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Advanced NMR Techniques for Biomarkers Identification : Development and application of advanced NMR based strategies for biomarkers investigations / Debora Paris
| Advanced NMR Techniques for Biomarkers Identification : Development and application of advanced NMR based strategies for biomarkers investigations / Debora Paris |
| Autore | Paris, Debora |
| Pubbl/distr/stampa | LAP Lambert Academic Publishing, c2010 |
| Descrizione fisica | VII, 110 p. ; 20 cm |
| Disciplina | 543.66 |
| Soggetto non controllato |
Risonanza magnetica nucleare
Spettroscopia |
| ISBN | 978-3-8433-8635-7 |
| Formato | Materiale a stampa  |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Record Nr. | UNINA-9910171559403321 |
Paris, Debora
|
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| LAP Lambert Academic Publishing, c2010 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Applications in food sciences / / edited by Atta-ur-Rahman, M. Iqbal Choudhary
| Applications in food sciences / / edited by Atta-ur-Rahman, M. Iqbal Choudhary |
| Pubbl/distr/stampa | Sharjah, United Arab Emirates : , : Bentham Science Publishers, , [2016] |
| Descrizione fisica | 1 online resource (304 pages) |
| Disciplina | 543.66 |
| Collana | Applications of NMR Spectroscopy |
| Soggetto topico |
Magnetic Resonance Spectroscopy
Nuclear magnetic resonance spectroscopy |
| ISBN | 1-68108-143-1 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Intro -- CONTENTS -- PREFACE -- List of Contributors -- Application of NMR to Resolve Food Structure, Composition and Quality -- FOOD DIMENSIONS -- Composition -- Nutrients -- Bio-availability -- Food Matrix -- Texture -- Structure -- The Macrostructure Level: -- The Microstructure Level: -- Stability and Processing -- Water Diffusion -- Thermal Conductivity -- NMR AS A MULTIPURPOSE TECHNIQUE FOR FOOD ASSAY -- Spectroscopy -- 1. Food Authentication -- 2. Food Origin -- 3. Food Traceability -- Relaxometry -- Magnetic Resonance Imaging -- Hybrid Methods -- Chemical Shift Imaging -- Relaxometry Mapping -- Spectral-Relaxation Deconvolution -- DATA ANALYSIS, INFORMATION EXTRACTION AND KNOWLEDGE GENERATION -- Analytic Approach -- Holistic View -- PROSPECTS -- CONCLUDING REMARKS -- CONFLICT OF INTEREST -- ACKNOWLEDGEMENTS -- REFERENCES -- NMR Spectroscopy for Evaluation of Lipid Oxidation -- INTRODUCTION -- Challenges in Assessing Lipid Oxidation -- 1H NMR Spectroscopy for Assessment of Lipid Oxidation -- Assessment of Lipid Oxidation by Monitoring 1H NMR Signal Intensities -- 1H NMR Spectroscopy for Identification of Oxidation Products -- 13C NMR spectroscopy for Assessment of Lipid Oxidation -- 31P NMR -- CONCLUSION -- CONFLICT OF INTEREST -- ACKNOWLEDGEMENTS -- REFERENCES -- The Application of NMR Spectroscopy to the Study of Pyranoanthocyanins: Structural Elucidation, Solution Equilibria and Exhibited Color in Foods and Beverages -- 1. PYRANOANTHOCYANINS: AN INTERESTING CLASS OF PIGMENTS DERIVED FROM ANTHOCYANINS -- 1.1. Introduction -- 1.2. Chemical Structure of Anthocyanins -- 1.3. Influence of Aqueous Solution Equilibria on Anthocyanin Chemical Structure -- 1.4. Reactivity of Anthocyanins. Formation of Anthocyanin-Derived Pigments -- 1.4.1. Thermal Degradation -- 1.4.2. Oxidation -- 1.4.3. Copigmentation.
