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Hypervalent Iodine Chemistry / / edited by Thomas Wirth
| Hypervalent Iodine Chemistry / / edited by Thomas Wirth |
| Edizione | [1st ed. 2016.] |
| Pubbl/distr/stampa | Cham : , : Springer International Publishing : , : Imprint : Springer, , 2016 |
| Descrizione fisica | 1 online resource (VIII, 316 p.) |
| Disciplina | 546.7342 |
| Collana | Topics in Current Chemistry |
| Soggetto topico |
Chemistry, Organic
Catalysis Chemical engineering Organic Chemistry Industrial Chemistry/Chemical Engineering |
| ISBN | 3-319-33733-5 |
| Formato | Materiale a stampa  |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto | Oxidative Coupling Reactions mediated by Hypervalent Iodine Reagents -- Phenol Dearomatization with Hypervalent Iodine Reagents -- Oxidative Heterocycle formation using Hypervalent Iodine Reagents -- Aminations with Hypervalent Iodine -- Arylation with Diaryliodium Salts -- Trifluoromethylation using Cyclic Iodine Derivatives -- Alkynylation with Iodine Reagents -- Rearrangements induced by Iodine Reagents -- Stereoselective Reactions with Hypervalent Iodine Reagents -- Hypervalent Iodine Reagents in Transition Metal Catalysis -- Halogen Bonding in Hypervalent Iodine Reagents. |
| Record Nr. | UNINA-9910254057503321 |
| Cham : , : Springer International Publishing : , : Imprint : Springer, , 2016 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Microreactors in organic chemistry and catalysis [[electronic resource] /] / edited by Thomas Wirth
| Microreactors in organic chemistry and catalysis [[electronic resource] /] / edited by Thomas Wirth |
| Edizione | [2nd completely rev. and enl. ed.] |
| Pubbl/distr/stampa | Weinheim, Germany, : Wiley-VCH, 2013 |
| Descrizione fisica | 1 online resource (487 p.) |
| Disciplina | 547.215 |
| Altri autori (Persone) | WirthThomas |
| Soggetto topico |
Microreactors
Catalysis Chemistry, Organic Chemical reactors |
| ISBN |
3-527-65972-2
3-527-65974-9 1-299-27709-8 3-527-65975-7 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Microreactors in Organic Chemistry and Catalysis; Contents; Preface to the First Edition; Preface to the Second Edition; List of Contributors; 1 Properties and Use of Microreactors; 1.1 Introduction; 1.1.1 A Brief History of Microreactors; 1.1.2 Advantages of Microreactors; 1.2 Physical Characteristics of Microreactors; 1.2.1 Geometries; 1.2.2 Constructional Materials and Their Properties; 1.3 Fluid Flow and Delivery Regimes; 1.3.1 Fluid Flow; 1.3.2 Fluid Delivery; 1.3.3 Mixing Mechanisms; 1.4 Multifunctional Integration; 1.5 Uses of Microreactors; 1.5.1 Overview
