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Chemical reactor design and control [[electronic resource] /] / William L. Luyben
Chemical reactor design and control [[electronic resource] /] / William L. Luyben
Autore Luyben William L
Pubbl/distr/stampa [New York], : AIChE
Descrizione fisica 1 online resource (437 p.)
Disciplina 660.2832
660/.2832
Soggetto topico Chemical reactors - Design and construction
Reactors químics
Soggetto genere / forma Llibres electrònics
ISBN 1-281-00186-4
9786611001865
0-470-13491-7
0-470-13490-9
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto CHEMICAL REACTOR DESIGN AND CONTROL; CONTENTS; PREFACE; 1 REACTOR BASICS; 1.1 Fundamentals of Kinetics and Reaction Equilibrium; 1.1.1 Power-Law Kinetics; 1.1.2 Heterogeneous Reaction Kinetics; 1.1.3 Biochemical Reaction Kinetics; 1.1.4 Literature; 1.2 Multiple Reactions; 1.2.1 Parallel Reactions; 1.2.2 Series Reactions; 1.3 Determining Kinetic Parameters; 1.4 Types and Fundamental Properties of Reactors; 1.4.1 Continuous Stirred-Tank Reactor; 1.4.2 Batch Reactor; 1.4.3 Tubular Plug Flow Reactor; 1.5 Heat Transfer in Reactors; 1.6 Reactor ScaleUp; 1.7 Conclusion
2.8.1 Simulation Setup2.8.2 Specifying Reactions; 2.8.3 Reactor Setup; 2.9 Optimization of CSTR Systems; 2.9.1 Economics of Series CSTRs; 2.9.2 Economics of a Reactor-Column Process; 2.9.3 CSTR Processes with Two Reactants; 2.10 Conclusion; 3 CONTROL OF CSTR SYSTEMS; 3.1 Irreversible, Single Reactant; 3.1.1 Nonlinear Dynamic Model; 3.1.2 Linear Model; 3.1.3 Effect of Conversion on Openloop and Closedloop Stability; 3.1.4 Nonlinear Dynamic Simulation; 3.1.5 Effect of Jacket Volume; 3.1.6 Cooling Coil; 3.1.7 External Heat Exchanger; 3.1.8 Comparison of CSTR-in-Series Processes
3.1.9 Dynamics of Reactor-Stripper Process3.2 Reactor-Column Process with Two Reactants; 3.2.1 Nonlinear Dynamic Model of Reactor and Column; 3.2.2 Control Structure for Reactor-Column Process; 3.2.3 Reactor-Column Process with Hot Reaction; 3.3 AutoRefrigerated Reactor Control; 3.3.1 Dynamic Model; 3.3.2 Simulation Results; 3.4 Reactor Temperature Control Using Feed Manipulation; 3.4.1 Introduction; 3.4.2 Revised Control Structure; 3.4.3 Results; 3.4.4 Valve Position Control; 3.5 Aspen Dynamics Simulation of CSTRs; 3.5.1 Setting up the Dynamic Simulation
3.5.2 Running the Simulation and Tuning Controllers3.5.3 Results with Several Heat Transfer Options; 3.5.4 Use of RGIBBS Reactor; 3.6 Conclusion; 4 CONTROL OF BATCH REACTORS; 4.1 Irreversible, Single Reactant; 4.1.1 Pure Batch Reactor; 4.1.2 Fed-Batch Reactor; 4.2 Batch Reactor with Two Reactants; 4.3 Batch Reactor with Consecutive Reactions; 4.4 Aspen Plus Simulation Using RBatch; 4.5 Ethanol Batch Fermentor; 4.6 Fed-Batch Hydrogenation Reactor; 4.7 Batch TML Reactor; 4.8 Fed-Batch Reactor with Multiple Reactions; 4.8.1 Equations; 4.8.2 Effect of Feed Trajectory on Conversion and Selectivity
4.8.3 Batch Optimization
Record Nr. UNINA-9910144003703321
Luyben William L  
[New York], : AIChE
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Chemical reactor design and control [[electronic resource] /] / William L. Luyben
Chemical reactor design and control [[electronic resource] /] / William L. Luyben
Autore Luyben William L
Pubbl/distr/stampa [New York], : AIChE
Descrizione fisica 1 online resource (437 p.)
