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Magnetic cell separation [[electronic resource] /] / edited by M. Zborowski, J.J. Chalmers
| Magnetic cell separation [[electronic resource] /] / edited by M. Zborowski, J.J. Chalmers |
| Pubbl/distr/stampa | Amsterdam ; ; London, : Elsevier, 2008 |
| Descrizione fisica | 1 online resource (473 p.) |
| Disciplina | 571.6 |
| Altri autori (Persone) |
ZborowskiM (Maciej)
ChalmersJ. J (Jeffrey J.) |
| Collana | Laboratory techniques in biochemistry and molecular biology |
| Soggetto topico |
Cell separation
Magnetic separation |
| ISBN |
1-281-05983-8
9786611059835 0-08-055350-8 |
| Classificazione | 35.71 |
| Formato | Materiale a stampa  |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Front Cover; Magnetic Cell Separation; Copyright Page; Contents; Preface; Chapter 1: Magnetic susceptibility; 1.1. Mass and volume magnetic susceptibilities; 1.2. Molar magnetic susceptibility; 1.3. Magnetic susceptibilities in CGS and SI systems of units; 1.4. Bulk magnetic susceptibility of a mixture; 1.5. Volume magnetic susceptibility and Bohr magneton; 1.6. Multiphase magnetic suspensions; 1.7. Magnetic phase separation; 1.7.1. Stationary fluid; 1.7.2. Laminar flow; References; Chapter 2: Magnetic formulary; 2.1. Langevin theory of paramagnetism
2.2. Paramagnetic substances: lanthanide solutions2.3. Paramagnetic substances: hemoglobin and its derivatives; 2.4. Superparamagnetic particles and ferrofluids; 2.5. Ferromagnetism and magnetic properties of iron; 2.6. Diamagnetism; 2.7. Magnetic field vectors; 2.8. Magnetic field magnitude; 2.9. Magnetic field sources; 2.10. Field gradients; 2.11. Magnetic field lines; 2.12. Magnetic field in matter; References; Chapter 3: Maxwell stress and magnetic force; 3.1. Introduction; 3.2. Magnetic force density and the body force 3.3. Magnetic force acting on a small, magnetically susceptible particle (diamagnetic and paramagnetic materials)3.4. Magnetic force on a small particle acting as a permanent magnetic dipole (ferromagnetic materials); 3.5. Potential energy of an elementary magnetic dipole; 3.6. Magnetic field-induced particle motion; 3.7. Magnetic pathlines; 3.8. Cell deposition contour surfaces; References; Chapter 4: Basic magnetic field configurations; 4.1. Introduction; 4.2. Infinite cylinder; 4.3. Sphere and a stack of spheres; 4.4. Interpolar gap; 4.5. Isodynamic field; 4.6. Quadrupole field 4.7. Other magnet configurationsReferences; Chapter 5: Magnetophoresis; 5.1. Magnetophoretic mobility; 5.1.1. Cross-section for magnetic capture; References; Chapter 6: Synthesis and characterization of nano- and micron-sized iron oxide and iron particles for biomedic; 6.1. Introduction; 6.2. Maghemite nanoparticles of narrow size distribution; 6.2.1. Synthesis and characterization; 6.2.2. Surface modification; 6.2.3. Biomedical applications; 6.2.4. MRI contrast agents; 6.2.5. X-ray contrast agents; 6.3. Air-stable iron nanocrystalline particles; 6.3.1. Conclusions 6.4. Solid and hollow maghemite/polystyrene and silica/maghemite/polystyrene micron-sized composite particles of narro6.4.1. Synthesis and characterization of solid and hollow microspheres; 6.4.2. Synthesis of immunomagnetic microspheres for specific removal of ASA and sperm cells; 6.5. Magnetic/nonmagnetic polystyrene/poly(methyl methacrylate) hemispherical composite micron-sized particles; Summary; References; Chapter 7: The biocompatibility and toxicity of magnetic particles; 7.1. Introduction; 7.2. Definition of toxicity and biocompatibility; 7.2.1. Biomaterials classifications 7.3. Particle characteristics that influence toxicity |
| Record Nr. | UNINA-9910784999103321 |
| Amsterdam ; ; London, : Elsevier, 2008 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Multidimensional liquid chromatography [[electronic resource] ] : theory and applications in industrial chemistry and the life sciences / / edited by Steven A. Cohen, Mark R. Schure
| Multidimensional liquid chromatography [[electronic resource] ] : theory and applications in industrial chemistry and the life sciences / / edited by Steven A. Cohen, Mark R. Schure |
| Pubbl/distr/stampa | Hoboken, N.J., : Wiley-Interscience, c2008 |
| Descrizione fisica | 1 online resource (490 p.) |
| Disciplina |
543.84
543/.84 |
| Altri autori (Persone) |
CohenSteven A. <1953->
SchureMark R |
| Soggetto topico |
Biochemistry
Chemical engineering Chemistry, Technical Liquid chromatography |
| Soggetto genere / forma | Electronic books. |
| ISBN |
1-281-28497-1
9786611284978 0-470-27626-6 0-470-27625-8 |
| Classificazione |
35.71
35.29 58.14 VG 7500 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
MULTIDIMENSIONAL LIQUID CHROMATOGRAPHY; CONTENTS; Foreword; Preface; Contributors; 1 Introduction; 1.1 Previous Literature Which Covers MDLC; 1.2 How this Book is Organized; References; PART I THEORY; 2 Elements of the Theory of Multidimensional Liquid Chromatography; 2.1 Introduction; 2.2 Peak Capacity; 2.3 Resolution; 2.4 Orthogonality; 2.5 Two-Dimensional Theory of Peak Overlap; 2.6 Dimensionality, Peak Ordering, and Clustering; 2.7 Theory of Zone Sampling; 2.8 Dilution and Limit of Detection; 2.9 Chemometric Analysis; 2.10 Future Directions; References
3 Peak Capacity in Two-Dimensional Liquid Chromatography3.1 Introduction; 3.2 Theory; 3.3 Procedures; 3.4 Results and Discussion; 3.5 Conclusions; Appendix 3A Generation of Random Correlated Coordinates; Appendix 3B Derivation of Limiting Correlation Coefficient r; References; 4 Decoding Complex 2D Separations; 4.1 Introduction; 4.2 Fundamentals: The Statistical Description of Complex Multicomponent Separations; 4.3 Decoding 1D and 2D Multicomponent Separations by Using the SMO Poisson Statistics; 4.4 Decoding Multicomponent Separations by the Autocovariance Function 4.5 Application to 2D Separations4.5.1 Results from SMO Method; 4.5.2 Results from 2D Autocovariance Function Method; 4.6 Concluding Remarks; Acknowledgments; References; PART II COLUMNS, INSTRUMENTATION AND METHODS DEVELOPMENT; 5 Instrumentation for Comprehensive Multidimensional Liquid Chromatography; 5.1 Introduction; 5.2 Heart-Cutting Versus Comprehensive Mode; 5.3 Chromatographic Hardware; 5.3.1 Valves; 5.4 CE Interfaces; 