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Basic gas chromatography / / Harold M. McNair, James M. Miller, Nicholas H. Snow
| Basic gas chromatography / / Harold M. McNair, James M. Miller, Nicholas H. Snow |
| Autore | McNair Harold Monroe <1933-> |
| Edizione | [Third edition.] |
| Pubbl/distr/stampa | Hoboken, New Jersey : , : Wiley, , [2019] |
| Descrizione fisica | 1 online resource (286 pages) |
| Disciplina | 543.85 |
| Collana | THEi Wiley ebooks |
| Soggetto topico | Gas chromatography |
| ISBN |
1-119-45078-0
1-5231-2792-9 1-119-45079-9 1-119-45073-X |
| Formato | Materiale a stampa  |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto | Introduction -- Basic concepts and terms -- Instrument overview -- Capillary columns -- Stationary phases -- Temperature programming -- Inlets -- Classical detectors: FID, TCD, ECD -- Qualitative and quantitative analysis -- GC-MS and spectrometric detectors -- Sampling methods -- Multidimensional gas chromatography -- Packed column gc -- Special topics -- Troubleshooting gc systems. |
| Record Nr. | UNINA-9910555275403321 |
McNair Harold Monroe <1933->
|
||
| Hoboken, New Jersey : , : Wiley, , [2019] | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Basic gas chromatography / / Harold M. McNair, James M. Miller, Nicholas H. Snow
| Basic gas chromatography / / Harold M. McNair, James M. Miller, Nicholas H. Snow |
| Autore | McNair Harold Monroe <1933-> |
| Edizione | [Third edition.] |
| Pubbl/distr/stampa | Hoboken, New Jersey : , : Wiley, , [2019] |
| Descrizione fisica | 1 online resource (286 pages) |
| Disciplina | 543.85 |
| Collana | THEi Wiley ebooks |
| Soggetto topico | Gas chromatography |
| ISBN |
1-119-45078-0
1-5231-2792-9 1-119-45079-9 1-119-45073-X |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto | Introduction -- Basic concepts and terms -- Instrument overview -- Capillary columns -- Stationary phases -- Temperature programming -- Inlets -- Classical detectors: FID, TCD, ECD -- Qualitative and quantitative analysis -- GC-MS and spectrometric detectors -- Sampling methods -- Multidimensional gas chromatography -- Packed column gc -- Special topics -- Troubleshooting gc systems. |
| Record Nr. | UNINA-9910826143503321 |
|
McNair Harold Monroe <1933->
|
||
| Hoboken, New Jersey : , : Wiley, , [2019] | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Basic gas chromatography [[electronic resource] /] / Harold M. McNair, James M. Miller
| Basic gas chromatography [[electronic resource] /] / Harold M. McNair, James M. Miller |
| Autore | McNair Harold Monroe <1933-> |
| Edizione | [2nd ed.] |
| Pubbl/distr/stampa | Hoboken, NJ, : John Wiley & Sons, 2009 |
| Descrizione fisica | 1 online resource (255 p.) |
| Disciplina |
543.85
543/.85 544.926 |
| Altri autori (Persone) | MillerJames M. <1933-> |
| Soggetto topico |
Gas chromatography
Chromatographic analysis |
| ISBN |
1-118-21120-0
9786612188343 1-282-18834-8 0-470-48009-2 0-470-48010-6 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
BASIC GAS CHROMATOGRAPHY; CONTENTS; PREFACE TO THE SECOND EDITION; PREFACE; ACKNOWLEDGMENTS; 1 INTRODUCTION; 2 INSTRUMENT OVERVIEW; 3 BASIC CONCEPTS AND TERMS; 4 STATIONARY PHASES; 5 PACKED COLUMNS AND INLETS; 6 CAPILLARY COLUMNS AND INLETS; 7 DETECTORS; 8 QUALITATIVE AND QUANTITATIVE ANALYSIS; 9 PROGRAMMED TEMPERATURE; 10 GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS); 11 MULTIDIMENSIONAL GAS CHROMATOGRAPHY; 12 SAMPLING METHODS; 13 SPECIAL TOPICS; 14 TROUBLESHOOTING GC SYSTEMS; APPENDIX I SYMBOLS AND ACRONYMS; APPENDIX II GUIDELINES FOR SELECTING CAPILLARY COLUMNS
