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Biblioteca

MARC Lista (tabellare)
Chlorofluoromethanes and the stratosphere [[electronic resource] /] / [Robert D. Hudson, editor]
Chlorofluoromethanes and the stratosphere [[electronic resource] /] / [Robert D. Hudson, editor]
Pubbl/distr/stampa Washington, D.C. : , : National Aeronautics and Space Administration, Scientific and Technical Information Office, , [1977]
Descrizione fisica 1 online resource (viii, 266 pages) : illustrations
Altri autori (Persone) HudsonRobert D. <1931->
Collana NASA reference publication
Soggetto topico Chlorofluoromethane - Environmental aspects
Stratosphere
Atmospheric ozone - Environmental aspects
Chlorine compounds
Chlorofluoromethane
Fluorine compounds
Methane
Ozone
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Record Nr. UNINA-9910701928803321
Washington, D.C. : , : National Aeronautics and Space Administration, Scientific and Technical Information Office, , [1977]
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Efficient preparations of fluorine compounds [[electronic resource] /] / edited by Herbert W. Roesky
Efficient preparations of fluorine compounds [[electronic resource] /] / edited by Herbert W. Roesky
Pubbl/distr/stampa Hoboken, N.J., : Wiley, 2013
Descrizione fisica 1 online resource (484 p.)
Disciplina 546/.7312
Altri autori (Persone) RoeskyH. W
Soggetto topico Fluorine compounds
ISBN 1-118-40946-9
1-283-66495-X
1-118-40942-6
Classificazione SCI013030
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Machine generated contents note: Foreword Preface Contributors 1 Preparation of Elemental Fluorine Karl O. Christe 2 Preparation of Highly Active Caesium Fluoride Konrad Seppelt 3 Preparation of Highly Active Silver Fluoride Konrad Seppelt 4 A Room Temperature, Non-Irradiative Synthesis of Xenon Difluoride (XeF2) Ulf Breddemann, John R. DeBackere, Gary J. Schrobilgen 5 Efficient Perfluorination of K2B12H12 in Neutralizing Acetonitrile Dmitry V. Peryshkov, Steven H. Strauss 6 Efficient Preparation of the Highly Soluble ortho- and para-C60(CF2C6F5)2 Derivatives Igor V. Kuvychko, Bryon W. Larson, Steven H. Strauss, and Olga V. Boltalina 7 Synthesis of Cs[1-H-CB11F11] Josef Michl 8 Synthesis of Zero-Valent Trifluoromethyl Chalcogenato Derivatives, [NMe4]ECF3 (E = S, Se, Te) and Related Compounds Wieland Tyrra, Silke Kremer 9 Synthesis Methods for Exotic Inorganic Fluorides with Varied Applications Dayal T. Meshri, N. C. Mathur, Ritesh R. Jain 10 Tris(pentafluorophenyl)boran, B(C6F5)3, a Powerful, Well-soluble, and Non-oxidizing Lewis Acid and the Weakly Coordinating Tetrakis(pentafluorophenyl)borate Anion, [B(C6F5)4]? Hermann-Josef Frohn 11 Pentafluorophenyldifluoroboran, C6F5BF2, and Pentafluorophenyltrifluorosilane, C6F5SiF3, Versatile Reagents for Fluorine/Pentafluorophenyl Substitution Reactions in Strongly Oxidizing Hypervalent Non-metal Fluorides Hermann-Josef Frohn 12 Iodine(III and V) Fluorides: Interesting Fluorinating Agents Hermann-Josef Frohn 13 Tetramethylammonium Fluoride, [N(CH3)4]F, a Widely Applicable Reagent to Introduce Fluoride Ions and a Suitable Nucleophile to Initiate the Transfer of Perfluoroorganyl Groups to Electrophiles Hermann-Josef Frohn 14 Preparation of Transition Metal Sulfide Fluorides Michael Gerken 15 Transition Metal Carbonyl Sulfur Dioxide and Thiazylfluoride Complexes: Reactions at the Metal Center and at the Ligand Rudiger Mews 16 Cesium-, Mercury- and Silver-Salts with Sulfur-Nitrogen-Fluorine Anions: Useful Transfer-Reagents for NSF-Building Blocks Rudiger Mews 17 Laboratory-Scale Synthesis of Gold Trifluoride and Uranium Hexafluoride Thomas M. Klapotke 18 Preparation of Transition Metal Fluorides using ClF3 Ralf Haiges 19 Preparation of Fluorine Containing Molecular Halides and Hetero polar Salts with Elements of Group 15 and Niobium and Tantalum Halides Lothar Kolditz 20 Fluoro- and Fluorohydroxy Complexes of As, Sb, and Sn Lothar Kolditz 21 Trifluoromethyl Compounds via Electrophilic and Nucleophilic Reactions Jeanne M. Shreeve 22 Introduction of Fluorine into Compounds via Electrophilic and Nucleophilic Reactions Jeanne M. Shreeve 23 The ?Real? Iodine and Bromine Mono-Fluorides Shlomo Rozen 24 The Versatile Chemistry of Acetyl Hypofluorite ? Hypofluorite not Bonded to Polyhaloalkyl group Shlomo Rozen 25 Direct Fluorination of Organic Compounds with Elemental Fluorine Shlomo Rozen 26 The Surprising Chemistry of Bromine Trifluoride Shlomo Rozen 27 Preparation of Silicon- and Sulfur-Based Fluorinated Methane Derivatives as Versatile Fluoromethylation Reagents G. K. Surya Prakash, Fang Wang 28 Pentafluoroethyl Lithium: Reactions with Carbonyl Compounds and Epoxides Gerd-Volker Roschenthaler 29 Synthesis of ?