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Asymmetric organocatalysis [[electronic resource] ] : from biomimetic concepts to applications in asymmetric synthesis / / Albrecht Berkessel, Harald Gröger
| Asymmetric organocatalysis [[electronic resource] ] : from biomimetic concepts to applications in asymmetric synthesis / / Albrecht Berkessel, Harald Gröger |
| Autore | Berkessel Albrecht |
| Pubbl/distr/stampa | Weinheim, : Wiley-VCH, c2005 |
| Descrizione fisica | 1 online resource (456 p.) |
| Disciplina | 547.215 |
| Altri autori (Persone) | GrögerHarald |
| Soggetto topico |
Asymmetric synthesis
Catalysis Organic compounds - Synthesis |
| Soggetto genere / forma | Electronic books. |
| ISBN |
1-280-51952-5
9786610519521 3-527-60467-7 3-527-60405-7 |
| Classificazione | 35.52 |
| Formato | Materiale a stampa  |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Asymmetric Organocatalysis - From Biomimetic Concepts to Applications in Asymmetric Synthesis; Contents; Preface; Foreword; 1 Introduction: Organocatalysis - From Biomimetic Concepts to Powerful Methods for Asymmetric Synthesis; References; 2 On the Structure of the Book, and a Few General Mechanistic Considerations; 2.1 The Structure of the Book; 2.2 General Mechanistic Considerations; References; 3 Nucleophilic Substitution at Aliphatic Carbon; 3.1 α-Alkylation of Cyclic Ketones and Related Compounds; 3.2 α-Alkylation of α-Amino Acid Derivatives
3.2.1 Development of Highly Efficient Organocatalysts3.2.2 Improving Enantioselectivity During Work-up; 3.2.3 Specific Application in the Synthesis of Non-natural Amino Acids; 3.2.4 Synthesis of α,α-Dialkylated Amino Acids; 3.2.5 Enantio- and Diastereoselective Processes - Synthesis of α-Amino Acid Derivatives with Two Stereogenic Centers; 3.2.6 Solid-phase Syntheses; 3.3 α-Alkylation of Other Acyclic Substrates; 3.4 Fluorination, Chlorination, and Bromination Reactions; 3.4.1 Fluorination Reactions; 3.4.2 Chlorination and Bromination Reactions; References 4 Nucleophilic Addition to Electron-deficient C=C Double Bonds4.1 Intermolecular Michael Addition; 4.1.1 Intermolecular Michael Addition of C-nucleophiles; 4.1.1.1 Chiral Bases and Phase-transfer Catalysis; 4.1.1.2 Activation of Michael Acceptors by Iminium Ion Formation, Activation of Carbonyl Donors by Enamine Formation; 4.1.1.3 Addition of C-nucleophiles to Azodicarboxylates; 4.1.1.4 Cyclopropanation of Enoates with Phenacyl Halides; 4.1.2 Intermolecular Michael Addition of N- and O-nucleophiles; 4.1.3 Intermolecular Michael Addition of S- and Se-nucleophiles 4.2 Intramolecular Michael Addition4.2.1 Intramolecular Michael Addition of C-nucleophiles; 4.2.2 Intramolecular Michael Addition of O-nucleophiles; References; 5 Nucleophilic Addition to C=N Double Bonds; 5.1 Hydrocyanation of Imines (Strecker Reaction); 5.1.1 Chiral Diketopiperazines as Catalysts; 5.1.2 Chiral Guanidines as Catalysts; 5.1.3 Chiral Ureas and Thioureas as Catalysts; 5.1.4 Chiral N-Oxides as ""Catalysts""; 5.2 The Mannich Reaction; 5.2.1 Enantioselective Direct Mannich Reaction: Products with One Stereogenic Center 5.2.2 Enantio- and Diastereoselective Direct Mannich Reaction: Products with Two Stereogenic Centers5.2.3 Proline-catalyzed Mannich Reaction: Process Development and Optimization; 5.2.4 Enantioselective Mannich Reaction using Silyl Ketene Acetals; 5.3 β-Lactam Synthesis; 5.4 Sulfur Ylide-based Aziridination of Imines; 5.5 Hydrophosphonylation of Imines; References; 6 Nucleophilic Addition to C=O Double Bonds; 6.1 Hydrocyanation; 6.1.1 The Mechanism of the Reaction; 6.2 Aldol Reactions; 6.2.1 Intermolecular Aldol Reactions 6.2.1.1 Intermolecular Aldol Reaction With Formation of One Stereogenic Center |
