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Fundamentals of industrial catalytic processes [[electronic resource] /] / Calvin H. Bartholomew, Robert J. Farrauto
| Fundamentals of industrial catalytic processes [[electronic resource] /] / Calvin H. Bartholomew, Robert J. Farrauto |
| Autore | Bartholomew Calvin H |
| Edizione | [2nd ed.] |
| Pubbl/distr/stampa | Hoboken, N.J., : Wiley, c2006 |
| Descrizione fisica | 1 online resource (1001 p.) |
| Disciplina |
660.2995
660/.2995 |
| Altri autori (Persone) | FarrautoRobert J. <1941-> |
| Soggetto topico |
Catalysis
Catalysts - Industrial applications |
| ISBN |
9780471730064
1-118-20973-7 1-282-78363-7 9786612783630 0-471-73007-6 0-471-73006-8 |
| Classificazione | 58.14 |
| Formato | Materiale a stampa  |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Fundamentals of Industrial Catalytic Processes; CONTENTS; Preface; Acknowledgments; Nomenclature; Part One: Introduction and Fundamentals; 1 Catalysis: Introduction and Fundamental Catalytic Phenomena; 2 Catalyst Materials, Properties and Preparation; 3 Catalyst Characterization and Selection; 4 Reactors, Reactor Design, and Activity Testing; 5 Catalyst Deactivation: Causes, Mechanisms, and Treatment; Part Two: Industrial Practice; 6 Hydrogen Production and Synthesis Gas Reactions; 7 Hydrogenation and Dehydrogenation of Organic Compounds
8 Catalytic Oxidations of Inorganic and Organic Compounds9 Petroleum Refining and Processing; 10 Environmental Catalysis: Mobile Sources; 11 Environmental Catalysis: Stationary Sources; 12 Homogeneous, Enzyme, And Polymerization Catalysis; 13 Hydrogen Production and Fuel Cells: Catalyst Technology; Glossary; Index |
| Record Nr. | UNINA-9910140757103321 |
Bartholomew Calvin H
|
||
| Hoboken, N.J., : Wiley, c2006 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Fundamentals of industrial catalytic processes [[electronic resource] /] / Calvin H. Bartholomew, Robert J. Farrauto
| Fundamentals of industrial catalytic processes [[electronic resource] /] / Calvin H. Bartholomew, Robert J. Farrauto |
| Autore | Bartholomew Calvin H |
| Edizione | [2nd ed.] |
| Pubbl/distr/stampa | Hoboken, N.J., : Wiley, c2006 |
| Descrizione fisica | 1 online resource (1001 p.) |
| Disciplina |
660.2995
660/.2995 |
| Altri autori (Persone) | FarrautoRobert J. <1941-> |
| Soggetto topico |
Catalysis
Catalysts - Industrial applications |
| ISBN |
9780471730064
1-118-20973-7 1-282-78363-7 9786612783630 0-471-73007-6 0-471-73006-8 |
| Classificazione | 58.14 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Fundamentals of Industrial Catalytic Processes; CONTENTS; Preface; Acknowledgments; Nomenclature; Part One: Introduction and Fundamentals; 1 Catalysis: Introduction and Fundamental Catalytic Phenomena; 2 Catalyst Materials, Properties and Preparation; 3 Catalyst Characterization and Selection; 4 Reactors, Reactor Design, and Activity Testing; 5 Catalyst Deactivation: Causes, Mechanisms, and Treatment; Part Two: Industrial Practice; 6 Hydrogen Production and Synthesis Gas Reactions; 7 Hydrogenation and Dehydrogenation of Organic Compounds