APPENDIX III GC: HOW TO AVOID PROBLEMSAPPENDIX IV CALCULATION OF SPLIT RATIO FOR SPLIT INJECTION ON OT COLUMNS; APPENDIX V OPERATING CONDITIONS FOR CAPILLARY COLUMNS; APPENDIX VI OV LIQUID PHASES PHYSICAL PROPERTY DATA; APPENDIX VII SOME COMPRESSIBILITY CORRECTION FACTORS (J); APPENDIX VIII SOME INTERNET WEBSITES FOR GAS CHROMATOGRAPHERS; APPENDIX IX OTHER BOOKS ON GAS CHROMATOGRAPHY; INDEX OF APPLICATIONS; INDEX |
| Record Nr. | UNINA-9910777931603321 |
|
McNair Harold Monroe <1933->
|
||
| Hoboken, NJ, : John Wiley & Sons, 2009 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Basic gas chromatography / / Harold M. McNair, James M. Miller
| Basic gas chromatography / / Harold M. McNair, James M. Miller |
| Autore | McNair Harold Monroe <1933-> |
| Edizione | [2nd ed.] |
| Pubbl/distr/stampa | Hoboken, NJ, : John Wiley & Sons, 2009 |
| Descrizione fisica | 1 online resource (255 p.) |
| Disciplina |
543.85
543/.85 544.926 |
| Altri autori (Persone) | MillerJames M. <1933-> |
| Soggetto topico |
Gas chromatography
Chromatographic analysis |
| ISBN |
1-118-21120-0
9786612188343 1-282-18834-8 0-470-48009-2 0-470-48010-6 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
BASIC GAS CHROMATOGRAPHY; CONTENTS; PREFACE TO THE SECOND EDITION; PREFACE; ACKNOWLEDGMENTS; 1 INTRODUCTION; 2 INSTRUMENT OVERVIEW; 3 BASIC CONCEPTS AND TERMS; 4 STATIONARY PHASES; 5 PACKED COLUMNS AND INLETS; 6 CAPILLARY COLUMNS AND INLETS; 7 DETECTORS; 8 QUALITATIVE AND QUANTITATIVE ANALYSIS; 9 PROGRAMMED TEMPERATURE; 10 GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS); 11 MULTIDIMENSIONAL GAS CHROMATOGRAPHY; 12 SAMPLING METHODS; 13 SPECIAL TOPICS; 14 TROUBLESHOOTING GC SYSTEMS; APPENDIX I SYMBOLS AND ACRONYMS; APPENDIX II GUIDELINES FOR SELECTING CAPILLARY COLUMNS
APPENDIX III GC: HOW TO AVOID PROBLEMSAPPENDIX IV CALCULATION OF SPLIT RATIO FOR SPLIT INJECTION ON OT COLUMNS; APPENDIX V OPERATING CONDITIONS FOR CAPILLARY COLUMNS; APPENDIX VI OV LIQUID PHASES PHYSICAL PROPERTY DATA; APPENDIX VII SOME COMPRESSIBILITY CORRECTION FACTORS (J); APPENDIX VIII SOME INTERNET WEBSITES FOR GAS CHROMATOGRAPHERS; APPENDIX IX OTHER BOOKS ON GAS CHROMATOGRAPHY; INDEX OF APPLICATIONS; INDEX |
| Record Nr. | UNINA-9910819422503321 |
|
McNair Harold Monroe <1933->
|
||
| Hoboken, NJ, : John Wiley & Sons, 2009 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Columns for gas chromatography [[electronic resource] ] : performance and selection / / Eugene F. Barry, Robert L. Grob
| Columns for gas chromatography [[electronic resource] ] : performance and selection / / Eugene F. Barry, Robert L. Grob |
| Autore | Barry Eugene F |
| Pubbl/distr/stampa | Hoboken, N.J., : Wiley-Interscience, c2007 |
| Descrizione fisica | 1 online resource (314 p.) |
| Disciplina |
543.85
543/.85 |
| Altri autori (Persone) | GrobRobert Lee |
| Soggetto topico |
Gas chromatography
Chromatographic analysis |
| ISBN |
1-280-82679-7
9786610826797 0-470-11418-5 0-470-11417-7 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