1.4.4. Formation of Anthocyanin-Derived Pigments -- 2. PYRANOANTHOCYANINS: STRUCTURES, PROPERTIES AND DISTRIBUTION AMONG FOODSTUFFS -- 2.1. Structures of Pyranoanthocyanins -- 2.1.1. Vitisin-Type Pyranoanthocyanins -- 2.1.2. Hydroxyphenyl-Pyranoanthocyanins -- 2.1.3. Flavanyl-Pyranoanthocyanins -- 2.1.4. Portisins -- 2.2. Properties of Pyranoanthocyanins -- 2.2.1. Color Features -- 2.2.2. Reactivity -- 2.3. Occurrence of Pyranoanthocyanins in Foodstuffs -- 2.3.1. Red Wine, Port Wine, Grape Pomace and Lees -- 2.3.2. Fruit and Vegetable Juices/Wines -- 2.3.3. Fruits and Vegetables -- 3. NUCLEAR MAGNETIC RESONANCE (NMR) SPECTROSCOPY APPLIED TO THE STRUCTURE ELUCIDATION OF ANTHOCYANINS, PYRANOANTHOCYANINS AND OTHER DERIVATIVES -- 3.1. Fundamentals of NMR Spectroscopy Applied to the Analysis of Anthocyanins and Pyranoanthocyanins -- 3.2. Application of NMR Spectroscopy in the Structural Identification of New Anthocyanins Derivatives in the Flavylium Form, and their Different Equilibrium Forms -- 3.2.1. Analysis of the Flavylium Cation Form -- 3.2.2. Analysis of the Different Forms in Equilibrium -- 3.3. Application of NMR Spectroscopy in the Structural Identification of New Pyranoanthocyanin Derivatives -- 3.3.1. Structural Identification of New Pigments of Pyranoanthocyanins, Chemical Behavior and Structural Identification of Equilibrium Forms -- 3.3.2. Structural Identification of New Pigments of Pyranoanthocyanins Linked to a Flavanyl Moiety or Hydroxyphenyl (Portisins) -- 3.3.3. Structural Identification of Pyranoanthocyanins Dimers and Other Rare Pyranoanthocyanins -- CONCLUDING REMARKS -- CONFLICT OF INTEREST -- ACKNOWLEDGEMENTS -- REFERENCES -- NMR Spectroscopy: A Powerful Tool to Investigate the Role of Tannins in the Taste of Wine and their Health Protective Effect -- INTRODUCTION -- INTERACTIONS BETWEEN TANNINS AND SALIVA PROTEINS. Mechanism of Binding -- Stoichiometry and Strength of Binding -- INTERACTIONS BETWEEN TANNINS AND BUCCAL MEMBRANE LIPIDS -- PROTECTIVE EFFECT OF TANNINS ON MEMBRANE OXIDATION -- CONCLUSION -- CONFLICT OF INTEREST -- ACKNOWLEDGEMENTS -- ABBREVIATIONS -- REFERENCES -- Applications of Quantitative 1H NMR in Food-Related Analysis -- INTRODUCTION -- QUANTITATIVE NMR (QNMR) -- Principles of qNMR -- Characteristics of qNMR -- qNMR Methods: Internal and External Standards Methods -- APPLICATIONS OF QNMR -- Purity Determination of Reference substances for Pesticide and Natural Toxins -- Determining Purity of a Pesticide Reference substance with qNMR [24] -- Purity Determination of Reference Substances for Natural Toxins [27] -- Application of qNMR to Natural Organic Compounds -- Quantification of Carminic Acid -- Quantification of Rutin, Isoquercitrin, and Quercetin -- Quantification of Steviol Glycosides -- Quantification of Carthamin -- Determination of Food Additives in Processed Foods by qNMR -- qNMR of Sorbic Acid, Dehydroacetic Acid, and Acesulfame Potassium -- Pre-treatment and Recovery Test -- Comparison of Methods using Commercially Available Food Products -- CONCLUSION -- CONFLICT OF INTEREST -- ACKNOWLEDGEMENTS -- ABBREVIATIONS -- REFERENCES -- Cell-Free Protein Synthesis for NMR Structural Analysis of Large Proteins and Complexes -- INTRODUCTION -- CELL-FREE EXPRESSION SYSTEMS AND TOOLS TO OPTIMISE PRODUCTION OF TARGET PROTEINS -- CELL-FREE SELECTIVE LABELING APPROACHES TO AID NMR ANALYSIS -- CELL-FREE COMBINATORIAL LABELING APPROACHES TO AID NMR ANALYSIS -- SEGMENTAL LABELLING STRATEGIES TO REDUCE SPECTRAL COMPLEXITY -- CELL-FREE DEUTERATION TO REDUCE LINE BROADENING -- CELL-FREE STEREO-ARRAY ISOTOPE LABELING (SAIL) TO ACQUIRE DISTANCE CONSTRAINTS -- CELL-FREE INCORPORATION OF UNNATURAL AMINO ACIDS TO PROVIDE LONG DISTANCE CONSTRAINTS. CONCLUSION -- CONFLICT OF INTEREST -- ACKNOWLEDGEMENTS -- REFERENCES -- SUBJECT INDEX. |
| Record Nr. | UNINA-9910798121503321 |
