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Guidelines for chemical reactivity evaluation and application to process design [[electronic resource]]
| Guidelines for chemical reactivity evaluation and application to process design [[electronic resource]] |
| Pubbl/distr/stampa | New York, N.Y., : Center for Chemical Process Safety of the American Institute of Chemical Engineers, c1995 |
| Descrizione fisica | 1 online resource (240 p.) |
| Disciplina |
620.0042
660.2812 660/.2812 |
| Soggetto topico |
Chemical processes
Reactivity (Chemistry) |
| Soggetto genere / forma | Electronic books. |
| ISBN |
1-282-81730-2
9786612817304 0-470-93805-6 1-59124-629-6 0-470-93804-8 |
| Formato | Materiale a stampa  |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Guidelines for Chemical Reactivity Evaluation and Application to Process Design; CONTENTS; List of Tables; List of figures; Preface; Acknowledgments; Glossary; List of Symbols; 1. INTRODUCTION; 1.1 GENERAL; 1.2 CHEMICAL REACTIVITY; 1.3 DETONATIONS, DEFLAGRATIONS, AND RUNAWAYS; 1.4 ASSESSMENT AND TESTING STRATEGIES; 2. IDENTIFICATION OF HAZARDOUS CHEMICAL REACTIVITY; 2.1. SUMMARY/STRATEGY; 2.1.1 Introduction; 2.1.2 Hazard Identification Strategy; 2.1.3 Exothermic Reactions; 2.1.4 Experimental Thermal and Reactivity Measurements; 2.1.5 Test Strategies
2.1.6 Overview of Thermal Stability Test Methods2.1.7 Examples of Interpretation and Application of Test Data; 2.2 TECHNICAL SECTION; 2.2.2 Identification of High Energy Substances; 2.2.3. Hazard Prediction by Thermodynamic Calculations; 2.2.3.1 Oxygen Balance; 2.2.3.2 Calculation of the Reaction Enthalpy; 2.2.3.3 Application of Computer Programs; 2.2.4 Instability/Incompatibility Factors; 2.2.4.1 Factors Influencing Stability; 2.2.4.2 Redox Systems; 2.2.4.3 Reactions with Water; 2.2.4.4 Reactions between Halogenated Hydrocarbons and Metals; 2.3 PRACTICAL TESTING; 2.3.1 Screening Tests 2.3.1.1 Thermal Analysis2.3.1.2 Isoperibolic Calorimetry; 2.3.2 Thermal Stability and Runaway Testing; 2.3.2.1 Isothermal Storage Tests; 2.3.2.2 Dewar Flak Testing and Adiabatic Storage Tests; 2.3.2.3 Accelerating Rate Calorimeter (ARC); 2.3.2.4 Stability Jests for Powders; 2.3.3 Explosibility Testing; 2.3.3.1 Detonation Testing; 2.3.3.2 Deflagration Testing and Autoclave Testing; 2.3.3.3 Mechanical Sensitivity Testing; 2.3.3.4 Sensitivity to Heating under Confinement; 2.3.4 Reactivity Testing; 2.3.4.1 Pyrophoric Properties; 2.3.4.2 Reactivity with Water; 2.3.4.3 Oxidizing Properties 2.3.5 Flammability Testing3. CHEMICAL REACTIVITY CONSIDERATIONS IN PROCESS/REACTOR DESIGN AND OPERATION; 3.1 INTRODUCTION; 3.1.1 Thermal Hazards: Identification and Analysis; 3.1.1.1 Cause, Definition, and Prevention of a Runaway; 3.1.1.2 Some Simple Rules for Inherent Safety; 3.1.1.3 Strategy for Inherent Safety in Design and Operation; 3.1.1.4 Equipment to be Used for the Analysis of Hazards; 3.2 REACTOR, HEAT AND MASS BALANCE CONSIDERATIONS; 3.2.1 Heat and Mass Balances, Kinetics, and Reaction Stability; 3.2.1.1 Adiabatic Temperature Rise; 3.2.1.2 The Reaction; 3.2.1.3 Reaction Rate 3.2.1.4 Reaction Rate Constant3.2.1.5 Concentration of Reactants; 3.2.1.6 Effect of Surrounding Temperature on Stability; 3.2.1.7 Effect of Agitation and Surface Fouling on stability; 3.2.1.8 Mass Balance; 3.2.2 Choice of Reactor; 3.2.3 Heat Transfer; 3.2.3.1 Heat Transfer in Nonagitated Vessels; 3.2.3.2 Heat Transfer in Agitated Vessels; 3.3 ACQUISITION AND USE OF PROCESS DESIGN DATA; 3.3.1 Introduction; 3.3.2 Bench-Scale Equipment for Batch/Tank Reactors; 3.3.2.1 Reaction Calorimeter (RC1); 3.3.2.2 Contalab; 3.3.2.3 CPA ThermoMetric Instruments; 3.3.2.4 Quantitative Reaction Calorimeter 3.3.2.5 Specialized Reactors |
