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Greene's protective groups in organic synthesis / / Peter G. M. Wuts
| Greene's protective groups in organic synthesis / / Peter G. M. Wuts |
| Autore | Wuts Peter G. M. |
| Edizione | [6th ed.] |
| Pubbl/distr/stampa | Hoboken, NJ : , : John Wiley & Sons, Incorporated, , [2025] |
| Descrizione fisica | 1 online resource (1804 pages) : illustrations |
| Disciplina | 547.2 |
| Soggetto topico |
Protective groups (Chemistry)
Organic compounds - Synthesis Chemistry, Organic - Methodology Chemistry Techniques, Synthetic Organic Chemicals Chemistry, Organic - methods |
| ISBN |
9781394233182
1394233183 9781394233199 1394233191 9781394233175 1394233175 |
| Formato | Materiale a stampa  |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Cover -- Volume 1 -- Title Page -- Copyright Page -- Dedication -- Contents -- Preface -- Abbreviations -- Chapter 1 The Role of Protective Groups in Organic Synthesis -- Properties of a Protective Group -- Historical Development -- Development of New Protective Groups -- Selection of a Protective Group from This Book -- Synthesis of Complex Substances. Two Examples (As Used in the Synthesis of Himastatin and Palytoxin) of the Selection, Introduction, and Removal of Protective Groups -- Synthesis of Himastatin -- Synthesis of Palytoxin Carboxylic Acid -- Chapter 2 Protection for the Hydroxyl Group Including 1,2- and 1,3-Diols -- Ethers -- Substituted Methyl Ethers -- Substituted Ethyl Ethers -- Methoxy-Substituted Benzyl Ethers -- Silyl Ethers -- Migration of Silyl Groups -- Cleavage -- Esters -- Proximity Assisted Deprotection for Ester Cleavage -- Miscellaneous Esters -- Sulfonates, Sulfenates and Sulfinates as Protective Groups for Alcohols -- Carbonates -- Carbamate Protection of Alcohols -- Protection for 1,2-and 1,3-Diols -- Monoprotection of Diols -- Cyclic Acetals and Ketals -- Chiral Ketones -- Cyclic Ortho Esters -- Silyl Derivatives -- Cyclic Carbonates -- Cyclic Boronates -- Chapter 3 Protection for Phenols and Catechols -- Protection for Phenols and Catechols -- Ethers -- Silyl Ethers -- Esters -- Carbonates -- Carbamates -- Phosphinates -- Sulfonates -- Protection for Catechols (1,2-Dihydroxybenzenes) -- Cyclic Acetals and Ketals -- Cyclic Esters -- Protection for 2-Hydroxybenzenethiols -- Chapter 4 Protection for the Carbonyl Group -- Acetals and Ketals -- Acyclic Acetals and Ketals -- Cyclic Acetals and Ketals -- Chiral Acetals and Ketals -- Dithio Acetals and Ketals -- Acyclic Dithio Acetals and Ketals -- Cyclic Dithio Acetals and Ketals -- Monothio Acetals and Ketals -- Acyclic Monothio Acetals and Ketals.
Cyclic Monothio Acetals and Ketals -- Miscellaneous Derivatives -- O-Substituted Cyanohydrins -- Substituted Hydrazones -- 1,2-Adducts to Aldehydes and Ketones -- Protection of the Carbonyl Group as an Enolate Anions, Enol Ethers, Enamines, and Imines -- Lithium Diisopropylamide (LDA) -- Monoprotection of Dicarbonyl Compounds -- Selective Protection of -and -Diketones -- Cyclic Ketals, Monothio, and Dithio Ketals -- Chapter 5 Protection for the Carboxyl Group -- Esters -- General Preparations of Esters -- General Cleavage of Esters -- Transesterification -- Enzymatically Cleavable Esters -- Substituted Methyl Esters -- 2-Substituted Ethyl Esters -- Substituted Benzyl Esters -- Silyl Esters -- Activated Esters -- Miscellaneous Derivatives -- Stannyl Esters -- Amides and Hydrazides -- Amides -- Protection of Sulfonic Acids -- Protection of Boronic Acids -- Chapter 6 Protection for the Thiol Group -- Thioethers -- S-Diphenylmethyl, Substituted S-Diphenylmethyl, and S-Triphenylmethyl Thioethers -- 4-Methoxytrityl (Mtt.SR) Thioether -- Substituted S-Methyl Derivatives: Monothio, Dithio, and Aminothio Acetals -- Substituted S-Ethyl Derivatives -- Silyl Thioethers -- Thioesters -- Thiocarbonate Derivatives -- Thiocarbamate Derivatives -- Miscellaneous