Paull
High performance chelation ion chromatography [[electronic resource] /] / Pavel N. Nesterenko, Phil Jones, Brett Paull
Autore Nesterenko Pavel N
Pubbl/distr/stampa Cambridge, : Royal Society of Chemistry, c2011
Descrizione fisica 1 online resource (317 p.)
Disciplina 543.82
Altri autori (Persone) JonesP (Phil)
PaullBrett
Collana RSC chromatography monographs
Soggetto topico High performance liquid chromatography
Ion exchange chromatography
Complexometric titration
Chelates
Trace elements - Analysis
ISBN 1-84973-231-0
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Record Nr. UNINA-9910790088503321
Nesterenko Pavel N  
Cambridge, : Royal Society of Chemistry, c2011
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
High performance chelation ion chromatography / / Pavel N. Nesterenko, Phil Jones, Brett Paull
High performance chelation ion chromatography / / Pavel N. Nesterenko, Phil Jones, Brett Paull
Autore Nesterenko Pavel N
Edizione [1st ed.]
Pubbl/distr/stampa Cambridge, : Royal Society of Chemistry, c2011
Descrizione fisica 1 online resource (317 p.)
Disciplina 543.82
Altri autori (Persone) JonesP (Phil)
PaullBrett
Collana ISSN
RSC chromatography monographs
Soggetto topico High performance liquid chromatography
Ion exchange chromatography
Complexometric titration
Chelates
Trace elements - Analysis
ISBN 1-84973-231-0
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto High Performance Chelation Ion Chromatography -- Contents -- Chapter 1 Chelation and its Role in Contemporary Liquid Chromatography -- 1.1 Basic Chromatographic Principles -- 1.2 Chelation as a Mechanism for Obtaining Separation Selectivity -- 1.3 Terminology and Definitions -- 1.4 Historical Developments -- 1.5 The Evolution of Chelating Stationary Phases -- 1.6 The Current State of HPCIC and Context -- References -- Chapter 2 Retention Mechanism and Chelation Theory -- 2.1 Introduction -- 2.2 Surface and Solution Complexation -- 2.2.1 Complexation Kinetics -- 2.3 Equilibria Within the Chelating Ion Exchanger -- 2.3.1 Distribution Ratio Within a Mixed Mode Mechanism -- 2.3.2 Selectivity in Non-complexing Mobile Phases -- 2.3.3 Secondary Equilibria Within the Mobile Phase -- 2.4 Temperature Effects in HPCIC -- 2.4.1 Thermodynamic Effects -- 2.4.2 Kinetic Effects -- 2.5 Mobile Phase pH -- 2.6 Organic Solvent Additives -- References -- Chapter 3 Chelating Stationary Phases -- 3.1 Introduction -- 3.2 Types and Properties of Chelating Ion Exchange Ligands -- 3.2.1 Adsorption of Metal Ions -- 3.2.2 Ligand Chemical Stability -- 3.2.3 Suitable Coordinating Sites -- 3.2.4 Functional Selectivity -- 3.2.5 Suitable Acid-Base Properties and Surface Charge -- 3.3 Chelating Ion Exchangers with Covalently Bonded Chelating Groups -- 3.3.1 Types of Chelating Ion Exchangers and Synthetic Methods -- 3.3.2 Polymer Based Chelating Ion Exchangers -- 3.3.3 Silica Based Chelating Ion Exchangers -- 3.3.4 Commercially Available Chelating Ion Exchange Phases -- 3.4 Stationary Phase Matrix Effects -- 3.4.1 Surface Distribution of Covalently Bound Ligands -- 3.4.2 Effects of Phase and Particle Porosity -- 3.4.3 Effect of Stationary Phase Structure upon Separation Selectivity -- 3.4.4 Monolithic Chelating Ion Exchangers.
3.5 Dynamically Modified and Impregnated Stationary Phases -- 3.5.1 Impregnated (Pre-coated) Phases Using Metallochromic Ligands -- 3.5.2 Dynamically Modified Phases -- References -- Chapter 4 Elution -- 4.1 Mobile Phase Parameters Influencing Separation Performance in HPCIC -- 4.1.1 Ionic Strength -- 4.1.2 Temperature Effects -- 4.1.3 pH of the Mobile Phase -- 4.1.4 Organic Solvents in HPCIC -- 4.1.5 Addition of Oxidising and Reducing Agents -- 4.2 Elution Modes -- 4.2.1 Isocratic Elution -- 4.2.2 Gradient Elution -- References -- Chapter 5 Liquid-Liquid Chromatographic Methods -- 5.1 High Speed Counter-current Chromatography of Metal Ions -- 5.1.1 Extracting Ligands and Metal Ion Selectivity -- 5.1.2 Efficiency of Metal Separations using HSCCC -- 5.1.3 Applications -- 5.2 High-performance Extraction Chromatography -- 5.2.1 Stationary Phase Supports -- 5.2.2 Ligand Loading Stability and Retention Mechanism -- 5.2.3 Type of Extracting Reagent -- 5.2.4 Applications -- References -- Chapter 6 Detection -- 6.1 Background -- 6.2 Post-column Reactions for the Photometric Detection of Metal Ions -- 6.2.1 Construction of Post-column Reactors -- 6.2.2 Reagents for Post-column Derivitisation -- 6.2.3 Recent Developments in High-sensitivity Reagents for Post-column Reactions -- 6.3 Practical Methods for Improving Limits of Detection in Liquid Chromatography -- 6.3.1 The Detection Limit -- 6.3.2 Types of Baseline Noise -- 6.3.3 Noise Reduction Methods -- 6.4 Other Types of Post-column Reaction Detection -- 6.4.1 Displacement Reactions -- 6.4.2 Fluorescence Detection -- 6.4.3 Chemiluminescence Post-column Reaction Detection -- 6.5 Hyphenated Techniques -- References -- Chapter 7 Practical Applications -- 7.1 Potential HPCIC Applications -- 7.2 Relative Advantages of HPCIC -- 7.3 Fresh and Potable Waters -- 7.4 Saline Samples -- 7.4.1 Seawater and Estuarine Water.