| Record Nr. | UNINA-9910143246203321 |
| New York, N.Y., : Center for Chemical Process Safety of the American Institute of Chemical Engineers, c1995 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Guidelines for chemical reactivity evaluation and application to process design [[electronic resource]]
| Guidelines for chemical reactivity evaluation and application to process design [[electronic resource]] |
| Pubbl/distr/stampa | New York, N.Y., : Center for Chemical Process Safety of the American Institute of Chemical Engineers, c1995 |
| Descrizione fisica | 1 online resource (240 p.) |
| Disciplina |
620.0042
660.2812 660/.2812 |
| Soggetto topico |
Chemical processes
Reactivity (Chemistry) |
| ISBN |
1-282-81730-2
9786612817304 0-470-93805-6 1-59124-629-6 0-470-93804-8 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Guidelines for Chemical Reactivity Evaluation and Application to Process Design; CONTENTS; List of Tables; List of figures; Preface; Acknowledgments; Glossary; List of Symbols; 1. INTRODUCTION; 1.1 GENERAL; 1.2 CHEMICAL REACTIVITY; 1.3 DETONATIONS, DEFLAGRATIONS, AND RUNAWAYS; 1.4 ASSESSMENT AND TESTING STRATEGIES; 2. IDENTIFICATION OF HAZARDOUS CHEMICAL REACTIVITY; 2.1. SUMMARY/STRATEGY; 2.1.1 Introduction; 2.1.2 Hazard Identification Strategy; 2.1.3 Exothermic Reactions; 2.1.4 Experimental Thermal and Reactivity Measurements; 2.1.5 Test Strategies
2.1.6 Overview of Thermal Stability Test Methods2.1.7 Examples of Interpretation and Application of Test Data; 2.2 TECHNICAL SECTION; 2.2.2 Identification of High Energy Substances; 2.2.3. Hazard Prediction by Thermodynamic Calculations; 2.2.3.1 Oxygen Balance; 2.2.3.2 Calculation of the Reaction Enthalpy; 2.2.3.3 Application of Computer Programs; 2.2.4 Instability/Incompatibility Factors; 2.2.4.1 Factors Influencing Stability; 2.2.4.2 Redox Systems; 2.2.4.3 Reactions with Water; 2.2.4.4 Reactions between Halogenated Hydrocarbons and Metals; 2.3 PRACTICAL TESTING; 2.3.1 Screening Tests 2.3.1.1 Thermal Analysis2.3.1.2 Isoperibolic Calorimetry; 2.3.2 Thermal Stability and Runaway Testing; 2.3.2.1 Isothermal Storage Tests; 2.3.2.2 Dewar Flak Testing and Adiabatic Storage Tests; 2.3.2.3 Accelerating Rate Calorimeter (ARC); 2.3.2.4 Stability Jests for Powders; 2.3.3 Explosibility Testing; 2.3.3.1 Detonation Testing; 2.3.3.2 Deflagration Testing and Autoclave Testing; 2.3.3.3 Mechanical Sensitivity Testing; 2.3.3.4 Sensitivity to Heating under Confinement; 2.3.4 Reactivity Testing; 2.3.4.1 Pyrophoric Properties; 2.3.4.2 Reactivity with Water; 2.3.4.3 Oxidizing Properties 2.3.5 Flammability Testing3. CHEMICAL REACTIVITY CONSIDERATIONS IN PROCESS/REACTOR DESIGN AND OPERATION; 3.1 INTRODUCTION; 3.1.1 Thermal Hazards: Identification and Analysis; 3.1.1.1 Cause, Definition, and Prevention of a Runaway; 3.1.1.2 Some Simple Rules for Inherent Safety; 3.1.1.3 Strategy for Inherent Safety