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Mass spectrometry for the analysis of pesticide residues and their metabolites / / edited by Despina Tsipi, Helen Botitsi, Anastasios Economou
| Mass spectrometry for the analysis of pesticide residues and their metabolites / / edited by Despina Tsipi, Helen Botitsi, Anastasios Economou |
| Pubbl/distr/stampa | Hoboken, New Jersey : , : John Wiley & Sons, Inc., , 2015 |
| Descrizione fisica | 1 online resource (291 p.) |
| Disciplina | 632/.95 |
| Collana |
Wiley Series on Mass Spectrometry
THEi Wiley ebooks |
| Soggetto topico |
Pesticides - Analysis
Mass spectrometry |
| ISBN |
1-119-07000-7
1-119-07077-5 |
| Formato | Materiale a stampa  |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Title Page; Copyright Page; Contents; List of Contributors; Foreword; Preface; Chapter 1 Pesticide Chemistry and Risk Assessment; 1.1 INTRODUCTION; 1.2 PESTICIDE CHEMISTRY; 1.2.1 Historical Perspective; 1.2.2 Identity and Physicochemical Properties of Pesticides; 1.2.3 Pesticide Classification; 1.2.4 Modes of Action (MoA); 1.3 PESTICIDE METABOLITES AND TRANSFORMATION PRODUCTS; 1.3.1 Biotransformation; 1.3.2 Environmental Fate; 1.4 RISK ASSESSMENT; 1.4.1 Safety Factors; 1.4.2 Ecological Risk Assessment for Pesticides; 1.5 DIETARY EXPOSURE TO PESTICIDES
1.5.1 Acute Exposure or Short-Term Intake 1.5.2 Chronic Exposure or Long-Term Intake; 1.5.3 Cumulative Exposure to Multiple Substances; 1.6 PESTICIDE RESIDUES IN FOOD; 1.6.1 Maximum Residue Limits; 1.6.2 Residue Definition; 1.6.3 Reporting of Results; 1.6.4 Residue Analysis; REFERENCES; Chapter 2 Legislation, Monitoring, and Analytical Quality Control for Pesticide Residues; 2.1 INTRODUCTION; 2.2 FOOD SAFETY; 2.2.1 CAC of Food and Agriculture Organization/World Health Organization; 2.2.2 EU Legislation; 2.2.3 US Food Regulations; 2.3 WATER QUALITY; 2.3.1 WHO; 2.3.2 EU Water Framework Directive 2.3.3 US EPA Legislation 2.4 METHOD VALIDATION AND QUALITY CONTROL PROCEDURES FOR PESTICIDE RESIDUES ANALYSIS; 2.4.1 CAC Guidelines; 2.4.2 EU Guidelines: SANCO Document; 2.4.3 FDA and EPA Guidelines; REFERENCES; Chapter 3 Advanced Sample Preparation Techniques for MS Analysis; 3.1 INTRODUCTION; 3.2 CONVENTIONAL EXTRACTION AND CLEANUP PROCEDURES; 3.2.1 LLE; 3.2.2 SPE; 3.2.3 MSPD; 3.2.4 QuEChERS; 3.3 MICROEXTRACTION TECHNIQUES; 3.3.1 Sorbent-Based Microextraction Techniques; 3.3.2 Liquid-Based Microextraction Techniques; 3.4 ALTERNATIVE EXTRACTION AND CLEANUP PROCEDURES 3.4.1 Alternative Energy Sources to Enhance the Extraction 3.4.2 Coupled-Column Liquid Chromatography (LC/PC, LC/LC Techniques); 3.4.3 Direct Analysis in Real Time; 3.5 CONCLUSIONS; ACKNOWLEDGMENTS; REFERENCES; Chapter 4 Recent Developments in Gas Chromatography-Mass Spectrometry; 4.1 INTRODUCTION; 4.2 ADVANCES IN GC SEPARATIONS; 4.2.1 Multidimensional and Comprehensive Two-Dimensional Gas Chromatography; 4.2.2 Fast GC; 4.2.3 LPGC; 4.3 MASS SPECTROMETRIC IONIZATION TECHNIQUES; 4.3.1 Electron Impact Ionization (EI); 4.3.2 CI (Positive/Negative Modes); 4.3.3 Atmospheric Pressure GC-MS 4.4 MASS ANALYZERS INTERFACED TO GC 4.4.1 Quadrupole Mass Analyzer; 4.4.2 Ion Trap Mass Analyzer; 4.4.3 QqQ; 4.4.4 TOF; 4.5 MASS SPECTRAL LIBRARIES AND SOFTWARE APPROACHES IN GC-MS ANALYSIS; 4.6. MATRIX EFFECTS IN GC-MS ANALYSIS; 4.7 CONCLUSIONS AND PERSPECTIVES; REFERENCES; Chapter 5 Recent Developments in Liquid Chromatography-Mass Spectrometry: Advances in Liquid Chromatographic Separations and Ionization Techniques/Interfaces; 5.1 INTRODUCTION; 5.2 ADVANCES IN LIQUID CHROMATOGRAPHIC SEPARATIONS; 5.2.1 Ultraperformance Liquid Chromatography 5.2.2 Hydrophilic Interaction Liquid Chromatography |
| Record Nr. | UNINA-9910140644103321 |