-hydroxy-[alpha],[alpha]-difluoromethylenephosphonates Gerd-Volker Roschenthaler 30 Synthesis of Pentafluoro-?6-sulfanyl Substituted Acetylenes for Liquid Crystals Gerd-Volker Roschenthaler 31 Delocalized Lipophilic Cations as a Source of Naked Fluoride and Phase-transfer Catalysts Gerd-Volker Roschenthaler 32 Methyltrifluoropyruvate Imines Possessing N-oxalyl and N-phosphonoformyl Groups ? Precursors to a Variety of [alpha]-CF3-[alpha]-amino Acid Derivatives Gerd-Volker Roschenthaler 33 Rhodium-mediated Synthesis of (3,3,3-Trifluoropropyl)trimethoxysilane and (3,3,3 trifluoropropyl)triphenylsilane Falk Wehmeier, Thomas Braun 34 Rhodium-mediated Synthesis of a Tetrafluoropyridyl-2-boronate Ester Michael Teltewskoi, Thomas Braun 35 Palladium-mediated Synthesis of 4-Vinyltetrafluoropyridine and 2,3,5,6-Tetrafluoropyridine David Breyer, Thomas Braun 36 Preparation of Polyfluoroaryl-1,2-difluorovinylsilanes Donald J. Burton, Ba V. Nguyen 37Preparation of (Z)-2-iodo-1,2-difluorostyrenes Donald J. Burton, Ling Xue 38 Preparation of 1,4-Bis(Z-2-iodo-1,2-difluoroethenyl)benzene Donald J. Burton, Craig A. Wesolowski 39Stereospecific Carboamidation Route to (Z)-N-Phenyl-2,3-difluoro-3-(triethylsilyl) acrylamide Donald J. Burton, Craig A. Wesolowski 40 Preparation of 2-Trifluoromethyl-3,3,3-trifluoropropanal Donald J. Burton, Donald A. Wiebe 41 Synthesis of Tetrafluorocatechol Sudharsanam Ramanathan, Dayong Sang, Vivek Kumar, David M. Lemal 42 Preparation of an Unsymmetrial Bis((perfluoroalkyl)sulfonyl)imide Darryl D. DesMarteau, Thomas D. Hickman 43 Preparation of Perfluoroalkyl Sulfilimines and Sulfoximines Emmanuel Magnier 44 Preparation of Trifluoromethylsulfonium Salts Emmanuel Magnier 45 Preparation of Organometallic Fluorides of Main Group and Transition Elements Herbert W. Roesky 46 Preparation of Pentafluorosulfanyl Carbonyl Compounds John T. Welch 47 Preparation of Power-variable Electrophilic Trifluoromethylating Agents, S-(Trifluoromethyl)dibenzothiophenium Salts Series Teruo Umemoto 48 Synthesis of Fluorine Containing Heterocycles from [alpha],[alpha]-Dihydropolyfluoroalkylsulfides and Fluorinated Thiocarboxylic Acids Vadim M. Timoshemko, Yuriy G.Shermolovich 49 Synthesis of Octafluorocyclooctatetraene John M. Buzby, Aldos C. Barefoot, III, Michael W. Grayston, Evan D. Laganis, Roy F. Waldron, David M. Lemal 50 Preparation of Fluoroolefins Moritz F. Kuhnel, Dieter Lentz 51 Preparation of Ionic Liquids of Fluorocomplex and Oxofluorocomplex Anions by Fluoroacid-base Reactions Kazuhiko Matsumoto, Rika Hagiwara 52 Synthesis of Difluorocyclopropyl Building Blocks: 2,2-Difluorocyclopropylmethanol and 2-(Bromomethyl)-1,1-Difluorocyclopropane Wei Xu, William R. Dolbier, Jr. 53 Preparation of 1,1,2,2,9,9,10,10-Octafluoro[2.2]paracyclophane and Perfluoro[2.2]paracyclophane William R. Dolbier, Jr., Jian-Xi Duan, Alex J. Roche, Lianhao Zhang 54 Efficient Preparation of Bioorganic Fluorine Compounds Xiao-Long Qiu 55 1,3-Dipolar Cycloaddition Reactions to Fluoroalkenes Hanna Wojtowicz-Rajchel, Henryk Koroniak 56 Synthesis of Fluorinated Vinyl Derivatives of Nucleic Acid Bases Hanna Wojtowicz-Rajchel, Donata Pluskota-Karwatka, Henryk Koroniak 57 Synthesis of CF3-substituted Aziridine Ring by the Gabriel Reaction Tomasz Cytlak, Bartosz Marciniak, Henryk Koroniak 58 Preparation of [alpha]-Fluoro Amino and [alpha]-Fluoro Enamino Reagents Henryk Koroniak, Justyna Walkowiak 59 Synthesis of Original Fluoromonomers and Their Radical copolymerization with Vinylidene fluoride Bruno Ameduri 60 Convergent 18F Radiosynthesis V. Gouverneur, O. Lozano 61 Asymmetric Fluorocyclization Reactions V. Gouverneur. O. Lozano 62 Preparation of Allylic Fluorides V. Gouverneur, O. Lozano 63 Dehydroxyfluorinations of Primary or Secondary Alcohols Using Perfluoro n-butylsulfonyl Fluoride (nonaflyl Fluoride, NfF) in Combination with 1,8-Diaza-bicyclo[5.4.0]undec-7-ene (DBU) Orlin Petrov, Matthias Schneider, Rolf Bohlmann, Stephan Vettel, Helmut Vorbruggen 64 Preparation of Rare Earth Fluorosulfides and Oxyfluorosulfides A. Demourgues, A.Tressaud 65 Preparation of Carbon-Fluorine Compounds and Fluoride or Oxide Fluoride-Intercalated Graphites Tsuyoshi Nakajima 66 Safe Synthesis of Superstoichiometric Mesoporous Fluorocarbons Valentin N. Mitkin 67 Preparation of Fluorinated ?-Alumina Erhard Kemnitz, Toma? Skapin, John M. Winfield Index.