in Design and Operation; 3.1.1.4 Equipment to be Used for the Analysis of Hazards; 3.2 REACTOR, HEAT AND MASS BALANCE CONSIDERATIONS; 3.2.1 Heat and Mass Balances, Kinetics, and Reaction Stability; 3.2.1.1 Adiabatic Temperature Rise; 3.2.1.2 The Reaction; 3.2.1.3 Reaction Rate 3.2.1.4 Reaction Rate Constant3.2.1.5 Concentration of Reactants; 3.2.1.6 Effect of Surrounding Temperature on Stability; 3.2.1.7 Effect of Agitation and Surface Fouling on stability; 3.2.1.8 Mass Balance; 3.2.2 Choice of Reactor; 3.2.3 Heat Transfer; 3.2.3.1 Heat Transfer in Nonagitated Vessels; 3.2.3.2 Heat Transfer in Agitated Vessels; 3.3 ACQUISITION AND USE OF PROCESS DESIGN DATA; 3.3.1 Introduction; 3.3.2 Bench-Scale Equipment for Batch/Tank Reactors; 3.3.2.1 Reaction Calorimeter (RC1); 3.3.2.2 Contalab; 3.3.2.3 CPA ThermoMetric Instruments; 3.3.2.4 Quantitative Reaction Calorimeter 3.3.2.5 Specialized Reactors |
| Record Nr. | UNISA-996212702603316 |
| New York, N.Y., : Center for Chemical Process Safety of the American Institute of Chemical Engineers, c1995 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. di Salerno | ||
| ||
Guidelines for chemical reactivity evaluation and application to process design [[electronic resource]]
| Guidelines for chemical reactivity evaluation and application to process design [[electronic resource]] |
| Pubbl/distr/stampa | New York, N.Y., : Center for Chemical Process Safety of the American Institute of Chemical Engineers, c1995 |
| Descrizione fisica | 1 online resource (240 p.) |
| Disciplina |
620.0042
660.2812 660/.2812 |
| Soggetto topico |
Chemical processes
Reactivity (Chemistry) |
| ISBN |
1-282-81730-2
9786612817304 0-470-93805-6 1-59124-629-6 0-470-93804-8 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Guidelines for Chemical Reactivity Evaluation and Application to Process Design; CONTENTS; List of Tables; List of figures; Preface; Acknowledgments; Glossary; List of Symbols; 1. INTRODUCTION; 1.1 GENERAL; 1.2 CHEMICAL REACTIVITY; 1.3 DETONATIONS, DEFLAGRATIONS, AND RUNAWAYS; 1.4 ASSESSMENT AND TESTING STRATEGIES; 2. IDENTIFICATION OF HAZARDOUS CHEMICAL REACTIVITY; 2.1. SUMMARY/STRATEGY; 2.1.1 Introduction; 2.1.2 Hazard Identification Strategy; 2.1.3 Exothermic Reactions; 2.1.4 Experimental Thermal and Reactivity Measurements; 2.1.5 Test Strategies
2.1.6 Overview of Thermal Stability Test Methods2.1.7 Examples of Interpretation and Application of Test Data; 2.2 TECHNICAL SECTION; 2.2.2 Identification of High Energy Substances; 2.2.3. Hazard Prediction by Thermodynamic Calculations; 2.2.3.1 Oxygen Balance; 2.2.3.2 Calculation of the Reaction Enthalpy; 2.2.3.3 Application of Computer Programs; 2.2.4 Instability/Incompatibility Factors; 2.2.4.1 Factors Influencing Stability; 2.2.4.2 Redox Systems; 2.2.4.3 Reactions with Water; 2.2.4.4 Reactions between Halogenated Hydrocarbons and Metals; 2.3 PRACTICAL TESTING; 2.3.1 Screening Tests 2.3.1.1 Thermal Analysis2.3.1.2 Isoperibolic Calorimetry; 2.3.2 Thermal Stability and Runaway Testing; 2.3.2.1 Isothermal Storage Tests; 2.3.2.2 Dewar Flak Testing and Adiabatic Storage Tests; 2.3.2.3 Accelerating Rate Calorimeter (ARC); 2.3.2.4 Stability Jests for Powders; 2.3.3 Explosibility Testing; 2.3.3.1 Detonation Testing; 2.3.3.2 Deflagration Testing and Autoclave Testing; 2.3.3.3 