| Sharjah, United Arab Emirates : , : Bentham Science Publishers, , [2016] | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Applications in food sciences / / edited by Atta-ur-Rahman, M. Iqbal Choudhary
| Applications in food sciences / / edited by Atta-ur-Rahman, M. Iqbal Choudhary |
| Pubbl/distr/stampa | Sharjah, United Arab Emirates : , : Bentham Science Publishers, , [2016] |
| Descrizione fisica | 1 online resource (304 pages) |
| Disciplina | 543.66 |
| Collana | Applications of NMR Spectroscopy |
| Soggetto topico |
Magnetic Resonance Spectroscopy
Nuclear magnetic resonance spectroscopy |
| ISBN | 1-68108-143-1 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Intro -- CONTENTS -- PREFACE -- List of Contributors -- Application of NMR to Resolve Food Structure, Composition and Quality -- FOOD DIMENSIONS -- Composition -- Nutrients -- Bio-availability -- Food Matrix -- Texture -- Structure -- The Macrostructure Level: -- The Microstructure Level: -- Stability and Processing -- Water Diffusion -- Thermal Conductivity -- NMR AS A MULTIPURPOSE TECHNIQUE FOR FOOD ASSAY -- Spectroscopy -- 1. Food Authentication -- 2. Food Origin -- 3. Food Traceability -- Relaxometry -- Magnetic Resonance Imaging -- Hybrid Methods -- Chemical Shift Imaging -- Relaxometry Mapping -- Spectral-Relaxation Deconvolution -- DATA ANALYSIS, INFORMATION EXTRACTION AND KNOWLEDGE GENERATION -- Analytic Approach -- Holistic View -- PROSPECTS -- CONCLUDING REMARKS -- CONFLICT OF INTEREST -- ACKNOWLEDGEMENTS -- REFERENCES -- NMR Spectroscopy for Evaluation of Lipid Oxidation -- INTRODUCTION -- Challenges in Assessing Lipid Oxidation -- 1H NMR Spectroscopy for Assessment of Lipid Oxidation -- Assessment of Lipid Oxidation by Monitoring 1H NMR Signal Intensities -- 1H NMR Spectroscopy for Identification of Oxidation Products -- 13C NMR spectroscopy for Assessment of Lipid Oxidation -- 31P NMR -- CONCLUSION -- CONFLICT OF INTEREST -- ACKNOWLEDGEMENTS -- REFERENCES -- The Application of NMR Spectroscopy to the Study of Pyranoanthocyanins: Structural Elucidation, Solution Equilibria and Exhibited Color in Foods and Beverages -- 1. PYRANOANTHOCYANINS: AN INTERESTING CLASS OF PIGMENTS DERIVED FROM ANTHOCYANINS -- 1.1. Introduction -- 1.2. Chemical Structure of Anthocyanins -- 1.3. Influence of Aqueous Solution Equilibria on Anthocyanin Chemical Structure -- 1.4. Reactivity of Anthocyanins. Formation of Anthocyanin-Derived Pigments -- 1.4.1. Thermal Degradation -- 1.4.2. Oxidation -- 1.4.3. Copigmentation.
1.4.4. Formation of Anthocyanin-Derived Pigments -- 2. PYRANOANTHOCYANINS: STRUCTURES, PROPERTIES AND DISTRIBUTION AMONG FOODSTUFFS -- 2.1. Structures of Pyranoanthocyanins -- 2.1.1. Vitisin-Type Pyranoanthocyanins -- 2.1.2. Hydroxyphenyl-Pyranoanthocyanins -- 2.1.3. Flavanyl-Pyranoanthocyanins -- 2.1.4. Portisins -- 2.2. Properties of Pyranoanthocyanins -- 2.2.1. Color Features -- 2.2.2. Reactivity -- 2.3. Occurrence of Pyranoanthocyanins in Foodstuffs -- 2.3.1. Red Wine, Port Wine, Grape Pomace and Lees -- 2.3.2. Fruit and Vegetable Juices/Wines -- 2.3.3. Fruits and Vegetables -- 3. NUCLEAR MAGNETIC RESONANCE (NMR) SPECTROSCOPY APPLIED TO THE STRUCTURE ELUCIDATION OF ANTHOCYANINS, PYRANOANTHOCYANINS AND OTHER DERIVATIVES -- 3.1. Fundamentals of NMR Spectroscopy Applied to the Analysis of Anthocyanins and Pyranoanthocyanins -- 3.2. Application of NMR Spectroscopy in the Structural Identification of New Anthocyanins Derivatives in the Flavylium Form, and their Different Equilibrium Forms -- 3.2.1. Analysis of the Flavylium Cation Form -- 3.2.2. Analysis of the Different Forms in Equilibrium -- 3.3. Application of NMR Spectroscopy in the Structural Identification of New Pyranoanthocyanin Derivatives -- 3.3.1. Structural Identification of New Pigments of Pyranoanthocyanins, Chemical Behavior and Structural Identification of Equilibrium Forms -- 3.3.2. Structural Identification of New Pigments of Pyranoanthocyanins Linked to a Flavanyl Moiety or Hydroxyphenyl (Portisins) -- 3.3.3. Structural Identification of Pyranoanthocyanins