8 Catalytic Oxidations of Inorganic and Organic Compounds9 Petroleum Refining and Processing; 10 Environmental Catalysis: Mobile Sources; 11 Environmental Catalysis: Stationary Sources; 12 Homogeneous, Enzyme, And Polymerization Catalysis; 13 Hydrogen Production and Fuel Cells: Catalyst Technology; Glossary; Index |
| Record Nr. | UNISA-996218416303316 |
|
Bartholomew Calvin H
|
||
| Hoboken, N.J., : Wiley, c2006 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. di Salerno | ||
| ||
Fundamentals of industrial catalytic processes [[electronic resource] /] / Calvin H. Bartholomew, Robert J. Farrauto
| Fundamentals of industrial catalytic processes [[electronic resource] /] / Calvin H. Bartholomew, Robert J. Farrauto |
| Autore | Bartholomew Calvin H |
| Edizione | [2nd ed.] |
| Pubbl/distr/stampa | Hoboken, N.J., : Wiley, c2006 |
| Descrizione fisica | 1 online resource (1001 p.) |
| Disciplina |
660.2995
660/.2995 |
| Altri autori (Persone) | FarrautoRobert J. <1941-> |
| Soggetto topico |
Catalysis
Catalysts - Industrial applications |
| ISBN |
9780471730064
1-118-20973-7 1-282-78363-7 9786612783630 0-471-73007-6 0-471-73006-8 |
| Classificazione | 58.14 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Fundamentals of Industrial Catalytic Processes; CONTENTS; Preface; Acknowledgments; Nomenclature; Part One: Introduction and Fundamentals; 1 Catalysis: Introduction and Fundamental Catalytic Phenomena; 2 Catalyst Materials, Properties and Preparation; 3 Catalyst Characterization and Selection; 4 Reactors, Reactor Design, and Activity Testing; 5 Catalyst Deactivation: Causes, Mechanisms, and Treatment; Part Two: Industrial Practice; 6 Hydrogen Production and Synthesis Gas Reactions; 7 Hydrogenation and Dehydrogenation of Organic Compounds
8 Catalytic Oxidations of Inorganic and Organic Compounds9 Petroleum Refining and Processing; 10 Environmental Catalysis: Mobile Sources; 11 Environmental Catalysis: Stationary Sources; 12 Homogeneous, Enzyme, And Polymerization Catalysis; 13 Hydrogen Production and Fuel Cells: Catalyst Technology; Glossary; Index |
| Record Nr. | UNINA-9910830759103321 |
|
Bartholomew Calvin H
|
||
| Hoboken, N.J., : Wiley, c2006 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Fundamentals of industrial catalytic processes [[electronic resource] /] / Calvin H. Bartholomew, Robert J. Farrauto
| Fundamentals of industrial catalytic processes [[electronic resource] /] / Calvin H. Bartholomew, Robert J. Farrauto |
| Autore | Bartholomew Calvin H |
| Edizione | [2nd ed.] |
| Pubbl/distr/stampa | Hoboken, N.J., : Wiley, c2006 |
| Descrizione fisica | 1 online resource (1001 p.) |
| Disciplina |
660.2995
660/.2995 |
| Altri autori (Persone) | FarrautoRobert J. <1941-> |
| Soggetto topico |
Catalysis
Catalysts - Industrial applications |
| ISBN |
9780471730064
1-118-20973-7 1-282-78363-7 9786612783630 0-471-73007-6 0-471-73006-8 |
| Classificazione | 58.14 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Fundamentals of Industrial Catalytic Processes; CONTENTS; Preface; Acknowledgments; Nomenclature; Part One: Introduction and Fundamentals; 1 Catalysis: Introduction and Fundamental Catalytic Phenomena; 2 Catalyst Materials, Properties and Preparation; 3 Catalyst Characterization and Selection; 4 Reactors, Reactor Design, and Activity Testing; 5 Catalyst Deactivation: Causes, Mechanisms, and Treatment; Part Two: Industrial Practice; 6 Hydrogen Production and Synthesis Gas Reactions; 7 Hydrogenation and Dehydrogenation of Organic Compounds
