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Advanced ESR methods in polymer research [[electronic resource] /] / edited by Shulamith Schlick
Advanced ESR methods in polymer research [[electronic resource] /] / edited by Shulamith Schlick
Pubbl/distr/stampa Hoboken, N.J., : Wiley-Interscience, c2006
Descrizione fisica 1 online resource (369 p.)
Disciplina 547.7046
547.840724
547/.7046
Altri autori (Persone) SchlickShulamith
Soggetto topico Electron paramagnetic resonance - Research
Polymers - Research
Soggetto genere / forma Electronic books.
ISBN 1-280-64907-0
9786610649075
0-470-05350-X
0-470-05349-6
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Continuous-wave and pulsed ESR methods / Gunnar Jeschke, Shulamith Schlick -- Double resonance ESR methods / Gunnar Jeschke -- Calculating slow-motion ESR spectra of spin-labeled polymers / Keith A. Earle, David E. Budil -- ESR imaging / Shulamith Schlick -- ESR study of radicals in conventional radical polymerization using radical precursors prepared by atom transfer radical polymerization / Atsushi Kajiwara, Krzysztof Matyjaszewski -- Local dynamics of polymers in solution by spin-label ESR / Jan Pilar -- Site-specific information on macromolecular materials by combining CW and pulsed ESR on spin probes / Gunnar Jeschke -- ESR methods for assessing the stability of polymer membranes used in fuel cells / Emil Roduner, Shulamith Schlick -- Spatially resolved degradation in heterophasic polymers from 1D and 2D spectral-spatial ESR imaging experiments / Shulamith Schlick, Krzysztof Kruczala -- ESR studies of photooxidation and stabilization of polymer coatings / David R. Bauer, John L. Gerlock -- Characterization of dendrimer structures by ESR techniques / M. Francesca Ottaviani, Nicholas J. Turro -- High-field ESR spectroscopy of conductive polymers / Victor I. Krinichnyi.
Record Nr. UNINA-9910143402103321
Hoboken, N.J., : Wiley-Interscience, c2006
Materiale a stampa
Lo trovi qui: Univ. Federico II
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Advanced ESR methods in polymer research [[electronic resource] /] / edited by Shulamith Schlick
Advanced ESR methods in polymer research [[electronic resource] /] / edited by Shulamith Schlick
Pubbl/distr/stampa Hoboken, N.J., : Wiley-Interscience, c2006
Descrizione fisica 1 online resource (369 p.)
Disciplina 547.7046
547.840724
547/.7046
Altri autori (Persone) SchlickShulamith
Soggetto topico Electron paramagnetic resonance - Research
Polymers - Research
ISBN 1-280-64907-0
9786610649075
0-470-05350-X
0-470-05349-6
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Continuous-wave and pulsed ESR methods / Gunnar Jeschke, Shulamith Schlick -- Double resonance ESR methods / Gunnar Jeschke -- Calculating slow-motion ESR spectra of spin-labeled polymers / Keith A. Earle, David E. Budil -- ESR imaging / Shulamith Schlick -- ESR study of radicals in conventional radical polymerization using radical precursors prepared by atom transfer radical polymerization / Atsushi Kajiwara, Krzysztof Matyjaszewski -- Local dynamics of polymers in solution by spin-label ESR / Jan Pilar -- Site-specific information on macromolecular materials by combining CW and pulsed ESR on spin probes / Gunnar Jeschke -- ESR methods for assessing the stability of polymer membranes used in fuel cells / Emil Roduner, Shulamith Schlick -- Spatially resolved degradation in heterophasic polymers from 1D and 2D spectral-spatial ESR imaging experiments / Shulamith Schlick, Krzysztof Kruczala -- ESR studies of photooxidation and stabilization of polymer coatings / David R. Bauer, John L. Gerlock -- Characterization of dendrimer structures by ESR techniques / M. Francesca Ottaviani, Nicholas J. Turro -- High-field ESR spectroscopy of conductive polymers / Victor I. Krinichnyi.
Record Nr. UNINA-9910830223803321
Hoboken, N.J., : Wiley-Interscience, c2006
Materiale a stampa
Lo trovi qui: Univ. Federico II
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Advances in Sustainable Polymeric Materials / / edited by Cristina Cazan
Advances in Sustainable Polymeric Materials / / edited by Cristina Cazan
Pubbl/distr/stampa [Place of publication not identified] : , : MDPI - Multidisciplinary Digital Publishing Institute, , 2023
Descrizione fisica 1 online resource (540 pages)
Disciplina 547.7046
Soggetto topico Polymers - Analysis
Sustainable development
ISBN 3-0365-7370-4
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Record Nr. UNINA-9910719767903321
[Place of publication not identified] : , : MDPI - Multidisciplinary Digital Publishing Institute, , 2023
Materiale a stampa
Lo trovi qui: Univ. Federico II
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Comprehensive desk reference of polymer characterization and analysis / Robert F.Brady
Comprehensive desk reference of polymer characterization and analysis / Robert F.Brady
Autore BRADY, Robert F.
Pubbl/distr/stampa Oxford [etc.] : American chemical society, 2003
Descrizione fisica XIII, 754 p. ; 29 cm
Disciplina 547.7046
Soggetto topico Polimeri - Analisi
ISBN 0-8412-3665-8
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Record Nr. UNISA-990001978200203316
BRADY, Robert F.  
Oxford [etc.] : American chemical society, 2003
Materiale a stampa
Lo trovi qui: Univ. di Salerno
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Fluorescence Studies of Polymer Containing Systems / / edited by Karel Procházka
Fluorescence Studies of Polymer Containing Systems / / edited by Karel Procházka
Edizione [1st ed. 2016.]
Pubbl/distr/stampa Cham : , : Springer International Publishing : , : Imprint : Springer, , 2016
Descrizione fisica 1 online resource (306 p.)
Disciplina 547.7046
Collana Springer Series on Fluorescence, Methods and Applications
Soggetto topico Spectrum analysis
Polymers
Chemistry, Physical and theoretical
Spectroscopy/Spectrometry
Polymer Sciences
Physical Chemistry
ISBN 3-319-26788-4
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Conformational and dynamic behavior of polymers in solutions -- Self-assembly of amphiphilic copolymers in selective solvents -- Electrostatically driven assembly of polyelectrolytes -- Theoretical principles of fluorescence spectroscopy -- Historical perspective of advances in fluorescence research on polymer systems -- Fluorescence studies of self- and co-assembling polymer systems -- Pyrene-labeled water-soluble macromolecules as fluorescent mimics of associative -- Fluorescence correlation spectroscopy studies of polymer systems. .
Record Nr. UNINA-9910254053503321
Cham : , : Springer International Publishing : , : Imprint : Springer, , 2016
Materiale a stampa
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Fundamentals of Phase Separation in Polymer Blend Thin Films / / by Sam Coveney
Fundamentals of Phase Separation in Polymer Blend Thin Films / / by Sam Coveney
Autore Coveney Sam
Edizione [1st ed. 2015.]
Pubbl/distr/stampa Cham : , : Springer International Publishing : , : Imprint : Springer, , 2015
Descrizione fisica 1 online resource (179 p.)
Disciplina 547.7046
Collana Springer Theses, Recognizing Outstanding Ph.D. Research
Soggetto topico Phase transformations (Statistical physics)
Thermodynamics
Materials—Surfaces
Thin films
Polymers
Surfaces (Physics)
Interfaces (Physical sciences)
Phase Transitions and Multiphase Systems
Surfaces and Interfaces, Thin Films
Polymer Sciences
Surface and Interface Science, Thin Films
ISBN 3-319-19399-6
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Development of Theory for Bulk Polymer-Blend Systems.-  Development of Theory for Polymer-Blend Thin Films -- Hamiltonian Phase Portraits for Polymer-Blend Thin Films -- Lateral Phase Separation via Surface Bifurcation -- Coupled Surface Roughening and Phase Separation.
Record Nr. UNINA-9910300419903321
Coveney Sam  
Cham : , : Springer International Publishing : , : Imprint : Springer, , 2015
Materiale a stampa
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Handbook of fourier transform Raman and infrared spectra of polymers / A.H. Kuptsov, G.N. Zhizhin
Handbook of fourier transform Raman and infrared spectra of polymers / A.H. Kuptsov, G.N. Zhizhin
Autore KUPTSOV, A.H
Pubbl/distr/stampa Amsterdam : Elseviar, c1998
Descrizione fisica XXXIV; 536 p : ill. ; 35 cm + floppy-disk
Disciplina 547.7046
Altri autori (Persone) ZHIZHIN, G.N.
Collana Physical sciences data
Soggetto non controllato Polimeri
Trasformazioni di fourier
Spettroscopia dell'infrarosso
ISBN 0-444-82620-3
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Record Nr. UNISA-990000325670203316
KUPTSOV, A.H  
Amsterdam : Elseviar, c1998
Materiale a stampa
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Mass spectrometry in polymer chemistry / / edited by Christopher Barner-Kowollik ... [et al.]