| Record Nr. | UNINA-9910142560503321 |
Berkessel Albrecht
|
||
| Weinheim, : Wiley-VCH, c2005 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Asymmetric organocatalysis [[electronic resource] ] : from biomimetic concepts to applications in asymmetric synthesis / / Albrecht Berkessel, Harald Gröger
| Asymmetric organocatalysis [[electronic resource] ] : from biomimetic concepts to applications in asymmetric synthesis / / Albrecht Berkessel, Harald Gröger |
| Autore | Berkessel Albrecht |
| Pubbl/distr/stampa | Weinheim, : Wiley-VCH, c2005 |
| Descrizione fisica | 1 online resource (456 p.) |
| Disciplina | 547.215 |
| Altri autori (Persone) | GrögerHarald |
| Soggetto topico |
Asymmetric synthesis
Catalysis Organic compounds - Synthesis |
| ISBN |
1-280-51952-5
9786610519521 3-527-60467-7 3-527-60405-7 |
| Classificazione | 35.52 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Asymmetric Organocatalysis - From Biomimetic Concepts to Applications in Asymmetric Synthesis; Contents; Preface; Foreword; 1 Introduction: Organocatalysis - From Biomimetic Concepts to Powerful Methods for Asymmetric Synthesis; References; 2 On the Structure of the Book, and a Few General Mechanistic Considerations; 2.1 The Structure of the Book; 2.2 General Mechanistic Considerations; References; 3 Nucleophilic Substitution at Aliphatic Carbon; 3.1 α-Alkylation of Cyclic Ketones and Related Compounds; 3.2 α-Alkylation of α-Amino Acid Derivatives
3.2.1 Development of Highly Efficient Organocatalysts3.2.2 Improving Enantioselectivity During Work-up; 3.2.3 Specific Application in the Synthesis of Non-natural Amino Acids; 3.2.4 Synthesis of α,α-Dialkylated Amino Acids; 3.2.5 Enantio- and Diastereoselective Processes - Synthesis of α-Amino Acid Derivatives with Two Stereogenic Centers; 3.2.6 Solid-phase Syntheses; 3.3 α-Alkylation of Other Acyclic Substrates; 3.4 Fluorination, Chlorination, and Bromination Reactions; 3.4.1 Fluorination Reactions; 3.4.2 Chlorination and Bromination Reactions; References 4 Nucleophilic Addition to Electron-deficient C=C Double Bonds4.1 Intermolecular Michael Addition; 4.1.1 Intermolecular Michael Addition of C-nucleophiles; 4.1.1.1 Chiral Bases and Phase-transfer Catalysis; 4.1.1.2 Activation of Michael Acceptors by Iminium Ion Formation, Activation of Carbonyl Donors by Enamine Formation; 4.1.1.3 Addition of C-nucleophiles to Azodicarboxylates; 4.1.1.4 Cyclopropanation of Enoates with Phenacyl Halides; 4.1.2 Intermolecular Michael Addition of N- and O-nucleophiles; 4.1.3 Intermolecular Michael Addition of S- and Se-nucleophiles 4.2 Intramolecular Michael Addition4.2.1 Intramolecular Michael Addition of C-nucleophiles; 4.2.2 Intramolecular Michael Addition of O-nucleophiles; References; 5 Nucleophilic Addition to C=N Double Bonds; 5.1 Hydrocyanation of Imines (Strecker Reaction); 5.1.1 Chiral Diketopiperazines as Catalysts; 5.1.2 Chiral Guanidines as Catalysts; 5.1.3 Chiral Ureas and Thioureas as Catalysts; 5.1.4 Chiral N-Oxides as ""Catalysts""; 5.2 The Mannich Reaction; 5.2.1 Enantioselective Direct Mannich Reaction: Products with One Stereogenic Center 5.2.2 Enantio- and Diastereoselective Direct Mannich Reaction: Products with Two Stereogenic Centers5.2.3 Proline-catalyzed Mannich Reaction: Process Development and Optimization; 5.2.4 Enantioselective Mannich Reaction using Silyl Ketene Acetals; 5.3 β-Lactam Synthesis; 5.4 Sulfur Ylide-based Aziridination of Imines; 5.5 Hydrophosphonylation of Imines; References; 6 Nucleophilic Addition to C=O Double Bonds; 6.1 Hydrocyanation; 6.1.1 The Mechanism of the Reaction; 6.2 Aldol Reactions; 6.2.1 Intermolecular Aldol Reactions 6.2.1.1 Intermolecular Aldol Reaction With Formation of One Stereogenic Center |