5.4.1 Gated Interface for HPLC-CE; 5.4.2 Microfluidic Valves for On-Chip Multidimensional Analysis; 5.5 Columns and Combinations 5.5.1 Column Systems, Dilution, and Splitting5.6 Detection; 5.7 Computer Hardware and Software; 5.7.1 Software Development; 5.7.2 Valve Sequencing; 5.7.3 Data Format and Storage; 5.8 Zone Visualization; 5.8.1 Contour Visualization; 5.8.2 2D Peak Presentation; 5.8.3 Zone Visualization in Specific Chemical (pI) Regions; 5.8.4 External Plotting Programs; 5.8.5 Difference Plots; 5.8.6 Multi-channel Data; 5.9 Data Analysis and Signal Processing; 5.10 Future Prospects; References; 6 Method Development in Comprehensive Multidimensional Liquid Chromatography; 6.1 Introduction; 6.2 Previous Work 6.3 Column Variables6.4 Method Development; 6.4.1 The Cardinal Rules of 2DLC Method Development; 6.5 Planning the Experiment; 6.6 General Comments on Optimizing the 2DLC Experiment: Speed-Resolution Trade-off; Acknowledgment; References; 7 Monolithic Columns and Their 2D-HPLC Applications; 7.1 Introduction; 7.2 Monolithic Polymer Columns; 7.2.1 Structural Properties of Polymer Monoliths; 7.2.2 Chromatographic Properties of Polymer Monolithic Columns; 7.2.3 Two-Dimensional HPLC Using Polymer Monoliths; 7.3 Monolithic Silica Columns; 7.3.1 Preparation 7.3.2 Structural Properties of Monolithic Silica Columns |
| Record Nr. | UNINA-9910145267303321 |
| Hoboken, N.J., : Wiley-Interscience, c2008 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Multidimensional liquid chromatography [[electronic resource] ] : theory and applications in industrial chemistry and the life sciences / / edited by Steven A. Cohen, Mark R. Schure
| Multidimensional liquid chromatography [[electronic resource] ] : theory and applications in industrial chemistry and the life sciences / / edited by Steven A. Cohen, Mark R. Schure |
| Pubbl/distr/stampa | Hoboken, N.J., : Wiley-Interscience, c2008 |
| Descrizione fisica | 1 online resource (490 p.) |
| Disciplina |
543.84
543/.84 |
| Altri autori (Persone) |
CohenSteven A. <1953->
SchureMark R |
| Soggetto topico |
Biochemistry
Chemical engineering Chemistry, Technical Liquid chromatography |
| ISBN |
1-281-28497-1
9786611284978 0-470-27626-6 0-470-27625-8 |
| Classificazione |
35.71
35.29 58.14 VG 7500 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
MULTIDIMENSIONAL LIQUID CHROMATOGRAPHY; CONTENTS; Foreword; Preface; Contributors; 1 Introduction; 1.1 Previous Literature Which Covers MDLC; 1.2 How this Book is Organized; References; PART I THEORY; 2 Elements of the Theory of Multidimensional Liquid Chromatography; 2.1 Introduction; 2.2 Peak Capacity; 2.3 Resolution; 2.4 Orthogonality; 2.5 Two-Dimensional Theory of Peak Overlap; 2.6 Dimensionality, Peak Ordering, and Clustering; 2.7 Theory of Zone Sampling; 2.8 Dilution and Limit of Detection; 2.9 Chemometric Analysis; 2.10 Future Directions; References