COLUMNS FOR GAS CHROMATOGRAPHY; CONTENTS; Preface; Acknowledgments; 1 Introduction; 1.1 Evolution of Gas Chromatographic Columns; 1.2 Central Role Played by the Column; 1.3 Justification for Column Selection and Care; 1.4 Literature on Gas Chromatographic Columns; 1.5 Gas Chromatographic Resources on the Internet; References; 2 Packed Column Gas Chromatography; 2.1 Introduction; 2.2 Solid Supports and Adsorbents; Supports for Gas-Liquid Chromatography; Adsorbents for Gas-Solid Chromatography; 2.3 Stationary Phases; Requirements of a Stationary Phase; USP Designation of Stationary Phases
Kovats Retention IndexMcReynolds and Rohrschneider Classifications of Stationary Phases; Evaluation of Column Operation; Optimization of Packed Column Separations; 2.4 Column Preparation; Coating Methods; Tubing Materials and Dimensions; Glass Wool Plugs and Column Fittings; Filling the Column; Conditioning the Column and Column Care; 2.5 United States Pharmacopeia and National Formulary Chromatographic Methods; References; 3 Capillary Column Gas Chromatography; 3.1 Introduction; Significance and Impact of Capillary Gas Chromatography Chronology of Achievements in Capillary Gas ChromatographyComparison of Packed and Capillary Columns; 3.2 Capillary Column Technology; Capillary Column Materials; Fused Silica and Other Glasses; Extrusion of a Fused-Silica Capillary Column; Aluminum-Clad Fused-Silica Capillary Columns; Fused-Silica-Lined Stainless Steel Capillary Columns; 3.3 Preparation of Fused-Silica Capillary Columns; Silanol Deactivation Procedures; Static Coating of Capillary Columns; Capillary Cages; Test Mixtures for Monitoring Column Performance; Diagnostic Role Played by Components of Test Mixtures 3.4 Chromatographic Performance of Capillary ColumnsGolay Equation Versus the van Deemter Expression; Choice of Carrier Gas; Measurement of Linear Velocity and Flow Rate; Effect of Carrier Gas Viscosity on Linear Velocity; Phase Ratio; Coating Efficiency; 3.5 Stationary-Phase Selection for Capillary Gas Chromatography; Requirements; History; Comparison of Columns from Manufacturers; Polysiloxane Phases; Polyethylene Glycol Phases; Cross-Linked Versus Chemically Bonded Phase; Chemical Bonding; MS-Grade Phases Versus Polysilarylene or Polysilphenylene Phases; Sol-Gel Stationary Phases Phenylpolycarborane-Siloxane Phases3.6 Specialty Columns; EPA Methods; Chiral Stationary Phases; Gas-Solid Adsorption Capillary Columns: PLOT Columns; 3.7 Capillary Column Selection; Practical Considerations of Column Diameter, Film Thickness, and Column Length; Capillary Columns of 0.53 mm i.d.: Megabore Columns; Correlation of Column Dimensions and Film Thickness with Parameters in the Fundamental Resolution Equation; Column Selection for Gas Chromatography by Specifications; 3.8 Column Installation and Care; Carrier Gas Purifiers; Ferrule Materials and Fittings; Column Installation Column Conditioning |
| Record Nr. | UNINA-9910143414203321 |
|
Barry Eugene F
|
||
| Hoboken, N.J., : Wiley-Interscience, c2007 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Columns for gas chromatography [[electronic resource] ] : performance and selection / / Eugene F. Barry, Robert L. Grob
| Columns for gas chromatography [[electronic resource] ] : performance and selection / / Eugene F. Barry, Robert L. Grob |
| Autore | Barry Eugene F |
| Pubbl/distr/stampa | Hoboken, N.J., : Wiley-Interscience, c2007 |
| Descrizione fisica | 1 online resource (314 p.) |
| Disciplina |
543.85
543/.85 |
| Altri autori (Persone) | GrobRobert Lee |
| Soggetto topico |
Gas chromatography
Chromatographic analysis |
| ISBN |
1-280-82679-7
9786610826797 0-470-11418-5 0-470-11417-7 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