7.4.2 Highly Saline Waters -- 7.4.3 Commercial Products and Fine Chemicals -- 7.5 Solid Samples -- 7.5.1 Sediments, Soils and Minerals -- 7.5.2 Biological Materials and Foodstuffs -- 7.5.3 Miscellaneous -- References -- Subject Index.
Record Nr. UNINA-9910807625003321
Nesterenko Pavel N  
Cambridge, : Royal Society of Chemistry, c2011
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Ion chromatography / / James S. Fritz, Douglas T. Gjerde
Ion chromatography / / James S. Fritz, Douglas T. Gjerde
Autore Fritz James S (James Sherwood)
Edizione [3rd ed.]
Pubbl/distr/stampa Weinheim, [Germany] : , : Wiley-VCH, , 2000
Descrizione fisica 1 online resource (269 p.)
Disciplina 543.0893
543/.0893
Soggetto topico Ion exchange chromatography
Soggetto genere / forma Electronic books.
ISBN 1-281-76411-6
9786611764111
3-527-61324-2
3-527-61325-0
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Ion Chromatography; Preface; Acknowledgements; Table of Contents; 1 Introduction and Overview; 1.1 Introduction; 1.2 Historical Development; 1.3 Principles of Ion Chromatographic Separation and Detection; 1.3.1 Requirements for Separation; 1.3.2 Experimental Setup; 1.3.3 Performing a Separation; 1.3.4 Migration of Sample Ions; 1.3.5 Detection; 1.3.6 Basis for Separation; 1.4 Hardware; 1.4.1 Components of an IC Instrument; 1.4.2 Dead Volume; 1.4.3 Degassing the Eluent; 1.4.4 Pumps; 1.4.5 Gradient Formation; 1.4.6 Pressure; 1.4.7 Injector; 1.4.8 Column Oven; 1.4.9 Column Hardware
1.4.10 Column Protection1.4.11 Detection and Data System; 1.4.12 Electrolytic Generation of Eluents; 1.5 Separation of Ions By Capillary Electrophoresis; 1.6 Literature; 2 Historical Development of Ion-Exchange Separations; 2.1 Introduction; 2.2 Separation of Cations; 2.2.1 Cation Separations Based On Affinity Differences; 2.2.2 Cation Separations with Complexing Eluents; 2.2.3 Effect of Organic Solvents; 2.3 Separation of Anions; 2.3.1 Separation of Anions with the Use of Affinity Differences; 2.3.2 Anion Separations Involving Complex Formation; 2.3.3. Effect of Organic Solvents
3 Ion-Exchange Resins3.1 Introduction; 3.2 Polymeric Resins; 3.2.1 Substrate and Cross-Linking; 3.2.2 Microporous Resins; 3.2.3 Macroporous Resins; 3.2.4 Chemical Functionalization; 3.2.5 Resin Capacity; 3.3 Anion Exchangers; 3.3.1 Poly(styrene-divinylbenzene) Backbone (PS-DVB); 3.3.2 Polyacrylate Anion Exchangers; 3.3.3 Effect of Functional Group Structure on Selectivity; 3.3.4 Effect of Spacer Arm Length; 3.3.5 Quaternary Phosphonium Resins; 3.3.6 Latex Agglomerated Ion Exchangers; 3.3.7 Effect of Latex Functional Group on Selectivity; 3.3.8 Silica-Based Anion Exchangers
3.3.9 Alumina Materials3.4 Cation Exchangers; 3.4.1 Polymeric Resins; 3.4.1.1 Sulfonated Resins; 3.4.1.2 Weak-Acid Cation Exchangers; 3.4.2 Pellicular Resins; 3.4.3 Silica-Based Cation Exchangers; 3.5 Chelating Ion-Exchange Resins; 4 Detectors; 4.1 Introduction; 4.2 Conductivity Detectors; 4.2.1 Conductivity Definitions and Equations; 4.2.2 Principles of Cell Operation; 4.2.3 Conductance Measurement; 4.2.4 Hardware and Detector Operation; 4.3 Ultraviolet-Visible Detectors; 4.3.1 Direct Spectrophotometric Measurement; 4.3.2 Post-Column Derivatization; 4.3.3 Hardware and Detector Operation
4.4 Electrochemical Detectors4.4.1 Detector Principles; 4.4.2 Pulsed Techniques; 4.4.3 Post-Column Derivatization; 4.4.4 Hardware and Detector Operation; 4.5 Refractive Index Detection; 4.6 Other Detectors; 5 Principles of Ion Chromatographic Separations; 5.1 Basic Chromatographic Considerations; 5.1.1 Chromatographic Terms; 5.1.2 Retention Factors; 5.2 Ion-Exchange Equilibria; 5.2.1 Selectivity Coefficients; 5.2.2 Other Ion-Exchange Interactions; 5.2.3 Distribution Coefficient; 5.2.4 Retention Factor; 5.3 Selectivity of Sulfonated Cation-Exchange Resin for Metal Cations
5.3.1 Elution with Perchloric Acid and Sodium Perchlorate
Record Nr. UNINA-9910144143103321
Fritz James S (James Sherwood)  
Weinheim, [Germany] : , : Wiley-VCH, , 2000
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui