Gas chromatography [[electronic resource] /] / Colin F. Poole |
Autore | Poole C. F |
Edizione | [1st ed.] |
Pubbl/distr/stampa | Amsterdam ; ; Boston, : Elsevier, 2012 |
Descrizione fisica | 1 online resource (753 p.) |
Disciplina | 543/.85 |
Soggetto topico |
Gas chromatography
Chromatographic analysis |
Soggetto genere / forma | Electronic books. |
ISBN |
1-280-77001-5
9786613680785 0-12-385541-1 |
Formato | Materiale a stampa |
Livello bibliografico | Monografia |
Lingua di pubblicazione | eng |
Nota di contenuto |
Front Cover; Gas Chromatography; Copyright; Contents; Contributors; Chapter 1 - Milestones in the Development of Gas Chromatography; 1.1.INTRODUCTION; 1.2.THE INVENTION OF GAS CHROMATOGRAPHY; 1.3.EARLY INSTRUMENTATION; 1.4.EARLY COLUMN DEVELOPMENTS; 1.5.INTERFACING GLASS CAPILLARY COLUMNS TO INJECTORS AND DETECTORS; 1.6.THE HINDELANG CONFERENCES AND THE FUSED-SILICA COLUMN; 1.7.INCREASING SOPHISTICATION OF INSTRUMENTATION; 1.8.DECLINE IN THE EXPERTISE OF THE AVERAGE GAS CHROMATOGRAPHER; References; Chapter 2 - Theory of Gas Chromatography; 2.1.INTRODUCTION
2.2.NOMENCLATURE AND OTHER CONVENTIONS 2.3.GENERAL DEFINITIONS; 2.4.SOLUTE-COLUMN INTERACTION; 2.5.PROPERTIES OF AN IDEAL GAS; 2.6.FLOW OF IDEAL GAS IN OPEN CIRCULAR TUBES; 2.7.MIGRATION AND ELUTION PARAMETERS OF THE SOLUTES; 2.8.PEAK SPACING AND REVERSAL OF PEAK ORDER; 2.9.PEAK WIDTH; 2.10.OPTIMIZATION; References; Chapter 3 - Column Technology: Open Tubular Columns; 3.1.INTRODUCTION; 3.2.OVERVIEW OF THE FUSED SILICA DRAWING PROCESS; 3.3.THE PREFORM - RAW MATERIAL; 3.4.SURFACE CHEMISTRY; 3.5.DRAWING OF THE CAPILLARY FROM THE PREFORM; 3.6.PROTECTIVE COATING; 3.7.ALTERNATIVE PROTECTIVE COATINGS 3.8. CLEAN ROOM ENVIRONMENT 3.9.QUALITY MONITORING; 3.10.OBSERVATIONS ON HANDLING OF FUSED-SILICA CAPILLARY TUBING; 3.11.COLUMN TECHNOLOGY - COATING THE STATIONARY PHASE; 3.12.STATIONARY PHASES; 3.13.COATING TECHNIQUES; 3.14.COLUMN TECHNOLOGY - QUALITY EVALUATION; 3.15.COLUMN TECHNOLOGY - SUMMARY; References; Chapter 4- Packed Columns for Gas-Liquid and Gas-Solid Chromatography; 4.1.INTRODUCTION; 4.2.GAS-LIQUID CHROMATOGRAPHY; 4.3.GAS-SOLID CHROMATOGRAPHY; References; Chapter 5 - Gas-Solid Chromatography (PLOT Columns); 5.1.ALUMINA ADSORBENTS; 5.2.MOLECULAR SIEVES; 5.3.POROUS POLYMERS 5.4.CARBON ADSORBENTS 5.5.OTHER ADSORBENTS; References; Chapter 6- Classification and Selection of Open-Tubular Columns for Analytical Separations; 6.1.INTRODUCTION; 6.2.STATIONARY-PHASE CLASSIFICATION; 6.3.POROUS-LAYER OPEN-TUBULAR COLUMNS; 6.4.TEMPERATURE-PROGRAMMED SEPARATIONS; 6.5.STATIONARY-PHASE SELECTIVITY TUNING; References; Chapter 7 - Multidimensional and Comprehensive Gas Chromatography; 7.1.INTRODUCTION; 7.2.A GRAPHICAL REPRESENTATION OF 2D GC SEPARATIONS; 7.3 .BACK FLUSHING 2D GC; 7.4.HEART CUTTING 2D GC; 7.5.COMPREHENSIVE 2D GC; 7.6.CONCLUSIONS; References Chapter 8 - Sample Introduction Methods 8.1.INTRODUCTION; 8.2.CHOOSING A SAMPLE INTRODUCTION SYSTEM; 8.3.SUPPORTING DEVICES; 8.4.THE COLD ON-COLUMN INJECTOR; 8.5.THE FLASH VAPORIZATION INJECTOR; 8.6.THE SPLIT/SPLITLESS INJECTOR; 8.7.THE PROGRAMMABLE TEMPERATURE VAPORIZING (PTV) INJECTOR; 8.8.THE GAS SAMPLING VALVE; 8.9.THE LIQUID SAMPLING VALVE; References; Chapter 9 - Head space-Gas Chromatography; 9.1.INTRODUCTION AND HISTORY; 9.2.FUNDAMENTALS OF HEAD SPACE EXTRACTION; 9.3.INSTRUMENTATION AND PRACTICE; 9.4.METHOD DEVELOPMENT CONSIDERATIONS; 9.5.CONCLUSIONS; References Chapter 10- Thermal Desorption for Gas Chromatography |
Record Nr. | UNINA-9910462088903321 |
Poole C. F | ||
Amsterdam ; ; Boston, : Elsevier, 2012 | ||
Materiale a stampa | ||