8 Catalytic Oxidations of Inorganic and Organic Compounds9 Petroleum Refining and Processing; 10 Environmental Catalysis: Mobile Sources; 11 Environmental Catalysis: Stationary Sources; 12 Homogeneous, Enzyme, And Polymerization Catalysis; 13 Hydrogen Production and Fuel Cells: Catalyst Technology; Glossary; Index |
| Record Nr. | UNINA-9910877565803321 |
|
Bartholomew Calvin H
|
||
| Hoboken, N.J., : Wiley, c2006 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Industrial gases processing / / edited by Heinz-Wolfgang Haring ; translated by Christine Ahner
| Industrial gases processing / / edited by Heinz-Wolfgang Haring ; translated by Christine Ahner |
| Pubbl/distr/stampa | Weinheim, Germany : , : Wiley-VCH Verlag GmbH & Co. KGaA, , 2008 |
| Descrizione fisica | 1 online resource (312 p.) |
| Disciplina | 665.7 |
| Soggetto topico | Gas manufacture and works |
| ISBN |
1-282-78422-6
9786612784224 3-527-62125-3 3-527-62124-5 |
| Classificazione |
58.14
58.20 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Industrial Gases Processing; Foreword; Contents; List of Contributors; 1 Introduction; References; 2 The Air Gases Nitrogen, Oxygen and Argon; 2.1 History, Occurrence and Properties; 2.1.1 Nitrogen; 2.1.1.1 History; 2.1.1.2 Occurrence; 2.1.1.3 Physical and Chemical Properties; 2.1.2 Oxygen; 2.1.2.1 History; 2.1.2.2 Occurrence; 2.1.2.3 Physical and Chemical Properties; 2.1.3 Argon; 2.1.3.1 History; 2.1.3.2 Occurrence; 2.1.3.3 Physical and Chemical Properties; 2.2 Recovery of Nitrogen, Oxygen and Argon; 2.2.1 Introduction
2.2.2 Application Range of Membrane Separation, Pressure Swing Adsorption and Cryogenic Rectification2.2.3 Nitrogen Recovery with Membranes; 2.2.3.1 Physical Principle; 2.2.3.2 Membrane Technology; 2.2.3.3 Design; 2.2.4 Nitrogen and Oxygen Recovery by Means of Pressure Swing Adsorption; 2.2.4.1 Physical Principle; 2.2.4.2 Properties of Molecular Sieves; 2.2.4.3 Nitrogen Recovery; 2.2.4.4 Oxygen Recovery; 2.2.5 Cryogenic Rectification; 2.2.5.1 Process with Air Booster and Medium-Pressure Turbine for the Recovery of Compressed Oxygen, Nitrogen and Argon; 2.2.5.2 Internal Compression 2.2.5.3 Nitrogen Generators2.2.5.4 Liquefiers; 2.2.5.5 High-purity Plants; 2.2.5.6 Apparatus; 2.2.5.7 Design, Assembly and Transport of the Coldbox; 2.3 Safety Aspects; 2.3.1 Introduction; 2.3.3 Air Pollution; 2.3.4 Ignition in Reboilers; 2.3.5 Other Hazards in Air Separation Units; 2.4 Process Analysis Air Separation Units; 2.5 Applications of the Air Gases; 2.5.1 Applications of Nitrogen; 2.5.1.1 Applications of Nitrogen for Inerting and Purging; 2.5.1.2 Applications of Nitrogen for Cooling, Preserving and Deep-Freezing; 2.5.2 Applications of Oxygen; 2.5.3 Applications of Argon; References 3 The Noble Gases Neon, Krypton and Xenon3.1 History and Occurrence; 3.2 Physical and Chemical Properties; 3.3 Recovery of Krypton and Xenon; 3.3.1 Pre-enrichment in the Air Separator; 3.3.2 Recovery of Pure Kr and Xe; 3.3.2.1 