Dimers and Other Rare Pyranoanthocyanins -- CONCLUDING REMARKS -- CONFLICT OF INTEREST -- ACKNOWLEDGEMENTS -- REFERENCES -- NMR Spectroscopy: A Powerful Tool to Investigate the Role of Tannins in the Taste of Wine and their Health Protective Effect -- INTRODUCTION -- INTERACTIONS BETWEEN TANNINS AND SALIVA PROTEINS. Mechanism of Binding -- Stoichiometry and Strength of Binding -- INTERACTIONS BETWEEN TANNINS AND BUCCAL MEMBRANE LIPIDS -- PROTECTIVE EFFECT OF TANNINS ON MEMBRANE OXIDATION -- CONCLUSION -- CONFLICT OF INTEREST -- ACKNOWLEDGEMENTS -- ABBREVIATIONS -- REFERENCES -- Applications of Quantitative 1H NMR in Food-Related Analysis -- INTRODUCTION -- QUANTITATIVE NMR (QNMR) -- Principles of qNMR -- Characteristics of qNMR -- qNMR Methods: Internal and External Standards Methods -- APPLICATIONS OF QNMR -- Purity Determination of Reference substances for Pesticide and Natural Toxins -- Determining Purity of a Pesticide Reference substance with qNMR [24] -- Purity Determination of Reference Substances for Natural Toxins [27] -- Application of qNMR to Natural Organic Compounds -- Quantification of Carminic Acid -- Quantification of Rutin, Isoquercitrin, and Quercetin -- Quantification of Steviol Glycosides -- Quantification of Carthamin -- Determination of Food Additives in Processed Foods by qNMR -- qNMR of Sorbic Acid, Dehydroacetic Acid, and Acesulfame Potassium -- Pre-treatment and Recovery Test -- Comparison of Methods using Commercially Available Food Products -- CONCLUSION -- CONFLICT OF INTEREST -- ACKNOWLEDGEMENTS -- ABBREVIATIONS -- REFERENCES -- Cell-Free Protein Synthesis for NMR Structural Analysis of Large Proteins and Complexes -- INTRODUCTION -- CELL-FREE EXPRESSION SYSTEMS AND TOOLS TO OPTIMISE PRODUCTION OF TARGET PROTEINS -- CELL-FREE SELECTIVE LABELING APPROACHES TO AID NMR ANALYSIS -- CELL-FREE COMBINATORIAL LABELING APPROACHES TO AID NMR ANALYSIS -- SEGMENTAL LABELLING STRATEGIES TO REDUCE SPECTRAL COMPLEXITY -- CELL-FREE DEUTERATION TO REDUCE LINE BROADENING -- CELL-FREE STEREO-ARRAY ISOTOPE LABELING (SAIL) TO ACQUIRE DISTANCE CONSTRAINTS -- CELL-FREE INCORPORATION OF UNNATURAL AMINO ACIDS TO PROVIDE LONG DISTANCE CONSTRAINTS. CONCLUSION -- CONFLICT OF INTEREST -- ACKNOWLEDGEMENTS -- REFERENCES -- SUBJECT INDEX. |
| Record Nr. | UNINA-9910819078703321 |
| Sharjah, United Arab Emirates : , : Bentham Science Publishers, , [2016] | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Applications of NMR spectroscopy : vol. 3 / edited by Atta-ur-Rahman, M. Iqbal Choudhary
| Applications of NMR spectroscopy : vol. 3 / edited by Atta-ur-Rahman, M. Iqbal Choudhary |
| Pubbl/distr/stampa | Amsterdam [et al.] : Elsevier : Bentham, @2015 |
| Descrizione fisica | xii, 267 p. ; 24 cm |
| Disciplina | 543.66 |
| Soggetto non controllato | Spettroscopia a risonanza magnetica nucleare |
| ISBN | 978-1-68108-063-5 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Record Nr. | UNINA-990010063240403321 |
| Amsterdam [et al.] : Elsevier : Bentham, @2015 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Basic 1H- and 13C-NMR spectroscopy [[electronic resource] /] / Metin Balcıi
| Basic 1H- and 13C-NMR spectroscopy [[electronic resource] /] / Metin Balcıi |
| Autore | Balcıi Metin |
| Edizione | [1st ed.] |
| Pubbl/distr/stampa | Amsterdam ; ; Boston, : Elsevier, 2005 |
| Descrizione fisica | 1 online resource (441 p.) |
| Disciplina | 543.66 |
| Soggetto topico |
Nuclear magnetic resonance spectroscopy
Spectrum analysis |
| Soggetto genere / forma | Electronic books. |
| ISBN |
1-281-02542-9
9786611025427 0-08-052553-9 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Front Cover; Basic 1H- and 13C-NMR Spectroscopy; Copyright Page; Preface; Contents; Part I: 1H-NMR Spectroscopy; Chapter 1. Introduction; 1.1 Structure Elucidation and NMR; 1.2 Development of NMR Spectroscopy; Chapter 2. Resonance Phenomena; 2.1 Magnetic Properties of Atomic Nuclei; 2.2 Spin Quantum Numbers of Elements; 2.3 Behavior of an Atomic Nucleus in a Magnetic Field; 2.4 Relaxation; 2.5 NMR Instrumentation; Chapter 3. Chemical shift; 3.1 Local Magnetic Fields Around a Nucleus; 3.2 The Unit of the Chemical Shift; 3.3 Sample Preparation; 3.4 Factors Influencing the Chemical Shift
