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Freeze-drying [[electronic resource]]
| Freeze-drying [[electronic resource]] |
| Autore | Oetjen Georg-Wilhelm |
| Edizione | [2nd, completely rev. and extended ed. /] |
| Pubbl/distr/stampa | Weinheim, : Wiley-VCH, c2004 |
| Descrizione fisica | 1 online resource (409 p.) |
| Disciplina |
615.19
660/.28426 |
| Altri autori (Persone) | HaseleyPeter |
| Soggetto topico | Freeze-drying |
| Soggetto genere / forma | Electronic books. |
| ISBN |
1-281-31173-1
9786611311735 3-527-61248-3 3-527-61249-1 |
| Formato | Materiale a stampa  |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Freeze-Drying; Table of Contents; Preface; Preface to the First Edition; 1 Foundations and Process Engineering; 1.1 Freezing; 1.1.1 Amount of Heat, Heat Conductivity, Heat Transfer and Cooling Rate; 1.1.2 Structure of Ice, Solutions and Dispersions; 1.1.3 Influence of Excipients; 1.1.4 Freezing of Cells and Bacteria; 1.1.5 Methods of Structure Analysis; 1.1.5.1 Measurements of Electrical Resistance (ER); 1.1.5.2 Differential Thermal Analysis (DTA); 1.1.5.3 Cryomicroscopy; 1.1.5.4 Differential Scanning Calorimetry (DSC); 1.1.5.5 Nuclear Magnetic Resonance
1.1.5.6 Thermomechanical Analysis (TMA)1.1.5.7 Dielectric Analysis (DEA); 1.1.5.8 X-ray Diffractometry-Raman Spectroscopy; 1.1.6 Changes of Structure in Freezing or Frozen Products; 1.2 Drying; 1.2.1 Main Drying (Sublimation Drying); 1.2.2 Secondary Drying (Desorption Drying); 1.2.3 Temperature and Pressure Measurement; 1.2.4 Water Vapor Transport During Drying; 1.2.5 Collapse and Recrystallization; 1.2.6 Drying Processes Without Vacuum; 1.3 Storage; 1.3.1 Measurement of the Residual Moisture Content (RM); 1.3.1.1 Gravimetric Method; 1.3.1.2 Karl Fischer (KF) Method 1.3.1.3 Thermogravimetry (TG, TG/MS)1.3.1.4 Infrared Spectroscopy; 1.3.2 Influence of Vial Stoppers on the Residual Moisture Content; 1.3.3 Qualities of the Dry Substances and Their Changes; 1.4 References for Chapter 1; 2 Installation and Equipment Technique; 2.1 Freezing Installation; 2.1.1 Cooling by Liquids: Shell-freezing and Spin-freezing; 2.1.2 Cooled Surfaces; 2.1.3 Product in the Flow of Cold Air, Foaming and Freezing of Extracts and Pulps; 2.1.4 Droplet Freezing in Cold Liquids; 2.1.5 Freezing by Evaporation of Product Water; 2.2 Components of a Freeze-drying Plant 2.2.1 Installations for Flasks and Manifolds2.2.2 Drying Chambers and Forms of Trays; Trays for Special Applications; 2.2.3 Shelves and their Cooling and Heating; 2.2.4 Water Vapor Condensers; 2.2.5 Refrigerating Systems and Refrigerants; 2.2.6 Vacuum Pumps; 2.2.7 Inlet Venting Filters; 2.2.8 Vacuum Measuring Systems; 2.2.9 Leak Rate Detection; 2.2.10 Process Control Systems; 2.2.11 Problems, Failures and Deviations; 2.3 Installations up to 10 kg Ice Capacity; 2.3.1 Universal Laboratory Plants; 2.3.2 Pilot Plants; 2.3.3 Manipulators and Stoppering Systems for Vials 2.3.4 Cleaning Installations, Sterilization by Steam and Vaporized Hydrogen Peroxide (VHP®)2.4 Production Plants; 2.4.1 Loading and Unloading Systems; 2.5 Production Plants for Food; 2.5.1 Discontinuous Plants; 2.5.2 Continuous Plants with Tray Transport; 2.5.3 Continuous Plants with Product Transport by Wipers or by Vibration; 2.6 Process Automation; 2.6.1 Prerequisites for Process and Related Plant Automation; 2.6.2 Control of the Process and Related Plant Data by Thermodynamic Data Measured During the Process: Thermodynamic Lyophilization Control (TLC) 2.6.2.1 Control of the Process Without Temperature Sensors in the Product |