| Record Nr. | UNISA-996203314103316 |
|
Berkessel Albrecht
|
||
| Weinheim, : Wiley-VCH, c2005 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. di Salerno | ||
| ||
Asymmetric organocatalysis [[electronic resource] ] : from biomimetic concepts to applications in asymmetric synthesis / / Albrecht Berkessel, Harald Gröger
| Asymmetric organocatalysis [[electronic resource] ] : from biomimetic concepts to applications in asymmetric synthesis / / Albrecht Berkessel, Harald Gröger |
| Autore | Berkessel Albrecht |
| Pubbl/distr/stampa | Weinheim, : Wiley-VCH, c2005 |
| Descrizione fisica | 1 online resource (456 p.) |
| Disciplina | 547.215 |
| Altri autori (Persone) | GrögerHarald |
| Soggetto topico |
Asymmetric synthesis
Catalysis Organic compounds - Synthesis |
| ISBN |
1-280-51952-5
9786610519521 3-527-60467-7 3-527-60405-7 |
| Classificazione | 35.52 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Asymmetric Organocatalysis - From Biomimetic Concepts to Applications in Asymmetric Synthesis; Contents; Preface; Foreword; 1 Introduction: Organocatalysis - From Biomimetic Concepts to Powerful Methods for Asymmetric Synthesis; References; 2 On the Structure of the Book, and a Few General Mechanistic Considerations; 2.1 The Structure of the Book; 2.2 General Mechanistic Considerations; References; 3 Nucleophilic Substitution at Aliphatic Carbon; 3.1 α-Alkylation of Cyclic Ketones and Related Compounds; 3.2 α-Alkylation of α-Amino Acid Derivatives
3.2.1 Development of Highly Efficient Organocatalysts3.2.2 Improving Enantioselectivity During Work-up; 3.2.3 Specific Application in the Synthesis of Non-natural Amino Acids; 3.2.4 Synthesis of α,α-Dialkylated Amino Acids; 3.2.5 Enantio- and Diastereoselective Processes - Synthesis of α-Amino Acid Derivatives with Two Stereogenic Centers; 3.2.6 Solid-phase Syntheses; 3.3 α-Alkylation of Other Acyclic Substrates; 3.4 Fluorination, Chlorination, and Bromination Reactions; 3.4.1 Fluorination Reactions; 3.4.2 Chlorination and Bromination Reactions; References 4 Nucleophilic Addition to Electron-deficient C=C Double Bonds4.1 Intermolecular Michael Addition; 4.1.1 Intermolecular Michael Addition of C-nucleophiles; 4.1.1.1 Chiral Bases and Phase-transfer Catalysis; 4.1.1.2 Activation of Michael Acceptors by Iminium Ion Formation, Activation of Carbonyl Donors by Enamine Formation; 4.1.1.3 Addition of C-nucleophiles to Azodicarboxylates; 4.1.1.4 Cyclopropanation of Enoates with Phenacyl Halides; 4.1.2 Intermolecular Michael Addition of N- and O-nucleophiles; 4.1.3 Intermolecular Michael Addition of S- and Se-nucleophiles 4.2 Intramolecular Michael Addition4.2.1 Intramolecular Michael Addition of C-nucleophiles; 4.2.2 Intramolecular Michael Addition of O-nucleophiles; References; 5 Nucleophilic Addition to C=N Double Bonds; 5.1 Hydrocyanation of Imines (Strecker Reaction); 5.1.1 Chiral Diketopiperazines as Catalysts; 5.1.2 Chiral Guanidines as Catalysts; 5.1.3 Chiral Ureas and Thioureas as Catalysts; 5.1.4 Chiral N-Oxides as ""Catalysts""; 5.2 The Mannich Reaction; 5.2.1 Enantioselective Direct Mannich Reaction: Products with