Lo trovi qui: Univ. Federico II | ||
|
Gas chromatography [[electronic resource] /] / Colin F. Poole |
Autore | Poole C. F |
Edizione | [1st ed.] |
Pubbl/distr/stampa | Amsterdam ; ; Boston, : Elsevier, 2012 |
Descrizione fisica | 1 online resource (753 p.) |
Disciplina | 543/.85 |
Soggetto topico |
Gas chromatography
Chromatographic analysis |
ISBN |
1-280-77001-5
9786613680785 0-12-385541-1 |
Formato | Materiale a stampa |
Livello bibliografico | Monografia |
Lingua di pubblicazione | eng |
Nota di contenuto |
Front Cover; Gas Chromatography; Copyright; Contents; Contributors; Chapter 1 - Milestones in the Development of Gas Chromatography; 1.1.INTRODUCTION; 1.2.THE INVENTION OF GAS CHROMATOGRAPHY; 1.3.EARLY INSTRUMENTATION; 1.4.EARLY COLUMN DEVELOPMENTS; 1.5.INTERFACING GLASS CAPILLARY COLUMNS TO INJECTORS AND DETECTORS; 1.6.THE HINDELANG CONFERENCES AND THE FUSED-SILICA COLUMN; 1.7.INCREASING SOPHISTICATION OF INSTRUMENTATION; 1.8.DECLINE IN THE EXPERTISE OF THE AVERAGE GAS CHROMATOGRAPHER; References; Chapter 2 - Theory of Gas Chromatography; 2.1.INTRODUCTION
2.2.NOMENCLATURE AND OTHER CONVENTIONS 2.3.GENERAL DEFINITIONS; 2.4.SOLUTE-COLUMN INTERACTION; 2.5.PROPERTIES OF AN IDEAL GAS; 2.6.FLOW OF IDEAL GAS IN OPEN CIRCULAR TUBES; 2.7.MIGRATION AND ELUTION PARAMETERS OF THE SOLUTES; 2.8.PEAK SPACING AND REVERSAL OF PEAK ORDER; 2.9.PEAK WIDTH; 2.10.OPTIMIZATION; References; Chapter 3 - Column Technology: Open Tubular Columns; 3.1.INTRODUCTION; 3.2.OVERVIEW OF THE FUSED SILICA DRAWING PROCESS; 3.3.THE PREFORM - RAW MATERIAL; 3.4.SURFACE CHEMISTRY; 3.5.DRAWING OF THE CAPILLARY FROM THE PREFORM; 3.6.PROTECTIVE COATING; 3.7.ALTERNATIVE PROTECTIVE COATINGS 3.8. CLEAN ROOM ENVIRONMENT 3.9.QUALITY MONITORING; 3.10.OBSERVATIONS ON HANDLING OF FUSED-SILICA CAPILLARY TUBING; 3.11.COLUMN TECHNOLOGY - COATING THE STATIONARY PHASE; 3.12.STATIONARY PHASES; 3.13.COATING TECHNIQUES; 3.14.COLUMN TECHNOLOGY - QUALITY EVALUATION; 3.15.COLUMN TECHNOLOGY - SUMMARY; References; Chapter 4- Packed Columns for Gas-Liquid and Gas-Solid Chromatography; 4.1.INTRODUCTION; 4.2.GAS-LIQUID CHROMATOGRAPHY; 4.3.GAS-SOLID CHROMATOGRAPHY; References; Chapter 5 - Gas-Solid Chromatography (PLOT Columns); 5.1.ALUMINA ADSORBENTS; 5.2.MOLECULAR SIEVES; 5.3.POROUS POLYMERS 5.4.CARBON ADSORBENTS 5.5.OTHER ADSORBENTS; References; Chapter 6- Classification and Selection of Open-Tubular Columns for Analytical Separations; 6.1.INTRODUCTION; 6.2.STATIONARY-PHASE CLASSIFICATION; 6.3.POROUS-LAYER OPEN-TUBULAR COLUMNS; 6.4.TEMPERATURE-PROGRAMMED SEPARATIONS; 6.5.STATIONARY-PHASE SELECTIVITY TUNING; References; Chapter 7 - Multidimensional and Comprehensive Gas Chromatography; 7.1.INTRODUCTION; 7.2.A GRAPHICAL REPRESENTATION OF 2D GC SEPARATIONS; 7.3 .BACK FLUSHING 2D GC; 7.4.HEART CUTTING 2D GC; 7.5.COMPREHENSIVE 2D GC; 7.6.CONCLUSIONS; References Chapter 8 - Sample Introduction Methods 8.1.INTRODUCTION; 8.2.CHOOSING A SAMPLE INTRODUCTION SYSTEM; 8.3.SUPPORTING DEVICES; 8.4.THE COLD ON-COLUMN INJECTOR; 8.5.THE FLASH VAPORIZATION INJECTOR; 8.6.THE SPLIT/SPLITLESS INJECTOR; 8.7.THE PROGRAMMABLE TEMPERATURE VAPORIZING (PTV) INJECTOR; 8.8.THE GAS SAMPLING VALVE; 8.9.THE LIQUID SAMPLING VALVE; References; Chapter 9 - Head space-Gas Chromatography; 9.1.INTRODUCTION AND HISTORY; 9.2.FUNDAMENTALS OF HEAD SPACE EXTRACTION; 9.3.INSTRUMENTATION AND PRACTICE; 9.4.METHOD DEVELOPMENT CONSIDERATIONS; 9.5.CONCLUSIONS; References Chapter 10- Thermal Desorption for Gas Chromatography |
Record Nr. | UNINA-9910790391703321 |
Poole C. F | ||
Amsterdam ; ; Boston, : Elsevier, 2012 | ||
Materiale a stampa | ||
Lo trovi qui: Univ. Federico II | ||
|