3.5 Exercises 1-30 Chapter 4. Spin-Spin Splitting in 1H-NMR Spectra; 4.1 Explanation of Spin-Spin Splitting; 4.2 Spin-Spin Coupling Mechanism; 4.3 Factors Influencing Spin-Spin Coupling Constants; Chapter 5. Spin-Spin Splitting to Different Protons; 5.1 General Rules; 5.2 Examples of Coupling with Different Protons; 5.3 Exercises 31-60; Chapter 6. Spin Systems: Analysis of the 1H-NMR Spectra; 6.1 Second-order Spectra; 6.2 Two-spin Systems; Chapter 7. NMR Shift Reagents and Double Resonance Experiments: Simplification of the NMR Spectra; 7.1 Shift Reagents; 7.2 Double Resonance Experiments Chapter 8. Dynamic NMR Spectroscopy 8.1 Basic Theories; 8.2 Exercises 61-101; Part II: 13C-NMR Spectroscopy; Chapter 9. Introduction; 9.1 Development of 13C-NMR Spectroscopy; 9.2 Comparison of the 'H and 13C Nucleus; 9.3 The Factors Influencing The Sensitivity Of The 13c Nucleus; 9.4 The Factors Increasing the Sensitivity In 13C-NMR Spectroscopy; Chapter 10. Absorption and Resonance; 10.1 Classical Treatment of Absorption and Resonance; 10.2 Relaxation Processes; Chapter 11. Pulse NMR Spectroscopy; 11.1 Introduction to the Pulse NMR Spectroscopy; 11.2 CW and FT Spectroscopy 11.3 Interaction of a Monochromatic Radio frequency With the Sample 11.4 Fourier Transformation; 11.5 Routine Pulsed 13C-NMR Measurement Techniques; 11.6 Broadband Decoupling; 11.7 Nuclear Overhauser Effect; 11.8 Measurements of NOE Enhanced Coupled 13C-NMR Spectra: Gated Decoupling; 11.9 Off Resonance 1H Decoupled and Selective Decoupled Experiments; 11.10 Inverse Gated Decoupling; 11.11 Sample Preparation and Solvents; Chapter 12. Chemical Shift; 12.1 Diamagnetic and Paramagnetic Shielding on Proton and Carbon Atoms; 12.2 Factors which Influence the Chemical Shifts Chapter 13. 13C Chemical Shifts of Organic Compounds 13.1 Alkanes; 13.2 Substituted Alkanes; 13.3 Cycloalkanes; 13.4 Alkenes; 13.5 Aromatic Compounds; 13.6 Carbonyl Compounds; 13.7 Heterocyclic Compounds; Chapter 14. Spin-Spin Coupling; 14.1 Couplings Over One Bond (1JCH); 14.2 Couplings Over Two Bonds (2JcH) (Geminal Coupling); 14.3 Couplings Over Three Bonds (3JcH) (Vicinal Coupling); 14.4 Carbon-Deuterium Coupling (1JcD); Chapter 15. Multiple-Pulse NMR Experiments; 15.1 Measurements of Relaxation Times; 15.2 J-Modulated Spin-echo Experiments 15.3 Signal Enhancement by Population Transfer: Selective Population Transfer and Selective Population Inversion |
| Record Nr. | UNINA-9910457297003321 |
|
Balcıi Metin
|
||
| Amsterdam ; ; Boston, : Elsevier, 2005 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Basic 1H- and 13C-NMR spectroscopy [[electronic resource] /] / Metin Balcıi
| Basic 1H- and 13C-NMR spectroscopy [[electronic resource] /] / Metin Balcıi |
| Autore | Balcıi Metin |
| Edizione | [1st ed.] |
| Pubbl/distr/stampa | Amsterdam ; ; Boston, : Elsevier, 2005 |
| Descrizione fisica | 1 online resource (441 p.) |
| Disciplina | 543.66 |
| Soggetto topico |
Nuclear magnetic resonance spectroscopy
Spectrum analysis |
| ISBN |
1-281-02542-9
9786611025427 0-08-052553-9 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Front Cover; Basic 1H- and 13C-NMR Spectroscopy; Copyright Page; Preface; Contents; Part I: 1H-NMR Spectroscopy; Chapter 1. Introduction; 1.1 Structure Elucidation and NMR; 1.2 Development of NMR Spectroscopy; Chapter 2. Resonance Phenomena; 2.1 Magnetic Properties of Atomic Nuclei; 2.2 Spin Quantum Numbers of Elements; 2.3 Behavior of an Atomic Nucleus in a Magnetic Field; 2.4 Relaxation; 2.5 NMR Instrumentation; Chapter 3. Chemical shift; 3.1 Local Magnetic Fields Around a Nucleus; 3.2 The Unit of the Chemical Shift; 3.3 Sample Preparation; 3.4 Factors Influencing the Chemical Shift