Derivatives -- Unsymmetrical Disulfides -- Sulfenyl Derivatives -- Protection for Dithiols: Dithio Acetals and Ketals -- Protection for Sulfides -- S-P Derivatives -- Protection for the Amino Thiol Group -- Protection for Selenols -- Volume 2 -- Title Page -- Copyright Page -- Dedication -- Contents -- Preface -- Abbreviations -- Chapter 7 Protection for the Amino Group -- Introduction to Amines -- Carbamates -- Substituted Ethyl Carbamates -- Carbamates Cleaved by a 1,6-Elimination -- Cleavage by -Elimination -- Photolytically Cleaved Carbamates -- Miscellaneous Carbamates -- Urea-Type Derivatives -- Amides. Transamidation -- Assisted Cleavage of Amides -- Amide Cleavage Induced by Nitro Group Reduction -- Amide Cleavage Induced by Release of an Alcohol -- Amides Cleaved by Other Chemical Reactions -- Bisprotection of Amines -- Special -NH Protective Groups -- N-Alkyl and N-Aryl Amines -- Imine Derivatives -- Enamine Derivatives -- N-Heteroatom Derivatives -- N-Metal Derivatives -- N-N Derivatives -- N-P Derivatives -- N-Si Derivatives -- N-S Derivatives -- N-Sulfenyl Derivatives -- Protection of Amino Alcohols -- Protection for Imidazoles, Pyrroles, Indoles, and Other Aromatic Heterocycles -- N-Sulfonyl Derivatives -- Carbamates -- N-Alkyl and N-Aryl Derivatives -- Amino Acetal Derivatives -- Amides -- Protection for the Amide -NH -- Amides -- Protection for the Sulfonamide -NH -- Chapter 8 Protection for the Alkyne -CH -- Chapter 9 Protection for the Phosphate Group -- Introduction -- Some General Methods for Phosphate Ester Formation -- Removal of Protective Groups from Phosphorus -- Alkyl Phosphates -- Phosphates Cleaved by Cyclodeesterification -- 2-Substituted Ethyl Phosphates -- Haloethyl Phosphates -- Benzyl Phosphates -- Phenyl Phosphates -- Photochemically Cleaved Phosphate Protective Groups -- Amidates -- Miscellaneous Derivatives -- Chapter 10 Protecting Group Effects in Carbohydrate Chemistry -- Introduction -- Early Observations Protecting Group-Induced Reactivity -- Relative Reactivities -- Fraser-Reidfs Concept of Armed and Disarmed -- Examples of How Protecting Groups Arm and Disarm Glycosides -- Aglycone Transfer -- Participating Groups -- Ester at the C-2 Hydroxyl -- Esters at Positions Other Than 2 -- Ethers Primarily at the C-2 Hydroxyl -- Conformational Restriction -- Benzylidene Group and other Acetals -- Directing Effect of Silylene Groups -- Carbonates as Conformational Restrictors -- Orthoester Conformational Restriction. Silyl Groups: Conformational and Reactivity Effect -- Studies on the Conformational Flip Using Silyl Groups -- Amino Sugar Protection -- Imine Protection -- Protection of the NH2 as An Azide -- Imide Protection -- Oxazolidinones -- Introduction to the Formation of Sialyl Glycosides -- Amides and Their Effects -- Protecting Group Effects in the Glycosylation of 2-Deoxy Sugars -- Furanosides -- Protecting Group Effects on Acceptors -- C-Glycosylation -- Sphingolipids -- Introduction -- Chapter 11 Reactivities, Reagents, and Reactivity Charts -- Reactivities -- Reagents -- Reactivity Charts -- Reactivity Chart 1. Protection for Hydroxyl Group: Ethers -- Reactivity Chart 2. Protection for Hydroxyl Group: Esters -- Reactivity Chart 3. Protection for 1,2-and 1,3-Diols -- Reactivity Chart 4. Protection for Phenols and Catechols -- Reactivity Chart 5. Protection for the Carbonyl Group -- Reactivity Chart 6. Protection for the Carboxyl Group -- Reactivity Chart 7. Protection for the Thiol Group -- Reactivity Chart 8. Protection for the Amino Group: Carbamates -- Reactivity Chart 9. Protection for the Amino Group: Amides -- Reactivity Chart 10. Protection for the Amino Group: Special -NH Protective Groups -- Reactivity Chart 11. Selective Deprotection of Silyl Ethers -- Index -- EULA. |
| Altri titoli varianti | Protective groups in organic synthesis |
| Record Nr. | UNINA-9911019677803321 |
Wuts Peter G. M.