Catalytic Combustion of Hydrocarbons; 3.3.2.2 Cryogenic Separation; 3.4 Recovery of Neon; 3.4.1 Pre-enrichment; 3.4.2 Fine Purification; 3.5 Industrial Product Purities and Analytics; 3.6 Applications of the Noble Gases Neon, Krypton and Xenon; 3.6.1 Applications of Neon; 3.6.2 Applications of Krypton; 3.6.3 Applications of Xenon; References; 4 The Noble Gas Helium 4.1 History, Occurrence and Properties4.1.1 History; 4.1.2 Occurrence; 4.1.3 Physical and Chemical Properties; 4.2 Recovery; 4.3 Applications; References; 5 Hydrogen and Carbon Monoxide: Synthesis Gases; 5.1 History, Occurrence and Properties; 5.1.1 Introduction; 5.1.2 History of Synthesis Gas; 5.1.3 Hydrogen; 5.1.3.1 History and Occurrence; 5.1.3.2 Physical and Chemical Properties; 5.1.4 Carbon Monoxide; 5.1.4.1 History and Occurrence; 5.1.4.2 Physical and Chemical Properties; 5.2 Production of Synthesis Gas; 5.2.1 Production of Hydrogen by Electrolysis 5.2.2 Production of Synthesis Gas from Hydrocarbons |
| Record Nr. | UNINA-9910830130203321 |
| Weinheim, Germany : , : Wiley-VCH Verlag GmbH & Co. KGaA, , 2008 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Multidimensional liquid chromatography [[electronic resource] ] : theory and applications in industrial chemistry and the life sciences / / edited by Steven A. Cohen, Mark R. Schure
| Multidimensional liquid chromatography [[electronic resource] ] : theory and applications in industrial chemistry and the life sciences / / edited by Steven A. Cohen, Mark R. Schure |
| Pubbl/distr/stampa | Hoboken, N.J., : Wiley-Interscience, c2008 |
| Descrizione fisica | 1 online resource (490 p.) |
| Disciplina |
543.84
543/.84 |
| Altri autori (Persone) |
CohenSteven A. <1953->
SchureMark R |
| Soggetto topico |
Biochemistry
Chemical engineering Chemistry, Technical Liquid chromatography |
| Soggetto genere / forma | Electronic books. |
| ISBN |
1-281-28497-1
9786611284978 0-470-27626-6 0-470-27625-8 |
| Classificazione |
35.71
35.29 58.14 VG 7500 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
MULTIDIMENSIONAL LIQUID CHROMATOGRAPHY; CONTENTS; Foreword; Preface; Contributors; 1 Introduction; 1.1 Previous Literature Which Covers MDLC; 1.2 How this Book is Organized; References; PART I THEORY; 2 Elements of the Theory of Multidimensional Liquid Chromatography; 2.1 Introduction; 2.2 Peak Capacity; 2.3 Resolution; 2.4 Orthogonality; 2.5 Two-Dimensional Theory of Peak Overlap; 2.6 Dimensionality, Peak Ordering, and Clustering; 2.7 Theory of Zone Sampling; 2.8 Dilution and Limit of Detection; 2.9 Chemometric Analysis; 2.10 Future Directions; References
3 Peak Capacity in Two-Dimensional Liquid Chromatography3.1 Introduction; 3.2 Theory; 3.3 Procedures; 3.4 Results and Discussion; 3.5 Conclusions; Appendix 3A Generation of Random Correlated Coordinates; Appendix 3B Derivation of Limiting Correlation Coefficient r; References; 4 Decoding Complex 2D Separations; 4.1 Introduction; 4.2 Fundamentals: The Statistical Description of Complex Multicomponent Separations; 4.3 Decoding 1D and 2D Multicomponent Separations by Using the SMO Poisson Statistics; 4.4 Decoding Multicomponent Separations by the Autocovariance Function 4.5 Application to 2D