3 Peak Capacity in Two-Dimensional Liquid Chromatography3.1 Introduction; 3.2 Theory; 3.3 Procedures; 3.4 Results and Discussion; 3.5 Conclusions; Appendix 3A Generation of Random Correlated Coordinates; Appendix 3B Derivation of Limiting Correlation Coefficient r; References; 4 Decoding Complex 2D Separations; 4.1 Introduction; 4.2 Fundamentals: The Statistical Description of Complex Multicomponent Separations; 4.3 Decoding 1D and 2D Multicomponent Separations by Using the SMO Poisson Statistics; 4.4 Decoding Multicomponent Separations by the Autocovariance Function 4.5 Application to 2D Separations4.5.1 Results from SMO Method; 4.5.2 Results from 2D Autocovariance Function Method; 4.6 Concluding Remarks; Acknowledgments; References; PART II COLUMNS, INSTRUMENTATION AND METHODS DEVELOPMENT; 5 Instrumentation for Comprehensive Multidimensional Liquid Chromatography; 5.1 Introduction; 5.2 Heart-Cutting Versus Comprehensive Mode; 5.3 Chromatographic Hardware; 5.3.1 Valves; 5.4 CE Interfaces; 5.4.1 Gated Interface for HPLC-CE; 5.4.2 Microfluidic Valves for On-Chip Multidimensional Analysis; 5.5 Columns and Combinations 5.5.1 Column Systems, Dilution, and Splitting5.6 Detection; 5.7 Computer Hardware and Software; 5.7.1 Software Development; 5.7.2 Valve Sequencing; 5.7.3 Data Format and Storage; 5.8 Zone Visualization; 5.8.1 Contour Visualization; 5.8.2 2D Peak Presentation; 5.8.3 Zone Visualization in Specific Chemical (pI) Regions; 5.8.4 External Plotting Programs; 5.8.5 Difference Plots; 5.8.6 Multi-channel Data; 5.9 Data Analysis and Signal Processing; 5.10 Future Prospects; References; 6 Method Development in Comprehensive Multidimensional Liquid Chromatography; 6.1 Introduction; 6.2 Previous Work 6.3 Column Variables6.4 Method Development; 6.4.1 The Cardinal Rules of 2DLC Method Development; 6.5 Planning the Experiment; 6.6 General Comments on Optimizing the 2DLC Experiment: Speed-Resolution Trade-off; Acknowledgment; References; 7 Monolithic Columns and Their 2D-HPLC Applications; 7.1 Introduction; 7.2 Monolithic Polymer Columns; 7.2.1 Structural Properties of Polymer Monoliths; 7.2.2 Chromatographic Properties of Polymer Monolithic Columns; 7.2.3 Two-Dimensional HPLC Using Polymer Monoliths; 7.3 Monolithic Silica Columns; 7.3.1 Preparation 7.3.2 Structural Properties of Monolithic Silica Columns |
| Record Nr. | UNINA-9910830737903321 |
| Hoboken, N.J., : Wiley-Interscience, c2008 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Multidimensional liquid chromatography : theory and applications in industrial chemistry and the life sciences / / edited by Steven A. Cohen, Mark R. Schure
| Multidimensional liquid chromatography : theory and applications in industrial chemistry and the life sciences / / edited by Steven A. Cohen, Mark R. Schure |
| Pubbl/distr/stampa | Hoboken, N.J., : Wiley-Interscience, c2008 |
| Descrizione fisica | 1 online resource (490 p.) |
| Disciplina |
543.84
543/.84 |
| Altri autori (Persone) |
CohenSteven A. <1953->
SchureMark R |
| Soggetto topico |
Biochemistry
Chemical engineering Chemistry, Technical Liquid chromatography |
| ISBN |
9786611284978
9781281284976 1281284971 9780470276266 0470276266 9780470276259 0470276258 |
| Classificazione |
35.71
35.29 58.14 VG 7500 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
