Info
- Utilizzare la checkbox di selezione a fianco di ciascun documento per attivare le funzionalità di stampa, invio email, download nei formati disponibili del (i) record.
Understanding mass spectra [[electronic resource] ] : a basic approach / / R. Martin Smith
| Understanding mass spectra [[electronic resource] ] : a basic approach / / R. Martin Smith |
| Autore | Smith R. Martin |
| Edizione | [2nd ed.] |
| Pubbl/distr/stampa | Hoboken, N.J., : Wiley Interscience, c2004 |
| Descrizione fisica | 1 online resource (394 p.) |
| Disciplina |
543
543.0873 543/.0873 |
| Soggetto topico | Mass spectrometry |
| ISBN |
1-280-26487-X
9786610264872 0-470-25207-3 0-471-47934-9 0-471-47935-7 |
| Formato | Materiale a stampa  |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
UNDERSTANDING MASS SPECTRA Second Edition; CONTENTS; Preface to the Second Edition; Acknowledgments; Abbreviations and Notations Used in This Book; 1 Instrumentation; 1.1. Introduction; 1.1.1. Overview; 1.1.2. Sample Introduction; 1.2. Ionization Source; 1.2.1. Electron Ionization Source; 1.2.2. Chemical Ionization; 1.2.3. Other Ionization Methods; 1.2.3.1. Electrospray Ionization; 1.2.3.2. Desorption Ionization; 1.3. m/z Analysis; 1.3.1. Time-of-Flight (TOF); 1.3.2. Magnetic Sector; 1.3.3. Transmission Quadrupole; 1.3.3.1. Selected Ion Monitoring (SIM); 1.3.4. Quadrupole Ion Trap (QIT)
1.3.5. Other Types of Mass Analysis1.3.5.1. Mass Spectrometry/Mass Spectrometry(MS/MS); 1.3.5.2. Accurate m/z Analysis; 1.3.6. Spectral Skewing; 1.4. Ion Detection; 1.4.1. Electron Multiplier; 1.4.2. Photomultiplier Detector; 1.5. Data System; 1.5.1. Instrument Tuning and Calibration; 1.5.2. The Mass Spectrum; 1.5.2.1. Production of the Mass Spectrum; 1.5.2.2. Terminology: Ions vs. Peaks; 1.5.3. Library Searches; 1.5.4. Using the Data System to Analyze GC/MS Data; 1.6. Criteria for Good-Quality Spectra; Additional Problems; Mass Spectrometric Resources on the Internet References and Suggested Reading2 Elemental Composition from Peak Intensities; 2.1. Natural Isotopic Abundances; 2.1.1. Atomic and Molecular Mass; 2.1.2. Calculated Exact Masses and Mass Defects; 2.2. Determining Elemental Composition from Isotope Peak Intensities; 2.2.1. One or More Atoms of a Single Element; 2.2.1.1. Chlorine and Bromine; 2.2.1.2. Ion Designation and Nomenclature; 2.2.1.3. Probability Considerations with Multiple Numbers of Atoms; 2.2.1.4. Isotope Peak Intensity Ratios for Carbon-Containing Ions-The X + 1 Peak; 2.2.1.5. A, A + 1, and A + 2 Elements 2.2.1.6 Isotope Peak Intensity Ratios for Carbon-Containing Ions-The X + 2 Peak2.2.1.7. Overlapping Peak Clusters-Contributions from (13)C Only; 2.2.1.8. Silicon; 2.2.2. Complex Isotope Clusters; 2.2.2.1. Sulfur Dioxide; 2.2.2.2. Diazepam; 2.3. Obtaining Elemental Compositions from Isotope Peak Intensities; Examples; Additional Problems; References; 3 Ionization, Fragmentation, and Electron Accounting; 3.1. A Brief Review of Orbitals and Bonding; 3.2. Even- and Odd-Electron Species; 3.3. Site of Initial Ionization; 3.4. Types of Fragmentation; 3.5. The Nitrogen Rule 3.6. Energy Considerations in Fragmentation Processes3.6.1. Fragmentation Rates; 3.6.2. Metastable Ions; 3.6.3. Energy Diagrams; 3.6.4. Stevenson's Rule; Additional Examples; Problems; References; 4 Neutral Losses and Ion Series; 4.1. Neutral Losses; 4.1.1. Losses from the Molecular Ion; 4.1.2. Loss of Small Molecules from Aromatic Ions; 4.2. Low-Mass Ion Series; 4.2.1. n-Alkane Spectra; 4.2.2. Effect of Chain Branching on the Spectra of Aliphatic Hydrocarbons; 4.2.3. Ion Series for Nonaromatic Compounds; 4.2.4. Aromatic Ion Series; 4.2.5. Use of Ion Series: Mass Chromatograms Additional Problems |
| Record Nr. | UNINA-9910146065903321 |