| Record Nr. | UNINA-9910144329103321 |
Oetjen Georg-Wilhelm
|
||
| Weinheim, : Wiley-VCH, c2004 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Freeze-drying [[electronic resource]]
| Freeze-drying [[electronic resource]] |
| Autore | Oetjen Georg-Wilhelm |
| Edizione | [2nd, completely rev. and extended ed. /] |
| Pubbl/distr/stampa | Weinheim, : Wiley-VCH, c2004 |
| Descrizione fisica | 1 online resource (409 p.) |
| Disciplina |
615.19
660/.28426 |
| Altri autori (Persone) | HaseleyPeter |
| Soggetto topico | Freeze-drying |
| ISBN |
1-281-31173-1
9786611311735 3-527-61248-3 3-527-61249-1 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Freeze-Drying; Table of Contents; Preface; Preface to the First Edition; 1 Foundations and Process Engineering; 1.1 Freezing; 1.1.1 Amount of Heat, Heat Conductivity, Heat Transfer and Cooling Rate; 1.1.2 Structure of Ice, Solutions and Dispersions; 1.1.3 Influence of Excipients; 1.1.4 Freezing of Cells and Bacteria; 1.1.5 Methods of Structure Analysis; 1.1.5.1 Measurements of Electrical Resistance (ER); 1.1.5.2 Differential Thermal Analysis (DTA); 1.1.5.3 Cryomicroscopy; 1.1.5.4 Differential Scanning Calorimetry (DSC); 1.1.5.5 Nuclear Magnetic Resonance
1.1.5.6 Thermomechanical Analysis (TMA)1.1.5.7 Dielectric Analysis (DEA); 1.1.5.8 X-ray Diffractometry-Raman Spectroscopy; 1.1.6 Changes of Structure in Freezing or Frozen Products; 1.2 Drying; 1.2.1 Main Drying (Sublimation Drying); 1.2.2 Secondary Drying (Desorption Drying); 1.2.3 Temperature and Pressure Measurement; 1.2.4 Water Vapor Transport During Drying; 1.2.5 Collapse and Recrystallization; 1.2.6 Drying Processes Without Vacuum; 1.3 Storage; 1.3.1 Measurement of the Residual Moisture Content (RM); 1.3.1.1 Gravimetric Method; 1.3.1.2 Karl Fischer (KF) Method 1.3.1.3 Thermogravimetry (TG, TG/MS)1.3.1.4 Infrared Spectroscopy; 1.3.2 Influence of Vial Stoppers on the Residual Moisture Content; 1.3.3 Qualities of the Dry Substances and Their Changes; 1.4 References for Chapter 1; 2 Installation and Equipment Technique; 2.1 Freezing Installation; 2.1.1 Cooling by Liquids: Shell-freezing and Spin-freezing; 2.1.2 Cooled Surfaces; 2.1.3 Product in the Flow of Cold Air, Foaming and Freezing of Extracts and Pulps; 2.1.4 Droplet Freezing in Cold Liquids; 2.1.5 Freezing by Evaporation of Product Water; 2.2 Components of a Freeze-drying Plant 2.2.1 Installations for Flasks and Manifolds2.2.2 Drying Chambers and Forms of Trays; Trays for Special Applications; 2.2.3 Shelves and their Cooling and Heating; 2.2.4 Water Vapor Condensers; 2.2.5 Refrigerating Systems and Refrigerants; 2.2.6 Vacuum Pumps; 2.2.7 Inlet Venting Filters; 2.2.8 Vacuum Measuring Systems; 2.2.9 Leak