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The electron capture detector and the study of reactions with thermal electrons [[electronic resource] /] / E.C.M. Chen, E.S.D. Chen
| The electron capture detector and the study of reactions with thermal electrons [[electronic resource] /] / E.C.M. Chen, E.S.D. Chen |
| Autore | Chen E. C. M (Edward C. M.) |
| Pubbl/distr/stampa | Hoboken, N.J., : Wiley-Interscience, c2004 |
| Descrizione fisica | 1 online resource (417 p.) |
| Disciplina |
541.36
543.26 543.85 |
| Altri autori (Persone) | ChenE. S. D |
| Soggetto topico |
Gas chromatography
Electrons - Capture |
| Soggetto genere / forma | Electronic books. |
| ISBN |
1-280-54201-2
9786610542017 0-471-65988-6 0-471-65989-4 |
| Formato | Materiale a stampa  |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
THE ELECTRON CAPTURE DETECTOR AND THE STUDY OF REACTIONS WITH THERMAL ELECTRONS; CONTENTS; FOREWORD; PREFACE; 1. Scope and History of the Electron; 1.1 General Objectives and Organization; 1.2 General Scope; 1.3 History of the Electron; References; 2. Definitions, Nomenclature, Reactions, and Equations; 2.1 Introduction; 2.2 Definition of Kinetic and Energetic Terms; 2.3 Additional Gas Phase Ionic Reactions; 2.4 Electron Affinities from Solution Data; 2.5 Semi-Empirical Calculations of Energetic Quantities; 2.6 Herschbach Ionic Morse Potential Energy Curves; 2.7 Summary; References
3. Thermal Electron Reactions at the University of Houston3.1 General Introduction; 3.2 The First Half-Century, 1900 to 1950; 3.3 Fundamental Discovery, 1950 to 1960; 3.4 General Accomplishments, 1960 to 1970; 3.4.1 Introduction; 3.4.2 The Wentworth Group; 3.4.3 Stable Negative-Ion Formation; 3.4.4 Dissociative Thermal Electron Attachment; 3.4.5 Nonlinear Least Squares; 3.5 Milestones in the Wentworth Laboratory and Complementary Methods, 1970 to 1980; 3.6 Negative-Ion Mass Spectrometry and Morse Potential Energy Curves, 1980 to 1990; 3.7 Experimental and Theoretical Milestones, 1990 to 2000 3.8 Summary of Contributions at the University of HoustonReferences; 4. Theoretical Basis of the Experimental Tools; 4.1 Introduction; 4.2 The Kinetic Model of the ECD and NIMS; 4.3 Nondissociative Electron Capture; 4.4 Dissociative Electron Attachment; 4.5 Electron Affinities and Half-Wave Reduction Potentials; 4.6 Electron Affinities and Ionization Potentials of Aromatic Hydrocarbons; 4.7 Electron Affinities and Charge Transfer Complex Energies; 4.8 Summary; References; 5. Experimental Procedures and Data Reduction; 5.1 Introduction; 5.2 Experimental ECD and NICI Procedures 5.3 Reduction of ECD Data to Fundamental Properties5.3.1 Introduction; 5.3.2 Acetophenone and Benzaldehyde; 5.3.3 Benzanthracene, Benz[a]pyrene, and 1-Naphthaldehyde; 5.3.4 Carbon Disulfide; 5.3.5 Nitromethane; 5.3.6 Consolidation of Electron Affinities for Molecular Oxygen; 5.4 Reduction of Negative-Ion Mass Spectral Data; 5.5 Precision and Accuracy; 5.6 Evaluation of Experimental Results; 5.7 Summary; References; 6. Complementary Experimental and Theoretical Procedures; 6.1 Introduction; 6.2 Equilibrium Methods for Determining Electron Affinities; 6.3 Photon Techniques 6.4 Thermal Charge Transfer Methods6.5 Electron and Particle Beam Techniques; 6.6 Condensed Phase Measurements of Electron Affinities; 6.7 Complementary Theoretical Calculations; 6.7.1 Atomic Electron Affinities; 6.7.2 Polyatomic Molecules; 6.8 Rate Constants for Attachment, Detachment, and Recombination; 6.9 Summary; References; 7. Consolidating Experimental, Theoretical, and Empirical Data; 7.1 Introduction; 7.2 Semi-Empirical Quantum Mechanical Calculations; 7.3 Morse Potential Energy Curves; 7.3.1 Classification of Negative-Ion Morse Potentials; 7.3.2 The Negative-Ion States of H(2) 7.3.3 The Negative-Ion States of I(2) |
| Record Nr. | UNINA-9910146070703321 |
Chen E. C. M (Edward C. M.)
|
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| Hoboken, N.J., : Wiley-Interscience, c2004 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
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The electron capture detector and the study of reactions with thermal electrons [[electronic resource] /] / E.C.M. Chen, E.S.D. Chen
| The electron capture detector and the study of reactions with thermal electrons [[electronic resource] /] / E.C.M. Chen, E.S.D. Chen |
| Autore | Chen E. C. M (Edward C. M.) |
| Pubbl/distr/stampa | Hoboken, N.J., : Wiley-Interscience, c2004 |
| Descrizione fisica | 1 online resource (417 p.) |
| Disciplina |
541.36
543.26 543.85 |
| Altri autori (Persone) | ChenE. S. D |
| Soggetto topico |
Gas chromatography
Electrons - Capture |
| ISBN |
1-280-54201-2
9786610542017 0-471-65988-6 0-471-65989-4 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
THE ELECTRON CAPTURE DETECTOR AND THE STUDY OF REACTIONS WITH THERMAL ELECTRONS; CONTENTS; FOREWORD; PREFACE; 1. Scope and History of the Electron; 1.1 General Objectives and Organization; 1.2 General Scope; 1.3 History of the Electron; References; 2. Definitions, Nomenclature, Reactions, and Equations; 2.1 Introduction; 2.2 Definition of Kinetic and Energetic Terms; 2.3 Additional Gas Phase Ionic Reactions; 2.4 Electron Affinities from Solution Data; 2.5 Semi-Empirical Calculations of Energetic Quantities; 2.6 Herschbach Ionic Morse Potential Energy Curves; 2.7 Summary; References
3. Thermal Electron Reactions at the University of Houston3.1 General Introduction; 3.2 The First Half-Century, 1900 to 1950; 3.3 Fundamental Discovery, 1950 to 1960; 3.4 General Accomplishments, 1960 to 1970; 3.4.1 Introduction; 3.4.2 The Wentworth Group; 3.4.3 Stable Negative-Ion Formation; 3.4.4 Dissociative Thermal Electron Attachment; 3.4.5 Nonlinear Least Squares; 3.5 Milestones in the Wentworth Laboratory and Complementary Methods, 1970 to 1980; 3.6 Negative-Ion Mass Spectrometry and Morse Potential Energy Curves, 1980 to 1990; 3.7 Experimental and Theoretical Milestones, 1990 to 2000 3.8 Summary of Contributions at the University of HoustonReferences; 4. Theoretical Basis of the Experimental Tools; 4.1 Introduction; 4.2 The Kinetic Model of the ECD and NIMS; 4.3 Nondissociative Electron Capture; 4.4 Dissociative Electron Attachment; 4.5 Electron Affinities and Half-Wave Reduction Potentials; 4.6 Electron Affinities and Ionization Potentials of Aromatic Hydrocarbons; 4.7 Electron Affinities and Charge Transfer Complex Energies; 4.8 Summary; References; 5. Experimental Procedures and Data Reduction; 5.1 Introduction; 5.2 Experimental ECD and NICI Procedures 5.3 Reduction of ECD Data to Fundamental Properties5.3.1 Introduction; 5.3.2 Acetophenone and Benzaldehyde; 5.3.3 Benzanthracene, Benz[a]pyrene, and 1-Naphthaldehyde; 5.3.4 Carbon Disulfide; 5.3.5 Nitromethane; 5.3.6 Consolidation of Electron Affinities for Molecular Oxygen; 5.4 Reduction of Negative-Ion Mass Spectral Data; 5.5 Precision and Accuracy; 5.6 Evaluation of Experimental Results; 5.7 Summary; References; 6. Complementary Experimental and Theoretical Procedures; 6.1 Introduction; 6.2 Equilibrium Methods for Determining Electron Affinities; 6.3 Photon Techniques 6.4 Thermal Charge Transfer Methods6.5 Electron and Particle Beam Techniques; 6.6 Condensed Phase Measurements of Electron Affinities; 6.7 Complementary Theoretical Calculations; 6.7.1 Atomic Electron Affinities; 6.7.2 Polyatomic Molecules; 6.8 Rate Constants for Attachment, Detachment, and Recombination; 6.9 Summary; References; 7. Consolidating Experimental, Theoretical, and Empirical Data; 7.1 Introduction; 7.2 Semi-Empirical Quantum Mechanical Calculations; 7.3 Morse Potential Energy Curves; 7.3.1 Classification of Negative-Ion Morse Potentials; 7.3.2 The Negative-Ion States of H(2) 7.3.3 The Negative-Ion States of I(2) |
| Record Nr. | UNINA-9910830435303321 |
|
Chen E. C. M (Edward C. M.)
|
||
| Hoboken, N.J., : Wiley-Interscience, c2004 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
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Handbook of thermal analysis and calorimetry / series editor Patrick K. Gallagher
| Handbook of thermal analysis and calorimetry / series editor Patrick K. Gallagher |
| Pubbl/distr/stampa | Amsterdam [etc.], : Elsevier |
| Descrizione fisica | v. ; 27 cm. |
| Disciplina |
543
543.26 |
| Soggetto topico | Calorimetria |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Record Nr. | UNISANNIO-UFI0307915 |
| Amsterdam [etc.], : Elsevier | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. del Sannio | ||
| ||
Introduction to thermal analysis : techniques and applications / Michael E. Brown
| Introduction to thermal analysis : techniques and applications / Michael E. Brown |
| Edizione | [2. ed] |
| Pubbl/distr/stampa | Dordrecht [etc.], : Kluwer academic publishers, c2001 |
| Descrizione fisica | XI, 264 p. : ill. ; 25 cm. |
| Disciplina |
543
543.26 |
| Collana | Hot topics in thermal analysis and calorimetry |
| Soggetto topico | CHIMICA ANALITICA |
| ISBN |
1402002114
1402004729 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Record Nr. | UNISANNIO-MIL0589305 |
| Dordrecht [etc.], : Kluwer academic publishers, c2001 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. del Sannio | ||
| ||
Principles and applications of thermal analysis [[electronic resource] /] / edited by Paul Gabbott
| Principles and applications of thermal analysis [[electronic resource] /] / edited by Paul Gabbott |
| Pubbl/distr/stampa | Oxford, : Blackwell Pub., 2008 |
| Descrizione fisica | 1 online resource (484 p.) |
| Disciplina |
543.26
543/.26 |
| Altri autori (Persone) | GabbottPaul |
| Soggetto topico |
Thermal analysis
Colorimetric analysis Thermal analysis - Industrial applications |
| ISBN |
1-282-12295-9
9786612122958 0-470-69770-9 0-470-69812-8 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Principles and Applications of Thermal Analysis; Contents; Abbreviations; List of Contributors; 1 A Practical Introduction to Differential Scanning Calorimetry; 1.1 Introduction; 1.2 Principles of DSC and types of measurements made; 1.2.1 A definition of DSC; 1.2.2 Heat low measurements; 1.2.3 Specific heat (Cp); 1.2.4 Enthalpy; 1.2.5 Derivative curves; 1.3 Practical issues; 1.3.1 Encapsulation; 1.3.2 Temperature range; 1.3.3 Scan rate; 1.3.4 Sample size; 1.3.5 Purge gas; 1.3.6 Sub-ambient operation; 1.3.7 General practical points; 1.3.8 Preparing power compensation systems for use
1.4 Calibration1.4.1 Why calibrate; 1.4.2 When to calibrate; 1.4.3 Checking performance; 1.4.4 Parameters to be calibrated; 1.4.5 Heat low calibration; 1.4.6 Temperature calibration; 1.4.7 Temperature control (furnace) calibration; 1.4.8 Choice of standards; 1.4.9 Factors affecting calibration; 1.4.10 Final comments; 1.5 Interpretation of data; 1.5.1 The instrumental transient; 1.5.2 Melting; 1.5.3 The glass transition; 1.5.4 Factors affecting Tg; 1.5.5 Calculating and assigning Tg; 1.5.6 Enthalpic relaxation; 1.5.7 Tg on cooling; 1.5.8 Methods of obtaining amorphous material; 1.5.9 Reactions 1.5.10 Guidelines for interpreting data1.6 Oscillatory temperature profiles; 1.6.1 Modulated temperature methods; 1.6.2 Stepwise methods; 1.7 DSC design; 1.7.1 Power compensation DSC; 1.7.2 Heat flux DSC; 1.7.3 Differential thermal analysis DTA; 1.7.4 Differential photocalorimetry DPC; 1.7.5 High-pressure cells; Appendix: standard DCS methods; References; 2 Fast Scanning DSC; 2.1 Introduction; 2.2 Proof of performance; 2.2.1 Effect of high scan rates on standards; 2.2.2 De.nition of HyperDSCTM; 2.2.3 The initial transient; 2.2.4 Fast cooling rates; 2.3 Benefits of fast scanning rates 2.3.1 Sensitivity2.3.2 Measurement of sample properties without unwanted annealing effects; 2.3.3 Separate overlapping events based on different kinetics; 2.3.4 Speed of analysis; 2.4 Application to polymers; 2.4.1 Melting and crystallisation processes; 2.4.2 Comparative studies; 2.4.3 Forensic studies; 2.4.4 Effect of heating rate on the sensitivity of the glass transition; 2.4.5 Effect of heating rate on the temperature of the glass transition; 2.4.6 Effect of heating rate on Tg of annealed materials (and enthalpic relaxation phenomena); 2.5 Application to pharmaceuticals 2.5.1 Purity of polymorphic form2.5.2 Identifying polymorphs; 2.5.3 Determination of amorphous content of materials; 2.5.4 Measurements of solubility; 2.6 Application to water-based solutions and the effect of moisture; 2.6.1 Measurement of Tg in frozen solutions and suspensions; 2.6.2 Material affected by moisture; 2.7 Practical aspects of scanning at fast rates; 2.7.1 Purge gas; 2.7.2 Sample pans; 2.7.3 Sample size; 2.7.4 Scan rate; 2.7.5 Instrumental settings; 2.7.6 Cleanliness; 2.7.7 Getting started; References; 3 Thermogravimetric Analysis; 3.1 Introduction 3.2 Design and measuring principle |
| Record Nr. | UNISA-996197247203316 |
| Oxford, : Blackwell Pub., 2008 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. di Salerno | ||
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Thermal analysis of plastics : theory and practice / Gottfried W. Ehrenstein, Gabriela Riedel, Pia Trawiel
| Thermal analysis of plastics : theory and practice / Gottfried W. Ehrenstein, Gabriela Riedel, Pia Trawiel |
| Autore | Ehrenstein, Gottfried Wilhelm <1937- > |
| Pubbl/distr/stampa | Munich, : Hanser |
| Descrizione fisica | XXIX, 368 p. : ill. ; 25 cm. |
| Disciplina |
543
543.26 |
| Altri autori (Persone) |
Riedel, Gabriela <1965- >
Trawiel, Pia <1972- > |
| Soggetto topico | Materie plastiche - Proprietà termiche |
| ISBN |
156990362X
3446226737 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Record Nr. | UNISANNIO-UFE0702408 |
|
Ehrenstein, Gottfried Wilhelm <1937- >
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| Munich, : Hanser | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. del Sannio | ||
| ||
Thermal analysis of plastics : theory and practice / Gottfried W. Ehrenstein, Gabriela Riedel, Pia Trawiel
| Thermal analysis of plastics : theory and practice / Gottfried W. Ehrenstein, Gabriela Riedel, Pia Trawiel |
| Autore | Ehrenstein, G. W. |
| Pubbl/distr/stampa | Munich : Hanser |
| Descrizione fisica | xxix, 368 p. : ill. (some col.) ; 25 cm |
| Disciplina | 543.26 |
| Altri autori (Persone) |
Riedel, Gabrielaauthor
Trawiel, Pia |
| Soggetto topico |
Plastics - Testing
Plastics - Thermal properties Thermal analysis |
| ISBN |
156990362X (Hanser Gardner Publications)
3446226737 (Carl Hanser Verlag) |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Record Nr. | UNISALENTO-991001900669707536 |
|
Ehrenstein, G. W.
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| Munich : Hanser | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. del Salento | ||
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