Mass spectrometry in polymer chemistry / / edited by Christopher Barner-Kowollik ... [et al.]
Edizione [1st ed.]
Pubbl/distr/stampa Weinheim, : Wiley-VCH, c2012
Descrizione fisica 1 online resource (483 p.)
Disciplina 547.7046
610.28
Altri autori (Persone) Barner-KowollikChristopher
Soggetto topico Mass spectrometry
Polymers - Spectra
Polymers
ISBN 1-283-37953-8
9786613379535
3-527-64182-3
3-527-64184-X
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Mass Spectrometry in Polymer Chemistry -- Contents -- List of Contributors -- Introduction -- 1 Mass Analysis -- 1.1 Introduction -- 1.2 Measures of Performance -- 1.2.1 Mass Resolving Power -- 1.2.2 Mass Accuracy -- 1.2.3 Mass Range -- 1.2.4 Linear Dynamic Range -- 1.2.5 Abundance Sensitivity -- 1.3 Instrumentation -- 1.3.1 Sector Mass Analyzers -- 1.3.2 Quadrupole Mass Filters -- 1.3.3 3D Ion Traps -- 1.3.4 Linear Ion Traps -- 1.3.5 Time-of-Flight Mass Analyzers -- 1.3.6 Fourier Transform Ion Cyclotron Resonance Mass Analyzers -- 1.3.7 Orbitraps -- 1.4 Instrumentation in Tandem and Multiple-Stage Mass Spectrometry -- 1.5 Conclusions and Outlook -- References -- 2 Ionization Techniques for Polymer Mass Spectrometry -- 2.1 Introduction -- 2.2 Small Molecule Ionization Era -- 2.2.1 Electron Ionization (EI) -- 2.2.2 Chemical Ionization (CI) -- 2.2.3 Pyrolysis Mass Spectrometry (Py-MS) -- 2.3 Macromass Era of Ionization -- 2.3.1 Field Desorption (FD) and Field Ionization (FI) -- 2.3.2 Secondary Ion Mass Spectrometry (SIMS) -- 2.3.3 Fast Atom Bombardment (FAB) and Liquid Secondary Ion Mass Spectrometry (LSIMS) -- 2.3.4 Laser Desorption (LD) -- 2.3.5 Plasma Desorption (PD) -- 2.3.6 Other Ionization Methods -- 2.4 Modern Era of Ionization Techniques -- 2.4.1 Electrospray Ionization (ESI) -- 2.4.2 New Trends -- 2.4.3 Atmospheric Pressure Chemical Ionization (APCI) -- 2.4.4 New Trends -- 2.4.5 Matrix-Assisted Laser Desorption/Ionization (MALDI) -- 2.4.6 New Trends -- 2.5 Conclusions -- References -- 3 Tandem Mass Spectrometry Analysis of Polymer Structures and Architectures -- 3.1 Introduction -- 3.2 Activation Methods -- 3.2.1 Collisionally Activated Dissociation (CAD) -- 3.2.2 Surface-Induced Dissociation (SID) -- 3.2.3 Photodissociation Methods -- 3.2.4 Electron Capture Dissociation and Electron Transfer Dissociation (ECD/ETD).