One Stereogenic Center 5.2.2 Enantio- and Diastereoselective Direct Mannich Reaction: Products with Two Stereogenic Centers5.2.3 Proline-catalyzed Mannich Reaction: Process Development and Optimization; 5.2.4 Enantioselective Mannich Reaction using Silyl Ketene Acetals; 5.3 β-Lactam Synthesis; 5.4 Sulfur Ylide-based Aziridination of Imines; 5.5 Hydrophosphonylation of Imines; References; 6 Nucleophilic Addition to C=O Double Bonds; 6.1 Hydrocyanation; 6.1.1 The Mechanism of the Reaction; 6.2 Aldol Reactions; 6.2.1 Intermolecular Aldol Reactions 6.2.1.1 Intermolecular Aldol Reaction With Formation of One Stereogenic Center |
| Record Nr. | UNINA-9910829871003321 |
|
Berkessel Albrecht
|
||
| Weinheim, : Wiley-VCH, c2005 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Asymmetric organocatalysis [[electronic resource] ] : from biomimetic concepts to applications in asymmetric synthesis / / Albrecht Berkessel, Harald Gröger
| Asymmetric organocatalysis [[electronic resource] ] : from biomimetic concepts to applications in asymmetric synthesis / / Albrecht Berkessel, Harald Gröger |
| Autore | Berkessel Albrecht |
| Pubbl/distr/stampa | Weinheim, : Wiley-VCH, c2005 |
| Descrizione fisica | 1 online resource (456 p.) |
| Disciplina | 547.215 |
| Altri autori (Persone) | GrögerHarald |
| Soggetto topico |
Asymmetric synthesis
Catalysis Organic compounds - Synthesis |
| ISBN |
1-280-51952-5
9786610519521 3-527-60467-7 3-527-60405-7 |
| Classificazione | 35.52 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Asymmetric Organocatalysis - From Biomimetic Concepts to Applications in Asymmetric Synthesis; Contents; Preface; Foreword; 1 Introduction: Organocatalysis - From Biomimetic Concepts to Powerful Methods for Asymmetric Synthesis; References; 2 On the Structure of the Book, and a Few General Mechanistic Considerations; 2.1 The Structure of the Book; 2.2 General Mechanistic Considerations; References; 3 Nucleophilic Substitution at Aliphatic Carbon; 3.1 α-Alkylation of Cyclic Ketones and Related Compounds; 3.2 α-Alkylation of α-Amino Acid Derivatives
3.2.1 Development of Highly Efficient Organocatalysts3.2.2 Improving Enantioselectivity During Work-up; 3.2.3 Specific Application in the Synthesis of Non-natural Amino Acids; 3.2.4 Synthesis of α,α-Dialkylated Amino Acids; 3.2.5 Enantio- and Diastereoselective Processes - Synthesis of α-Amino Acid Derivatives with Two Stereogenic Centers; 3.2.6 Solid-phase Syntheses; 3.3 α-Alkylation of Other Acyclic Substrates; 3.4 Fluorination, Chlorination, and Bromination Reactions; 3.4.1 Fluorination Reactions; 3.4.2 Chlorination and Bromination Reactions; References 4 Nucleophilic Addition to Electron-deficient C=C Double Bonds4.1 Intermolecular Michael Addition; 4.1.1 Intermolecular Michael Addition of C-nucleophiles; 4.1.1.1 Chiral Bases and Phase-transfer Catalysis; 4.1.1.2 Activation of Michael Acceptors by Iminium Ion Formation, Activation of Carbonyl Donors by Enamine Formation; 4.1.1.3 Addition of C-nucleophiles to Azodicarboxylates; 4.1.1.4 Cyclopropanation of Enoates with Phenacyl Halides; 4.1.2 Intermolecular Michael Addition of N- and O-nucleophiles; 4.1.3 Intermolecular Michael Addition of S- and Se-nucleophiles 4.2 Intramolecular Michael Addition4.2.1 Intramolecular Michael Addition of C-nucleophiles; 4.2.2 Intramolecular Michael Addition of O-nucleophiles; References; 5 Nucleophilic Addition to C=N Double Bonds; 5.1 Hydrocyanation of Imines (Strecker Reaction); 5.1.1 Chiral Diketopiperazines as Catalysts; 