COLUMNS FOR GAS CHROMATOGRAPHY; CONTENTS; Preface; Acknowledgments; 1 Introduction; 1.1 Evolution of Gas Chromatographic Columns; 1.2 Central Role Played by the Column; 1.3 Justification for Column Selection and Care; 1.4 Literature on Gas Chromatographic Columns; 1.5 Gas Chromatographic Resources on the Internet; References; 2 Packed Column Gas Chromatography; 2.1 Introduction; 2.2 Solid Supports and Adsorbents; Supports for Gas-Liquid Chromatography; Adsorbents for Gas-Solid Chromatography; 2.3 Stationary Phases; Requirements of a Stationary Phase; USP Designation of Stationary Phases
Kovats Retention IndexMcReynolds and Rohrschneider Classifications of Stationary Phases; Evaluation of Column Operation; Optimization of Packed Column Separations; 2.4 Column Preparation; Coating Methods; Tubing Materials and Dimensions; Glass Wool Plugs and Column Fittings; Filling the Column; Conditioning the Column and Column Care; 2.5 United States Pharmacopeia and National Formulary Chromatographic Methods; References; 3 Capillary Column Gas Chromatography; 3.1 Introduction; Significance and Impact of Capillary Gas Chromatography Chronology of Achievements in Capillary Gas ChromatographyComparison of Packed and Capillary Columns; 3.2 Capillary Column Technology; Capillary Column Materials; Fused Silica and Other Glasses; Extrusion of a Fused-Silica Capillary Column; Aluminum-Clad Fused-Silica Capillary Columns; Fused-Silica-Lined Stainless Steel Capillary Columns; 3.3 Preparation of Fused-Silica Capillary Columns; Silanol Deactivation Procedures; Static Coating of Capillary Columns; Capillary Cages; Test Mixtures for Monitoring Column Performance; Diagnostic Role Played by Components of Test Mixtures 3.4 Chromatographic Performance of Capillary ColumnsGolay Equation Versus the van Deemter Expression; Choice of Carrier Gas; Measurement of Linear Velocity and Flow Rate; Effect of Carrier Gas Viscosity on Linear Velocity; Phase Ratio; Coating Efficiency; 3.5 Stationary-Phase Selection for Capillary Gas Chromatography; Requirements; History; Comparison of Columns from Manufacturers; Polysiloxane Phases; Polyethylene Glycol Phases; Cross-Linked Versus Chemically Bonded Phase; Chemical Bonding; MS-Grade Phases Versus Polysilarylene or Polysilphenylene Phases; Sol-Gel Stationary Phases Phenylpolycarborane-Siloxane Phases3.6 Specialty Columns; EPA Methods; Chiral Stationary Phases; Gas-Solid Adsorption Capillary Columns: PLOT Columns; 3.7 Capillary Column Selection; Practical Considerations of Column Diameter, Film Thickness, and Column Length; Capillary Columns of 0.53 mm i.d.: Megabore Columns; Correlation of Column Dimensions and Film Thickness with Parameters in the Fundamental Resolution Equation; Column Selection for Gas Chromatography by Specifications; 3.8 Column Installation and Care; Carrier Gas Purifiers; Ferrule Materials and Fittings; Column Installation Column Conditioning |
| Record Nr. | UNINA-9910830531803321 |
|
Barry Eugene F
|
||
| Hoboken, N.J., : Wiley-Interscience, c2007 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
The electron capture detector and the study of reactions with thermal electrons [[electronic resource] /] / E.C.M. Chen, E.S.D. Chen
| The electron capture detector and the study of reactions with thermal electrons [[electronic resource] /] / E.C.M. Chen, E.S.D. Chen |
| Autore | Chen E. C. M (Edward C. M.) |