Separations4.5.1 Results from SMO Method; 4.5.2 Results from 2D Autocovariance Function Method; 4.6 Concluding Remarks; Acknowledgments; References; PART II COLUMNS, INSTRUMENTATION AND METHODS DEVELOPMENT; 5 Instrumentation for Comprehensive Multidimensional Liquid Chromatography; 5.1 Introduction; 5.2 Heart-Cutting Versus Comprehensive Mode; 5.3 Chromatographic Hardware; 5.3.1 Valves; 5.4 CE Interfaces; 5.4.1 Gated Interface for HPLC-CE; 5.4.2 Microfluidic Valves for On-Chip Multidimensional Analysis; 5.5 Columns and Combinations 5.5.1 Column Systems, Dilution, and Splitting5.6 Detection; 5.7 Computer Hardware and Software; 5.7.1 Software Development; 5.7.2 Valve Sequencing; 5.7.3 Data Format and Storage; 5.8 Zone Visualization; 5.8.1 Contour Visualization; 5.8.2 2D Peak Presentation; 5.8.3 Zone Visualization in Specific Chemical (pI) Regions; 5.8.4 External Plotting Programs; 5.8.5 Difference Plots; 5.8.6 Multi-channel Data; 5.9 Data Analysis and Signal Processing; 5.10 Future Prospects; References; 6 Method Development in Comprehensive Multidimensional Liquid Chromatography; 6.1 Introduction; 6.2 Previous Work 6.3 Column Variables6.4 Method Development; 6.4.1 The Cardinal Rules of 2DLC Method Development; 6.5 Planning the Experiment; 6.6 General Comments on Optimizing the 2DLC Experiment: Speed-Resolution Trade-off; Acknowledgment; References; 7 Monolithic Columns and Their 2D-HPLC Applications; 7.1 Introduction; 7.2 Monolithic Polymer Columns; 7.2.1 Structural Properties of Polymer Monoliths; 7.2.2 Chromatographic Properties of Polymer Monolithic Columns; 7.2.3 Two-Dimensional HPLC Using Polymer Monoliths; 7.3 Monolithic Silica Columns; 7.3.1 Preparation 7.3.2 Structural Properties of Monolithic Silica Columns |
| Record Nr. | UNINA-9910145267303321 |
| Hoboken, N.J., : Wiley-Interscience, c2008 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Multidimensional liquid chromatography [[electronic resource] ] : theory and applications in industrial chemistry and the life sciences / / edited by Steven A. Cohen, Mark R. Schure
| Multidimensional liquid chromatography [[electronic resource] ] : theory and applications in industrial chemistry and the life sciences / / edited by Steven A. Cohen, Mark R. Schure |
| Pubbl/distr/stampa | Hoboken, N.J., : Wiley-Interscience, c2008 |
| Descrizione fisica | 1 online resource (490 p.) |
| Disciplina |
543.84
543/.84 |
| Altri autori (Persone) |
CohenSteven A. <1953->
SchureMark R |
| Soggetto topico |
Biochemistry
Chemical engineering Chemistry, Technical Liquid chromatography |
| ISBN |
1-281-28497-1
9786611284978 0-470-27626-6 0-470-27625-8 |
| Classificazione |
35.71
35.29 58.14 VG 7500 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
MULTIDIMENSIONAL LIQUID CHROMATOGRAPHY; CONTENTS; Foreword; Preface; Contributors; 1 Introduction; 1.1 Previous Literature Which Covers MDLC; 1.2 How this Book is Organized; References; PART I THEORY; 2 Elements of the Theory of Multidimensional Liquid Chromatography; 2.1 Introduction; 2.2 Peak Capacity; 2.3 Resolution; 2.4 Orthogonality; 2.5 Two-Dimensional Theory of Peak Overlap; 2.6 Dimensionality, Peak Ordering, and Clustering; 2.7 Theory of Zone Sampling; 2.8 Dilution and Limit of Detection; 2.9 Chemometric Analysis; 2.10 Future Directions; References