| Hoboken, New Jersey : , : John Wiley & Sons, Inc., , 2015 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Mass spectrometry for the analysis of pesticide residues and their metabolites / / edited by Despina Tsipi, Helen Botitsi, Anastasios Economou
| Mass spectrometry for the analysis of pesticide residues and their metabolites / / edited by Despina Tsipi, Helen Botitsi, Anastasios Economou |
| Pubbl/distr/stampa | Hoboken, New Jersey : , : John Wiley & Sons, Inc., , 2015 |
| Descrizione fisica | 1 online resource (291 p.) |
| Disciplina | 632/.95 |
| Collana |
Wiley Series on Mass Spectrometry
THEi Wiley ebooks |
| Soggetto topico |
Pesticides - Analysis
Mass spectrometry |
| ISBN |
1-119-07000-7
1-119-07077-5 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Title Page; Copyright Page; Contents; List of Contributors; Foreword; Preface; Chapter 1 Pesticide Chemistry and Risk Assessment; 1.1 INTRODUCTION; 1.2 PESTICIDE CHEMISTRY; 1.2.1 Historical Perspective; 1.2.2 Identity and Physicochemical Properties of Pesticides; 1.2.3 Pesticide Classification; 1.2.4 Modes of Action (MoA); 1.3 PESTICIDE METABOLITES AND TRANSFORMATION PRODUCTS; 1.3.1 Biotransformation; 1.3.2 Environmental Fate; 1.4 RISK ASSESSMENT; 1.4.1 Safety Factors; 1.4.2 Ecological Risk Assessment for Pesticides; 1.5 DIETARY EXPOSURE TO PESTICIDES
1.5.1 Acute Exposure or Short-Term Intake 1.5.2 Chronic Exposure or Long-Term Intake; 1.5.3 Cumulative Exposure to Multiple Substances; 1.6 PESTICIDE RESIDUES IN FOOD; 1.6.1 Maximum Residue Limits; 1.6.2 Residue Definition; 1.6.3 Reporting of Results; 1.6.4 Residue Analysis; REFERENCES; Chapter 2 Legislation, Monitoring, and Analytical Quality Control for Pesticide Residues; 2.1 INTRODUCTION; 2.2 FOOD SAFETY; 2.2.1 CAC of Food and Agriculture Organization/World Health Organization; 2.2.2 EU Legislation; 2.2.3 US Food Regulations; 2.3 WATER QUALITY; 2.3.1 WHO; 2.3.2 EU Water Framework Directive 2.3.3 US EPA Legislation 2.4 METHOD VALIDATION AND QUALITY CONTROL PROCEDURES FOR PESTICIDE RESIDUES ANALYSIS; 2.4.1 CAC Guidelines; 2.4.2 EU Guidelines: SANCO Document; 2.4.3 FDA and EPA Guidelines; REFERENCES; Chapter 3 Advanced Sample Preparation Techniques for MS Analysis; 3.1 INTRODUCTION; 3.2 CONVENTIONAL EXTRACTION AND CLEANUP PROCEDURES; 3.2.1 LLE; 3.2.2 SPE; 3.2.3 MSPD; 3.2.4 QuEChERS; 3.3 MICROEXTRACTION TECHNIQUES; 3.3.1 Sorbent-Based Microextraction Techniques; 3.3.2 Liquid-Based Microextraction Techniques; 3.4 ALTERNATIVE EXTRACTION AND CLEANUP PROCEDURES 3.4.1 Alternative Energy Sources to Enhance the Extraction 3.4.2 Coupled-Column Liquid Chromatography (LC/PC, LC/LC Techniques); 3.4.3 Direct Analysis in Real Time; 3.5 CONCLUSIONS; ACKNOWLEDGMENTS; REFERENCES; Chapter 4 Recent Developments in Gas Chromatography-Mass Spectrometry; 4.1 INTRODUCTION; 4.2 ADVANCES IN GC SEPARATIONS; 4.2.1 Multidimensional and Comprehensive Two-Dimensional Gas Chromatography; 4.2.2 Fast GC; 4.2.3 LPGC; 4.3 MASS SPECTROMETRIC IONIZATION TECHNIQUES; 4.3.1 Electron Impact Ionization (EI); 4.3.2 CI (Positive/Negative Modes); 4.3.3 Atmospheric Pressure GC-MS 4.4 MASS ANALYZERS INTERFACED TO GC 4.4.1 Quadrupole Mass Analyzer; 4.4.2 Ion Trap Mass Analyzer; 4.4.3 QqQ; 4.4.4 TOF; 4.5 MASS SPECTRAL LIBRARIES AND SOFTWARE APPROACHES IN GC-MS ANALYSIS; 4.6. MATRIX EFFECTS IN GC-MS ANALYSIS; 4.7 CONCLUSIONS AND PERSPECTIVES; REFERENCES; Chapter 5 Recent Developments in Liquid Chromatography-Mass Spectrometry: Advances in Liquid Chromatographic Separations and Ionization Techniques/Interfaces; 5.1 INTRODUCTION; 5.2 ADVANCES IN LIQUID CHROMATOGRAPHIC SEPARATIONS; 5.2.1 Ultraperformance Liquid Chromatography 5.2.2 Hydrophilic Interaction Liquid Chromatography |
| Record Nr. | UNINA-9910815220103321 |
| Hoboken, New Jersey : , : John Wiley & Sons, Inc., , 2015 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||