| Pubbl/distr/stampa | Hoboken, N.J., : Wiley-Interscience, c2004 |
| Descrizione fisica | 1 online resource (417 p.) |
| Disciplina |
541.36
543.26 543.85 |
| Altri autori (Persone) | ChenE. S. D |
| Soggetto topico |
Gas chromatography
Electrons - Capture |
| Soggetto genere / forma | Electronic books. |
| ISBN |
1-280-54201-2
9786610542017 0-471-65988-6 0-471-65989-4 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
THE ELECTRON CAPTURE DETECTOR AND THE STUDY OF REACTIONS WITH THERMAL ELECTRONS; CONTENTS; FOREWORD; PREFACE; 1. Scope and History of the Electron; 1.1 General Objectives and Organization; 1.2 General Scope; 1.3 History of the Electron; References; 2. Definitions, Nomenclature, Reactions, and Equations; 2.1 Introduction; 2.2 Definition of Kinetic and Energetic Terms; 2.3 Additional Gas Phase Ionic Reactions; 2.4 Electron Affinities from Solution Data; 2.5 Semi-Empirical Calculations of Energetic Quantities; 2.6 Herschbach Ionic Morse Potential Energy Curves; 2.7 Summary; References
3. Thermal Electron Reactions at the University of Houston3.1 General Introduction; 3.2 The First Half-Century, 1900 to 1950; 3.3 Fundamental Discovery, 1950 to 1960; 3.4 General Accomplishments, 1960 to 1970; 3.4.1 Introduction; 3.4.2 The Wentworth Group; 3.4.3 Stable Negative-Ion Formation; 3.4.4 Dissociative Thermal Electron Attachment; 3.4.5 Nonlinear Least Squares; 3.5 Milestones in the Wentworth Laboratory and Complementary Methods, 1970 to 1980; 3.6 Negative-Ion Mass Spectrometry and Morse Potential Energy Curves, 1980 to 1990; 3.7 Experimental and Theoretical Milestones, 1990 to 2000 3.8 Summary of Contributions at the University of HoustonReferences; 4. Theoretical Basis of the Experimental Tools; 4.1 Introduction; 4.2 The Kinetic Model of the ECD and NIMS; 4.3 Nondissociative Electron Capture; 4.4 Dissociative Electron Attachment; 4.5 Electron Affinities and Half-Wave Reduction Potentials; 4.6 Electron Affinities and Ionization Potentials of Aromatic Hydrocarbons; 4.7 Electron Affinities and Charge Transfer Complex Energies; 4.8 Summary; References; 5. Experimental Procedures and Data Reduction; 5.1 Introduction; 5.2 Experimental ECD and NICI Procedures 5.3 Reduction of ECD Data to Fundamental Properties5.3.1 Introduction; 5.3.2 Acetophenone and Benzaldehyde; 5.3.3 Benzanthracene, Benz[a]pyrene, and 1-Naphthaldehyde; 5.3.4 Carbon Disulfide; 5.3.5 Nitromethane; 5.3.6 Consolidation of Electron Affinities for Molecular Oxygen; 5.4 Reduction of Negative-Ion Mass Spectral Data; 5.5 Precision and Accuracy; 5.6 Evaluation of Experimental Results; 5.7 Summary; References; 6. Complementary Experimental and Theoretical Procedures; 6.1 Introduction; 6.2 Equilibrium Methods for Determining Electron Affinities; 6.3 Photon Techniques 6.4 Thermal Charge Transfer Methods6.5 Electron and Particle Beam Techniques; 6.6 Condensed Phase Measurements of Electron Affinities; 6.7 Complementary Theoretical Calculations; 6.7.1 Atomic Electron Affinities; 6.7.2 Polyatomic Molecules; 6.8 Rate Constants for Attachment, Detachment, and Recombination; 6.9 Summary; References; 7. Consolidating Experimental, Theoretical, and Empirical Data; 7.1 Introduction; 7.2 Semi-Empirical Quantum Mechanical Calculations; 7.3 Morse Potential Energy Curves; 7.3.1 Classification of Negative-Ion Morse Potentials; 7.3.2 The Negative-Ion States of H(2) 7.3.3 The Negative-Ion States of I(2) |
| Record Nr. | UNINA-9910146070703321 |
|
Chen E. C. M (Edward C. M.)