5.1.2 Chiral Guanidines as Catalysts; 5.1.3 Chiral Ureas and Thioureas as Catalysts; 5.1.4 Chiral N-Oxides as ""Catalysts""; 5.2 The Mannich Reaction; 5.2.1 Enantioselective Direct Mannich Reaction: Products with One Stereogenic Center 5.2.2 Enantio- and Diastereoselective Direct Mannich Reaction: Products with Two Stereogenic Centers5.2.3 Proline-catalyzed Mannich Reaction: Process Development and Optimization; 5.2.4 Enantioselective Mannich Reaction using Silyl Ketene Acetals; 5.3 β-Lactam Synthesis; 5.4 Sulfur Ylide-based Aziridination of Imines; 5.5 Hydrophosphonylation of Imines; References; 6 Nucleophilic Addition to C=O Double Bonds; 6.1 Hydrocyanation; 6.1.1 The Mechanism of the Reaction; 6.2 Aldol Reactions; 6.2.1 Intermolecular Aldol Reactions 6.2.1.1 Intermolecular Aldol Reaction With Formation of One Stereogenic Center |
| Record Nr. | UNINA-9910841425003321 |
|
Berkessel Albrecht
|
||
| Weinheim, : Wiley-VCH, c2005 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Handbook of C-H transformations : applications in organic synthesis
| Handbook of C-H transformations : applications in organic synthesis |
| Pubbl/distr/stampa | [Place of publication not identified], : Wiley VCH, 2005 |
| Disciplina | 547.2 |
| Soggetto topico |
Organic compounds - Synthesis
Organic Chemistry Chemistry Physical Sciences & Mathematics |
| ISBN | 3-527-61945-3 |
| Classificazione | 35.52 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Record Nr. | UNINA-9910144277503321 |
| [Place of publication not identified], : Wiley VCH, 2005 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Handbook of C-H transformations : applications in organic synthesis
| Handbook of C-H transformations : applications in organic synthesis |
| Pubbl/distr/stampa | [Place of publication not identified], : Wiley VCH, 2005 |
| Disciplina | 547.2 |
| Soggetto topico |
Organic compounds - Synthesis
Organic Chemistry Chemistry Physical Sciences & Mathematics |
| ISBN | 3-527-61945-3 |
| Classificazione | 35.52 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Record Nr. | UNINA-9910830242803321 |
| [Place of publication not identified], : Wiley VCH, 2005 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Handbook of C-H transformations : applications in organic synthesis
| Handbook of C-H transformations : applications in organic synthesis |
| Pubbl/distr/stampa | [Place of publication not identified], : Wiley VCH, 2005 |
| Disciplina | 547.2 |
| Soggetto topico |
Organic compounds - Synthesis
Organic Chemistry Chemistry Physical Sciences & Mathematics |
| ISBN | 3-527-61945-3 |
| Classificazione | 35.52 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Record Nr. | UNINA-9910840549403321 |
| [Place of publication not identified], : Wiley VCH, 2005 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Microreactors in organic synthesis and catalysis / / edited by Thomas Wirth
| Microreactors in organic synthesis and catalysis / / edited by Thomas Wirth |
| Pubbl/distr/stampa | Weinheim, [Germany] : , : Wiley-VCH Verlag GmbH & Co. KGaA, , 2008 |
| Descrizione fisica | 1 online resource (299 p.) |
| Disciplina |
547.2
660.2832 |
| Soggetto topico |
Microreactors
Organic compounds - Synthesis Catalysis |
| ISBN |
1-281-94705-9
9786611947057 3-527-62285-3 3-527-62286-1 |