Disciplina 660.2832
660/.2832
Soggetto topico Chemical reactors - Design and construction
Reactors químics
Soggetto genere / forma Llibres electrònics
ISBN 1-281-00186-4
9786611001865
0-470-13491-7
0-470-13490-9
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto CHEMICAL REACTOR DESIGN AND CONTROL; CONTENTS; PREFACE; 1 REACTOR BASICS; 1.1 Fundamentals of Kinetics and Reaction Equilibrium; 1.1.1 Power-Law Kinetics; 1.1.2 Heterogeneous Reaction Kinetics; 1.1.3 Biochemical Reaction Kinetics; 1.1.4 Literature; 1.2 Multiple Reactions; 1.2.1 Parallel Reactions; 1.2.2 Series Reactions; 1.3 Determining Kinetic Parameters; 1.4 Types and Fundamental Properties of Reactors; 1.4.1 Continuous Stirred-Tank Reactor; 1.4.2 Batch Reactor; 1.4.3 Tubular Plug Flow Reactor; 1.5 Heat Transfer in Reactors; 1.6 Reactor ScaleUp; 1.7 Conclusion
2.8.1 Simulation Setup2.8.2 Specifying Reactions; 2.8.3 Reactor Setup; 2.9 Optimization of CSTR Systems; 2.9.1 Economics of Series CSTRs; 2.9.2 Economics of a Reactor-Column Process; 2.9.3 CSTR Processes with Two Reactants; 2.10 Conclusion; 3 CONTROL OF CSTR SYSTEMS; 3.1 Irreversible, Single Reactant; 3.1.1 Nonlinear Dynamic Model; 3.1.2 Linear Model; 3.1.3 Effect of Conversion on Openloop and Closedloop Stability; 3.1.4 Nonlinear Dynamic Simulation; 3.1.5 Effect of Jacket Volume; 3.1.6 Cooling Coil; 3.1.7 External Heat Exchanger; 3.1.8 Comparison of CSTR-in-Series Processes
3.1.9 Dynamics of Reactor-Stripper Process3.2 Reactor-Column Process with Two Reactants; 3.2.1 Nonlinear Dynamic Model of Reactor and Column; 3.2.2 Control Structure for Reactor-Column Process; 3.2.3 Reactor-Column Process with Hot Reaction; 3.3 AutoRefrigerated Reactor Control; 3.3.1 Dynamic Model; 3.3.2 Simulation Results; 3.4 Reactor Temperature Control Using Feed Manipulation; 3.4.1 Introduction; 3.4.2 Revised Control Structure; 3.4.3 Results; 3.4.4 Valve Position Control; 3.5 Aspen Dynamics Simulation of CSTRs; 3.5.1 Setting up the Dynamic Simulation
3.5.2 Running the Simulation and Tuning Controllers3.5.3 Results with Several Heat Transfer Options; 3.5.4 Use of RGIBBS Reactor; 3.6 Conclusion; 4 CONTROL OF BATCH REACTORS; 4.1 Irreversible, Single Reactant; 4.1.1 Pure Batch Reactor; 4.1.2 Fed-Batch Reactor; 4.2 Batch Reactor with Two Reactants; 4.3 Batch Reactor with Consecutive Reactions; 4.4 Aspen Plus Simulation Using RBatch; 4.5 Ethanol Batch Fermentor; 4.6 Fed-Batch Hydrogenation Reactor; 4.7 Batch TML Reactor; 4.8 Fed-Batch Reactor with Multiple Reactions; 4.8.1 Equations; 4.8.2 Effect of Feed Trajectory on Conversion and Selectivity
4.8.3 Batch Optimization
Record Nr. UNINA-9910830065603321
Luyben William L  
[New York], : AIChE
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Chemical reactor design and control [[electronic resource] /] / William L. Luyben
Chemical reactor design and control [[electronic resource] /] / William L. Luyben
Autore Luyben William L
Pubbl/distr/stampa [New York], : AIChE
Descrizione fisica 1 online resource (437 p.)