1.5.1.1 Fast and Exothermic Reactions1.5.2 Precision Particle Manufacture; 1.5.3 Wider Industrial Context; 1.5.3.1 Sustainability Agenda; 1.5.3.2 Point-of-Demand Synthesis; References; 2 Fabrication of Microreactors Made from Metals and Ceramic; 2.1 Manufacturing Techniques for Metals; 2.2 Etching; 2.3 Machining; 2.4 Generative Method: Selective Laser Melting; 2.5 Metal Forming Techniques; 2.6 Assembling and Bonding of Metal Microstructures; 2.7 Ceramic Devices; 2.8 Joining and Sealing; References; 3 Microreactors Made of Glass and Silicon; 3.1 How Microreactors Are Constructed 3.1.1 Glass As Material3.1.2 Silicon As Material; 3.2 The Structuring of Glass and Silicon; 3.2.1 Structuring by Means of Masked Etching As in Microsystems Technology; 3.2.2 Etching Technologies; 3.2.2.1 Anisotropic (Crystallographic) Wet Chemical Etching of Silicon (KOH); 3.3 Isotropic Wet Chemical Etching of Silicon; 3.3.1 3.3.1.1 Isotropic Wet Chemical Etching of Silicon; 3.3.1.2 Isotropic Wet Chemical Etching of Silicon Glass; 3.3.2 Other Processes; 3.3.2.1 Photostructuring of Special Glass; 3.3.3 Drilling, Diamond Lapping, Ultrasonic Lapping; 3.3.4 Micro Powder Blasting; 3.3.5 Summary 3.4 Other Processes3.4.1 Sensor Integration; 3.5 Thin Films; 3.6 Bonding Methods; 3.6.1 Anodic Bonding of Glass and Silicon; 3.6.2 Glass Fusion Bonding; 3.6.3 Silicon Direct Bonding (Silicon Fusion Bonding); 3.6.4 Establishing Fluid Contact; 3.7 Other Materials; References; 4 Automation in Microreactor Systems; 4.1 Introduction; 4.2 Automation System; 4.3 Automated Optimization with HPLC Sampling; 4.4 Automated Multi-Trajectory Optimization; 4.5 Kinetic Model Discrimination and Parameter Fitting; 4.6 Conclusions and Outlook; References; 5 Homogeneous Reactions; 5.1 Acid-Promoted Reactions 5.2 Base-Promoted Reactions5.3 Radical Reactions; 5.4 Condensation Reactions; 5.5 Metal-Catalyzed Reactions; 5.6 High Temperature Reactions; 5.7 Oxidation Reactions; 5.8 Reaction with Organometallic Reagents; References; 6 Homogeneous Reactions II: Photochemistry and Electrochemistry and Radiopharmaceutical Synthesis; 6.1 Photochemistry in Flow Reactors; 6.2 Electrochemistry in Microreactors; 6.3 Radiopharmaceutical Synthesis in Microreactors; 6.3.1 Fluorinations in Microreactors; 6.3.2 Synthesis of 11C-Labeled PET Radiopharmaceuticals in Microreactors; 6.4 Conclusion and Outlook; References 7 Heterogeneous Reactions |
| Record Nr. | UNINA-9910139059603321 |
| Weinheim, Germany, : Wiley-VCH, 2013 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Microreactors in organic chemistry and catalysis / / edited by Thomas Wirth
| Microreactors in organic chemistry and catalysis / / edited by Thomas Wirth |
| Edizione | [2nd completely rev. and enl. ed.] |
| Pubbl/distr/stampa | Weinheim, Germany, : Wiley-VCH, 2013 |
| Descrizione fisica | 1 online resource (487 p.) |
| Disciplina | 547.215 |
| Altri autori (Persone) | WirthThomas |
| Soggetto topico |
Microreactors
Catalysis Chemistry, Organic Chemical reactors |
| ISBN |
9783527659722
3527659722 9783527659746 3527659749 9781299277090 1299277098 9783527659753 3527659757 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Microreactors in Organic Chemistry and Catalysis; Contents; Preface to the First Edition; Preface to the Second Edition; List of Contributors; 1 Properties and Use of Microreactors; 1.1 Introduction; 1.1.1 A Brief History of Microreactors; 1.1.2 Advantages of Microreactors; 1.2 Physical Characteristics of Microreactors; 1.2.1 Geometries; 1.2.2 Constructional Materials and Their Properties; 1.3 Fluid Flow and Delivery Regimes; 1.3.1 Fluid Flow; 1.3.2 Fluid Delivery; 1.3.3 Mixing Mechanisms; 1.4 Multifunctional Integration; 1.5 Uses of Microreactors; 1.5.1 Overview
1.5.1.1 Fast and Exothermic Reactions1.5.2 Precision Particle Manufacture; 1.5.3 Wider Industrial Context; 1.5.3.1 Sustainability Agenda; 1.5.3.2 Point-of-Demand Synthesis; References; 2 Fabrication of Microreactors Made from Metals and Ceramic; 2.1 Manufacturing Techniques for Metals; 2.2 Etching; 2.3 Machining; 2.4 Generative Method: Selective Laser Melting; 2.5 Metal Forming Techniques; 2.6 Assembling and Bonding of Metal Microstructures; 2.7 Ceramic Devices; 2.8 Joining and Sealing; References; 3 Microreactors Made of Glass and Silicon; 3.1 How Microreactors Are Constructed 3.1.1 Glass As Material3.1.2 Silicon As Material; 3.2 The Structuring of Glass and Silicon; 3.2.1 Structuring by Means of Masked Etching As in Microsystems Technology; 3.2.2 Etching Technologies; 3.2.2.1 Anisotropic (Crystallographic) Wet Chemical Etching of Silicon (KOH); 3.3 Isotropic Wet Chemical Etching of Silicon; 3.3.1 3.3.1.1 Isotropic Wet Chemical Etching of Silicon; 3.3.1.2 Isotropic Wet Chemical Etching of Silicon Glass; 3.3.2 Other Processes; 3.3.2.1 Photostructuring of Special Glass; 3.3.3 Drilling, Diamond Lapping, Ultrasonic Lapping; 3.3.4 Micro Powder Blasting; 3.3.5 Summary 3.4 Other Processes3.4.1 Sensor Integration; 3.5 Thin Films; 3.6 Bonding Methods; 3.6.1 Anodic Bonding of Glass and Silicon; 3.6.2 Glass Fusion Bonding; 3.6.3 Silicon Direct Bonding (Silicon Fusion Bonding); 3.6.4 Establishing Fluid Contact; 3.7 Other Materials; References; 4 Automation in Microreactor Systems; 4.1 Introduction; 4.2 Automation System; 4.3 Automated Optimization with HPLC Sampling; 4.4 Automated Multi-Trajectory Optimization; 4.5 Kinetic Model Discrimination and Parameter Fitting; 4.6 Conclusions and Outlook; References; 5 Homogeneous Reactions; 5.1 Acid-Promoted Reactions 5.2 Base-Promoted Reactions5.3 Radical Reactions; 5.4 Condensation Reactions; 5.5 Metal-Catalyzed Reactions; 5.6 High Temperature Reactions; 5.7 Oxidation Reactions; 5.8 Reaction with Organometallic Reagents; References; 6 Homogeneous Reactions II: Photochemistry and Electrochemistry and Radiopharmaceutical Synthesis; 6.1 Photochemistry in Flow Reactors; 6.2 Electrochemistry in Microreactors; 6.3 Radiopharmaceutical Synthesis in Microreactors; 6.3.1 Fluorinations in Microreactors; 6.3.2 Synthesis of 11C-Labeled PET Radiopharmaceuticals in Microreactors; 6.4 Conclusion and Outlook; References 7 Heterogeneous Reactions |
| Record Nr. | UNINA-9910825220103321 |
| Weinheim, Germany, : Wiley-VCH, 2013 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Operative Approaches in Orthopedic Surgery and Traumatology / / by: Kerschbaumer, Fridun, Weise, Kuno, Wirth, Carl Joachim, Vaccaro, Alexander R.