Mechanical Sensitivity Testing; 2.3.3.4 Sensitivity to Heating under Confinement; 2.3.4 Reactivity Testing; 2.3.4.1 Pyrophoric Properties; 2.3.4.2 Reactivity with Water; 2.3.4.3 Oxidizing Properties 2.3.5 Flammability Testing3. CHEMICAL REACTIVITY CONSIDERATIONS IN PROCESS/REACTOR DESIGN AND OPERATION; 3.1 INTRODUCTION; 3.1.1 Thermal Hazards: Identification and Analysis; 3.1.1.1 Cause, Definition, and Prevention of a Runaway; 3.1.1.2 Some Simple Rules for Inherent Safety; 3.1.1.3 Strategy for Inherent Safety in Design and Operation; 3.1.1.4 Equipment to be Used for the Analysis of Hazards; 3.2 REACTOR, HEAT AND MASS BALANCE CONSIDERATIONS; 3.2.1 Heat and Mass Balances, Kinetics, and Reaction Stability; 3.2.1.1 Adiabatic Temperature Rise; 3.2.1.2 The Reaction; 3.2.1.3 Reaction Rate 3.2.1.4 Reaction Rate Constant3.2.1.5 Concentration of Reactants; 3.2.1.6 Effect of Surrounding Temperature on Stability; 3.2.1.7 Effect of Agitation and Surface Fouling on stability; 3.2.1.8 Mass Balance; 3.2.2 Choice of Reactor; 3.2.3 Heat Transfer; 3.2.3.1 Heat Transfer in Nonagitated Vessels; 3.2.3.2 Heat Transfer in Agitated Vessels; 3.3 ACQUISITION AND USE OF PROCESS DESIGN DATA; 3.3.1 Introduction; 3.3.2 Bench-Scale Equipment for Batch/Tank Reactors; 3.3.2.1 Reaction Calorimeter (RC1); 3.3.2.2 Contalab; 3.3.2.3 CPA ThermoMetric Instruments; 3.3.2.4 Quantitative Reaction Calorimeter 3.3.2.5 Specialized Reactors |
| Record Nr. | UNINA-9910830105403321 |
| New York, N.Y., : Center for Chemical Process Safety of the American Institute of Chemical Engineers, c1995 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Guidelines for chemical reactivity evaluation and application to process design
| Guidelines for chemical reactivity evaluation and application to process design |
| Pubbl/distr/stampa | New York, N.Y., : Center for Chemical Process Safety of the American Institute of Chemical Engineers, c1995 |
| Descrizione fisica | 1 online resource (240 p.) |
| Disciplina | 660/.2812 |
| Soggetto topico |
Chemical processes
Reactivity (Chemistry) |
| ISBN |
1-282-81730-2
9786612817304 0-470-93805-6 1-59124-629-6 0-470-93804-8 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Guidelines for Chemical Reactivity Evaluation and Application to Process Design; CONTENTS; List of Tables; List of figures; Preface; Acknowledgments; Glossary; List of Symbols; 1. INTRODUCTION; 1.1 GENERAL; 1.2 CHEMICAL REACTIVITY; 1.3 DETONATIONS, DEFLAGRATIONS, AND RUNAWAYS; 1.4 ASSESSMENT AND TESTING STRATEGIES; 2. IDENTIFICATION OF HAZARDOUS CHEMICAL REACTIVITY; 2.1. SUMMARY/STRATEGY; 2.1.1 Introduction; 2.1.2 Hazard Identification Strategy; 2.1.3 Exothermic Reactions; 2.1.4 Experimental Thermal and Reactivity Measurements; 2.1.5 Test Strategies
2.1.6 Overview of Thermal Stability Test Methods2.1.7 Examples of Interpretation and Application of Test Data; 2.2 TECHNICAL SECTION; 2.2.2 Identification of High Energy Substances; 2.2.3. Hazard Prediction by Thermodynamic Calculations; 2.2.3.1 Oxygen Balance; 2.2.3.2 Calculation of the Reaction Enthalpy; 2.2.3.3 Application of Computer Programs; 2.2.4 Instability/Incompatibility Factors; 2.2.4.1 Factors Influencing Stability; 2.2.4.2 Redox Systems; 2.2.4.3 Reactions with Water; 2.2.4.4 Reactions between Halogenated Hydrocarbons and Metals; 2.3 PRACTICAL TESTING; 