Record Nr. UNINA-9910141398103321
Hoboken, N.J., : Wiley, 2013
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Efficient preparations of fluorine compounds / / edited by Herbert W. Roesky
Efficient preparations of fluorine compounds / / edited by Herbert W. Roesky
Edizione [1st ed.]
Pubbl/distr/stampa Hoboken, N.J., : Wiley, 2013
Descrizione fisica 1 online resource (484 p.)
Disciplina 546/.7312
Altri autori (Persone) RoeskyH. W
Soggetto topico Fluorine compounds
ISBN 1-118-40946-9
1-283-66495-X
1-118-40942-6
Classificazione SCI013030
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Machine generated contents note: Foreword Preface Contributors 1 Preparation of Elemental Fluorine Karl O. Christe 2 Preparation of Highly Active Caesium Fluoride Konrad Seppelt 3 Preparation of Highly Active Silver Fluoride Konrad Seppelt 4 A Room Temperature, Non-Irradiative Synthesis of Xenon Difluoride (XeF2) Ulf Breddemann, John R. DeBackere, Gary J. Schrobilgen 5 Efficient Perfluorination of K2B12H12 in Neutralizing Acetonitrile Dmitry V. Peryshkov, Steven H. Strauss 6 Efficient Preparation of the Highly Soluble ortho- and para-C60(CF2C6F5)2 Derivatives Igor V. Kuvychko, Bryon W. Larson, Steven H. Strauss, and Olga V. Boltalina 7 Synthesis of Cs[1-H-CB11F11] Josef Michl 8 Synthesis of Zero-Valent Trifluoromethyl Chalcogenato Derivatives, [NMe4]ECF3 (E = S, Se, Te) and Related Compounds Wieland Tyrra, Silke Kremer 9 Synthesis Methods for Exotic Inorganic Fluorides with Varied Applications Dayal T. Meshri, N. C. Mathur, Ritesh R. Jain 10 Tris(pentafluorophenyl)boran, B(C6F5)3, a Powerful, Well-soluble, and Non-oxidizing Lewis Acid and the Weakly Coordinating Tetrakis(pentafluorophenyl)borate Anion, [B(C6F5)4]? Hermann-Josef Frohn 11 Pentafluorophenyldifluoroboran, C6F5BF2, and Pentafluorophenyltrifluorosilane, C6F5SiF3, Versatile Reagents for Fluorine/Pentafluorophenyl Substitution Reactions in Strongly Oxidizing Hypervalent Non-metal Fluorides Hermann-Josef Frohn 12 Iodine(III and V) Fluorides: Interesting Fluorinating Agents Hermann-Josef Frohn 13 Tetramethylammonium Fluoride, [N(CH3)4]F, a Widely Applicable Reagent to Introduce Fluoride Ions and a Suitable Nucleophile to Initiate the Transfer of Perfluoroorganyl Groups to Electrophiles Hermann-Josef Frohn 14 Preparation of Transition Metal Sulfide Fluorides Michael Gerken 15 Transition Metal Carbonyl Sulfur Dioxide and Thiazylfluoride Complexes: Reactions at the Metal Center and at the Ligand Rudiger Mews 16 Cesium-, Mercury- and Silver-Salts with Sulfur-Nitrogen-Fluorine Anions: Useful Transfer-Reagents for NSF-Building Blocks Rudiger Mews 17 Laboratory-Scale Synthesis of Gold Trifluoride and Uranium Hexafluoride Thomas M. Klapotke 18 Preparation of Transition Metal Fluorides using ClF3 Ralf Haiges 19 Preparation of Fluorine Containing Molecular Halides and Hetero polar Salts with Elements of Group 15 and Niobium and Tantalum Halides Lothar Kolditz 20 Fluoro- and Fluorohydroxy Complexes of As, Sb, and Sn Lothar Kolditz 21 Trifluoromethyl Compounds via Electrophilic and Nucleophilic Reactions Jeanne M. Shreeve 22 Introduction of Fluorine into Compounds via Electrophilic and Nucleophilic Reactions Jeanne M. Shreeve 23 The ?Real? Iodine and Bromine Mono-Fluorides Shlomo Rozen 24 The Versatile Chemistry of Acetyl Hypofluorite ? Hypofluorite not Bonded to Polyhaloalkyl group Shlomo Rozen 25 Direct Fluorination of Organic Compounds with Elemental Fluorine Shlomo Rozen 26 The Surprising Chemistry of Bromine Trifluoride Shlomo Rozen 27 Preparation of Silicon- and Sulfur-Based Fluorinated Methane Derivatives as Versatile Fluoromethylation Reagents G. K. Surya Prakash, Fang Wang 28 Pentafluoroethyl Lithium: Reactions with Carbonyl Compounds and Epoxides Gerd-Volker Roschenthaler 29 Synthesis of ?