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| Hoboken, NJ : , : John Wiley & Sons, Incorporated, , [2025] | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
JoVE science education Chemistry Organic chemistry II
| JoVE science education Chemistry Organic chemistry II |
| Pubbl/distr/stampa | Cambridge, Massachusetts : , : MyJoVE Corporation |
| Descrizione fisica | 1 online resource (streaming video files) |
| Disciplina | 547 |
| Soggetto topico |
Chemistry, Organic
Chemistry, Organic - Methodology Science - Study and teaching |
| Formato | Materiale a stampa |
| Livello bibliografico | Periodico |
| Lingua di pubblicazione | eng |
| Altri titoli varianti |
JoVE science education > Chemistry > Organic chemistry II
JoVE science education database. Organic chemistry II JoVE science education library. Organic chemistry II JoVE science education collection. Organic chemistry II Journal of visualized experiments. Science education. Organic chemistry II |
| Record Nr. | UNINA-9910295820803321 |
| Cambridge, Massachusetts : , : MyJoVE Corporation | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
JoVE science education Chemistry Organic chemistry
| JoVE science education Chemistry Organic chemistry |
| Pubbl/distr/stampa | Cambridge, Massachusetts : , : MyJoVE Corporation |
| Descrizione fisica | 1 online resource (streaming video files) |
| Disciplina | 547 |
| Soggetto topico |
Chemistry, Organic
Chemistry, Organic - Methodology Science - Study and teaching |
| Formato | Videoregistrazioni  |
| Livello bibliografico | Periodico |
| Lingua di pubblicazione | eng |
| Altri titoli varianti |
JoVE science education > Chemistry > Organic chemistry
JoVE science education database. Organic chemistry JoVE science education library. Organic chemistry JoVE science education collection. Organic chemistry Journal of visualized experiments. Science education. Organic chemistry |
| Record Nr. | UNINA-9910295822703321 |
| Cambridge, Massachusetts : , : MyJoVE Corporation | ||
| Videoregistrazioni | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
JoVE science education Organic chemistry
| JoVE science education Organic chemistry |
| Pubbl/distr/stampa | Cambridge, Massachusetts : , : MyJoVE Corporation |
| Descrizione fisica | 1 online resource (streaming video files) |
| Disciplina | 547 |
| Soggetto topico |
Chemistry, Organic
Chemistry, Organic - Methodology Science - Study and teaching |
| Formato | Videoregistrazioni |
| Livello bibliografico | Periodico |
| Lingua di pubblicazione | eng |
| Altri titoli varianti |
JoVE science education > Chemistry > Organic chemistry
JoVE science education database. Organic chemistry JoVE science education library. Organic chemistry JoVE science education collection. Organic chemistry Journal of visualized experiments. Science education. Organic chemistry |
| Record Nr. | UNINA-9910887839503321 |
| Cambridge, Massachusetts : , : MyJoVE Corporation | ||
| Videoregistrazioni | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
JoVE science education Organic chemistry II
| JoVE science education Organic chemistry II |
| Pubbl/distr/stampa | Cambridge, Massachusetts : , : MyJoVE Corporation |
| Descrizione fisica | 1 online resource (streaming video files) |
| Disciplina | 547 |
| Soggetto topico |
Chemistry, Organic
Chemistry, Organic - Methodology Science - Study and teaching |
| Formato | Videoregistrazioni |
| Livello bibliografico | Periodico |
| Lingua di pubblicazione | eng |
| Altri titoli varianti |
JoVE science education > Chemistry > Organic chemistry II
JoVE science education database. Organic chemistry II JoVE science education library. Organic chemistry II JoVE science education collection. Organic chemistry II Journal of visualized experiments. Science education. Organic chemistry II |
| Record Nr. | UNINA-9910887840103321 |
| Cambridge, Massachusetts : , : MyJoVE Corporation | ||
| Videoregistrazioni | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Tetrahedron computer methodology
| Tetrahedron computer methodology |
| Pubbl/distr/stampa | Oxford ; ; New York, : Pergamon Press, ©1988-[1990] |
| Descrizione fisica | computer discs ; ; 5 1/4 in |
| Disciplina | 542 |
| Soggetto topico |
Chemistry, Organic - Methodology
Chemistry, Organic - Data processing Chemistry Computers Software |
| Soggetto genere / forma |
Periodicals.
Periodical |
| ISSN | 1878-335X |
| Formato | Materiale a stampa |
| Livello bibliografico | Periodico |
| Lingua di pubblicazione | eng |
| Altri titoli varianti | TCM |
| Record Nr. | UNISA-996211030903316 |
| Oxford ; ; New York, : Pergamon Press, ©1988-[1990] | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. di Salerno | ||
| ||