3 Peak Capacity in Two-Dimensional Liquid Chromatography3.1 Introduction; 3.2 Theory; 3.3 Procedures; 3.4 Results and Discussion; 3.5 Conclusions; Appendix 3A Generation of Random Correlated Coordinates; Appendix 3B Derivation of Limiting Correlation Coefficient r; References; 4 Decoding Complex 2D Separations; 4.1 Introduction; 4.2 Fundamentals: The Statistical Description of Complex Multicomponent Separations; 4.3 Decoding 1D and 2D Multicomponent Separations by Using the SMO Poisson Statistics; 4.4 Decoding Multicomponent Separations by the Autocovariance Function 4.5 Application to 2D Separations4.5.1 Results from SMO Method; 4.5.2 Results from 2D Autocovariance Function Method; 4.6 Concluding Remarks; Acknowledgments; References; PART II COLUMNS, INSTRUMENTATION AND METHODS DEVELOPMENT; 5 Instrumentation for Comprehensive Multidimensional Liquid Chromatography; 5.1 Introduction; 5.2 Heart-Cutting Versus Comprehensive Mode; 5.3 Chromatographic Hardware; 5.3.1 Valves; 5.4 CE Interfaces; 5.4.1 Gated Interface for HPLC-CE; 5.4.2 Microfluidic Valves for On-Chip Multidimensional Analysis; 5.5 Columns and Combinations 5.5.1 Column Systems, Dilution, and Splitting5.6 Detection; 5.7 Computer Hardware and Software; 5.7.1 Software Development; 5.7.2 Valve Sequencing; 5.7.3 Data Format and Storage; 5.8 Zone Visualization; 5.8.1 Contour Visualization; 5.8.2 2D Peak Presentation; 5.8.3 Zone Visualization in Specific Chemical (pI) Regions; 5.8.4 External Plotting Programs; 5.8.5 Difference Plots; 5.8.6 Multi-channel Data; 5.9 Data Analysis and Signal Processing; 5.10 Future Prospects; References; 6 Method Development in Comprehensive Multidimensional Liquid Chromatography; 6.1 Introduction; 6.2 Previous Work 6.3 Column Variables6.4 Method Development; 6.4.1 The Cardinal Rules of 2DLC Method Development; 6.5 Planning the Experiment; 6.6 General Comments on Optimizing the 2DLC Experiment: Speed-Resolution Trade-off; Acknowledgment; References; 7 Monolithic Columns and Their 2D-HPLC Applications; 7.1 Introduction; 7.2 Monolithic Polymer Columns; 7.2.1 Structural Properties of Polymer Monoliths; 7.2.2 Chromatographic Properties of Polymer Monolithic Columns; 7.2.3 Two-Dimensional HPLC Using Polymer Monoliths; 7.3 Monolithic Silica Columns; 7.3.1 Preparation 7.3.2 Structural Properties of Monolithic Silica Columns |
| Record Nr. | UNINA-9910830737903321 |
| Hoboken, N.J., : Wiley-Interscience, c2008 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Multidimensional liquid chromatography : theory and applications in industrial chemistry and the life sciences / / edited by Steven A. Cohen, Mark R. Schure
| Multidimensional liquid chromatography : theory and applications in industrial chemistry and the life sciences / / edited by Steven A. Cohen, Mark R. Schure |
| Pubbl/distr/stampa | Hoboken, N.J., : Wiley-Interscience, c2008 |
| Descrizione fisica | 1 online resource (490 p.) |
| Disciplina |
543.84
543/.84 |
| Altri autori (Persone) |
CohenSteven A. <1953->
SchureMark R |
| Soggetto topico |
Biochemistry
Chemical engineering Chemistry, Technical Liquid chromatography |
| ISBN |