| Classificazione | 35.52 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Microreactors in Organic Synthesis and Catalysis; Contents; Preface; List of Contributors; 1 Fabrication of Microreactors Made from Metals and Ceramics; 1.1 Manufacturing Techniques for Metals; 1.1.1 Etching; 1.1.2 Machining; 1.1.3 Generative Method: Selective Laser Melting (SLM); 1.1.4 Metal-Forming Techniques; 1.1.5 Assembling and Bonding of Metal Microstructures; 1.2 Ceramic Devices; 1.2.1 Joining and Sealing; References; 2 Fabrication and Assembling of Microreactors Made from Glass and Silicon; 2.1 How Microreactors are Constructed; 2.2 Glass as Material; 2.3 Silicon as Material
2.4 The Structuring of Glass and Silicon2.5 Structuring by Means of Masked Etching in Microsystems Technology; 2.6 Etching Technologies; 2.6.1 Anisotropic (Crystallographic) Wet Chemical Etching of Silicon (KOH); 2.6.2 Isotropic Wet Chemical Etching of Silicon; 2.6.3 Anisotropic Dry Etching of Silicon; 2.6.4 Isotropic Wet Chemical Etching of Silicon Glass; 2.6.5 Photostructuring of Special Glass; 2.7 Chip Removing Processing; 2.7.1 Drilling, Diamond Lapping, Ultrasonic Lapping; 2.7.2 Micropowder Blasting; 2.7.3 Summary; 2.8 Bonding Methods; 2.8.1 Anodic Bonding of Glass and Silicon 2.8.2 Silicon Direct Bonding (Silicon Fusion Bonding)2.8.3 Glass Fusion Bonding; 2.9 Establishing Fluid Contact; 2.10 Other Materials; References; 3 Properties and Use of Microreactors; 3.1 Introduction; 3.2 Physical Characteristics of Microreactors; 3.2.1 Geometries; 3.2.2 Constructional Materials and Their Properties; 3.3 Fluid Flow and Delivery Regimes; 3.3.1 Fluid Flow; 3.3.2 Fluid Delivery; 3.3.3 Mixing Mechanisms; 3.4 Multifunctional Integration; 3.5 Uses of Microreactors; 3.5.1 Overview; 3.5.2 Unstable Intermediates Fast and Exothermic Reactions; 3.5.3 Precision Particle Manufacture 3.5.4 Wider Industrial Context3.5.4.1 Sustainability Agenda; 3.5.4.2 Point-of-Demand Synthesis; References; 4 Organic Chemistry in Microreactors; 4.1 Homogeneous Reactions; 4.1.1 Acid-Promoted Reactions; 4.1.2 Base-Promoted Reactions; 4.1.3 Condensation Reactions; 4.1.4 Metal-Catalyzed Reactions; 4.1.5 Photochemical Reactions; 4.1.6 Electrochemical Reactions; 4.1.7 Miscellaneous; 4.1.7.1 Swern Oxidation; 4.1.7.2 Grignard Exchange Reaction; 4.1.7.3 Lithium-Halogen Exchange Reaction; 4.1.7.4 Phenyl Boronic Acid Synthesis; References; 4.2 Heterogeneous Reactions; 4.2.1 Introduction 4.2.2 Concepts in Flow Mode Synthesis4.2.3 Methods of Conducting Flow Chemistry; 4.2.3.1 On-Bead Synthesis; 4.2.3.2 Solution-Phase Synthesis; 4.2.3.3 Library Synthesis in Flow; 4.2.3.4 Heterocycle Synthesis; 4.2.4 Introduction to Monoliths; 4.2.5 Transition Metal Chemistry Under Flow Conditions; 4.2.5.1 Reduction; 4.2.5.2 Oxidation; 4.2.5.3 Cross-Coupling Reactions; 4.2.5.4 Olefin Metathesis; 4.2.6 Enantioselective Reactions; 4.2.6.1 Hydrolytic Kinetic Resolution; 4.2.6.2 Organometallic Additions; 4.2.6.3 Enantioselective Diels-Alder Reactions; 4.2.6.4 Ene Reactions; 4.2.6.5 Cyclopropanation 4.2.6.6 Asymmetric Conjugate Addition |
| Record Nr. | UNINA-9910144109703321 |
| Weinheim, [Germany] : , : Wiley-VCH Verlag GmbH & Co. KGaA, , 2008 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Microreactors in organic synthesis and catalysis / / edited by Thomas Wirth
| Microreactors in organic synthesis and catalysis / / edited by Thomas Wirth |
| Pubbl/distr/stampa | Weinheim, [Germany] : , : Wiley-VCH Verlag GmbH & Co. KGaA, , 2008 |
| Descrizione fisica | 1 online resource (299 p.) |
| Disciplina |
547.2
660.2832 |
| Soggetto topico |
Microreactors
Organic compounds - Synthesis Catalysis |
| ISBN |
1-281-94705-9
9786611947057 3-527-62285-3 3-527-62286-1 |