2.3.1 Screening Tests 2.3.1.1 Thermal Analysis2.3.1.2 Isoperibolic Calorimetry; 2.3.2 Thermal Stability and Runaway Testing; 2.3.2.1 Isothermal Storage Tests; 2.3.2.2 Dewar Flak Testing and Adiabatic Storage Tests; 2.3.2.3 Accelerating Rate Calorimeter (ARC); 2.3.2.4 Stability Jests for Powders; 2.3.3 Explosibility Testing; 2.3.3.1 Detonation Testing; 2.3.3.2 Deflagration Testing and Autoclave Testing; 2.3.3.3 Mechanical Sensitivity Testing; 2.3.3.4 Sensitivity to Heating under Confinement; 2.3.4 Reactivity Testing; 2.3.4.1 Pyrophoric Properties; 2.3.4.2 Reactivity with Water; 2.3.4.3 Oxidizing Properties 2.3.5 Flammability Testing3. CHEMICAL REACTIVITY CONSIDERATIONS IN PROCESS/REACTOR DESIGN AND OPERATION; 3.1 INTRODUCTION; 3.1.1 Thermal Hazards: Identification and Analysis; 3.1.1.1 Cause, Definition, and Prevention of a Runaway; 3.1.1.2 Some Simple Rules for Inherent Safety; 3.1.1.3 Strategy for Inherent Safety in Design and Operation; 3.1.1.4 Equipment to be Used for the Analysis of Hazards; 3.2 REACTOR, HEAT AND MASS BALANCE CONSIDERATIONS; 3.2.1 Heat and Mass Balances, Kinetics, and Reaction Stability; 3.2.1.1 Adiabatic Temperature Rise; 3.2.1.2 The Reaction; 3.2.1.3 Reaction Rate 3.2.1.4 Reaction Rate Constant3.2.1.5 Concentration of Reactants; 3.2.1.6 Effect of Surrounding Temperature on Stability; 3.2.1.7 Effect of Agitation and Surface Fouling on stability; 3.2.1.8 Mass Balance; 3.2.2 Choice of Reactor; 3.2.3 Heat Transfer; 3.2.3.1 Heat Transfer in Nonagitated Vessels; 3.2.3.2 Heat Transfer in Agitated Vessels; 3.3 ACQUISITION AND USE OF PROCESS DESIGN DATA; 3.3.1 Introduction; 3.3.2 Bench-Scale Equipment for Batch/Tank Reactors; 3.3.2.1 Reaction Calorimeter (RC1); 3.3.2.2 Contalab; 3.3.2.3 CPA ThermoMetric Instruments; 3.3.2.4 Quantitative Reaction Calorimeter 3.3.2.5 Specialized Reactors |
| Altri titoli varianti | Chemical reactivity evaluation and application to process design |
| Record Nr. | UNINA-9910876968303321 |
| New York, N.Y., : Center for Chemical Process Safety of the American Institute of Chemical Engineers, c1995 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Principles and case studies of simultaneous design [[electronic resource] /] / William L. Luyben
| Principles and case studies of simultaneous design [[electronic resource] /] / William L. Luyben |
| Autore | Luyben William L |
| Pubbl/distr/stampa | Hoboken, N.J., : John Wiley, c2011 |
| Descrizione fisica | 1 online resource (342 p.) |
| Disciplina |
660.2812
660/.2812 |
| Soggetto topico |
Chemical engineering
Engineering design |
| Soggetto genere / forma | Electronic books. |
| ISBN |
1-283-92758-6
1-118-00164-8 1-118-00165-6 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
PRINCIPLES ANDCASE STUDIES OFSIMULTANEOUS DESIGN; PREFACE; 1 INTRODUCTION; 1.1 Overview; 1.2 History; 1.3 Books; 1.4 Tools; Reference Textbooks; 2 PRINCIPLES OF REACTOR DESIGN AND CONTROL; 2.1 Background; 2.2 Principles Derived from Chemistry; 2.2.1 Heat of Reaction; 2.2.2 Reversible and Irreversible Reactions; 2.2.3 Multiple Reactions; 2.3 Principles Derived from Phase of Reaction; 2.4 Determining Kinetic Parameters; 2.4.1 Thermodynamic Constraints; 2.4.2 Kinetic Parameters from Plant Data; 2.5 Principles of Reactor Heat Exchange; 2.5.1 Continuous Stirred-Tank Reactors
