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The troubleshooting and maintenance guide for gas chromatographers [[electronic resource] /] / Dean Rood
| The troubleshooting and maintenance guide for gas chromatographers [[electronic resource] /] / Dean Rood |
| Autore | Rood Dean |
| Edizione | [4th ed.] |
| Pubbl/distr/stampa | Weinheim, : Wiley-VCH |
| Descrizione fisica | 1 online resource (347 p.) |
| Disciplina |
543.0896
543.85 |
| Altri autori (Persone) | RoodDean |
| Soggetto topico |
Gas chromatography
Gas chromatography - Instruments - Maintenance and repair |
| Soggetto genere / forma | Electronic books. |
| ISBN |
1-281-08790-4
9786611087906 3-527-61130-4 3-527-61131-2 |
| Formato | Materiale a stampa  |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
The Troubleshootingand Maintenance Guide for Gas Chromatographers; Preface; Contents; Intentions and Introduction; 1 Introduction to Capillary Gas Chromatography; 1.1 What Is Gas Chromatography?; 1.2 What Types of Compounds Are Suitable for GC Analysis?; 1.3 The Basic Parts of a Gas Chromatograph; 1.3.1 Gas Supply and Flow Controllers; 1.3.2 Injector; 1.3.3 Capillary Column and Oven; 1.3.4 Detector; 1.3.5 Data System; 1.4 The Chromatogram; 1.5 The Mechanism of Compound Separation; 1.5.1 A Simple Description of the Chromatographic Process
1.5.2 A Detailed Description of the Chromatographic Process1.6 Factors Affecting Separation; 1.6.1 Stationary Phase; 1.6.2 Compound Structure; 1.6.3 Column Temperature; 2 Basic Definitions and Equations; 2.1 Why Bother?; 2.2 Peak Shapes; 2.2.1 Peak Width (W); 2.2.2 Peak Symmetry; 2.3 Retention; 2.3.1 Retention Time (t(r)); 2.3.2 Adjusted Retention Time (t( ́)(r)); 2.3.3 Retention Factor (k); 2.3.4 Retention Index (I); 2.4 Phase Ratio (β); 2.5 Distribution Constant (K(C)); 2.5.1 K(C) and Column Dimensions; 2.5.2 K(C) and Column Temperature; 2.6 Column Efficiency 2.6.1 Number of Theoretical Plates (N)2.6.2 Height Equivalent to a Theoretical Plate (H); 2.6.3 Effective Theoretical Plates (N(eff)) and Effective Plate Heights (H(eff)); 2.6.4 Precautions When Using Theoretical Plates; 2.7 Utilization of Theoretical Efficiency (UTE%); 2.8 Separation Factor (α); 2.9 Resolution (R); 2.10 Trennzahl (TZ); 2.11 Column Capacity; 3 Capillary GC Columns: Tubing; 3.1 Fused Silica Capillary Columns; 3.2 Fused Silica Tubing; 3.3 Outer Coating; 3.4 Other Tubing Materials; 3.5 Polyimide Fused Silica Tubing Bending Stress; 4 Capillary GC Columns: Stationary Phases 4.1 Stationary Phases4.2 Types of Stationary Phases; 4.2.1 Polysiloxanes or Silicones; 4.2.2 Arylene-Modified Polysiloxanes; 4.2.3 Polyethylene Glycols; 4.2.4 Porous Layer Stationary Phases; 4.3 Characteristics of Stationary Phases; 4.3.1 Bonded and Cross-linked Stationary Phases; 4.3.2 Stationary Phase Polarity; 4.3.3 Stationary Phase Selectivity; 4.4 Stationary Phase Interactions; 4.4.1 Dispersion Interaction; 4.4.2 Dipole Interaction; 4.4.3 Hydrogen Bonding Interaction; 4.4.4 When There are Multiple Interactions; 4.5 Stationary Phase Equivalencies; 4.6 Column Temperature Limits 4.7 Column Bleed4.7.1 What is Column Bleed?; 4.7.2 Measuring Column Bleed; 4.7.3 Sensitivity Considerations; 4.7.4 Detector Considerations; 4.7.5 Minimizing Column Bleed; 4.8 Selecting Stationary Phases; 5 Capillary GC Columns: Dimensions; 5.1 Introduction; 5.2 Column Length; 5.2.1 Column Length and Efficiency/Resolution; 5.2.2 Column Length and Retention; 5.2.3 Column Length and Pressure; 5.2.4 Column Length and Bleed; 5.2.5 Column Length and Cost; 5.2.6 Selecting Column Length; 5.3 Column Diameter; 5.3.1 Column Diameter and Efficiency/Resolution; 5.3.2 Column Diameter and Retention 5.3.3 Column Diameter and Pressure |
| Record Nr. | UNINA-9910144143303321 |