MULTIDIMENSIONAL LIQUID CHROMATOGRAPHY; CONTENTS; Foreword; Preface; Contributors; 1 Introduction; 1.1 Previous Literature Which Covers MDLC; 1.2 How this Book is Organized; References; PART I THEORY; 2 Elements of the Theory of Multidimensional Liquid Chromatography; 2.1 Introduction; 2.2 Peak Capacity; 2.3 Resolution; 2.4 Orthogonality; 2.5 Two-Dimensional Theory of Peak Overlap; 2.6 Dimensionality, Peak Ordering, and Clustering; 2.7 Theory of Zone Sampling; 2.8 Dilution and Limit of Detection; 2.9 Chemometric Analysis; 2.10 Future Directions; References
3 Peak Capacity in Two-Dimensional Liquid Chromatography3.1 Introduction; 3.2 Theory; 3.3 Procedures; 3.4 Results and Discussion; 3.5 Conclusions; Appendix 3A Generation of Random Correlated Coordinates; Appendix 3B Derivation of Limiting Correlation Coefficient r; References; 4 Decoding Complex 2D Separations; 4.1 Introduction; 4.2 Fundamentals: The Statistical Description of Complex Multicomponent Separations; 4.3 Decoding 1D and 2D Multicomponent Separations by Using the SMO Poisson Statistics; 4.4 Decoding Multicomponent Separations by the Autocovariance Function 4.5 Application to 2D Separations4.5.1 Results from SMO Method; 4.5.2 Results from 2D Autocovariance Function Method; 4.6 Concluding Remarks; Acknowledgments; References; PART II COLUMNS, INSTRUMENTATION AND METHODS DEVELOPMENT; 5 Instrumentation for Comprehensive Multidimensional Liquid Chromatography; 5.1 Introduction; 5.2 Heart-Cutting Versus Comprehensive Mode; 5.3 Chromatographic Hardware; 5.3.1 Valves; 5.4 CE Interfaces; 5.4.1 Gated Interface for HPLC-CE; 5.4.2 Microfluidic Valves for On-Chip Multidimensional Analysis; 5.5 Columns and Combinations 5.5.1 Column Systems, Dilution, and Splitting5.6 Detection; 5.7 Computer Hardware and Software; 5.7.1 Software Development; 5.7.2 Valve Sequencing; 5.7.3 Data Format and Storage; 5.8 Zone Visualization; 5.8.1 Contour Visualization; 5.8.2 2D Peak Presentation; 5.8.3 Zone Visualization in Specific Chemical (pI) Regions; 5.8.4 External Plotting Programs; 5.8.5 Difference Plots; 5.8.6 Multi-channel Data; 5.9 Data Analysis and Signal Processing; 5.10 Future Prospects; References; 6 Method Development in Comprehensive Multidimensional Liquid Chromatography; 6.1 Introduction; 6.2 Previous Work 6.3 Column Variables6.4 Method Development; 6.4.1 The Cardinal Rules of 2DLC Method Development; 6.5 Planning the Experiment; 6.6 General Comments on Optimizing the 2DLC Experiment: Speed-Resolution Trade-off; Acknowledgment; References; 7 Monolithic Columns and Their 2D-HPLC Applications; 7.1 Introduction; 7.2 Monolithic Polymer Columns; 7.2.1 Structural Properties of Polymer Monoliths; 7.2.2 Chromatographic Properties of Polymer Monolithic Columns; 7.2.3 Two-Dimensional HPLC Using Polymer Monoliths; 7.3 Monolithic Silica Columns; 7.3.1 Preparation 7.3.2 Structural Properties of Monolithic Silica Columns |
| Record Nr. | UNINA-9911020059603321 |
| Hoboken, N.J., : Wiley-Interscience, c2008 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Protein NMR spectroscopy [[electronic resource] ] : principles and practice / / editors, John Cavanagh ... [et al.]