2.5.2 Tubular Reactors2.5.3 Feed-Effluent Heat Exchangers; 2.6 Heuristic Design of Reactor/Separation Processes; 2.6.1 Introduction; 2.6.2 Process Studied; 2.6.3 Economic Optimization; 2.6.4 Other Cases; 2.6.5 Real Example; 2.7 Conclusion; References; 3 PRINCIPLES OF DISTILLATION DESIGN AND CONTROL; 3.1 Principles of Economic Distillation Design; 3.1.1 Operating Pressure; 3.1.2 Heuristic Optimization; 3.1.3 Rigorous Optimization; 3.1.4 Feed Preheating and Intermediate Reboilers and Condensers; 3.1.5 Heat Integration; 3.2 Principles of Distillation Control; 3.2.1 Single-End Control 3.2.2 Dual-End Control3.2.3 Alternative Control Structures; 3.3 Conclusion; References; 4 PRINCIPLES OF PLANTWIDE CONTROL; 4.1 History; 4.2 Effects of Recycle; 4.2.1 Time Constants of Integrated Plant with Recycle; 4.2.2 Recycle Snowball Effect; 4.3 Management of Fresh Feed Streams; 4.3.1 Fundamentals; 4.3.2 Process with Two Recycles and Two Fresh Feeds; 4.4 Conclusion; 5 ECONOMIC BASIS; 5.1 Level of Accuracy; 5.2 Sizing Equipment; 5.2.1 Vessels; 5.2.2 Heat Exchangers; 5.2.3 Compressors; 5.2.4 Pumps, Valves, and Piping; 5.3 Equipment Capital Cost; 5.3.1 Vessels (diameter and length in meters) 5.3.2 Heat Exchangers (area in square meters)5.3.3 Compressors (work in horsepower); 5.4 Energy Costs; 5.5 Chemical Costs; References; 6 DESIGN AND CONTROL OF THE ACETONE PROCESS VIA DEHYDROGENATION OF ISOPROPANOL; 6.1 Process Description; 6.1.1 Reaction Kinetics; 6.1.2 Phase Equilibrium; 6.2 Turton Flowsheet; 6.2.1 Vaporizer; 6.2.2 Reactor; 6.2.3 Heat Exchangers, Flash Tank, and Absorber; 6.2.4 Acetone Column C1; 6.2.5 Water Column C2; 6.3 Revised Flowsheet; 6.3.1 Effect of Absorber Pressure; 6.3.2 Effect of Water Solvent and Absorber Stages; 6.3.3 Effect of Reactor Size 6.3.4 Optimum Distillation Design6.4 Economic Comparison; 6.5 Plantwide Control; 6.5.1 Control Structure; 6.5.2 Column Control Structure Selection; 6.5.3 Dynamic Performance Results; 6.6 Conclusion; References; 7 DESIGN AND CONTROL OF AN AUTO-REFRIGERATED ALKYLATION PROCESS; 7.1 Introduction; 7.2 Process Description; 7.2.1 Reaction Kinetics; 7.2.2 Phase Equilibrium; 7.2.3 Flowsheet; 7.2.4 Design Optimization Variables; 7.3 Design of Distillation Columns; 7.3.1 Depropanizer; 7.3.2 Deisobutanizer; 7.4 Economic Optimization of Entire Process; 7.4.1 Flowsheet Convergence; 7.4.2 Yield 7.4.3 Effect of Reactor Size |
| Record Nr. | UNINA-9910141234903321 |
Luyben William L
|
||
| Hoboken, N.J., : John Wiley, c2011 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Principles and case studies of simultaneous design [[electronic resource] /] / William L. Luyben
| Principles and case studies of simultaneous design [[electronic resource] /] / William L. Luyben |
| Autore | Luyben William L |
| Pubbl/distr/stampa | Hoboken, N.J., : John Wiley, c2011 |
| Descrizione fisica | 1 online resource (342 p.) |
| Disciplina |
660.2812
660/.2812 |
| Soggetto topico |
Chemical engineering
Engineering design |
| ISBN |
1-283-92758-6
1-118-00164-8 1-118-00165-6 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