Disciplina 660.2832
660/.2832
Soggetto topico Chemical reactors - Design and construction
Reactors químics
Soggetto genere / forma Llibres electrònics
ISBN 1-281-00186-4
9786611001865
0-470-13491-7
0-470-13490-9
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto CHEMICAL REACTOR DESIGN AND CONTROL; CONTENTS; PREFACE; 1 REACTOR BASICS; 1.1 Fundamentals of Kinetics and Reaction Equilibrium; 1.1.1 Power-Law Kinetics; 1.1.2 Heterogeneous Reaction Kinetics; 1.1.3 Biochemical Reaction Kinetics; 1.1.4 Literature; 1.2 Multiple Reactions; 1.2.1 Parallel Reactions; 1.2.2 Series Reactions; 1.3 Determining Kinetic Parameters; 1.4 Types and Fundamental Properties of Reactors; 1.4.1 Continuous Stirred-Tank Reactor; 1.4.2 Batch Reactor; 1.4.3 Tubular Plug Flow Reactor; 1.5 Heat Transfer in Reactors; 1.6 Reactor ScaleUp; 1.7 Conclusion
2.8.1 Simulation Setup2.8.2 Specifying Reactions; 2.8.3 Reactor Setup; 2.9 Optimization of CSTR Systems; 2.9.1 Economics of Series CSTRs; 2.9.2 Economics of a Reactor-Column Process; 2.9.3 CSTR Processes with Two Reactants; 2.10 Conclusion; 3 CONTROL OF CSTR SYSTEMS; 3.1 Irreversible, Single Reactant; 3.1.1 Nonlinear Dynamic Model; 3.1.2 Linear Model; 3.1.3 Effect of Conversion on Openloop and Closedloop Stability; 3.1.4 Nonlinear Dynamic Simulation; 3.1.5 Effect of Jacket Volume; 3.1.6 Cooling Coil; 3.1.7 External Heat Exchanger; 3.1.8 Comparison of CSTR-in-Series Processes
3.1.9 Dynamics of Reactor-Stripper Process3.2 Reactor-Column Process with Two Reactants; 3.2.1 Nonlinear Dynamic Model of Reactor and Column; 3.2.2 Control Structure for Reactor-Column Process; 3.2.3 Reactor-Column Process with Hot Reaction; 3.3 AutoRefrigerated Reactor Control; 3.3.1 Dynamic Model; 3.3.2 Simulation Results; 3.4 Reactor Temperature Control Using Feed Manipulation; 3.4.1 Introduction; 3.4.2 Revised Control Structure; 3.4.3 Results; 3.4.4 Valve Position Control; 3.5 Aspen Dynamics Simulation of CSTRs; 3.5.1 Setting up the Dynamic Simulation
3.5.2 Running the Simulation and Tuning Controllers3.5.3 Results with Several Heat Transfer Options; 3.5.4 Use of RGIBBS Reactor; 3.6 Conclusion; 4 CONTROL OF BATCH REACTORS; 4.1 Irreversible, Single Reactant; 4.1.1 Pure Batch Reactor; 4.1.2 Fed-Batch Reactor; 4.2 Batch Reactor with Two Reactants; 4.3 Batch Reactor with Consecutive Reactions; 4.4 Aspen Plus Simulation Using RBatch; 4.5 Ethanol Batch Fermentor; 4.6 Fed-Batch Hydrogenation Reactor; 4.7 Batch TML Reactor; 4.8 Fed-Batch Reactor with Multiple Reactions; 4.8.1 Equations; 4.8.2 Effect of Feed Trajectory on Conversion and Selectivity
4.8.3 Batch Optimization
Record Nr. UNINA-9910840578603321
Luyben William L  
[New York], : AIChE
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Design and control of distillation systems for separating azeotropes [[electronic resource] /] / William L Luyben, I-Lung Chien
Design and control of distillation systems for separating azeotropes [[electronic resource] /] / William L Luyben, I-Lung Chien
Autore Luyben William L
Pubbl/distr/stampa Hoboken, N.J., : Wiley, : AIChE, c2010
Descrizione fisica 1 online resource (473 p.)