| Protein NMR spectroscopy [[electronic resource] ] : principles and practice / / editors, John Cavanagh ... [et al.] |
| Edizione | [2nd ed.] |
| Pubbl/distr/stampa | Amsterdam ; ; Boston, : Academic Press, c2007 |
| Descrizione fisica | 1 online resource (915 pages) |
| Disciplina | 572/.636 |
| Altri autori (Persone) | CavanaghJohn <1963-> |
| Soggetto topico |
Proteins - Analysis
Nuclear magnetic resonance spectroscopy |
| ISBN |
1-280-96292-5
9786610962921 0-08-047103-X |
| Classificazione |
35.62
35.71 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Front cover; Title page; Copyright page; Preface; Preface to the First Edition; Acknowledgements; Table of Contents; 1 Classical NMR Spectroscopy; 1.1 Nuclear Magnetism; 1.2 The Bloch Equations; 1.3 The One-Pulse NMR Experiment; 1.4 Linewidth; 1.5 Chemical Shift; 1.6 Scalar Coupling and Limitations of the Bloch Equations; References; 2 Theoretical Description of NMR Spectroscopy; 2.1 Postulates of Quantum Mechanics; 2.2 The Density Matrix; 2.3 Pulses and Rotation Operators; 2.4 Quantum Mechanical NMR Spectroscopy; 2.5 Quantum Mechanics of Multispin Systems; 2.6 Coherence
2.7 Product Operator Formalism2.8 Averaging of the Spin Hamiltonians and Residual Interactions; References; 3 Experimental Aspects of NMR Spectroscopy; 3.1 NMR Instrumentation; 3.2 Data Acquisition; 3.3 Data Processing; 3.4 Pulse Techniques; 3.5 Spin Decoupling; 3.6 B0 Field Gradients; 3.7 Water Suppression Techniques; 3.8 One-Dimensional 1H NMR Spectroscopy; References; 4 Multidimensional NMR Spectroscopy; 4.1 Two-Dimensional NMR Spectroscopy; 4.2 Coherence Transfer and Mixing; 4.3 Coherence Selection, Phase Cycling, and Field Gradients; 4.4 Resolution and Sensitivity 4.5 Three- and Four-Dimensional NMR SpectroscopyReferences; 5 Relaxation and Dynamic Processes; 5.1 Introduction and Survey of Theoretical Approaches; 5.2 The Master Equation; 5.3 Spectral Density Functions; 5.4 Relaxation Mechanisms; 5.5 Nuclear Overhauser Effect; 5.6 Chemical Exchange Effects in NMR Spectroscopy; References; 6 Experimental 1H NMR Methods; 6.1 Assessment of the 1D 1H Spectrum; 6.2 COSY-Type Experiments; 6.3 Multiple-Quantum Filtered COSY; 6.4 Multiple-Quantum Spectroscopy; 6.5 TOCSY; 6.6 Cross-Relaxation NMR Experiments; 6.7 1H 3D Experiments; References 7 Heteronuclear NMR Experiments7.1 Heteronuclear Correlation NMR Spectroscopy; 7.2 Heteronuclear-Edited NMR Spectroscopy; 7.3 13C-13C Correlations: The HCCH-COSY and HCCH-TOCSY Experiments; 7.4 3D Triple-Resonance Experiments; 7.5 Measurement of Scalar Coupling Constants; 7.6 Measurement of Residual Dipolar Coupling Constants; References; 8 Experimental NMR Relaxation Methods; 8.1 Pulse Sequences and Experimental Methods; 8.2 Picosecond-Nanosecond Dynamics; 8.3 Microsecond-Second Dynamics; References; 9 Larger Proteins and Molecular Interactions; 9.1 Larger Proteins 9.2 Intermolecular Interactions9.3 Methods for Rapid Data Acquisition; References; 10 Sequential Assignment, Structure Determination, and Other Applications; 10.1 Resonance Assignment Strategies; 10.2 Three-Dimensional Solution Structures; 10.3 Conclusion; References; Table of Symbols; List of Figures; List of Tables; Suggested Reading; Biomolecular NMR Spectroscopy; NMR Spectroscopy; Quantum Mechanics; Index; Spin-1/2 Product Operator Equations; Table of Constants |
| Record Nr. | UNINA-9910784645003321 |
| Amsterdam ; ; Boston, : Academic Press, c2007 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Protein NMR spectroscopy : principles and practice / / editors, John Cavanagh ... [et al.]