PRINCIPLES ANDCASE STUDIES OFSIMULTANEOUS DESIGN; PREFACE; 1 INTRODUCTION; 1.1 Overview; 1.2 History; 1.3 Books; 1.4 Tools; Reference Textbooks; 2 PRINCIPLES OF REACTOR DESIGN AND CONTROL; 2.1 Background; 2.2 Principles Derived from Chemistry; 2.2.1 Heat of Reaction; 2.2.2 Reversible and Irreversible Reactions; 2.2.3 Multiple Reactions; 2.3 Principles Derived from Phase of Reaction; 2.4 Determining Kinetic Parameters; 2.4.1 Thermodynamic Constraints; 2.4.2 Kinetic Parameters from Plant Data; 2.5 Principles of Reactor Heat Exchange; 2.5.1 Continuous Stirred-Tank Reactors
2.5.2 Tubular Reactors2.5.3 Feed-Effluent Heat Exchangers; 2.6 Heuristic Design of Reactor/Separation Processes; 2.6.1 Introduction; 2.6.2 Process Studied; 2.6.3 Economic Optimization; 2.6.4 Other Cases; 2.6.5 Real Example; 2.7 Conclusion; References; 3 PRINCIPLES OF DISTILLATION DESIGN AND CONTROL; 3.1 Principles of Economic Distillation Design; 3.1.1 Operating Pressure; 3.1.2 Heuristic Optimization; 3.1.3 Rigorous Optimization; 3.1.4 Feed Preheating and Intermediate Reboilers and Condensers; 3.1.5 Heat Integration; 3.2 Principles of Distillation Control; 3.2.1 Single-End Control 3.2.2 Dual-End Control3.2.3 Alternative Control Structures; 3.3 Conclusion; References; 4 PRINCIPLES OF PLANTWIDE CONTROL; 4.1 History; 4.2 Effects of Recycle; 4.2.1 Time Constants of Integrated Plant with Recycle; 4.2.2 Recycle Snowball Effect; 4.3 Management of Fresh Feed Streams; 4.3.1 Fundamentals; 4.3.2 Process with Two Recycles and Two Fresh Feeds; 4.4 Conclusion; 5 ECONOMIC BASIS; 5.1 Level of Accuracy; 5.2 Sizing Equipment; 5.2.1 Vessels; 5.2.2 Heat Exchangers; 5.2.3 Compressors; 5.2.4 Pumps, Valves, and Piping; 5.3 Equipment Capital Cost; 5.3.1 Vessels (diameter and length in meters) 5.3.2 Heat Exchangers (area in square meters)5.3.3 Compressors (work in horsepower); 5.4 Energy Costs; 5.5 Chemical Costs; References; 6 DESIGN AND CONTROL OF THE ACETONE PROCESS VIA DEHYDROGENATION OF ISOPROPANOL; 6.1 Process Description; 6.1.1 Reaction Kinetics; 6.1.2 Phase Equilibrium; 6.2 Turton Flowsheet; 6.2.1 Vaporizer; 6.2.2 Reactor; 6.2.3 Heat Exchangers, Flash Tank, and Absorber; 6.2.4 Acetone Column C1; 6.2.5 Water Column C2; 6.3 Revised Flowsheet; 6.3.1 Effect of Absorber Pressure; 6.3.2 Effect of Water Solvent and Absorber Stages; 6.3.3 Effect of Reactor Size 6.3.4 Optimum Distillation Design6.4 Economic Comparison; 6.5 Plantwide Control; 6.5.1 Control Structure; 6.5.2 Column Control Structure Selection; 6.5.3 Dynamic Performance Results; 6.6 Conclusion; References; 7 DESIGN AND CONTROL OF AN AUTO-REFRIGERATED ALKYLATION PROCESS; 7.1 Introduction; 7.2 Process Description; 7.2.1 Reaction Kinetics; 7.2.2 Phase Equilibrium; 7.2.3 Flowsheet; 7.2.4 Design Optimization Variables; 7.3 Design of Distillation Columns; 7.3.1 Depropanizer; 7.3.2 Deisobutanizer; 7.4 Economic Optimization of Entire Process; 7.4.1 Flowsheet Convergence; 7.4.2 Yield 7.4.3 Effect of Reactor Size |
| Record Nr. | UNINA-9910830583403321 |
|
Luyben William L
|
||
| Hoboken, N.J., : John Wiley, c2011 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Principles and case studies of simultaneous design / / William L. Luyben
| Principles and case studies of simultaneous design / / William L. Luyben |
| Autore | Luyben William L |
| Pubbl/distr/stampa | Hoboken, N.J., : John Wiley, c2011 |
| Descrizione fisica | 1 online resource (342 p.) |
| Disciplina |
660.2812
660/.2812 |
| Soggetto topico |
Chemical engineering
Engineering design |
| ISBN |
1-283-92758-6