Smith R. Martin
|
||
| Hoboken, N.J., : Wiley Interscience, c2004 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Understanding mass spectra [[electronic resource] ] : a basic approach / / R. Martin Smith
| Understanding mass spectra [[electronic resource] ] : a basic approach / / R. Martin Smith |
| Autore | Smith R. Martin |
| Edizione | [2nd ed.] |
| Pubbl/distr/stampa | Hoboken, N.J., : Wiley Interscience, c2004 |
| Descrizione fisica | 1 online resource (394 p.) |
| Disciplina |
543
543.0873 543/.0873 |
| Soggetto topico | Mass spectrometry |
| ISBN |
1-280-26487-X
9786610264872 0-470-25207-3 0-471-47934-9 0-471-47935-7 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
UNDERSTANDING MASS SPECTRA Second Edition; CONTENTS; Preface to the Second Edition; Acknowledgments; Abbreviations and Notations Used in This Book; 1 Instrumentation; 1.1. Introduction; 1.1.1. Overview; 1.1.2. Sample Introduction; 1.2. Ionization Source; 1.2.1. Electron Ionization Source; 1.2.2. Chemical Ionization; 1.2.3. Other Ionization Methods; 1.2.3.1. Electrospray Ionization; 1.2.3.2. Desorption Ionization; 1.3. m/z Analysis; 1.3.1. Time-of-Flight (TOF); 1.3.2. Magnetic Sector; 1.3.3. Transmission Quadrupole; 1.3.3.1. Selected Ion Monitoring (SIM); 1.3.4. Quadrupole Ion Trap (QIT)
1.3.5. Other Types of Mass Analysis1.3.5.1. Mass Spectrometry/Mass Spectrometry(MS/MS); 1.3.5.2. Accurate m/z Analysis; 1.3.6. Spectral Skewing; 1.4. Ion Detection; 1.4.1. Electron Multiplier; 1.4.2. Photomultiplier Detector; 1.5. Data System; 1.5.1. Instrument Tuning and Calibration; 1.5.2. The Mass Spectrum; 1.5.2.1. Production of the Mass Spectrum; 1.5.2.2. Terminology: Ions vs. Peaks; 1.5.3. Library Searches; 1.5.4. Using the Data System to Analyze GC/MS Data; 1.6. Criteria for Good-Quality Spectra; Additional Problems; Mass Spectrometric Resources on the Internet References and Suggested Reading2 Elemental Composition from Peak Intensities; 2.1. Natural Isotopic Abundances; 2.1.1. Atomic and Molecular Mass; 2.1.2. Calculated Exact Masses and Mass Defects; 2.2. Determining Elemental Composition from Isotope Peak Intensities; 2.2.1. One or More Atoms of a Single Element; 2.2.1.1. Chlorine and Bromine; 2.2.1.2. Ion Designation and Nomenclature; 2.2.1.3. Probability Considerations with Multiple Numbers of Atoms; 2.2.1.4. Isotope Peak Intensity Ratios for Carbon-Containing Ions-The X + 1 Peak; 2.2.1.5. A, A + 1, and A + 2 Elements 2.2.1.6 Isotope Peak Intensity Ratios for Carbon-Containing Ions-The X + 2 Peak2.2.1.7. Overlapping Peak Clusters-Contributions from (13)C Only; 2.2.1.8. Silicon; 2.2.2. Complex Isotope Clusters; 2.2.2.1. Sulfur Dioxide; 2.2.2.2. Diazepam; 2.3. Obtaining Elemental Compositions from Isotope Peak Intensities; Examples; Additional Problems; References; 3 Ionization, Fragmentation, and Electron Accounting; 3.1. A Brief Review of Orbitals and Bonding; 3.2. Even- and Odd-Electron Species; 3.3. Site of Initial Ionization; 3.4. Types of Fragmentation; 3.5. The Nitrogen Rule 3.6. Energy Considerations in Fragmentation Processes3.6.1. Fragmentation Rates; 3.6.2. Metastable Ions; 3.6.3. Energy Diagrams; 3.6.4. Stevenson's Rule; Additional Examples; Problems; References; 4 Neutral Losses and Ion Series; 4.1. Neutral Losses; 4.1.1. Losses from the Molecular Ion; 4.1.2. Loss of Small Molecules from Aromatic Ions; 4.2. Low-Mass Ion Series; 4.2.1. n-Alkane Spectra; 4.2.2. Effect of Chain Branching on the Spectra of Aliphatic Hydrocarbons; 4.2.3. Ion Series for Nonaromatic Compounds; 4.2.4. Aromatic Ion Series; 4.2.5. Use of Ion Series: Mass Chromatograms Additional Problems |
| Record Nr. | UNINA-9910830551103321 |
|
Smith R. Martin
|
||
| Hoboken, N.J., : Wiley Interscience, c2004 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Understanding mass spectra [[electronic resource] ] : a basic approach / / R. Martin Smith
| Understanding mass spectra [[electronic resource] ] : a basic approach / / R. Martin Smith |
| Autore | Smith R. Martin |
| Edizione | [2nd ed.] |
| Pubbl/distr/stampa | Hoboken, N.J., : Wiley Interscience, c2004 |
| Descrizione fisica | 1 online resource (394 p.) |
| Disciplina |
543
543.0873 543/.0873 |
| Soggetto topico | Mass spectrometry |
| ISBN |
1-280-26487-X
9786610264872 0-470-25207-3 0-471-47934-9 0-471-47935-7 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
UNDERSTANDING MASS SPECTRA Second Edition; CONTENTS; Preface to the Second Edition; Acknowledgments; Abbreviations and Notations Used in This Book; 1 Instrumentation; 1.1. Introduction; 1.1.1. Overview; 1.1.2. Sample Introduction; 1.2. Ionization Source; 1.2.1. Electron Ionization Source; 1.2.2. Chemical Ionization; 1.2.3. Other Ionization Methods; 1.2.3.1. Electrospray Ionization; 1.2.3.2. Desorption Ionization; 1.3. m/z Analysis; 1.3.1. Time-of-Flight (TOF); 1.3.2. Magnetic Sector; 1.3.3. Transmission Quadrupole; 1.3.3.1. Selected Ion Monitoring (SIM); 1.3.4. Quadrupole Ion Trap (QIT)
1.3.5. Other Types of Mass Analysis1.3.5.1. Mass Spectrometry/Mass Spectrometry(MS/MS); 1.3.5.2. Accurate m/z Analysis; 1.3.6. Spectral Skewing; 1.4. Ion Detection; 1.4.1. Electron Multiplier; 1.4.2. Photomultiplier Detector; 1.5. Data System; 1.5.1. Instrument Tuning and Calibration; 1.5.2. The Mass Spectrum; 1.5.2.1. Production of the Mass Spectrum; 1.5.2.2. Terminology: Ions vs. Peaks; 1.5.3. Library Searches; 1.5.4. Using the Data System to Analyze GC/MS Data; 1.6. Criteria for Good-Quality Spectra; Additional Problems; Mass Spectrometric Resources on the Internet References and Suggested Reading2 Elemental Composition from Peak Intensities; 2.1. Natural Isotopic Abundances; 2.1.1. Atomic and Molecular Mass; 2.1.2. Calculated Exact Masses and Mass Defects; 2.2. Determining Elemental Composition from Isotope Peak Intensities; 2.2.1. One or More Atoms of a Single Element; 2.2.1.1. Chlorine and Bromine; 2.2.1.2. Ion Designation and Nomenclature; 2.2.1.3. Probability Considerations with Multiple Numbers of Atoms; 2.2.1.4. Isotope Peak Intensity Ratios for Carbon-Containing Ions-The X + 1 Peak; 2.2.1.5. A, A + 1, and A + 2 Elements 2.2.1.6 Isotope Peak Intensity Ratios for Carbon-Containing Ions-The X + 2 Peak2.2.1.7. Overlapping Peak Clusters-Contributions from (13)C Only; 2.2.1.8. Silicon; 2.2.2. Complex Isotope Clusters; 2.2.2.1. Sulfur Dioxide; 2.2.2.2. Diazepam; 2.3. Obtaining Elemental Compositions from Isotope Peak Intensities; Examples; Additional Problems; References; 3 Ionization, Fragmentation, and Electron Accounting; 3.1. A Brief Review of Orbitals and Bonding; 3.2. Even- and Odd-Electron Species; 3.3. Site of Initial Ionization; 3.4. Types of Fragmentation; 3.5. The Nitrogen Rule 3.6. Energy Considerations in Fragmentation Processes3.6.1. Fragmentation Rates; 3.6.2. Metastable Ions; 3.6.3. Energy Diagrams; 3.6.4. Stevenson's Rule; Additional Examples; Problems; References; 4 Neutral Losses and Ion Series; 4.1. Neutral Losses; 4.1.1. Losses from the Molecular Ion; 4.1.2. Loss of Small Molecules from Aromatic Ions; 4.2. Low-Mass Ion Series; 4.2.1. n-Alkane Spectra; 4.2.2. Effect of Chain Branching on the Spectra of Aliphatic Hydrocarbons; 4.2.3. Ion Series for Nonaromatic Compounds; 4.2.4. Aromatic Ion Series; 4.2.5. Use of Ion Series: Mass Chromatograms Additional Problems |
| Record Nr. | UNINA-9910841065503321 |
|
Smith R. Martin
|
||
| Hoboken, N.J., : Wiley Interscience, c2004 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||