Rood Dean
|
||
| Weinheim, : Wiley-VCH | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
The troubleshooting and maintenance guide for gas chromatographers [[electronic resource] /] / Dean Rood
| The troubleshooting and maintenance guide for gas chromatographers [[electronic resource] /] / Dean Rood |
| Autore | Rood Dean |
| Edizione | [4th ed.] |
| Pubbl/distr/stampa | Weinheim, : Wiley-VCH |
| Descrizione fisica | 1 online resource (347 p.) |
| Disciplina |
543.0896
543.85 |
| Altri autori (Persone) | RoodDean |
| Soggetto topico |
Gas chromatography
Gas chromatography - Instruments - Maintenance and repair |
| ISBN |
1-281-08790-4
9786611087906 3-527-61130-4 3-527-61131-2 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
The Troubleshootingand Maintenance Guide for Gas Chromatographers; Preface; Contents; Intentions and Introduction; 1 Introduction to Capillary Gas Chromatography; 1.1 What Is Gas Chromatography?; 1.2 What Types of Compounds Are Suitable for GC Analysis?; 1.3 The Basic Parts of a Gas Chromatograph; 1.3.1 Gas Supply and Flow Controllers; 1.3.2 Injector; 1.3.3 Capillary Column and Oven; 1.3.4 Detector; 1.3.5 Data System; 1.4 The Chromatogram; 1.5 The Mechanism of Compound Separation; 1.5.1 A Simple Description of the Chromatographic Process
1.5.2 A Detailed Description of the Chromatographic Process1.6 Factors Affecting Separation; 1.6.1 Stationary Phase; 1.6.2 Compound Structure; 1.6.3 Column Temperature; 2 Basic Definitions and Equations; 2.1 Why Bother?; 2.2 Peak Shapes; 2.2.1 Peak Width (W); 2.2.2 Peak Symmetry; 2.3 Retention; 2.3.1 Retention Time (t(r)); 2.3.2 Adjusted Retention Time (t( ́)(r)); 2.3.3 Retention Factor (k); 2.3.4 Retention Index (I); 2.4 Phase Ratio (β); 2.5 Distribution Constant (K(C)); 2.5.1 K(C) and Column Dimensions; 2.5.2 K(C) and Column Temperature; 2.6 Column Efficiency 2.6.1 Number of Theoretical Plates (N)2.6.2 Height Equivalent to a Theoretical Plate (H); 2.6.3 Effective Theoretical Plates (N(eff)) and Effective Plate Heights (H(eff)); 2.6.4 Precautions When Using Theoretical Plates; 2.7 Utilization of Theoretical Efficiency (UTE%); 2.8 Separation Factor (α); 2.9 Resolution (R); 2.10 Trennzahl (TZ); 2.11 Column Capacity; 3 Capillary GC Columns: Tubing; 3.1 Fused Silica Capillary Columns; 3.2 Fused Silica Tubing; 3.3 Outer Coating; 3.4 Other Tubing Materials; 3.5 Polyimide Fused Silica Tubing Bending Stress; 4 Capillary GC Columns: Stationary Phases 4.1 Stationary Phases4.2 Types of Stationary Phases; 4.2.1 Polysiloxanes or Silicones; 4.2.2 Arylene-Modified Polysiloxanes; 4.2.3 Polyethylene Glycols; 4.2.4 Porous Layer Stationary Phases; 4.3 Characteristics of Stationary Phases; 4.3.1 Bonded and Cross-linked Stationary Phases; 4.3.2 Stationary Phase Polarity; 4.3.3 Stationary Phase Selectivity; 4.4 Stationary Phase Interactions; 4.4.1 Dispersion Interaction; 4.4.2 Dipole Interaction; 4.4.3 Hydrogen Bonding Interaction; 4.4.4 When There are Multiple Interactions; 4.5 Stationary Phase Equivalencies; 4.6 Column Temperature Limits 4.7 Column Bleed4.7.1 What is Column Bleed?; 4.7.2 Measuring Column Bleed; 4.7.3 Sensitivity Considerations; 4.7.4 Detector Considerations; 4.7.5 Minimizing Column Bleed; 4.8 Selecting Stationary Phases; 5 Capillary GC Columns: Dimensions; 5.1 Introduction; 5.2 Column Length; 5.2.1 Column Length and Efficiency/Resolution; 5.2.2 Column Length and Retention; 5.2.3 Column Length and Pressure; 5.2.4 Column Length and Bleed; 5.2.5 Column Length and Cost; 5.2.6 Selecting Column Length; 5.3 Column Diameter; 5.3.1 Column Diameter and Efficiency/Resolution; 5.3.2 Column Diameter and Retention 5.3.3 Column Diameter and Pressure |
| Record Nr. | UNINA-9910829968503321 |
|
Rood Dean
|
||