1-118-00164-8 1-118-00165-6 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
PRINCIPLES ANDCASE STUDIES OFSIMULTANEOUS DESIGN; PREFACE; 1 INTRODUCTION; 1.1 Overview; 1.2 History; 1.3 Books; 1.4 Tools; Reference Textbooks; 2 PRINCIPLES OF REACTOR DESIGN AND CONTROL; 2.1 Background; 2.2 Principles Derived from Chemistry; 2.2.1 Heat of Reaction; 2.2.2 Reversible and Irreversible Reactions; 2.2.3 Multiple Reactions; 2.3 Principles Derived from Phase of Reaction; 2.4 Determining Kinetic Parameters; 2.4.1 Thermodynamic Constraints; 2.4.2 Kinetic Parameters from Plant Data; 2.5 Principles of Reactor Heat Exchange; 2.5.1 Continuous Stirred-Tank Reactors
2.5.2 Tubular Reactors2.5.3 Feed-Effluent Heat Exchangers; 2.6 Heuristic Design of Reactor/Separation Processes; 2.6.1 Introduction; 2.6.2 Process Studied; 2.6.3 Economic Optimization; 2.6.4 Other Cases; 2.6.5 Real Example; 2.7 Conclusion; References; 3 PRINCIPLES OF DISTILLATION DESIGN AND CONTROL; 3.1 Principles of Economic Distillation Design; 3.1.1 Operating Pressure; 3.1.2 Heuristic Optimization; 3.1.3 Rigorous Optimization; 3.1.4 Feed Preheating and Intermediate Reboilers and Condensers; 3.1.5 Heat Integration; 3.2 Principles of Distillation Control; 3.2.1 Single-End Control 3.2.2 Dual-End Control3.2.3 Alternative Control Structures; 3.3 Conclusion; References; 4 PRINCIPLES OF PLANTWIDE CONTROL; 4.1 History; 4.2 Effects of Recycle; 4.2.1 Time Constants of Integrated Plant with Recycle; 4.2.2 Recycle Snowball Effect; 4.3 Management of Fresh Feed Streams; 4.3.1 Fundamentals; 4.3.2 Process with Two Recycles and Two Fresh Feeds; 4.4 Conclusion; 5 ECONOMIC BASIS; 5.1 Level of Accuracy; 5.2 Sizing Equipment; 5.2.1 Vessels; 5.2.2 Heat Exchangers; 5.2.3 Compressors; 5.2.4 Pumps, Valves, and Piping; 5.3 Equipment Capital Cost; 5.3.1 Vessels (diameter and length in meters) 5.3.2 Heat Exchangers (area in square meters)5.3.3 Compressors (work in horsepower); 5.4 Energy Costs; 5.5 Chemical Costs; References; 6 DESIGN AND CONTROL OF THE ACETONE PROCESS VIA DEHYDROGENATION OF ISOPROPANOL; 6.1 Process Description; 6.1.1 Reaction Kinetics; 6.1.2 Phase Equilibrium; 6.2 Turton Flowsheet; 6.2.1 Vaporizer; 6.2.2 Reactor; 6.2.3 Heat Exchangers, Flash Tank, and Absorber; 6.2.4 Acetone Column C1; 6.2.5 Water Column C2; 6.3 Revised Flowsheet; 6.3.1 Effect of Absorber Pressure; 6.3.2 Effect of Water Solvent and Absorber Stages; 6.3.3 Effect of Reactor Size 6.3.4 Optimum Distillation Design6.4 Economic Comparison; 6.5 Plantwide Control; 6.5.1 Control Structure; 6.5.2 Column Control Structure Selection; 6.5.3 Dynamic Performance Results; 6.6 Conclusion; References; 7 DESIGN AND CONTROL OF AN AUTO-REFRIGERATED ALKYLATION PROCESS; 7.1 Introduction; 7.2 Process Description; 7.2.1 Reaction Kinetics; 7.2.2 Phase Equilibrium; 7.2.3 Flowsheet; 7.2.4 Design Optimization Variables; 7.3 Design of Distillation Columns; 7.3.1 Depropanizer; 7.3.2 Deisobutanizer; 7.4 Economic Optimization of Entire Process; 7.4.1 Flowsheet Convergence; 7.4.2 Yield 7.4.3 Effect of Reactor Size |
| Record Nr. | UNINA-9910877225503321 |
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Luyben William L
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| Hoboken, N.J., : John Wiley, c2011 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
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