|
||
| Hoboken, N.J., : Wiley-Interscience, c2004 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
The electron capture detector and the study of reactions with thermal electrons [[electronic resource] /] / E.C.M. Chen, E.S.D. Chen
| The electron capture detector and the study of reactions with thermal electrons [[electronic resource] /] / E.C.M. Chen, E.S.D. Chen |
| Autore | Chen E. C. M (Edward C. M.) |
| Pubbl/distr/stampa | Hoboken, N.J., : Wiley-Interscience, c2004 |
| Descrizione fisica | 1 online resource (417 p.) |
| Disciplina |
541.36
543.26 543.85 |
| Altri autori (Persone) | ChenE. S. D |
| Soggetto topico |
Gas chromatography
Electrons - Capture |
| ISBN |
1-280-54201-2
9786610542017 0-471-65988-6 0-471-65989-4 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
THE ELECTRON CAPTURE DETECTOR AND THE STUDY OF REACTIONS WITH THERMAL ELECTRONS; CONTENTS; FOREWORD; PREFACE; 1. Scope and History of the Electron; 1.1 General Objectives and Organization; 1.2 General Scope; 1.3 History of the Electron; References; 2. Definitions, Nomenclature, Reactions, and Equations; 2.1 Introduction; 2.2 Definition of Kinetic and Energetic Terms; 2.3 Additional Gas Phase Ionic Reactions; 2.4 Electron Affinities from Solution Data; 2.5 Semi-Empirical Calculations of Energetic Quantities; 2.6 Herschbach Ionic Morse Potential Energy Curves; 2.7 Summary; References
3. Thermal Electron Reactions at the University of Houston3.1 General Introduction; 3.2 The First Half-Century, 1900 to 1950; 3.3 Fundamental Discovery, 1950 to 1960; 3.4 General Accomplishments, 1960 to 1970; 3.4.1 Introduction; 3.4.2 The Wentworth Group; 3.4.3 Stable Negative-Ion Formation; 3.4.4 Dissociative Thermal Electron Attachment; 3.4.5 Nonlinear Least Squares; 3.5 Milestones in the Wentworth Laboratory and Complementary Methods, 1970 to 1980; 3.6 Negative-Ion Mass Spectrometry and Morse Potential Energy Curves, 1980 to 1990; 3.7 Experimental and Theoretical Milestones, 1990 to 2000 3.8 Summary of Contributions at the University of HoustonReferences; 4. Theoretical Basis of the Experimental Tools; 4.1 Introduction; 4.2 The Kinetic Model of the ECD and NIMS; 4.3 Nondissociative Electron Capture; 4.4 Dissociative Electron Attachment; 4.5 Electron Affinities and Half-Wave Reduction Potentials; 4.6 Electron Affinities and Ionization Potentials of Aromatic Hydrocarbons; 4.7 Electron Affinities and Charge Transfer Complex Energies; 4.8 Summary; References; 5. Experimental Procedures and Data Reduction; 5.1 Introduction; 5.2 Experimental ECD and NICI Procedures 5.3 Reduction of ECD Data to Fundamental Properties5.3.1 Introduction; 5.3.2 Acetophenone and Benzaldehyde; 5.3.3 Benzanthracene, Benz[a]pyrene, and 1-Naphthaldehyde; 5.3.4 Carbon Disulfide; 5.3.5 Nitromethane; 5.3.6 Consolidation of Electron Affinities for Molecular Oxygen; 5.4 Reduction of Negative-Ion Mass Spectral Data; 5.5 Precision and Accuracy; 5.6 Evaluation of Experimental Results; 5.7 Summary; References; 6. Complementary Experimental and Theoretical Procedures; 6.1 Introduction; 6.2 Equilibrium Methods for Determining Electron Affinities; 6.3 Photon Techniques 6.4 Thermal Charge Transfer Methods6.5 Electron and Particle Beam Techniques; 6.6 Condensed Phase Measurements of Electron Affinities; 6.7 Complementary Theoretical Calculations; 6.7.1 Atomic Electron Affinities; 6.7.2 Polyatomic Molecules; 6.8 Rate Constants for Attachment, Detachment, and Recombination; 6.9 Summary; References; 7. Consolidating Experimental, Theoretical, and Empirical Data; 7.1 Introduction; 7.2 Semi-Empirical Quantum Mechanical Calculations; 7.3 Morse Potential Energy Curves; 7.3.1 Classification of Negative-Ion Morse Potentials; 7.3.2 The Negative-Ion States of H(2) 7.3.3 The Negative-Ion States of I(2) |
| Record Nr. | UNINA-9910830435303321 |
|
Chen E. C. M (Edward C. M.)