1-281-28497-1
9786611284978 0-470-27626-6 0-470-27625-8 |
| Classificazione |
35.71
35.29 58.14 VG 7500 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
MULTIDIMENSIONAL LIQUID CHROMATOGRAPHY; CONTENTS; Foreword; Preface; Contributors; 1 Introduction; 1.1 Previous Literature Which Covers MDLC; 1.2 How this Book is Organized; References; PART I THEORY; 2 Elements of the Theory of Multidimensional Liquid Chromatography; 2.1 Introduction; 2.2 Peak Capacity; 2.3 Resolution; 2.4 Orthogonality; 2.5 Two-Dimensional Theory of Peak Overlap; 2.6 Dimensionality, Peak Ordering, and Clustering; 2.7 Theory of Zone Sampling; 2.8 Dilution and Limit of Detection; 2.9 Chemometric Analysis; 2.10 Future Directions; References
3 Peak Capacity in Two-Dimensional Liquid Chromatography3.1 Introduction; 3.2 Theory; 3.3 Procedures; 3.4 Results and Discussion; 3.5 Conclusions; Appendix 3A Generation of Random Correlated Coordinates; Appendix 3B Derivation of Limiting Correlation Coefficient r; References; 4 Decoding Complex 2D Separations; 4.1 Introduction; 4.2 Fundamentals: The Statistical Description of Complex Multicomponent Separations; 4.3 Decoding 1D and 2D Multicomponent Separations by Using the SMO Poisson Statistics; 4.4 Decoding Multicomponent Separations by the Autocovariance Function 4.5 Application to 2D Separations4.5.1 Results from SMO Method; 4.5.2 Results from 2D Autocovariance Function Method; 4.6 Concluding Remarks; Acknowledgments; References; PART II COLUMNS, INSTRUMENTATION AND METHODS DEVELOPMENT; 5 Instrumentation for Comprehensive Multidimensional Liquid Chromatography; 5.1 Introduction; 5.2 Heart-Cutting Versus Comprehensive Mode; 5.3 Chromatographic Hardware; 5.3.1 Valves; 5.4 CE Interfaces; 5.4.1 Gated Interface for HPLC-CE; 5.4.2 Microfluidic Valves for On-Chip Multidimensional Analysis; 5.5 Columns and Combinations 5.5.1 Column Systems, Dilution, and Splitting5.6 Detection; 5.7 Computer Hardware and Software; 5.7.1 Software Development; 5.7.2 Valve Sequencing; 5.7.3 Data Format and Storage; 5.8 Zone Visualization; 5.8.1 Contour Visualization; 5.8.2 2D Peak Presentation; 5.8.3 Zone Visualization in Specific Chemical (pI) Regions; 5.8.4 External Plotting Programs; 5.8.5 Difference Plots; 5.8.6 Multi-channel Data; 5.9 Data Analysis and Signal Processing; 5.10 Future Prospects; References; 6 Method Development in Comprehensive Multidimensional Liquid Chromatography; 6.1 Introduction; 6.2 Previous Work 6.3 Column Variables6.4 Method Development; 6.4.1 The Cardinal Rules of 2DLC Method Development; 6.5 Planning the Experiment; 6.6 General Comments on Optimizing the 2DLC Experiment: Speed-Resolution Trade-off; Acknowledgment; References; 7 Monolithic Columns and Their 2D-HPLC Applications; 7.1 Introduction; 7.2 Monolithic Polymer Columns; 7.2.1 Structural Properties of Polymer Monoliths; 7.2.2 Chromatographic Properties of Polymer Monolithic Columns; 7.2.3 Two-Dimensional HPLC Using Polymer Monoliths; 7.3 Monolithic Silica Columns; 7.3.1 Preparation 7.3.2 Structural Properties of Monolithic Silica Columns |
| Record Nr. | UNINA-9910877457703321 |
| Hoboken, N.J., : Wiley-Interscience, c2008 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||