3.2.5 Post-Source Decay (PSD) -- 3.3 Instrumentation -- 3.3.1 Quadrupole Ion Trap (QIT) Mass Spectrometers -- 3.3.2 Quadrupole/time-of-flight (Q/ToF) Mass Spectrometers -- 3.3.3 ToF/ToF Instruments -- 3.4 Structural Information from MS2 Studies -- 3.4.1 End-Group Analysis and Isomer/Isobar Differentiation -- 3.4.2 Polymer Architectures -- 3.4.3 Copolymer Sequences -- 3.4.4 Assessment of Intrinsic Stabilities and Binding Energies -- 3.5 Summary and Outlook -- References -- 4 Matrix-Assisted Inlet Ionization and Solvent-Free Gas-Phase Separation Using Ion Mobility Spectrometry for Imaging and Electron Transfer Dissociation Mass Spectrometry of Polymers -- 4.1 Overview -- 4.2 Introduction -- 4.3 New Sample Introduction Technologies -- 4.3.1 Laserspray Ionization - Ion Mobility Spectrometry-Mass Spectrometry -- 4.3.2 Matrix Assisted Inlet Ionization (MAII) -- 4.3.3 LSIV in Reflection Geometry at Intermediate Pressure (IP) -- 4.4 Fragmentation by ETD and CID -- 4.5 Surface Analyses by Imaging MS -- 4.5.1 Ultraf Fast LSII-MS Imaging in Transmission Geometry (TG) -- 4.5.2 LSIV-IMS-MS Imaging in Reflection Geometry (RG) -- 4.6 Future Outlook -- References -- 5 Polymer MALDI Sample Preparation -- 5.1 Introduction -- 5.2 Roles of the Matrix -- 5.2.1 Intimate Contact -- 5.2.2 Absorption of Laser Light -- 5.2.3 Efficient Desorption -- 5.2.4 Effective Ionization -- 5.3 Choice of Matrix -- 5.4 Choice of the Solvent -- 5.5 Basic Solvent-Based Sample Preparation Recipe -- 5.6 Deposition Methods -- 5.7 Solvent-Free Sample Preparation -- 5.8 The Vortex Method -- 5.9 Matrix-to-Analyte Ratio -- 5.10 Salt-to-Analyte Ratio -- 5.11 Chromatography as Sample Preparation -- 5.12 Problems in MALDI Sample Preparation -- 5.13 Predicting MALDI Sample Preparation -- 5.14 Conclusions -- References -- 6 Surface Analysis and Imaging Techniques -- 6.1 Imaging Mass Spectrometry.
6.2 Secondary Ion Mass Spectrometry -- 6.2.1 Static SIMS of Polymers -- 6.2.1.1 The Fingerprint Region -- 6.2.1.2 High-Mass Region -- 6.2.2 Imaging in Polymer Blends and Multicomponent Systems -- 6.2.3 Data Analysis Methods -- 6.2.4 Polymer Depth Profiling with Cluster Ion Beams -- 6.2.4.1 A Brief Discussion on the Physics and Chemistry of Sputtering and its Role in Optimized Beam Conditions -- 6.2.5 3-D Analysis in Polymer Systems -- 6.3 Matrix-Assisted Laser Desorption Ionization (MALDI) -- 6.3.1 History of MALDI Imaging Mass Spectrometry -- 6.3.2 Sample Preparation in MALDI Imaging -- 6.3.3 MALDI Imaging of Polymers -- 6.3.4 Outlook -- 6.4 Other Surface Mass Spectrometry Methods -- 6.4.1 Desorption Electrospray Ionization -- 6.4.2 Plasma Desorption Ionization Methods -- 6.4.3 Electrospray Droplet Impact for SIMS -- 6.5 Outlook -- References -- 7 Hyphenated Techniques -- 7.1 Introduction -- 7.2 Polymer Separation Techniques -- 7.3 Principles of Coupling: Transfer Devices -- 7.3.1 Online Coupling Devices -- 7.3.2 Off-Line Coupling Devices -- 7.4 Examples -- 7.4.1 Coupling of SEC with MALDI-/ESI-MS -- 7.4.2 Coupling of LAC/LC-CC with MALDI-/ESI-MS -- 7.5 Conclusions -- References -- 8 Automated Data Processing and Quantification in Polymer Mass Spectrometry -- 8.1 Introduction -- 8.2 File and Data Formats -- 8.3 Optimization of Ionization Conditions -- 8.4 Automated Spectral Analysis and Data Reduction in MS -- 8.4.1 Long-Standing Approaches -- 8.4.2 Some New Concepts -- 8.4.3 Mass Autocorrelation -- 8.4.4 Time-Series Segmentation -- 8.5 Copolymer Analysis -- 8.6 Data Interpretation in MS/MS -- 8.7 Quantitative MS and the Determination of MMDs by MS -- 8.7.1 Quantitative MMD Measurement by MALDI-MS -- 8.7.1.1 Example for Mixtures of Monodisperse Components -- 8.7.1.2 Example for Mixtures of Polydisperse Components.