| Operative Approaches in Orthopedic Surgery and Traumatology / / by: Kerschbaumer, Fridun, Weise, Kuno, Wirth, Carl Joachim, Vaccaro, Alexander R. |
| Autore | Bauer Rudolf |
| Edizione | [2nd ed.] |
| Pubbl/distr/stampa | Stuttgart, Germany : , : Thieme, , 2015 |
| Descrizione fisica | 1 online resource (416 p.) |
| Disciplina | 617.4/71 |
| Soggetto topico |
Orthopedics
Bones - Surgery Wounds and injuries - Surgery |
| ISBN | 3-13-258060-0 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Operative Approaches in Orthopedic Surgery and Traumatology; Title Page; Copyright; Contents; Foreword to the Second Edition; Foreword to the First Edition; Preface; Contributors; Spine, Anterior Approaches; 1 Cervical Spine and Cervicothoracic Junction; 1.1 Transoropharyngeal Approach C1-C2 (C3); 1.2 Anterior Approach to the Cervical Spine C3-T2; 1.3 Anterior Approach to the Lower Cervical and Upper Thoracic Spine C4-T3 According to Cauchoix, Binet, and Evrard; 2 Thoracic Spine; 2.1 Transthoracic Approach to the Thoracic Spine T4-T11
2.2 Anterior Transpleural Approach to the Spine T3-T11 According to Louis2.3 High Thoracotomy T1-T4; 2.4 Thoracoscopic and Minimally Invasive, Thoracoscopy-Assisted Access to the Thoracic Spine; 3 Thoracolumbar Junction; 3.1 Retroperitoneal Extrapleural Approach to the Thoracolumbar Spine T9-L5 According to Hodgson; 3.2 Approach to Thoracolumbar Spine with Two-fold Thoracotomy T4-L5 According to Bauer; 3.3 Retroperitoneal Extrapleural Approach to Thoracolumbar Spine T11-L5 According to Mirbaha; 4 Lumbar Spine and Lumbosacral Junction; 4.1 Retroperitoneal Approach to the Lumbar Spine L2-L5 4.2 Transperitoneal Approach to the Lumbosacral Junction L4-S14.3 Minimally Invasive Lateral Approach to the Lumbar Spine L2-L5; Spine, Posterior Approaches; 5 Cervical Spine; 5.1 Posterior Approach to the Cervical Spine and Occipitocervical Junction; 6 Thoracic and Lumbar Spine; 6.1 Costotransversectomy T3-T10; 6.2 Posterior Approach to the Thoracic and Lumbar Spine; 6.3 Paraspinal Approach to the Lumbosacral Junction According to Wiltse; 6.4 Short Posterior Approach to the Lumbar Spine for Laminotomy and Removal of an Intervertebral Disk; Pelvis and Lower Extremity; 7 Pelvis: Pelvic Ring 7.1 Approach to the Symphysis and Anterior Pelvis7.2 Anterior Approach to the Posterior Pelvis; 7.3 Posterior Approach to the Sacrum; 7.4 Lateral Minimally Invasive Approach for Trans-sacroiliac Screw Placement; 7.5 Approach to the Ischium and Pubis; 8 Pelvis: Acetabulum; 8.1 Ilioinguinal Approach According to Letournel; 8.2 Posterior Approach to the Hip According to Kocher-Langenbeck; 8.3 Anterior Limited Approach According to Stoppa; 8.4 Transiliac Approach According to Judet; 8.5 Approach to the Acetabulum According to Judet; 9 Hip Joint 9.1 Posterior Approach to the Hip Joint with Dislocation According to Ganz9.2 Posterior Minimally Invasive Approach; 9.3 Transgluteal Approach According to Bauer; 9.4 Minimally Invasive Transgluteal Approach; 9.5 Anterolateral Approach to the Hip Joint; 9.6 Minimally Invasive Anterolateral Approach to the Hip Joint; 9.7 Anterior Approach to the Hip Joint; 9.8 Anterior Minimally Invasive Approach; 9.9 Arthroscopic Approaches to the Hip Joint; 10 Femur; 10.1 Anterior Approach; 10.2 Lateral Proximal Approach to the Medullary Cavity of the Femur; 10.3 Lateral Approach to the Femur 10.3a Lateral Approach-General Points |
| Record Nr. | UNINA-9910788022203321 |
Bauer Rudolf
|
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| Stuttgart, Germany : , : Thieme, , 2015 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Operative Approaches in Orthopedic Surgery and Traumatology / / by: Kerschbaumer, Fridun, Weise, Kuno, Wirth, Carl Joachim, Vaccaro, Alexander R.