Rate Detection; 2.2.10 Process Control Systems; 2.2.11 Problems, Failures and Deviations; 2.3 Installations up to 10 kg Ice Capacity; 2.3.1 Universal Laboratory Plants; 2.3.2 Pilot Plants; 2.3.3 Manipulators and Stoppering Systems for Vials 2.3.4 Cleaning Installations, Sterilization by Steam and Vaporized Hydrogen Peroxide (VHP®)2.4 Production Plants; 2.4.1 Loading and Unloading Systems; 2.5 Production Plants for Food; 2.5.1 Discontinuous Plants; 2.5.2 Continuous Plants with Tray Transport; 2.5.3 Continuous Plants with Product Transport by Wipers or by Vibration; 2.6 Process Automation; 2.6.1 Prerequisites for Process and Related Plant Automation; 2.6.2 Control of the Process and Related Plant Data by Thermodynamic Data Measured During the Process: Thermodynamic Lyophilization Control (TLC) 2.6.2.1 Control of the Process Without Temperature Sensors in the Product |
| Record Nr. | UNINA-9910830886303321 |
|
Oetjen Georg-Wilhelm
|
||
| Weinheim, : Wiley-VCH, c2004 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Freeze-drying
| Freeze-drying |
| Autore | Oetjen Georg-Wilhelm |
| Edizione | [2nd, completely rev. and extended ed. /] |
| Pubbl/distr/stampa | Weinheim, : Wiley-VCH, c2004 |
| Descrizione fisica | 1 online resource (409 p.) |
| Disciplina |
615.19
660/.28426 |
| Altri autori (Persone) | HaseleyPeter |
| Soggetto topico | Freeze-drying |
| ISBN |
1-281-31173-1
9786611311735 3-527-61248-3 3-527-61249-1 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Freeze-Drying; Table of Contents; Preface; Preface to the First Edition; 1 Foundations and Process Engineering; 1.1 Freezing; 1.1.1 Amount of Heat, Heat Conductivity, Heat Transfer and Cooling Rate; 1.1.2 Structure of Ice, Solutions and Dispersions; 1.1.3 Influence of Excipients; 1.1.4 Freezing of Cells and Bacteria; 1.1.5 Methods of Structure Analysis; 1.1.5.1 Measurements of Electrical Resistance (ER); 1.1.5.2 Differential Thermal Analysis (DTA); 1.1.5.3 Cryomicroscopy; 1.1.5.4 Differential Scanning Calorimetry (DSC); 1.1.5.5 Nuclear Magnetic Resonance
1.1.5.6 Thermomechanical Analysis (TMA)1.1.5.7 Dielectric Analysis (DEA); 1.1.5.8 X-ray Diffractometry-Raman Spectroscopy; 1.1.6 Changes of Structure in Freezing or Frozen Products; 1.2 Drying; 1.2.1 Main Drying (Sublimation Drying); 1.2.2 Secondary Drying (Desorption Drying); 1.2.3 Temperature and Pressure Measurement; 1.2.4 Water Vapor Transport During Drying; 1.2.5 Collapse and Recrystallization; 1.2.6 Drying Processes Without Vacuum; 1.3 Storage; 1.3.1 Measurement of the Residual Moisture Content (RM); 1.3.1.1 Gravimetric Method; 1.3.1.2 Karl Fischer (KF) Method 1.3.1.3 Thermogravimetry (TG, TG/MS)1.3.1.4 Infrared Spectroscopy; 1.3.2 Influence of Vial Stoppers on the Residual Moisture Content; 1.3.3 Qualities of the Dry Substances and Their Changes; 1.4 References for Chapter 1; 2 Installation and Equipment Technique; 2.1 Freezing Installation; 2.1.1 Cooling by Liquids: Shell-freezing and Spin-freezing; 2.1.2 Cooled Surfaces; 2.1.3 Product in the Flow of Cold Air, Foaming and Freezing of Extracts and Pulps; 2.1.4 Droplet Freezing in Cold Liquids; 2.1.5 Freezing