-hydroxy-[alpha],[alpha]-difluoromethylenephosphonates Gerd-Volker Roschenthaler 30 Synthesis of Pentafluoro-?6-sulfanyl Substituted Acetylenes for Liquid Crystals Gerd-Volker Roschenthaler 31 Delocalized Lipophilic Cations as a Source of Naked Fluoride and Phase-transfer Catalysts Gerd-Volker Roschenthaler 32 Methyltrifluoropyruvate Imines Possessing N-oxalyl and N-phosphonoformyl Groups ? Precursors to a Variety of [alpha]-CF3-[alpha]-amino Acid Derivatives Gerd-Volker Roschenthaler 33 Rhodium-mediated Synthesis of (3,3,3-Trifluoropropyl)trimethoxysilane and (3,3,3 trifluoropropyl)triphenylsilane Falk Wehmeier, Thomas Braun 34 Rhodium-mediated Synthesis of a Tetrafluoropyridyl-2-boronate Ester Michael Teltewskoi, Thomas Braun 35 Palladium-mediated Synthesis of 4-Vinyltetrafluoropyridine and 2,3,5,6-Tetrafluoropyridine David Breyer, Thomas Braun 36 Preparation of Polyfluoroaryl-1,2-difluorovinylsilanes Donald J. Burton, Ba V. Nguyen 37Preparation of (Z)-2-iodo-1,2-difluorostyrenes Donald J. Burton, Ling Xue 38 Preparation of 1,4-Bis(Z-2-iodo-1,2-difluoroethenyl)benzene Donald J. Burton, Craig A. Wesolowski 39Stereospecific Carboamidation Route to (Z)-N-Phenyl-2,3-difluoro-3-(triethylsilyl) acrylamide Donald J. Burton, Craig A. Wesolowski 40 Preparation of 2-Trifluoromethyl-3,3,3-trifluoropropanal Donald J. Burton, Donald A. Wiebe 41 Synthesis of Tetrafluorocatechol Sudharsanam Ramanathan, Dayong Sang, Vivek Kumar, David M. Lemal 42 Preparation of an Unsymmetrial Bis((perfluoroalkyl)sulfonyl)imide Darryl D. DesMarteau, Thomas D. Hickman 43 Preparation of Perfluoroalkyl Sulfilimines and Sulfoximines Emmanuel Magnier 44 Preparation of Trifluoromethylsulfonium Salts Emmanuel Magnier 45 Preparation of Organometallic Fluorides of Main Group and Transition Elements Herbert W. Roesky 46 Preparation of Pentafluorosulfanyl Carbonyl Compounds John T. Welch 47 Preparation of Power-variable Electrophilic Trifluoromethylating Agents, S-(Trifluoromethyl)dibenzothiophenium Salts Series Teruo Umemoto 48 Synthesis of Fluorine Containing Heterocycles from [alpha],[alpha]-Dihydropolyfluoroalkylsulfides and Fluorinated Thiocarboxylic Acids Vadim M. Timoshemko, Yuriy G.Shermolovich 49 Synthesis of Octafluorocyclooctatetraene John M. Buzby, Aldos C. Barefoot, III, Michael W. Grayston, Evan D. Laganis, Roy F. Waldron, David M. Lemal 50 Preparation of Fluoroolefins Moritz F. Kuhnel, Dieter Lentz 51 Preparation of Ionic Liquids of Fluorocomplex and Oxofluorocomplex Anions by Fluoroacid-base Reactions Kazuhiko Matsumoto, Rika Hagiwara 52 Synthesis of Difluorocyclopropyl Building Blocks: 2,2-Difluorocyclopropylmethanol and 2-(Bromomethyl)-1,1-Difluorocyclopropane Wei Xu, William R. Dolbier, Jr. 53 Preparation of 1,1,2,2,9,9,10,10-Octafluoro[2.2]paracyclophane and Perfluoro[2.2]paracyclophane William R. Dolbier, Jr., Jian-Xi Duan, Alex J. Roche, Lianhao Zhang 54 Efficient Preparation of Bioorganic Fluorine Compounds Xiao-Long Qiu 55 1,3-Dipolar Cycloaddition Reactions to Fluoroalkenes Hanna Wojtowicz-Rajchel, Henryk Koroniak 56 Synthesis of Fluorinated Vinyl Derivatives of Nucleic Acid Bases Hanna Wojtowicz-Rajchel, Donata Pluskota-Karwatka, Henryk Koroniak 57 Synthesis of CF3-substituted Aziridine Ring by the Gabriel Reaction Tomasz Cytlak, Bartosz Marciniak, Henryk Koroniak 58 Preparation of [alpha]-Fluoro Amino and [alpha]-Fluoro Enamino Reagents Henryk Koroniak, Justyna Walkowiak 59 Synthesis of Original Fluoromonomers and Their Radical copolymerization with Vinylidene fluoride Bruno Ameduri 60 Convergent 18F Radiosynthesis V. Gouverneur, O. Lozano 61 Asymmetric Fluorocyclization Reactions V. Gouverneur. O. Lozano 62 Preparation of Allylic Fluorides V. Gouverneur, O. Lozano 63 Dehydroxyfluorinations of Primary or Secondary Alcohols Using Perfluoro n-butylsulfonyl Fluoride (nonaflyl Fluoride, NfF) in Combination with 1,8-Diaza-bicyclo[5.4.0]undec-7-ene (DBU) Orlin Petrov, Matthias Schneider, Rolf Bohlmann, Stephan Vettel, Helmut Vorbruggen 64 Preparation of Rare Earth Fluorosulfides and Oxyfluorosulfides A. Demourgues, A.Tressaud 65 Preparation of Carbon-Fluorine Compounds and Fluoride or Oxide Fluoride-Intercalated Graphites Tsuyoshi Nakajima 66 Safe Synthesis of Superstoichiometric Mesoporous Fluorocarbons Valentin N. Mitkin 67 Preparation of Fluorinated ?-Alumina Erhard Kemnitz, Toma? Skapin, John M. Winfield Index.
Record Nr. UNINA-9910816262303321
Hoboken, N.J., : Wiley, 2013
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Emerging fluorinated motifs Synthesis, properties and applications . Volume 1 / / edited by Dominique Cahard, Jun-An Ma
Emerging fluorinated motifs Synthesis, properties and applications . Volume 1 / / edited by Dominique Cahard, Jun-An Ma
Pubbl/distr/stampa Wiesbaden, Germany : , : Wiley-VCH, , [2020]
Descrizione fisica 1 online resource (868 pages)
Disciplina 546.7312
Soggetto topico Fluorine compounds
Soggetto genere / forma Electronic books.