3.5 Exercises 1-30 Chapter 4. Spin-Spin Splitting in 1H-NMR Spectra; 4.1 Explanation of Spin-Spin Splitting; 4.2 Spin-Spin Coupling Mechanism; 4.3 Factors Influencing Spin-Spin Coupling Constants; Chapter 5. Spin-Spin Splitting to Different Protons; 5.1 General Rules; 5.2 Examples of Coupling with Different Protons; 5.3 Exercises 31-60; Chapter 6. Spin Systems: Analysis of the 1H-NMR Spectra; 6.1 Second-order Spectra; 6.2 Two-spin Systems; Chapter 7. NMR Shift Reagents and Double Resonance Experiments: Simplification of the NMR Spectra; 7.1 Shift Reagents; 7.2 Double Resonance Experiments Chapter 8. Dynamic NMR Spectroscopy 8.1 Basic Theories; 8.2 Exercises 61-101; Part II: 13C-NMR Spectroscopy; Chapter 9. Introduction; 9.1 Development of 13C-NMR Spectroscopy; 9.2 Comparison of the 'H and 13C Nucleus; 9.3 The Factors Influencing The Sensitivity Of The 13c Nucleus; 9.4 The Factors Increasing the Sensitivity In 13C-NMR Spectroscopy; Chapter 10. Absorption and Resonance; 10.1 Classical Treatment of Absorption and Resonance; 10.2 Relaxation Processes; Chapter 11. Pulse NMR Spectroscopy; 11.1 Introduction to the Pulse NMR Spectroscopy; 11.2 CW and FT Spectroscopy 11.3 Interaction of a Monochromatic Radio frequency With the Sample 11.4 Fourier Transformation; 11.5 Routine Pulsed 13C-NMR Measurement Techniques; 11.6 Broadband Decoupling; 11.7 Nuclear Overhauser Effect; 11.8 Measurements of NOE Enhanced Coupled 13C-NMR Spectra: Gated Decoupling; 11.9 Off Resonance 1H Decoupled and Selective Decoupled Experiments; 11.10 Inverse Gated Decoupling; 11.11 Sample Preparation and Solvents; Chapter 12. Chemical Shift; 12.1 Diamagnetic and Paramagnetic Shielding on Proton and Carbon Atoms; 12.2 Factors which Influence the Chemical Shifts Chapter 13. 13C Chemical Shifts of Organic Compounds 13.1 Alkanes; 13.2 Substituted Alkanes; 13.3 Cycloalkanes; 13.4 Alkenes; 13.5 Aromatic Compounds; 13.6 Carbonyl Compounds; 13.7 Heterocyclic Compounds; Chapter 14. Spin-Spin Coupling; 14.1 Couplings Over One Bond (1JCH); 14.2 Couplings Over Two Bonds (2JcH) (Geminal Coupling); 14.3 Couplings Over Three Bonds (3JcH) (Vicinal Coupling); 14.4 Carbon-Deuterium Coupling (1JcD); Chapter 15. Multiple-Pulse NMR Experiments; 15.1 Measurements of Relaxation Times; 15.2 J-Modulated Spin-echo Experiments 15.3 Signal Enhancement by Population Transfer: Selective Population Transfer and Selective Population Inversion |
| Record Nr. | UNINA-9910784592503321 |
|
Balcıi Metin
|
||
| Amsterdam ; ; Boston, : Elsevier, 2005 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Basic 1H- and 13C-NMR spectroscopy [[electronic resource] /] / Metin Balcıi
| Basic 1H- and 13C-NMR spectroscopy [[electronic resource] /] / Metin Balcıi |
| Autore | Balcıi Metin |
| Edizione | [1st ed.] |
| Pubbl/distr/stampa | Amsterdam ; ; Boston, : Elsevier, 2005 |
| Descrizione fisica | 1 online resource (441 p.) |
| Disciplina | 543.66 |
| Soggetto topico |
Nuclear magnetic resonance spectroscopy
Spectrum analysis |
| ISBN |
1-281-02542-9
9786611025427 0-08-052553-9 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Front Cover; Basic 1H- and 13C-NMR Spectroscopy; Copyright Page; Preface; Contents; Part I: 1H-NMR Spectroscopy; Chapter 1. Introduction; 1.1 Structure Elucidation and NMR; 1.2 Development of NMR Spectroscopy; Chapter 2. Resonance Phenomena; 2.1 Magnetic Properties of Atomic Nuclei; 2.2 Spin Quantum Numbers of Elements; 2.3 Behavior of an Atomic Nucleus in a Magnetic Field; 2.4 Relaxation; 2.5 NMR Instrumentation; Chapter 3. Chemical shift; 3.1 Local Magnetic Fields Around a Nucleus; 3.2 The Unit of the Chemical Shift; 3.3 Sample Preparation; 3.4 Factors Influencing the Chemical Shift
3.5 Exercises 1-30 Chapter 4. Spin-Spin Splitting in 1H-NMR Spectra; 4.1 Explanation of Spin-Spin Splitting; 4.2 Spin-Spin Coupling Mechanism; 4.3 Factors Influencing Spin-Spin Coupling Constants; Chapter 5. Spin-Spin Splitting to Different Protons; 5.1 General Rules; 5.2 Examples of Coupling with Different Protons; 5.3 Exercises 31-60; Chapter 6. Spin Systems: Analysis of the 1H-NMR Spectra; 6.1 Second-order Spectra; 6.2 Two-spin Systems; Chapter 7. NMR Shift Reagents and Double Resonance Experiments: Simplification of the NMR Spectra; 7.1 Shift Reagents; 7.2 Double Resonance Experiments Chapter 8. Dynamic NMR Spectroscopy 8.1 Basic Theories; 8.2 Exercises 61-101; Part II: 13C-NMR Spectroscopy; Chapter 9. Introduction; 9.1 Development of 13C-NMR Spectroscopy; 9.2 Comparison of the 'H and 13C Nucleus; 9.3 The Factors Influencing The Sensitivity Of The 13c Nucleus; 9.4 The Factors Increasing the Sensitivity In 13C-NMR Spectroscopy; Chapter 10. Absorption and Resonance; 10.1 Classical Treatment of Absorption and Resonance; 10.2 Relaxation Processes; Chapter 11. Pulse NMR Spectroscopy; 11.1 Introduction to the Pulse NMR Spectroscopy; 11.2 CW and FT Spectroscopy 11.3 Interaction of a Monochromatic Radio frequency With the Sample 11.4 Fourier Transformation; 11.5 Routine Pulsed 13C-NMR Measurement Techniques; 11.6 Broadband Decoupling; 11.7 Nuclear Overhauser Effect; 11.8 Measurements of NOE Enhanced Coupled 13C-NMR Spectra: Gated Decoupling; 11.9 Off Resonance 1H Decoupled and Selective Decoupled Experiments; 11.10 Inverse Gated Decoupling; 11.11 Sample Preparation and Solvents; Chapter 12. Chemical Shift; 12.1 Diamagnetic and Paramagnetic Shielding on Proton and Carbon Atoms; 12.2 Factors which Influence the Chemical Shifts Chapter 13. 13C Chemical Shifts of Organic Compounds 13.1 Alkanes; 13.2 Substituted Alkanes; 13.3 Cycloalkanes; 13.4 Alkenes; 13.5 Aromatic Compounds; 13.6 Carbonyl Compounds; 13.7 Heterocyclic Compounds; Chapter 14. Spin-Spin Coupling; 14.1 Couplings Over One Bond (1JCH); 14.2 Couplings Over Two Bonds (2JcH) (Geminal Coupling); 14.3 Couplings Over Three Bonds (3JcH) (Vicinal Coupling); 14.4 Carbon-Deuterium Coupling (1JcD); Chapter 15. Multiple-Pulse NMR Experiments; 15.1 Measurements of Relaxation Times; 15.2 J-Modulated Spin-echo Experiments 15.3 Signal Enhancement by Population Transfer: Selective Population Transfer and Selective Population Inversion |
| Record Nr. | UNINA-9910808892603321 |
|
Balcıi Metin
|
||
| Amsterdam ; ; Boston, : Elsevier, 2005 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Basic one- and two-dimensional NMR spectroscopy / Horst Friebolin
| Basic one- and two-dimensional NMR spectroscopy / Horst Friebolin |
| Autore | Friebolin, Horst |
| Edizione | [5. completely rev. and updated ed] |
| Pubbl/distr/stampa | Weinheim : Wiley-VCH, 2011 |
| Descrizione fisica | XXIV, 418 p. : ill. ; 24 cm. |
| Disciplina | 543.66 |
| Soggetto topico | Risonanza magnetica nucleare |
| ISBN | 978-3-527-32782-9 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Titolo uniforme | |
| Record Nr. | UNIBAS-000034946 |
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Friebolin, Horst
|
||
| Weinheim : Wiley-VCH, 2011 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. della Basilicata | ||
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Basic one- and two-dimensional NMR spectroscopy / Horst Friebolin ; translated by Jack K. Becconsall
| Basic one- and two-dimensional NMR spectroscopy / Horst Friebolin ; translated by Jack K. Becconsall |
| Autore | Friebolin, Horst |
| Edizione | [2nd ed.] |
| Pubbl/distr/stampa | Weinheim ; New York : VCH, 1993 |
| Descrizione fisica | xxi, 368 p. : ill. ; 25 cm |
| Disciplina | 543.66 |
| Altri autori (Persone) | Becconsall, Jack K. |
| Soggetto topico |
Nuclear magnetic resonance spectroscopy
Nuclear Magnetic Resonance - Methods |
| ISBN | 1560817968 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Record Nr. | UNISALENTO-991001450679707536 |
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Friebolin, Horst
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| Weinheim ; New York : VCH, 1993 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. del Salento | ||