| Classificazione | 35.52 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Microreactors in Organic Synthesis and Catalysis; Contents; Preface; List of Contributors; 1 Fabrication of Microreactors Made from Metals and Ceramics; 1.1 Manufacturing Techniques for Metals; 1.1.1 Etching; 1.1.2 Machining; 1.1.3 Generative Method: Selective Laser Melting (SLM); 1.1.4 Metal-Forming Techniques; 1.1.5 Assembling and Bonding of Metal Microstructures; 1.2 Ceramic Devices; 1.2.1 Joining and Sealing; References; 2 Fabrication and Assembling of Microreactors Made from Glass and Silicon; 2.1 How Microreactors are Constructed; 2.2 Glass as Material; 2.3 Silicon as Material
2.4 The Structuring of Glass and Silicon2.5 Structuring by Means of Masked Etching in Microsystems Technology; 2.6 Etching Technologies; 2.6.1 Anisotropic (Crystallographic) Wet Chemical Etching of Silicon (KOH); 2.6.2 Isotropic Wet Chemical Etching of Silicon; 2.6.3 Anisotropic Dry Etching of Silicon; 2.6.4 Isotropic Wet Chemical Etching of Silicon Glass; 2.6.5 Photostructuring of Special Glass; 2.7 Chip Removing Processing; 2.7.1 Drilling, Diamond Lapping, Ultrasonic Lapping; 2.7.2 Micropowder Blasting; 2.7.3 Summary; 2.8 Bonding Methods; 2.8.1 Anodic Bonding of Glass and Silicon 2.8.2 Silicon Direct Bonding (Silicon Fusion Bonding)2.8.3 Glass Fusion Bonding; 2.9 Establishing Fluid Contact; 2.10 Other Materials; References; 3 Properties and Use of Microreactors; 3.1 Introduction; 3.2 Physical Characteristics of Microreactors; 3.2.1 Geometries; 3.2.2 Constructional Materials and Their Properties; 3.3 Fluid Flow and Delivery Regimes; 3.3.1 Fluid Flow; 3.3.2 Fluid Delivery; 3.3.3 Mixing Mechanisms; 3.4 Multifunctional Integration; 3.5 Uses of Microreactors; 3.5.1 Overview; 3.5.2 Unstable Intermediates Fast and Exothermic Reactions; 3.5.3 Precision Particle Manufacture 3.5.4 Wider Industrial Context3.5.4.1 Sustainability Agenda; 3.5.4.2 Point-of-Demand Synthesis; References; 4 Organic Chemistry in Microreactors; 4.1 Homogeneous Reactions; 4.1.1 Acid-Promoted Reactions; 4.1.2 Base-Promoted Reactions; 4.1.3 Condensation Reactions; 4.1.4 Metal-Catalyzed Reactions; 4.1.5 Photochemical Reactions; 4.1.6 Electrochemical Reactions; 4.1.7 Miscellaneous; 4.1.7.1 Swern Oxidation; 4.1.7.2 Grignard Exchange Reaction; 4.1.7.3 Lithium-Halogen Exchange Reaction; 4.1.7.4 Phenyl Boronic Acid Synthesis; References; 4.2 Heterogeneous Reactions; 4.2.1 Introduction 4.2.2 Concepts in Flow Mode Synthesis4.2.3 Methods of Conducting Flow Chemistry; 4.2.3.1 On-Bead Synthesis; 4.2.3.2 Solution-Phase Synthesis; 4.2.3.3 Library Synthesis in Flow; 4.2.3.4 Heterocycle Synthesis; 4.2.4 Introduction to Monoliths; 4.2.5 Transition Metal Chemistry Under Flow Conditions; 4.2.5.1 Reduction; 4.2.5.2 Oxidation; 4.2.5.3 Cross-Coupling Reactions; 4.2.5.4 Olefin Metathesis; 4.2.6 Enantioselective Reactions; 4.2.6.1 Hydrolytic Kinetic Resolution; 4.2.6.2 Organometallic Additions; 4.2.6.3 Enantioselective Diels-Alder Reactions; 4.2.6.4 Ene Reactions; 4.2.6.5 Cyclopropanation 4.2.6.6 Asymmetric Conjugate Addition |
| Record Nr. | UNINA-9910830276603321 |
| Weinheim, [Germany] : , : Wiley-VCH Verlag GmbH & Co. KGaA, , 2008 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Multimetallic catalysts in organic synthesis [[electronic resource] /] / edited by Masakatsu Shibasaki and Yoshinori Yamamoto
| Multimetallic catalysts in organic synthesis [[electronic resource] /] / edited by Masakatsu Shibasaki and Yoshinori Yamamoto |
| Pubbl/distr/stampa | Weinheim ; ; [Great Britain], : Wiley-VCH, c2004 |