ISBN 3-527-82434-0
3-527-82432-4
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Record Nr. UNINA-9910555147603321
Wiesbaden, Germany : , : Wiley-VCH, , [2020]
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Emerging fluorinated motifs Synthesis, properties and applications . Volume 1 / / edited by Dominique Cahard, Jun-An Ma
Emerging fluorinated motifs Synthesis, properties and applications . Volume 1 / / edited by Dominique Cahard, Jun-An Ma
Pubbl/distr/stampa Wiesbaden, Germany : , : Wiley-VCH, , [2020]
Descrizione fisica 1 online resource (868 pages)
Disciplina 546.7312
Soggetto topico Fluorine compounds
ISBN 3-527-82434-0
3-527-82432-4
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Record Nr. UNINA-9910830855903321
Wiesbaden, Germany : , : Wiley-VCH, , [2020]
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Functionalized inorganic fluorides [[electronic resource] ] : synthesis, characterization & properties of nanostructured solids / / edited by Alain Tressaud
Functionalized inorganic fluorides [[electronic resource] ] : synthesis, characterization & properties of nanostructured solids / / edited by Alain Tressaud
Pubbl/distr/stampa Hoboken, NJ, : Wiley, 2010
Descrizione fisica 1 online resource (617 p.)
Disciplina 546.731
546/.731
Altri autori (Persone) TressaudAlain
Soggetto topico Fluorides
Fluorine compounds
Soggetto genere / forma Electronic books.
ISBN 1-282-68579-1
9786612685798
0-470-66076-7
0-470-66075-9
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Functionalized Inorganic Fluorides; Contents; Preface; List of Contributors; 1 Sol-Gel Synthesis of Nano-Scaled Metal Fluorides - Mechanism and Properties; 1.1 Introduction; 1.1.1 Sol-Gel Syntheses of Oxides - An Intensively Studied and Widely Used Process; 1.1.2 Sol-Gel Syntheses of Metal Fluorides - Overview of Methods; 1.2 Fluorolytic Sol-Gel Synthesis; 1.2.1 Mechanism and Properties; 1.2.2 Insight into Mechanism by Analytical Methods; 1.2.3 Exploring Properties; 1.2.4 Possible Fields of Application; References; 2 Microwave-Assisted Route Towards Fluorinated Nanomaterials; 2.1 Introduction
2.2 Introduction to Microwave Synthesis2.2.1 A Brief History; 2.2.2 Mechanisms to Generate Heat; 2.2.3 Advantages of Microwave Synthesis; 2.2.4 Examples of Microwave Experiments; 2.3 Preparation of Nanosized Metal Fluorides; 2.3.1 Aluminium-based Fluoride Materials; 2.3.2 Microwave-assisted Synthesis of Transition Metal Oxy-Hydroxy-Fluorides; 2.4 Concluding Remarks; Acknowledgements; References; 3 High Surface Area Metal Fluorides as Catalysts; 3.1 Introduction; 3.2 High Surface Area Aluminium Fluoride as Catalyst; 3.3 Host-Guest Metal Fluoride Systems
3.4 Hydroxy(oxo)fluorides as Bi-acidic Catalysts3.5 Oxidation Catalysis; 3.6 Metal Fluoride Supported Noble Metal Catalysts; 3.6.1 Hydrodechlorination of Monochlorodifluoromethane; 3.6.2 Hydrodechlorination of Dichloroacetic Acid (DCA); 3.6.3 Suzuki Coupling; References; 4 Investigation of Surface Acidity using a Range of Probe Molecules; 4.1 Introduction; 4.1.1 Setting the Scene: Metal Fluorides versus Metal Oxides; 4.1.2 Some Examples of the Application of FTIR Spectroscopy to the Study of Surface Acidity in Metal Oxides; 4.1.3 A Preview
4.2 Characterization of Acidity on a Surface: Contrasts with Molecular Fluorides4.2.1 Molecular Brnsted and Molecular Lewis Acids; 4.2.2 A Possible Benchmark for Solid Metal Fluoride, Lewis Acids: Aluminium Chlorofluoride; 4.3 Experimental Methodology; 4.3.1 FTIR Spectroscopy; 4.3.2 Characteristic Reactions and the Detection of Adsorbed Species by a Radiotracer Method; 4.4 Experimental Studies of Surface Acidity; 4.4.1 Using FTIR Spectroscopy; 4.4.2 Using HCl as a Probe with Detection via [36Cl]-Labelling
4.4.3 Metal Fluoride Surfaces that Contain Surface Hydroxyl Groups: Aluminium Hydroxy Fluorides with the Hexagonal Tungsten Bronze Structure4.4.4 Possible Geometries for HCl Adsorbed at Metal Fluoride Surfaces: Relation to Oxide and Oxyfluoride Surfaces; 4.5 Conclusions; References; 5 Probing Short and Medium Range Order in Al-based Fluorides using High Resolution Solid State Nuclear Magnetic Resonance and Parameter Modelling; 5.1 Introduction; 5.2 High Resolution NMR Techniques; 5.2.1 Fast MAS and High Magnetic Field; 5.2.2 27Al NMR; 5.2.3 High Resolution Correlation NMR Techniques
5.3 Application to Functionalized Al-Based Fluorides with Catalytic Properties
Record Nr. UNINA-9910140558803321
Hoboken, NJ, : Wiley, 2010
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Functionalized inorganic fluorides [[electronic resource] ] : synthesis, characterization & properties of nanostructured solids / / edited by Alain Tressaud
Functionalized inorganic fluorides [[electronic resource] ] : synthesis, characterization & properties of nanostructured solids / / edited by Alain Tressaud
Pubbl/distr/stampa Hoboken, NJ, : Wiley, 2010
Descrizione fisica 1 online resource (617 p.)