8.7.1.3 Calculating the Correction Factor for Each Oligomer -- 8.7.1.4 Step by Step Procedure for Quantitation -- 8.7.1.5 Determination of the Absolute MMD -- 8.7.2 Quantitative MMD Measurement by SEC/ESI-MS -- 8.7.2.1 Exact Measurement of the MMD of Homopolymers -- 8.7.2.2 MMD of the Individual Components in Mixtures of Functional Homopolymers -- 8.7.3 Comparison of the Two Methods for MMD Calculation -- 8.7.4 Simple Methods for the Determination of the Molar Abundance of Functional Polymers in Mixtures -- 8.8 Conclusions and Outlook -- References -- 9 Comprehensive Copolymer Characterization -- 9.1 Introduction -- 9.2 Scope -- 9.3 Reviews -- 9.4 Soft Ionization Techniques -- 9.4.1 MALDI -- 9.4.2 ESI -- 9.4.3 APCI -- 9.5 Separation Prior MS -- 9.5.1 LC-MS -- 9.5.2 Ion Mobility Spectrometry-Mass Spectrometry (IMS-MS) -- 9.6 Tandem MS (MS/MS) -- 9.7 Quantitative MS -- 9.8 Copolymers for Biological or (Bio)medical Application -- 9.9 Software Development -- 9.10 Summary and Outlook -- References -- 10 Elucidation of Reaction Mechanisms: Conventional Radical Polymerization -- 10.1 Introduction -- 10.2 Basic Principles and General Considerations -- 10.3 Initiation -- 10.3.1 Radical Generation -- 10.3.1.1 Thermally Induced Initiator Decomposition -- 10.3.1.2 Photoinduced Initiator Decomposition -- 10.3.1.3 Other Means -- 10.3.2 Initiator Efficiency -- 10.4 Propagation -- 10.4.1 Propagation Rate Coefficients -- 10.4.2 Chain-Length Dependence of Propagation -- 10.4.3 Copolymerization -- 10.5 Termination -- 10.6 Chain Transfer -- 10.6.1 Transfer to Small Molecules -- 10.6.2 Acrylate Systems -- 10.7 Emulsion Polymerization -- 10.8 Conclusion -- References -- 11 Elucidation of Reaction Mechanisms and Polymer Structure: Living/Controlled Radical Polymerization -- 11.1 Protocols Based on a Persistent Radical Effect (NMP, ATRP, and Related).
11.2 Protocols Based on Degenerative Chain Transfer (RAFT, MADIX) -- 11.3 Protocols based on CCT -- 11.4 Novel Protocols and Minor Protocols -- 11.5 Conclusions -- References -- 12 Elucidation of Reaction Mechanisms: Other Polymerization Mechanisms -- 12.1 Introduction -- 12.2 Ring-Opening Polymerization Mechanisms of Cyclic Ethers -- 12.3 Ring-Opening Polymerization Mechanisms of Cyclic Esters and Carbonates -- 12.4 Ring-Opening Metathesis Polymerization -- 12.5 Mechanisms of Step-Growth Polymerization -- 12.6 Concluding Remarks -- References -- 13 Polymer Degradation -- 13.1 Introduction -- 13.2 Thermal and Thermo-Oxidative Degradation -- 13.3 Photolysis and Photooxidation -- 13.4 Biodegradation -- 13.5 Other Degradation Processes -- 13.6 Conclusions -- References -- 14 Outlook -- Index.
Record Nr. UNINA-9910828020503321
Weinheim, : Wiley-VCH, c2012
Materiale a stampa
Lo trovi qui: Univ. Federico II
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Mass spectrometry in polymer chemistry / / edited by Christopher Barner-Kowollik ... [et al.] [[electronic resource]]
Mass spectrometry in polymer chemistry / / edited by Christopher Barner-Kowollik ... [et al.] [[electronic resource]]
Pubbl/distr/stampa Weinheim, : Wiley-VCH, 2011
Descrizione fisica 1 online resource (483 p.)
Disciplina 547.7046
610.28
Altri autori (Persone) Barner-KowollikChristopher
Soggetto topico Biomedical engineering
Polymers -- Spectra
Polymers - Spectra
Polymers
Mass spectrometry
Chemistry
Physical Sciences & Mathematics
Analytical Chemistry
ISBN 1-283-37953-8
9786613379535
3-527-64182-3
3-527-64184-X
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Record Nr. UNINA-9910141155703321
Weinheim, : Wiley-VCH, 2011
Materiale a stampa
Lo trovi qui: Univ. Federico II
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Modern polymer spectroscopy / edited by Giuseppe Zerbi
Modern polymer spectroscopy / edited by Giuseppe Zerbi
Pubbl/distr/stampa Weinheim [etc.] : Wiley-VCH, copyr.1999
Descrizione fisica XIV, 289 p. ; 25 cm
Disciplina 547.7046
Soggetto non controllato Polimeri spettroscopia
ISBN 3-527-29655-7
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Record Nr. UNISA-990000084530203316
Weinheim [etc.] : Wiley-VCH, copyr.1999
Materiale a stampa
Lo trovi qui: Univ. di Salerno
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