|
||
| Hoboken, N.J., : Wiley-Interscience, c2004 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Gas chromatography / / Colin F. Poole
| Gas chromatography / / Colin F. Poole |
| Autore | Poole Colin F |
| Edizione | [1st ed.] |
| Pubbl/distr/stampa | Amsterdam ; ; Boston, : Elsevier, 2012 |
| Descrizione fisica | 1 online resource (753 p.) |
| Disciplina |
543/.85
543.85 |
| Soggetto topico |
Gas chromatography
Chromatographic analysis |
| ISBN |
1-280-77001-5
9786613680785 0-12-385541-1 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Front Cover; Gas Chromatography; Copyright; Contents; Contributors; Chapter 1 - Milestones in the Development of Gas Chromatography; 1.1.INTRODUCTION; 1.2.THE INVENTION OF GAS CHROMATOGRAPHY; 1.3.EARLY INSTRUMENTATION; 1.4.EARLY COLUMN DEVELOPMENTS; 1.5.INTERFACING GLASS CAPILLARY COLUMNS TO INJECTORS AND DETECTORS; 1.6.THE HINDELANG CONFERENCES AND THE FUSED-SILICA COLUMN; 1.7.INCREASING SOPHISTICATION OF INSTRUMENTATION; 1.8.DECLINE IN THE EXPERTISE OF THE AVERAGE GAS CHROMATOGRAPHER; References; Chapter 2 - Theory of Gas Chromatography; 2.1.INTRODUCTION
2.2.NOMENCLATURE AND OTHER CONVENTIONS 2.3.GENERAL DEFINITIONS; 2.4.SOLUTE-COLUMN INTERACTION; 2.5.PROPERTIES OF AN IDEAL GAS; 2.6.FLOW OF IDEAL GAS IN OPEN CIRCULAR TUBES; 2.7.MIGRATION AND ELUTION PARAMETERS OF THE SOLUTES; 2.8.PEAK SPACING AND REVERSAL OF PEAK ORDER; 2.9.PEAK WIDTH; 2.10.OPTIMIZATION; References; Chapter 3 - Column Technology: Open Tubular Columns; 3.1.INTRODUCTION; 3.2.OVERVIEW OF THE FUSED SILICA DRAWING PROCESS; 3.3.THE PREFORM - RAW MATERIAL; 3.4.SURFACE CHEMISTRY; 3.5.DRAWING OF THE CAPILLARY FROM THE PREFORM; 3.6.PROTECTIVE COATING; 3.7.ALTERNATIVE PROTECTIVE COATINGS 3.8. CLEAN ROOM ENVIRONMENT 3.9.QUALITY MONITORING; 3.10.OBSERVATIONS ON HANDLING OF FUSED-SILICA CAPILLARY TUBING; 3.11.COLUMN TECHNOLOGY - COATING THE STATIONARY PHASE; 3.12.STATIONARY PHASES; 3.13.COATING TECHNIQUES; 3.14.COLUMN TECHNOLOGY - QUALITY EVALUATION; 3.15.COLUMN TECHNOLOGY - SUMMARY; References; Chapter 4- Packed Columns for Gas-Liquid and Gas-Solid Chromatography; 4.1.INTRODUCTION; 4.2.GAS-LIQUID CHROMATOGRAPHY; 4.3.GAS-SOLID CHROMATOGRAPHY; References; Chapter 5 - Gas-Solid Chromatography (PLOT Columns); 5.1.ALUMINA ADSORBENTS; 5.2.MOLECULAR SIEVES; 5.3.POROUS POLYMERS 5.4.CARBON ADSORBENTS 5.5.OTHER ADSORBENTS; References; Chapter 6- Classification and Selection of Open-Tubular Columns for Analytical Separations; 6.1.INTRODUCTION; 6.2.STATIONARY-PHASE CLASSIFICATION; 6.3.POROUS-LAYER OPEN-TUBULAR COLUMNS; 6.4.TEMPERATURE-PROGRAMMED SEPARATIONS; 6.5.STATIONARY-PHASE SELECTIVITY TUNING; References; Chapter 7 - Multidimensional and Comprehensive Gas Chromatography; 7.1.INTRODUCTION; 7.2.A GRAPHICAL REPRESENTATION OF 2D GC SEPARATIONS; 7.3 .BACK FLUSHING 2D GC; 7.4.HEART CUTTING 2D GC; 7.5.COMPREHENSIVE 2D GC; 7.6.CONCLUSIONS; References Chapter 8 - Sample Introduction Methods 8.1.INTRODUCTION; 8.2.CHOOSING A SAMPLE INTRODUCTION SYSTEM; 8.3.SUPPORTING DEVICES; 8.4.THE COLD ON-COLUMN INJECTOR; 8.5.THE FLASH VAPORIZATION INJECTOR; 8.6.THE SPLIT/SPLITLESS INJECTOR; 8.7.THE PROGRAMMABLE TEMPERATURE VAPORIZING (PTV) INJECTOR; 8.8.THE GAS SAMPLING VALVE; 8.9.THE LIQUID SAMPLING VALVE; References; Chapter 9 - Head space-Gas Chromatography; 9.1.INTRODUCTION AND HISTORY; 9.2.FUNDAMENTALS OF HEAD SPACE EXTRACTION; 9.3.INSTRUMENTATION AND PRACTICE; 9.4.METHOD DEVELOPMENT CONSIDERATIONS; 9.5.CONCLUSIONS; References Chapter 10- Thermal Desorption for Gas Chromatography |