Disciplina 546.731
546/.731
Altri autori (Persone) TressaudAlain
Soggetto topico Fluorides
Fluorine compounds
ISBN 1-282-68579-1
9786612685798
0-470-66076-7
0-470-66075-9
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Functionalized Inorganic Fluorides; Contents; Preface; List of Contributors; 1 Sol-Gel Synthesis of Nano-Scaled Metal Fluorides - Mechanism and Properties; 1.1 Introduction; 1.1.1 Sol-Gel Syntheses of Oxides - An Intensively Studied and Widely Used Process; 1.1.2 Sol-Gel Syntheses of Metal Fluorides - Overview of Methods; 1.2 Fluorolytic Sol-Gel Synthesis; 1.2.1 Mechanism and Properties; 1.2.2 Insight into Mechanism by Analytical Methods; 1.2.3 Exploring Properties; 1.2.4 Possible Fields of Application; References; 2 Microwave-Assisted Route Towards Fluorinated Nanomaterials; 2.1 Introduction
2.2 Introduction to Microwave Synthesis2.2.1 A Brief History; 2.2.2 Mechanisms to Generate Heat; 2.2.3 Advantages of Microwave Synthesis; 2.2.4 Examples of Microwave Experiments; 2.3 Preparation of Nanosized Metal Fluorides; 2.3.1 Aluminium-based Fluoride Materials; 2.3.2 Microwave-assisted Synthesis of Transition Metal Oxy-Hydroxy-Fluorides; 2.4 Concluding Remarks; Acknowledgements; References; 3 High Surface Area Metal Fluorides as Catalysts; 3.1 Introduction; 3.2 High Surface Area Aluminium Fluoride as Catalyst; 3.3 Host-Guest Metal Fluoride Systems
3.4 Hydroxy(oxo)fluorides as Bi-acidic Catalysts3.5 Oxidation Catalysis; 3.6 Metal Fluoride Supported Noble Metal Catalysts; 3.6.1 Hydrodechlorination of Monochlorodifluoromethane; 3.6.2 Hydrodechlorination of Dichloroacetic Acid (DCA); 3.6.3 Suzuki Coupling; References; 4 Investigation of Surface Acidity using a Range of Probe Molecules; 4.1 Introduction; 4.1.1 Setting the Scene: Metal Fluorides versus Metal Oxides; 4.1.2 Some Examples of the Application of FTIR Spectroscopy to the Study of Surface Acidity in Metal Oxides; 4.1.3 A Preview
4.2 Characterization of Acidity on a Surface: Contrasts with Molecular Fluorides4.2.1 Molecular Brnsted and Molecular Lewis Acids; 4.2.2 A Possible Benchmark for Solid Metal Fluoride, Lewis Acids: Aluminium Chlorofluoride; 4.3 Experimental Methodology; 4.3.1 FTIR Spectroscopy; 4.3.2 Characteristic Reactions and the Detection of Adsorbed Species by a Radiotracer Method; 4.4 Experimental Studies of Surface Acidity; 4.4.1 Using FTIR Spectroscopy; 4.4.2 Using HCl as a Probe with Detection via [36Cl]-Labelling
4.4.3 Metal Fluoride Surfaces that Contain Surface Hydroxyl Groups: Aluminium Hydroxy Fluorides with the Hexagonal Tungsten Bronze Structure4.4.4 Possible Geometries for HCl Adsorbed at Metal Fluoride Surfaces: Relation to Oxide and Oxyfluoride Surfaces; 4.5 Conclusions; References; 5 Probing Short and Medium Range Order in Al-based Fluorides using High Resolution Solid State Nuclear Magnetic Resonance and Parameter Modelling; 5.1 Introduction; 5.2 High Resolution NMR Techniques; 5.2.1 Fast MAS and High Magnetic Field; 5.2.2 27Al NMR; 5.2.3 High Resolution Correlation NMR Techniques
5.3 Application to Functionalized Al-Based Fluorides with Catalytic Properties
Record Nr. UNINA-9910830353303321
Hoboken, NJ, : Wiley, 2010
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Functionalized inorganic fluorides : synthesis, characterization & properties of nanostructured solids / / edited by Alain Tressaud
Functionalized inorganic fluorides : synthesis, characterization & properties of nanostructured solids / / edited by Alain Tressaud
Pubbl/distr/stampa Hoboken, NJ, : Wiley, 2010
Descrizione fisica 1 online resource (617 p.)