| Protein NMR spectroscopy : principles and practice / / editors, John Cavanagh ... [et al.] |
| Edizione | [2nd ed.] |
| Pubbl/distr/stampa | Amsterdam ; ; Boston, : Academic Press, c2007 |
| Descrizione fisica | 1 online resource (915 pages) |
| Disciplina | 572/.636 |
| Altri autori (Persone) | CavanaghJohn <1963-> |
| Soggetto topico |
Proteins - Analysis
Nuclear magnetic resonance spectroscopy |
| ISBN |
1-280-96292-5
9786610962921 0-08-047103-X |
| Classificazione |
35.62
35.71 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Front cover; Title page; Copyright page; Preface; Preface to the First Edition; Acknowledgements; Table of Contents; 1 Classical NMR Spectroscopy; 1.1 Nuclear Magnetism; 1.2 The Bloch Equations; 1.3 The One-Pulse NMR Experiment; 1.4 Linewidth; 1.5 Chemical Shift; 1.6 Scalar Coupling and Limitations of the Bloch Equations; References; 2 Theoretical Description of NMR Spectroscopy; 2.1 Postulates of Quantum Mechanics; 2.2 The Density Matrix; 2.3 Pulses and Rotation Operators; 2.4 Quantum Mechanical NMR Spectroscopy; 2.5 Quantum Mechanics of Multispin Systems; 2.6 Coherence
2.7 Product Operator Formalism2.8 Averaging of the Spin Hamiltonians and Residual Interactions; References; 3 Experimental Aspects of NMR Spectroscopy; 3.1 NMR Instrumentation; 3.2 Data Acquisition; 3.3 Data Processing; 3.4 Pulse Techniques; 3.5 Spin Decoupling; 3.6 B0 Field Gradients; 3.7 Water Suppression Techniques; 3.8 One-Dimensional 1H NMR Spectroscopy; References; 4 Multidimensional NMR Spectroscopy; 4.1 Two-Dimensional NMR Spectroscopy; 4.2 Coherence Transfer and Mixing; 4.3 Coherence Selection, Phase Cycling, and Field Gradients; 4.4 Resolution and Sensitivity 4.5 Three- and Four-Dimensional NMR SpectroscopyReferences; 5 Relaxation and Dynamic Processes; 5.1 Introduction and Survey of Theoretical Approaches; 5.2 The Master Equation; 5.3 Spectral Density Functions; 5.4 Relaxation Mechanisms; 5.5 Nuclear Overhauser Effect; 5.6 Chemical Exchange Effects in NMR Spectroscopy; References; 6 Experimental 1H NMR Methods; 6.1 Assessment of the 1D 1H Spectrum; 6.2 COSY-Type Experiments; 6.3 Multiple-Quantum Filtered COSY; 6.4 Multiple-Quantum Spectroscopy; 6.5 TOCSY; 6.6 Cross-Relaxation NMR Experiments; 6.7 1H 3D Experiments; References 7 Heteronuclear NMR Experiments7.1 Heteronuclear Correlation NMR Spectroscopy; 7.2 Heteronuclear-Edited NMR Spectroscopy; 7.3 13C-13C Correlations: The HCCH-COSY and HCCH-TOCSY Experiments; 7.4 3D Triple-Resonance Experiments; 7.5 Measurement of Scalar Coupling Constants; 7.6 Measurement of Residual Dipolar Coupling Constants; References; 8 Experimental NMR Relaxation Methods; 8.1 Pulse Sequences and Experimental Methods; 8.2 Picosecond-Nanosecond Dynamics; 8.3 Microsecond-Second Dynamics; References; 9 Larger Proteins and Molecular Interactions; 9.1 Larger Proteins 9.2 Intermolecular Interactions9.3 Methods for Rapid Data Acquisition; References; 10 Sequential Assignment, Structure Determination, and Other Applications; 10.1 Resonance Assignment Strategies; 10.2 Three-Dimensional Solution Structures; 10.3 Conclusion; References; Table of Symbols; List of Figures; List of Tables; Suggested Reading; Biomolecular NMR Spectroscopy; NMR Spectroscopy; Quantum Mechanics; Index; Spin-1/2 Product Operator Equations; Table of Constants |
| Record Nr. | UNINA-9910963811303321 |
| Amsterdam ; ; Boston, : Academic Press, c2007 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||