| Record Nr. | UNINA-9910824584603321 |
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Poole Colin F
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| Amsterdam ; ; Boston, : Elsevier, 2012 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
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Gas chromatography and mass spectrometry : a practical guide / / O. David Sparkman, Zelda E. Penton, Fulton G. Kitson
| Gas chromatography and mass spectrometry : a practical guide / / O. David Sparkman, Zelda E. Penton, Fulton G. Kitson |
| Autore | Sparkman O. David (Orrin David), <1942-> |
| Edizione | [2nd ed.] |
| Pubbl/distr/stampa | Boston, : Elsevier, 2011 |
| Descrizione fisica | 1 online resource (633 p.) |
| Disciplina |
543/.85
543.85 |
| Altri autori (Persone) |
PentonZelda
KitsonFulton G |
| Soggetto topico |
Gas chromatography
Mass spectrometry |
| ISBN |
1-283-17107-4
9786613171078 0-08-092015-2 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto | The fundamentals of GC/MS -- Introduction and history -- Gas chromatography -- The gc/ms interface -- Mass spectrometry instrumentation -- Mass spectral data interpretation -- Quantitation with GC/MS -- GC conditions, derivatization, and mass spectral interpretation -- Of specific compound types -- Acids -- Alcohols -- Aldehydes -- Amides -- Amines -- Amino acid -- Common contaminants -- Drugs and their metabolites -- Esters -- Ethers -- Fluorinated compounds -- Gases -- Glycols -- Halogenated compounds (other than fluorinated) -- Hydrocarbons -- Isocyanates -- Ketones -- Nitriles -- Nitroaromatics -- Nitrogen-containing heterocyclics -- Nucleosides (TMS derivatives) -- Pesticides -- Phenols -- Phosphorus compounds -- Plasticizers and other polymer additives (including phthalates) -- Prostaglandins (MO-TMS derivatives) -- Solvents and their impurities -- Steroids -- Sugars (monosaccharides) -- Sulfur compounds -- Appendices -- A definitions of terms related to gas chromatography -- B definitions of terms related to mass spectrometry -- C atomic masses and isotope abundances -- X+1 and x+2 values for ions containing atoms of C and H based on -- Isotope contributions -- E isotope peak patterns for ions containing atoms of Cl and/or Br -- F steps to follow in the determination of an elemental composition -- Based on isotope peak intensity ratios -- G derivatization in GC/MS -- H points of comparison of LC/MS vs GC/MS -- I list of available EI mass spectral databases -- J information required for reporting a GC/MS analysis -- K third-party software for use with GC/MS -- GC installation and maintenance -- Troubleshooting common GC problems -- N maintenance, operating tips, and troubleshooting for mass spectrometers -- O mixtures for determining mass spectral resolution -- P cross-index chart for GC stationary phases -- Q ions for determining unknown structures. |
| Record Nr. | UNINA-9910827470903321 |
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Sparkman O. David (Orrin David), <1942->
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| Boston, : Elsevier, 2011 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
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