Disciplina 546/.731
Altri autori (Persone) TressaudAlain
Soggetto topico Fluorides
Fluorine compounds
ISBN 1-282-68579-1
9786612685798
0-470-66076-7
0-470-66075-9
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Functionalized Inorganic Fluorides; Contents; Preface; List of Contributors; 1 Sol-Gel Synthesis of Nano-Scaled Metal Fluorides - Mechanism and Properties; 1.1 Introduction; 1.1.1 Sol-Gel Syntheses of Oxides - An Intensively Studied and Widely Used Process; 1.1.2 Sol-Gel Syntheses of Metal Fluorides - Overview of Methods; 1.2 Fluorolytic Sol-Gel Synthesis; 1.2.1 Mechanism and Properties; 1.2.2 Insight into Mechanism by Analytical Methods; 1.2.3 Exploring Properties; 1.2.4 Possible Fields of Application; References; 2 Microwave-Assisted Route Towards Fluorinated Nanomaterials; 2.1 Introduction
2.2 Introduction to Microwave Synthesis2.2.1 A Brief History; 2.2.2 Mechanisms to Generate Heat; 2.2.3 Advantages of Microwave Synthesis; 2.2.4 Examples of Microwave Experiments; 2.3 Preparation of Nanosized Metal Fluorides; 2.3.1 Aluminium-based Fluoride Materials; 2.3.2 Microwave-assisted Synthesis of Transition Metal Oxy-Hydroxy-Fluorides; 2.4 Concluding Remarks; Acknowledgements; References; 3 High Surface Area Metal Fluorides as Catalysts; 3.1 Introduction; 3.2 High Surface Area Aluminium Fluoride as Catalyst; 3.3 Host-Guest Metal Fluoride Systems
3.4 Hydroxy(oxo)fluorides as Bi-acidic Catalysts3.5 Oxidation Catalysis; 3.6 Metal Fluoride Supported Noble Metal Catalysts; 3.6.1 Hydrodechlorination of Monochlorodifluoromethane; 3.6.2 Hydrodechlorination of Dichloroacetic Acid (DCA); 3.6.3 Suzuki Coupling; References; 4 Investigation of Surface Acidity using a Range of Probe Molecules; 4.1 Introduction; 4.1.1 Setting the Scene: Metal Fluorides versus Metal Oxides; 4.1.2 Some Examples of the Application of FTIR Spectroscopy to the Study of Surface Acidity in Metal Oxides; 4.1.3 A Preview
4.2 Characterization of Acidity on a Surface: Contrasts with Molecular Fluorides4.2.1 Molecular Brnsted and Molecular Lewis Acids; 4.2.2 A Possible Benchmark for Solid Metal Fluoride, Lewis Acids: Aluminium Chlorofluoride; 4.3 Experimental Methodology; 4.3.1 FTIR Spectroscopy; 4.3.2 Characteristic Reactions and the Detection of Adsorbed Species by a Radiotracer Method; 4.4 Experimental Studies of Surface Acidity; 4.4.1 Using FTIR Spectroscopy; 4.4.2 Using HCl as a Probe with Detection via [36Cl]-Labelling
4.4.3 Metal Fluoride Surfaces that Contain Surface Hydroxyl Groups: Aluminium Hydroxy Fluorides with the Hexagonal Tungsten Bronze Structure4.4.4 Possible Geometries for HCl Adsorbed at Metal Fluoride Surfaces: Relation to Oxide and Oxyfluoride Surfaces; 4.5 Conclusions; References; 5 Probing Short and Medium Range Order in Al-based Fluorides using High Resolution Solid State Nuclear Magnetic Resonance and Parameter Modelling; 5.1 Introduction; 5.2 High Resolution NMR Techniques; 5.2.1 Fast MAS and High Magnetic Field; 5.2.2 27Al NMR; 5.2.3 High Resolution Correlation NMR Techniques
5.3 Application to Functionalized Al-Based Fluorides with Catalytic Properties
Record Nr. UNINA-9910877181903321
Hoboken, NJ, : Wiley, 2010
Materiale a stampa
Lo trovi qui: Univ. Federico II
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Handbook of fluorous chemistry [[electronic resource] /] / John A. Gladysz, Dennis P. Curran, István T. Horváth (Eds.)
Handbook of fluorous chemistry [[electronic resource] /] / John A. Gladysz, Dennis P. Curran, István T. Horváth (Eds.)
Pubbl/distr/stampa Weinheim, : Wiley-VCH, c2004
Descrizione fisica 1 online resource (627 p.)
Disciplina 546/.731
547.02
Altri autori (Persone) GladyszJohn A
CurranDennis P
HorváthIstván T
Soggetto topico Fluorine compounds
Fluorine
ISBN 1-280-51979-7
9786610519798
3-527-60390-5
3-527-60449-9
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Handbook of Fluorous Chemistry; Contents; Preface; Contributors; 1 Fluorous Chemistry: Scope and Definition; 1.1 The Birth of a Term; 1.2 The Definition of Fluorous Today; 1.3 Other Definitions within the Fluorous Repertoire; 1.4 Present Scope of Fluorous Chemistry; References; 2 A Personal View of the History of Fluorous Chemistry; References; 3 Fluorous Solvents and Related Media; 3.1 Introductory Remarks; 3.2 Commercial Fluorous Solvents; 3.3 Related Solvents and Media; 3.3.1 Amphiphilic or Hybrid Solvents; 3.3.2 Fluorous Ionic Liquids; 3.3.3 ""Faux Fluorous"" Solvents
3.3.4 Fluorous Greases3.3.5 Bonded Fluorous Phases; 3.4 Polarities of Fluorous Solvents; 3.5 Solubilities of Solutes in Fluorous Solvents; 3.5.1 General Aspects; 3.5.2 Gas Solubilities; 3.6 Fluorous/Non-fluorous Solvent Miscibilities; 3.7 Special Reactivity Phenomena in Fluorous Solvents; References; 4 Strategies for the Recovery of Fluorous Catalysts and Reagents: Design and Evaluation; 4.1 Introduction; Basic Recycling Concepts; 4.2 Fluorous/Non-Fluorous Liquid/Liquid Biphase Catalysis; 4.3 Fluorous Catalysis in Amphiphilic or Hybrid Solvents
4.4 Fluorous Catalysis Without Non-Fluorous Solvents4.5 Fluorous Catalysis Without Fluorous Solvents; 4.5.1 Thermomorphic Catalysts; 4.5.2 Other Approaches; 4.6 Fluorous Catalysis Without Solvents; 4.7 Recovery of Fluorous Catalysts using Supports; 4.8 Criteria for Recoverability; 4.8.1 Yield as a Function of Cycle; 4.8.2 TOF as a Function of Cycle; 4.8.3 Catalyst Inventory; 4.9 Slanting Data: How to Make a Non-recoverable Catalyst Appear Recoverable; 4.10 Prospects; References; 5 Ponytails: Structural and Electronic Considerations; 5.1 Introduction; 5.2 Structural Aspects of Ponytails
5.3 NMR Characterization of Ponytails5.4 Electronic Effects: Introduction; 5.5 Electronic Effects: IR Data; 5.6 Electronic Effects: Gas Phase Ionization Data; 5.7 Electronic Effects: Calorimetry; 5.8 Electronic Effects: Solution Equilibria; 5.9 Electronic Effects: Computational Data; 5.10 Electronic Effects: Reactivity; 5.11 Electronic Effects: Additional Probes; 5.12 Electronic Effects: Conclusions; References; 6 Partition Coefficients Involving Fluorous Solvents; 6.1 Introduction; 6.2 Literature Data; 6.3 Trends with Respect to Functional Groups; 6.3.1 Non-Aromatic Hydrocarbons
6.3.2 Non-Aromatic Monofunctional Compounds6.3.3 Simple Monoarenes; 6.3.4 Triarylphosphines; 6.3.5 Pyridines; 6.3.6 Metal Complexes; 6.4 General Trends and Special Situations; 6.5 Quantitative Analysis and Prediction of Partition Coefficients; 6.6 Future Directions; 6.7 Sample Experimental Determinations; References; 7 Separations with Fluorous Silica Gel and Related Materials; 7.1 Introduction; 7.1.1 Fluorous Silica Gel; 7.1.2 Types and Sources of Fluorous Silica Gel Materials and Products; 7.2 Fluorous Solid Phase Extraction (FSPE)
7.2.1 Fluorous Solid Phase Extraction and its Relationship to Chromatography and Liquid/Liquid Extraction
Record Nr. UNINA-9910144297603321
Weinheim, : Wiley-VCH, c2004
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Handbook of fluorous chemistry [[electronic resource] /] / John A. Gladysz, Dennis P. Curran, István T. Horváth (Eds.)