by Evaporation of Product Water; 2.2 Components of a Freeze-drying Plant 2.2.1 Installations for Flasks and Manifolds2.2.2 Drying Chambers and Forms of Trays; Trays for Special Applications; 2.2.3 Shelves and their Cooling and Heating; 2.2.4 Water Vapor Condensers; 2.2.5 Refrigerating Systems and Refrigerants; 2.2.6 Vacuum Pumps; 2.2.7 Inlet Venting Filters; 2.2.8 Vacuum Measuring Systems; 2.2.9 Leak Rate Detection; 2.2.10 Process Control Systems; 2.2.11 Problems, Failures and Deviations; 2.3 Installations up to 10 kg Ice Capacity; 2.3.1 Universal Laboratory Plants; 2.3.2 Pilot Plants; 2.3.3 Manipulators and Stoppering Systems for Vials 2.3.4 Cleaning Installations, Sterilization by Steam and Vaporized Hydrogen Peroxide (VHP®)2.4 Production Plants; 2.4.1 Loading and Unloading Systems; 2.5 Production Plants for Food; 2.5.1 Discontinuous Plants; 2.5.2 Continuous Plants with Tray Transport; 2.5.3 Continuous Plants with Product Transport by Wipers or by Vibration; 2.6 Process Automation; 2.6.1 Prerequisites for Process and Related Plant Automation; 2.6.2 Control of the Process and Related Plant Data by Thermodynamic Data Measured During the Process: Thermodynamic Lyophilization Control (TLC) 2.6.2.1 Control of the Process Without Temperature Sensors in the Product |
| Record Nr. | UNINA-9910877518303321 |
|
Oetjen Georg-Wilhelm
|
||
| Weinheim, : Wiley-VCH, c2004 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Gefriertrocknen
| Gefriertrocknen |
| Autore | Oetjen Georg-Wilhelm |
| Pubbl/distr/stampa | [Place of publication not identified], : VCH, 1997 |
| Soggetto topico |
Technology, Pharmaceutical
Freeze Drying - methods Food Preservation Pharmaceutical Preparations |
| ISBN | 3-527-62440-6 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | ger |
| Altri titoli varianti | Gefriertrocknen |
| Record Nr. | UNINA-9910144379003321 |
|
Oetjen Georg-Wilhelm
|
||
| [Place of publication not identified], : VCH, 1997 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Gefriertrocknen
| Gefriertrocknen |
| Autore | Oetjen Georg-Wilhelm |
| Pubbl/distr/stampa | [Place of publication not identified], : VCH, 1997 |
| Soggetto topico |
Technology, Pharmaceutical
Freeze Drying - methods Food Preservation Pharmaceutical Preparations |
| ISBN | 3-527-62440-6 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | ger |
| Altri titoli varianti | Gefriertrocknen |
| Record Nr. | UNINA-9910831192703321 |
|
Oetjen Georg-Wilhelm
|
||
| [Place of publication not identified], : VCH, 1997 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Gefriertrocknen
| Gefriertrocknen |
| Autore | Oetjen Georg-Wilhelm |
| Pubbl/distr/stampa | [Place of publication not identified], : VCH, 1997 |
| Soggetto topico |
Technology, Pharmaceutical
Freeze Drying - methods Food Preservation Pharmaceutical Preparations |
| ISBN | 3-527-62440-6 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | ger |
| Altri titoli varianti | Gefriertrocknen |
| Record Nr. | UNINA-9910878083203321 |
|
Oetjen Georg-Wilhelm
|
||
| [Place of publication not identified], : VCH, 1997 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||