| Operative Approaches in Orthopedic Surgery and Traumatology / / by: Kerschbaumer, Fridun, Weise, Kuno, Wirth, Carl Joachim, Vaccaro, Alexander R. |
| Autore | Bauer Rudolf |
| Edizione | [2nd ed.] |
| Pubbl/distr/stampa | Stuttgart, Germany : , : Thieme, , 2015 |
| Descrizione fisica | 1 online resource (416 p.) |
| Disciplina | 617.4/71 |
| Soggetto topico |
Orthopedics
Bones - Surgery Wounds and injuries - Surgery |
| ISBN | 3-13-258060-0 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Operative Approaches in Orthopedic Surgery and Traumatology; Title Page; Copyright; Contents; Foreword to the Second Edition; Foreword to the First Edition; Preface; Contributors; Spine, Anterior Approaches; 1 Cervical Spine and Cervicothoracic Junction; 1.1 Transoropharyngeal Approach C1-C2 (C3); 1.2 Anterior Approach to the Cervical Spine C3-T2; 1.3 Anterior Approach to the Lower Cervical and Upper Thoracic Spine C4-T3 According to Cauchoix, Binet, and Evrard; 2 Thoracic Spine; 2.1 Transthoracic Approach to the Thoracic Spine T4-T11
2.2 Anterior Transpleural Approach to the Spine T3-T11 According to Louis2.3 High Thoracotomy T1-T4; 2.4 Thoracoscopic and Minimally Invasive, Thoracoscopy-Assisted Access to the Thoracic Spine; 3 Thoracolumbar Junction; 3.1 Retroperitoneal Extrapleural Approach to the Thoracolumbar Spine T9-L5 According to Hodgson; 3.2 Approach to Thoracolumbar Spine with Two-fold Thoracotomy T4-L5 According to Bauer; 3.3 Retroperitoneal Extrapleural Approach to Thoracolumbar Spine T11-L5 According to Mirbaha; 4 Lumbar Spine and Lumbosacral Junction; 4.1 Retroperitoneal Approach to the Lumbar Spine L2-L5 4.2 Transperitoneal Approach to the Lumbosacral Junction L4-S14.3 Minimally Invasive Lateral Approach to the Lumbar Spine L2-L5; Spine, Posterior Approaches; 5 Cervical Spine; 5.1 Posterior Approach to the Cervical Spine and Occipitocervical Junction; 6 Thoracic and Lumbar Spine; 6.1 Costotransversectomy T3-T10; 6.2 Posterior Approach to the Thoracic and Lumbar Spine; 6.3 Paraspinal Approach to the Lumbosacral Junction According to Wiltse; 6.4 Short Posterior Approach to the Lumbar Spine for Laminotomy and Removal of an Intervertebral Disk; Pelvis and Lower Extremity; 7 Pelvis: Pelvic Ring 7.1 Approach to the Symphysis and Anterior Pelvis7.2 Anterior Approach to the Posterior Pelvis; 7.3 Posterior Approach to the Sacrum; 7.4 Lateral Minimally Invasive Approach for Trans-sacroiliac Screw Placement; 7.5 Approach to the Ischium and Pubis; 8 Pelvis: Acetabulum; 8.1 Ilioinguinal Approach According to Letournel; 8.2 Posterior Approach to the Hip According to Kocher-Langenbeck; 8.3 Anterior Limited Approach According to Stoppa; 8.4 Transiliac Approach According to Judet; 8.5 Approach to the Acetabulum According to Judet; 9 Hip Joint 9.1 Posterior Approach to the Hip Joint with Dislocation According to Ganz9.2 Posterior Minimally Invasive Approach; 9.3 Transgluteal Approach According to Bauer; 9.4 Minimally Invasive Transgluteal Approach; 9.5 Anterolateral Approach to the Hip Joint; 9.6 Minimally Invasive Anterolateral Approach to the Hip Joint; 9.7 Anterior Approach to the Hip Joint; 9.8 Anterior Minimally Invasive Approach; 9.9 Arthroscopic Approaches to the Hip Joint; 10 Femur; 10.1 Anterior Approach; 10.2 Lateral Proximal Approach to the Medullary Cavity of the Femur; 10.3 Lateral Approach to the Femur 10.3a Lateral Approach-General Points |
| Record Nr. | UNINA-9910821927503321 |
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Bauer Rudolf