Handbook of fluorous chemistry [[electronic resource] /] / John A. Gladysz, Dennis P. Curran, István T. Horváth (Eds.)
Pubbl/distr/stampa Weinheim, : Wiley-VCH, c2004
Descrizione fisica 1 online resource (627 p.)
Disciplina 546/.731
547.02
Altri autori (Persone) GladyszJohn A
CurranDennis P
HorváthIstván T
Soggetto topico Fluorine compounds
Fluorine
ISBN 1-280-51979-7
9786610519798
3-527-60390-5
3-527-60449-9
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Handbook of Fluorous Chemistry; Contents; Preface; Contributors; 1 Fluorous Chemistry: Scope and Definition; 1.1 The Birth of a Term; 1.2 The Definition of Fluorous Today; 1.3 Other Definitions within the Fluorous Repertoire; 1.4 Present Scope of Fluorous Chemistry; References; 2 A Personal View of the History of Fluorous Chemistry; References; 3 Fluorous Solvents and Related Media; 3.1 Introductory Remarks; 3.2 Commercial Fluorous Solvents; 3.3 Related Solvents and Media; 3.3.1 Amphiphilic or Hybrid Solvents; 3.3.2 Fluorous Ionic Liquids; 3.3.3 ""Faux Fluorous"" Solvents
3.3.4 Fluorous Greases3.3.5 Bonded Fluorous Phases; 3.4 Polarities of Fluorous Solvents; 3.5 Solubilities of Solutes in Fluorous Solvents; 3.5.1 General Aspects; 3.5.2 Gas Solubilities; 3.6 Fluorous/Non-fluorous Solvent Miscibilities; 3.7 Special Reactivity Phenomena in Fluorous Solvents; References; 4 Strategies for the Recovery of Fluorous Catalysts and Reagents: Design and Evaluation; 4.1 Introduction; Basic Recycling Concepts; 4.2 Fluorous/Non-Fluorous Liquid/Liquid Biphase Catalysis; 4.3 Fluorous Catalysis in Amphiphilic or Hybrid Solvents
4.4 Fluorous Catalysis Without Non-Fluorous Solvents4.5 Fluorous Catalysis Without Fluorous Solvents; 4.5.1 Thermomorphic Catalysts; 4.5.2 Other Approaches; 4.6 Fluorous Catalysis Without Solvents; 4.7 Recovery of Fluorous Catalysts using Supports; 4.8 Criteria for Recoverability; 4.8.1 Yield as a Function of Cycle; 4.8.2 TOF as a Function of Cycle; 4.8.3 Catalyst Inventory; 4.9 Slanting Data: How to Make a Non-recoverable Catalyst Appear Recoverable; 4.10 Prospects; References; 5 Ponytails: Structural and Electronic Considerations; 5.1 Introduction; 5.2 Structural Aspects of Ponytails
5.3 NMR Characterization of Ponytails5.4 Electronic Effects: Introduction; 5.5 Electronic Effects: IR Data; 5.6 Electronic Effects: Gas Phase Ionization Data; 5.7 Electronic Effects: Calorimetry; 5.8 Electronic Effects: Solution Equilibria; 5.9 Electronic Effects: Computational Data; 5.10 Electronic Effects: Reactivity; 5.11 Electronic Effects: Additional Probes; 5.12 Electronic Effects: Conclusions; References; 6 Partition Coefficients Involving Fluorous Solvents; 6.1 Introduction; 6.2 Literature Data; 6.3 Trends with Respect to Functional Groups; 6.3.1 Non-Aromatic Hydrocarbons
6.3.2 Non-Aromatic Monofunctional Compounds6.3.3 Simple Monoarenes; 6.3.4 Triarylphosphines; 6.3.5 Pyridines; 6.3.6 Metal Complexes; 6.4 General Trends and Special Situations; 6.5 Quantitative Analysis and Prediction of Partition Coefficients; 6.6 Future Directions; 6.7 Sample Experimental Determinations; References; 7 Separations with Fluorous Silica Gel and Related Materials; 7.1 Introduction; 7.1.1 Fluorous Silica Gel; 7.1.2 Types and Sources of Fluorous Silica Gel Materials and Products; 7.2 Fluorous Solid Phase Extraction (FSPE)
7.2.1 Fluorous Solid Phase Extraction and its Relationship to Chromatography and Liquid/Liquid Extraction
Record Nr. UNINA-9910830242903321
Weinheim, : Wiley-VCH, c2004
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui