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Iron oxides in the laboratory : preparation and characterization / / U. Schwertmann, R.M. Cornell
| Iron oxides in the laboratory : preparation and characterization / / U. Schwertmann, R.M. Cornell |
| Autore | Schwertmann Udo |
| Edizione | [Second, completely revised and extended edition.] |
| Pubbl/distr/stampa | Weinheim, [Germany] : , : Wiley-VCH, , 2000 |
| Descrizione fisica | 1 online resource (209 p.) |
| Disciplina |
546.6212
546/.6212 |
| Soggetto topico | Iron oxides |
| Soggetto genere / forma | Electronic books. |
| ISBN |
1-281-84246-X
9786611842468 3-527-61322-6 3-527-61323-4 |
| Formato | Materiale a stampa  |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Iron Oxides in the Laboratory; Contents; Introduction; 1 The Iron Oxides; 1.1 The Major Iron Oxides; 1.2 Less Conmon or Rare Iron Oxides; 1.3 Iron Oxides in the Environment; 2 General Preparative Techniques; 2.1 Quantity of Product; 2.2 Treatment after Synthesis; 2.2.1 Washing; 2.2.2 Drying; 2.2.3 Storage; 2.3 Chemical Analysis; 2.3.1 Total Analysis; 2.3.2 Extent of Isomorphous Substitution; 2.3.3 Impurities; 2.4 Removal of Iron Oxides from Reaction Vessels; 2.5 Purity of Reagents; 3 Methods of Characterization; 3.1 Introduction; 3.2 Color (A. Scheinost); 3.2.1 Origin of Color
3.2.2 Color Measurement3.2.3 Color Systems; 3.2.4 Identification of Iron Oxides by Color and Crystal-Field Bands; 3.3 X-Ray Powder Diffraction; 3.4 Microscopy; 3.5 Surface Area, Porosity and Fractal Dimensions; 3.6 Acid Oxalate Extraction; 3.7 Infrared Spectroscopy; 3.8 Thermoanalysis; 3.9 Mössbauer Spectroscopy; 4 Synthesis Pathways; 4.1 Nucleation and Crystal Growth; 4.1.1 Nucleation; 4.1.2 Crystal Growth; 4.1.3 Production of Monodispersed Particles; 4.1.4 Production of Nanoparticles; 4.2 Main Routes of Synthesis; 4.2.1 Hydrolysis of Acidic Solutions of FeIII Salts 4.2.2 Transformation of Ferrihydrite4.2.3 Oxidative Hydrolysis of FeII Salts; 4.2.4 Phase Transformations; 4.2.5 The Gel-Sol Method; 4.2.6 Hydrothermal Precipitation; 4.2.7 Decomposition of Metal Chelates; 5 Goethite; 5.1 Introductions; 5.2 Pure Goethite from FeIII Systems; 5.2.1 Preparation from an Alkaline System (acc. to Böhm. 1925); 5.2.2 Preparation fiom an Acid System (acc. to Mørup et al., 1983); 5.2.3 Preparation From a Cysteine/2-line Ferrihydrite System; 5.3 Pure Goethite from an FeII System; 5.4 General Comments; 5.5 Metal (M)-Substituted Goethites Fe1-xMx OOH 5.5.1 Al-Substituted Goethite Fe1-xAIxOOH5.5.1.1 Preparation from an Alkaline FeIII Systemn; 5.5.1.2 Preparation from an FeII-System; 5.5.2 Cr-Substituted Goethite Fe1-x CrxOOH; 5.5.3 Mn-Substituted Goethite Fe1-x MnxOOH; 5.5.4 V-Substituted Goethite Fe1-x VxOOH; 6 Lepidocrocite; 6.1 Introduction; 6.2 Preparation; 6.3 Other Methods; 7 Feroxyhyte; 7.1 Introduction; 7.2 Preparation; 8 Ferrihydrite; 8.1 Introduction; 8.2 6-Line Ferrihydrite; 8.3 2-Line Ferrihydrite; 8.4 Ferrihydrites with a Range of Crystallinities (acc. to D. G. Lewis); 9 Akaganéite; 9.1 Introduction 9.2 Preparation by Hydrolysis of Acidic FeCI3 Solutions (Somatoids)9.3 Preparation by Hydrolysis of a Partially Neutralized FeCl3 solution (Rod-like Crystals); 9.4 Si-containing Akaganéite; 10 Hematite; 10.1 Introduction; 10.2 Preparation by Forced Hydrolysis of FeIII Salt Solutions; 10.3 Preparation by Transformation of 2-Line Ferrihydrite; 10.4 Monodisperse Hematites of Different Crystal Shapes; 10.5 Other Methods; 10.6 Al-substituted Hematite; 10.7 Coated Hematite; 11 Magnetite; 11.1 Introduction; 11.2 Preparation by Oxidation of a FeII Solution; 11.3 Cation-substituted Magnetites 12 Maghemite |
| Record Nr. | UNINA-9910144332303321 |
Schwertmann Udo
|
||
| Weinheim, [Germany] : , : Wiley-VCH, , 2000 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Iron oxides in the laboratory : preparation and characterization / / U. Schwertmann, R.M. Cornell
| Iron oxides in the laboratory : preparation and characterization / / U. Schwertmann, R.M. Cornell |
| Autore | Schwertmann Udo |
| Edizione | [Second, completely revised and extended edition.] |
| Pubbl/distr/stampa | Weinheim, [Germany] : , : Wiley-VCH, , 2000 |
| Descrizione fisica | 1 online resource (209 p.) |
| Disciplina |
546.6212
546/.6212 |
| Soggetto topico | Iron oxides |
| ISBN |
1-281-84246-X
9786611842468 3-527-61322-6 3-527-61323-4 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Iron Oxides in the Laboratory; Contents; Introduction; 1 The Iron Oxides; 1.1 The Major Iron Oxides; 1.2 Less Conmon or Rare Iron Oxides; 1.3 Iron Oxides in the Environment; 2 General Preparative Techniques; 2.1 Quantity of Product; 2.2 Treatment after Synthesis; 2.2.1 Washing; 2.2.2 Drying; 2.2.3 Storage; 2.3 Chemical Analysis; 2.3.1 Total Analysis; 2.3.2 Extent of Isomorphous Substitution; 2.3.3 Impurities; 2.4 Removal of Iron Oxides from Reaction Vessels; 2.5 Purity of Reagents; 3 Methods of Characterization; 3.1 Introduction; 3.2 Color (A. Scheinost); 3.2.1 Origin of Color
3.2.2 Color Measurement3.2.3 Color Systems; 3.2.4 Identification of Iron Oxides by Color and Crystal-Field Bands; 3.3 X-Ray Powder Diffraction; 3.4 Microscopy; 3.5 Surface Area, Porosity and Fractal Dimensions; 3.6 Acid Oxalate Extraction; 3.7 Infrared Spectroscopy; 3.8 Thermoanalysis; 3.9 Mössbauer Spectroscopy; 4 Synthesis Pathways; 4.1 Nucleation and Crystal Growth; 4.1.1 Nucleation; 4.1.2 Crystal Growth; 4.1.3 Production of Monodispersed Particles; 4.1.4 Production of Nanoparticles; 4.2 Main Routes of Synthesis; 4.2.1 Hydrolysis of Acidic Solutions of FeIII Salts 4.2.2 Transformation of Ferrihydrite4.2.3 Oxidative Hydrolysis of FeII Salts; 4.2.4 Phase Transformations; 4.2.5 The Gel-Sol Method; 4.2.6 Hydrothermal Precipitation; 4.2.7 Decomposition of Metal Chelates; 5 Goethite; 5.1 Introductions; 5.2 Pure Goethite from FeIII Systems; 5.2.1 Preparation from an Alkaline System (acc. to Böhm. 1925); 5.2.2 Preparation fiom an Acid System (acc. to Mørup et al., 1983); 5.2.3 Preparation From a Cysteine/2-line Ferrihydrite System; 5.3 Pure Goethite from an FeII System; 5.4 General Comments; 5.5 Metal (M)-Substituted Goethites Fe1-xMx OOH 5.5.1 Al-Substituted Goethite Fe1-xAIxOOH5.5.1.1 Preparation from an Alkaline FeIII Systemn; 5.5.1.2 Preparation from an FeII-System; 5.5.2 Cr-Substituted Goethite Fe1-x CrxOOH; 5.5.3 Mn-Substituted Goethite Fe1-x MnxOOH; 5.5.4 V-Substituted Goethite Fe1-x VxOOH; 6 Lepidocrocite; 6.1 Introduction; 6.2 Preparation; 6.3 Other Methods; 7 Feroxyhyte; 7.1 Introduction; 7.2 Preparation; 8 Ferrihydrite; 8.1 Introduction; 8.2 6-Line Ferrihydrite; 8.3 2-Line Ferrihydrite; 8.4 Ferrihydrites with a Range of Crystallinities (acc. to D. G. Lewis); 9 Akaganéite; 9.1 Introduction 9.2 Preparation by Hydrolysis of Acidic FeCI3 Solutions (Somatoids)9.3 Preparation by Hydrolysis of a Partially Neutralized FeCl3 solution (Rod-like Crystals); 9.4 Si-containing Akaganéite; 10 Hematite; 10.1 Introduction; 10.2 Preparation by Forced Hydrolysis of FeIII Salt Solutions; 10.3 Preparation by Transformation of 2-Line Ferrihydrite; 10.4 Monodisperse Hematites of Different Crystal Shapes; 10.5 Other Methods; 10.6 Al-substituted Hematite; 10.7 Coated Hematite; 11 Magnetite; 11.1 Introduction; 11.2 Preparation by Oxidation of a FeII Solution; 11.3 Cation-substituted Magnetites 12 Maghemite |
| Record Nr. | UNINA-9910830538103321 |
|
Schwertmann Udo
|
||
| Weinheim, [Germany] : , : Wiley-VCH, , 2000 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||