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| Stuttgart, Germany : , : Thieme, , 2015 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
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Organic synthesis highlights V / / edited by Hans-Cunther Schmalz and Thomas Wirth
| Organic synthesis highlights V / / edited by Hans-Cunther Schmalz and Thomas Wirth |
| Pubbl/distr/stampa | Weinheim, [Germany] : , : Wiley-VCH, , 2003 |
| Descrizione fisica | 1 online resource (454 p.) |
| Disciplina | 547.2 |
| Soggetto topico | Organic compounds - Synthesis |
| Soggetto genere / forma | Electronic books. |
| ISBN |
1-281-84284-2
9786611842840 3-527-61998-4 3-527-62049-4 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Organic Synthesis Highlights V; Contents; Preface; List of Contributors; Part I. Synthetic Methods; Direct Conversion of Sugar Glycosides into Carbocycles; Synthesis of Diaryl Ethers: A Long-standing Problem Has Been Solved; Take The Right Catalyst: Palladium-Catalyzed CC-, CN- and CO-Bond Formation on Chloro-Arenes; Alkyne Metathesis in Natural Product Synthesis; Transition Metal-Catalyzed Functionalization of Alkanes; An Eldorado for Homogeneous Catalysis?; New and Selective Transition Metal Catalyzed Reactions of Allenes
Controlling Stereoselectivity with the Aid of a Reagent-Directing GroupSolvent-Free Organic Syntheses; Fluorous Techniques: Progress in Reaction-Processing and Purification; Recent Developments in Using Ionic Liquids as Solvents and Catalysts for Organic Synthesis; Recent Advances on the Sharpless Asymmetric Aminohydroxylation; Asymmetric Phase Transfer Catalysis; Asymmetric Catalytic Aminoalkylations: New Powerful Methods for the Enantioselective Synthesis of Amino Acid Derivatives, Mannich Bases, and Homoallylic Amines; IBX - New Reactions with an Old Reagent; Parallel Kinetic Resolutions The Asymmetric Baylis-Hillman-ReactionSimple Amino Acids and Short-Chain Peptides as Efficient Metal-free Catalysts in Asymmetric Synthesis; Recent Developments in Catalytic Asymmetric Strecker-Type Reactions; Highly Enantioselective or Not? - Chiral Monodentate Monophosphorus Ligands in the Asymmetric Hydrogenation; Improving Enantioselective Fluorination Reactions: Chiral N-Fluoro Ammonium Salts and Transition Metal Catalysts; Catalytic Asymmetric Olefin Metathesis; Activating Protecting Groups for the Solid Phase Synthesis and Modification of Peptides, Oligonucleotides and Oligosaccharides Traceless Linkers for Solid-Phase Organic SynthesisMerging Solid-Phase and Solution-Phase Synthesis: The "Resin-Capture-Release" Hybrid Technique; Polymeric Scavenger Reagents in Organic Synthesis; Part II. Applications; Total Syntheses of Vancomycin; Bryostatin and Their Analogues; Eleutherobin: Synthesis, Structure/Activity Relationship, and Pharmacophore; Total Synthesis of the Natural Products CP-263,114 and CP-225,917; Polyene Cyclization to Adociasulfate 1; Sanglifehrin A: an Immunosuppressant Natural Product from Malawi; Short Syntheses of the Spirotryprostatins The Chemical Total Synthesis of ProteinsSolid-Phase Synthesis of Oligosaccharides; Polymer-Supported Synthesis of Non-Oligomeric Natural Products; Explosions as a Synthetic Tool? Cycloalkynes as Precursors to Fullerenes, Buckytubes and Buckyonions; Dendralenes: From a Neglected Class of Polyenes to Versatile Starting Materials in Organic Synthesis; Fascinating Natural and Artificial Cyclopropane Architectures; Index |
| Record Nr. | UNINA-9910144123403321 |
| Weinheim, [Germany] : , : Wiley-VCH, , 2003 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||