| Weinheim, : Wiley-VCH | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
The troubleshooting and maintenance guide for gas chromatographers [[electronic resource] /] / Dean Rood
| The troubleshooting and maintenance guide for gas chromatographers [[electronic resource] /] / Dean Rood |
| Autore | Rood Dean |
| Edizione | [4th ed.] |
| Pubbl/distr/stampa | Weinheim, : Wiley-VCH |
| Descrizione fisica | 1 online resource (347 p.) |
| Disciplina |
543.0896
543.85 |
| Altri autori (Persone) | RoodDean |
| Soggetto topico |
Gas chromatography
Gas chromatography - Instruments - Maintenance and repair |
| ISBN |
1-281-08790-4
9786611087906 3-527-61130-4 3-527-61131-2 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
The Troubleshootingand Maintenance Guide for Gas Chromatographers; Preface; Contents; Intentions and Introduction; 1 Introduction to Capillary Gas Chromatography; 1.1 What Is Gas Chromatography?; 1.2 What Types of Compounds Are Suitable for GC Analysis?; 1.3 The Basic Parts of a Gas Chromatograph; 1.3.1 Gas Supply and Flow Controllers; 1.3.2 Injector; 1.3.3 Capillary Column and Oven; 1.3.4 Detector; 1.3.5 Data System; 1.4 The Chromatogram; 1.5 The Mechanism of Compound Separation; 1.5.1 A Simple Description of the Chromatographic Process
1.5.2 A Detailed Description of the Chromatographic Process1.6 Factors Affecting Separation; 1.6.1 Stationary Phase; 1.6.2 Compound Structure; 1.6.3 Column Temperature; 2 Basic Definitions and Equations; 2.1 Why Bother?; 2.2 Peak Shapes; 2.2.1 Peak Width (W); 2.2.2 Peak Symmetry; 2.3 Retention; 2.3.1 Retention Time (t(r)); 2.3.2 Adjusted Retention Time (t( ́)(r)); 2.3.3 Retention Factor (k); 2.3.4 Retention Index (I); 2.4 Phase Ratio (β); 2.5 Distribution Constant (K(C)); 2.5.1 K(C) and Column Dimensions; 2.5.2 K(C) and Column Temperature; 2.6 Column Efficiency 2.6.1 Number of Theoretical Plates (N)2.6.2 Height Equivalent to a Theoretical Plate (H); 2.6.3 Effective Theoretical Plates (N(eff)) and Effective Plate Heights (H(eff)); 2.6.4 Precautions When Using Theoretical Plates; 2.7 Utilization of Theoretical Efficiency (UTE%); 2.8 Separation Factor (α); 2.9 Resolution (R); 2.10 Trennzahl (TZ); 2.11 Column Capacity; 3 Capillary GC Columns: Tubing; 3.1 Fused Silica Capillary Columns; 3.2 Fused Silica Tubing; 3.3 Outer Coating; 3.4 Other Tubing Materials; 3.5 Polyimide Fused Silica Tubing Bending Stress; 4 Capillary GC Columns: Stationary Phases 4.1 Stationary Phases4.2 Types of Stationary Phases; 4.2.1 Polysiloxanes or Silicones; 4.2.2 Arylene-Modified Polysiloxanes; 4.2.3 Polyethylene Glycols; 4.2.4 Porous Layer Stationary Phases; 4.3 Characteristics of Stationary Phases; 4.3.1 Bonded and Cross-linked Stationary Phases; 4.3.2 Stationary Phase Polarity; 4.3.3 Stationary Phase Selectivity; 4.4 Stationary Phase Interactions; 4.4.1 Dispersion Interaction; 4.4.2 Dipole Interaction; 4.4.3 Hydrogen Bonding Interaction; 4.4.4 When There are Multiple Interactions; 4.5 Stationary Phase Equivalencies; 4.6 Column Temperature Limits 4.7 Column Bleed4.7.1 What is Column Bleed?; 4.7.2 Measuring Column Bleed; 4.7.3 Sensitivity Considerations; 4.7.4 Detector Considerations; 4.7.5 Minimizing Column Bleed; 4.8 Selecting Stationary Phases; 5 Capillary GC Columns: Dimensions; 5.1 Introduction; 5.2 Column Length; 5.2.1 Column Length and Efficiency/Resolution; 5.2.2 Column Length and Retention; 5.2.3 Column Length and Pressure; 5.2.4 Column Length and Bleed; 5.2.5 Column Length and Cost; 5.2.6 Selecting Column Length; 5.3 Column Diameter; 5.3.1 Column Diameter and Efficiency/Resolution; 5.3.2 Column Diameter and Retention 5.3.3 Column Diameter and Pressure |
| Record Nr. | UNINA-9910841430503321 |
|
Rood Dean
|
||
| Weinheim, : Wiley-VCH | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