| Descrizione fisica | 1 online resource (313 p.) |
| Disciplina |
547.1395
547.2 |
| Altri autori (Persone) |
ShibasakiMasakatsu
YamamotoY (Yoshinori) |
| Soggetto topico |
Organic compounds - Synthesis
Metal catalysts |
| Soggetto genere / forma | Electronic books. |
| ISBN |
1-280-51967-3
9786610519675 3-527-60355-7 3-527-60432-4 |
| Classificazione |
35.52
35.17 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Multimetallic Catalysts in Organic Synthesis; Contents; Preface; List of Contributors; 1 Organic Synthesis with Bimetallic Systems; 1.1 Introduction; 1.2 Reactions Promoted by a Combination of Catalytic and Stoichiometric Amounts of Metals; 1.2.1 Transition Metal-Catalyzed Cross-Coupling Reactions; 1.2.2 The Wacker Reaction; 1.2.3 The Heck Reaction; 1.2.4 Reactions Involving π-Allylpalladium Intermediates; 1.2.4.1 Electrophilic Reactions; 1.2.4.2 Nucleophilic Reactions; 1.2.5 Nickel-Catalyzed Three-Component Coupling Reaction; 1.2.6 The Nozaki-Hiyama-Kishi Reaction
1.3 Reactions Promoted by a Combination of Catalytic Amounts of Two Metals1.3.1 Transition Metal Catalyzed Cross-Coupling Reactions; 1.3.1.1 The Stille Reaction; 1.3.1.2 The Hiyama Reaction; 1.3.1.3 The Sonogashira Reaction; 1.3.2 The Wacker Reaction; 1.3.3 Reactions Involving π-Allylpalladium Intermediates; 1.3.4 Transition Metal Catalyzed Cyclization Reactions; 1.3.4.1 [3+2] Cycloaddition Reactions; 1.3.4.2 Intramolecular [n+2] Cyclization Reactions; 1.3.4.3 Intermolecular [n+2+2] Cyclotrimerization Reactions; 1.3.4.4 [2+2+1] Cycloaddition Reactions; The Pauson-Khand Reaction 1.3.4.5 Cycloisomerization Reactions1.3.4.6 Indole-Forming Reaction; 1.3.4.7 Furan- and Pyrrole-Forming Reactions; 1.3.5 Reactions Involving Nucleophilic Addition of Carbonyl Compounds; 1.3.5.1 The Aldol Reaction; 1.3.5.2 Alkynylation Reactions; 1.3.5.3 Conjugate Addition Reactions; 1.3.6 Miscellaneous Reactions; 1.3.6.1 Transition Metal Catalyzed Reactions; 1.3.6.2 Lewis Acid Catalyzed Reactions; 1.3.6.3 Sequential Reactions; References; 2 Zinc Polymetallic Asymmetric Catalysis; 2.1 Introduction; 2.2 Asymmetric Alternating Copolymerization with Dimeric Zn Complexes 2.3 Direct Catalytic Asymmetric Aldol Reaction with Zn Polymetallic Catalysts2.3.1 Introduction; 2.3.2 Direct Catalytic Asymmetric Aldol Reaction with Methyl Ketones; 2.3.3 Direct Catalytic Asymmetric Aldol Reaction with α-Hydroxy Ketones; 2.4 Direct Catalytic Asymmetric Mannich-Type Reactions; 2.5 Direct Catalytic Asymmetric Michael Reaction; 2.6 Nitroaldol (Henry) Reaction; 2.7 Conclusions; References; 3 Group 13-Alkali Metal Heterobimetallic Asymmetric Catalysis; 3.1 Introduction; 3.2 Catalytic Asymmetric Michael Reaction of Stabilized Carbon Nucleophiles 3.2.1 Development of ALB - The First Example of a Group 13-Alkali Metal Heterobimetallic Asymmetric Catalyst3.2.2 Development of the Second-Generation Heterobimetallic Catalysts - Self-Assembly of Heterobimetallic Catalysts and Reactive Nucleophiles; 3.3 Catalytic Asymmetric Ring-Opening Reaction of meso-Epoxides; 3.3.1 Ring-Opening Reaction with Thiols; 3.3.2 Ring-Opening Reaction with Phenolic Oxygen - Development of a Novel Linked-BINOL Complex; 3.4 Catalytic Asymmetric Mannich Reactions; 3.4.1 Direct Catalytic Asymmetric Mannich-Type Reaction of Unmodified Ketones 3.4.2 Enantio- and Diastereoselective Catalytic Nitro-Mannich Reactions |
| Record Nr. | UNINA-9910144298903321 |
| Weinheim ; ; [Great Britain], : Wiley-VCH, c2004 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