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Calculation of NMR and EPR parameters [[electronic resource] ] : theory and applications / / [edited by] Martin Kaupp, Michael Bühl, Vladimir G. Malkin
| Calculation of NMR and EPR parameters [[electronic resource] ] : theory and applications / / [edited by] Martin Kaupp, Michael Bühl, Vladimir G. Malkin |
| Pubbl/distr/stampa | Weinheim, : Wiley-VCH, c2004 |
| Descrizione fisica | 1 online resource (623 p.) |
| Disciplina |
543
543.66 543/.66 |
| Altri autori (Persone) |
KauppMartin
BühlMichael MalkinVladimir G |
| Soggetto topico |
Nuclear magnetic resonance spectroscopy
Electron paramagnetic resonance spectroscopy Quantum chemistry |
| Soggetto genere / forma | Electronic books. |
| ISBN |
1-280-52011-6
9786610520114 3-527-60496-0 3-527-60167-8 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Calculation of NMR and EPR Parameters; Contents; Foreword; List of Contributors; Part A Introductory Chapters; 1 Introduction: The Quantum Chemical Calculation of NMR and EPR Parameters; 2 Theory of NMR parameters. From Ramsey to Relativity, 1953 to 1983; 2.1 Introduction; 2.2 Spin-Spin Coupling; 2.3 Chemical Shifts; 2.4 General Aspects; 2.5 From 1983 to 2003; 3 Historical Aspects of EPR Parameter Calculations; 4 The Effective Spin Hamiltonian Concept from a Quantum Chemical Perspective; 5 Fundamentals of Nonrelativistic and Relativistic Theory of NMR and EPR Parameters; 5.1 Introduction
5.2 Classical Theory of the Interaction of a Charged Particle with an Electromagnetic Field5.3 Quantum Mechanical Hamiltonians in a Time-Independent Electromagnetic Field; 5.4 Perturbation Theory of Magnetic Effects; 5.5 Non-Relativistic Theory of EPR and NMR Parameters; 5.6 Relativistic Theory of Magnetic Properties; 5.7 The Leading Relativistic Corrections; 5.8 Concluding Remarks; Part B NMR Parameters, Methodological Aspects; 6 Chemical Shifts with Hartree-Fock and Density Functional Methods; 6.1 Introduction; 6.2 Linear Response and the Gauge Origin Problem 6.3 Determination of the First-Order Orbitals6.4 Distributed Gauge Origins, IGLO and GIAO Approaches; 6.5 Distributed Gauge Origins in Real Space, a "Continuous Set of Gauge Transformations"; 6.6 Beyond Pure Density Functional Theory; 6.7 Conclusions; 7 Spin-Spin Coupling Constants with HF and DFT Methods; 7.1 Introduction; 7.2 The Calculation of Indirect Nuclear Spin-Spin Coupling Constants; 7.3 Examples of Applications; 7.4 Conclusions; 8 Electron-Correlated Methods for the Calculation of NMR Chemical Shifts; 8.1 Introduction; 8.2 Theoretical Background 8.3 Electron-Correlated Treatment of NMR Chemical Shifts8.4 Special developments; 8.5 Numerical Results; 8.6 Summary and Outlook; 9 Semiempirical Methods for the Calculation of NMR Chemical Shifts; 9.1 Introduction; 9.2 Methods; 9.3 Representative Applications; 9.4 Concluding Remarks: Limitations of Semiempirical Methods for the Calculation of NMR Parameters; 10 Ro-Vibrational Corrections to NMR Parameters; 10.1 Introduction; 10.2 Perturbation Theory; 10.3 Other Approaches for Calculating Vibrationally Averaged NMR Properties; 10.4 Examples of Vibrational Contributions to NMR Properties 10.5 Summary11 Molecular Dynamics and NMR Parameter Calculations; 11.1 Introduction; 11.2 Methods; 11.3 Examples; 11.4 Summary and Conclusions; 12 Use of Continuum Solvent Models in Magnetic Resonance Parameter Calculations; 12.1 Introduction; 12.2 General Features of Continuum Models; 12.3 Applications of Continuum Models to the Prediction of NMR Parameters; 12.4 Applications of Continuum Models to the Prediction of EPR Parameters; 12.5 Conclusions; 13 Perturbational and ECP Calculation of Relativistic Effects in NMR Shielding and Spin-Spin Coupling; 13.1 Introduction 13.2 Nuclear Shielding and Spin-Spin Coupling |
| Record Nr. | UNINA-9910146236303321 |
| Weinheim, : Wiley-VCH, c2004 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
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