Disciplina 660.2842
660/.2842
Altri autori (Persone) ChienI-Lung <1955->
Soggetto topico Azeotropic distillation - Design
Azeotropes
ISBN 1-118-20983-4
1-282-68445-0
9786612684456
0-470-57580-8
0-470-57579-4
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto DESIGN AND CONTROL OF DISTILLATION SYSTEMS FOR SEPARATING AZEOTROPES; CONTENTS; PREFACE; ACKNOWLEDGEMENTS; PART 1 FUNDAMENTALS AND TOOLS; 1 INTRODUCTION; 2 PHASE EQUILIBRIUM; 3 STEADY-STATE DESIGN IN ASPEN PLUS; 4 DYNAMICS AND CONTROL IN ASPEN DYNAMICS; PART 2 SEPARATIONS WITHOUT ADDING OTHER COMPONENTS; 5 PRESSURE-SWING AZEOTROPIC DISTILLATION; 6 PRESSURE SWING WITH HEAT INTEGRATION; 7 HETEROGENEOUS BINARY AZEOTROPES; PART 3 SEPARATIONS USING A LIGHT ENTRAINER (HETEROGENEOUS AZEOTROPIC DISTILLATION); 8 ISOPROPANOL-WATER (CYCLOHEXANE AS THE ENTRAINER)
9 ACETIC ACID-WATER (ISOBUTYL ACETATE AS THE ENTRAINER)PART 4 SEPARATIONS USING HEAVY ENTRAINER (EXTRACTIVE DISTILLATION); 10 ISOPROPANOL-WATER (DIMETHYL SULFOXIDE AS THE ENTRAINER); 11 EXTRACTIVE DISTILLATION OF THE ACETONE-METHANOL SYSTEM; 12 MAXIMUM-BOILING AZEOTROPES; PART 5 OTHER WAYS FOR SEPARATING AZEOTROPES; 13 BATCH DISTILLATION OF AZEOTROPES; 14 HYBRID DISTILLATION-PERVAPORATION SYSTEMS; INDEX
Record Nr. UNINA-9910830410103321
Luyben William L  
Hoboken, N.J., : Wiley, : AIChE, c2010
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Design and control of distillation systems for separating azeotropes [[electronic resource] /] / William L Luyben, I-Lung Chien
Design and control of distillation systems for separating azeotropes [[electronic resource] /] / William L Luyben, I-Lung Chien
Autore Luyben William L
Pubbl/distr/stampa Hoboken, N.J., : Wiley, : AIChE, c2010
Descrizione fisica 1 online resource (473 p.)
Disciplina 660.2842
660/.2842
Altri autori (Persone) ChienI-Lung <1955->
Soggetto topico Azeotropic distillation - Design
Azeotropes
ISBN 1-118-20983-4
1-282-68445-0
9786612684456
0-470-57580-8
0-470-57579-4
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto DESIGN AND CONTROL OF DISTILLATION SYSTEMS FOR SEPARATING AZEOTROPES; CONTENTS; PREFACE; ACKNOWLEDGEMENTS; PART 1 FUNDAMENTALS AND TOOLS; 1 INTRODUCTION; 2 PHASE EQUILIBRIUM; 3 STEADY-STATE DESIGN IN ASPEN PLUS; 4 DYNAMICS AND CONTROL IN ASPEN DYNAMICS; PART 2 SEPARATIONS WITHOUT ADDING OTHER COMPONENTS; 5 PRESSURE-SWING AZEOTROPIC DISTILLATION; 6 PRESSURE SWING WITH HEAT INTEGRATION; 7 HETEROGENEOUS BINARY AZEOTROPES; PART 3 SEPARATIONS USING A LIGHT ENTRAINER (HETEROGENEOUS AZEOTROPIC DISTILLATION); 8 ISOPROPANOL-WATER (CYCLOHEXANE AS THE ENTRAINER)
9 ACETIC ACID-WATER (ISOBUTYL ACETATE AS THE ENTRAINER)PART 4 SEPARATIONS USING HEAVY ENTRAINER (EXTRACTIVE DISTILLATION); 10 ISOPROPANOL-WATER (DIMETHYL SULFOXIDE AS THE ENTRAINER); 11 EXTRACTIVE DISTILLATION OF THE ACETONE-METHANOL SYSTEM; 12 MAXIMUM-BOILING AZEOTROPES; PART 5 OTHER WAYS FOR SEPARATING AZEOTROPES; 13 BATCH DISTILLATION OF AZEOTROPES; 14 HYBRID DISTILLATION-PERVAPORATION SYSTEMS; INDEX
Record Nr. UNINA-9910840803503321
Luyben William L  
Hoboken, N.J., : Wiley, : AIChE, c2010
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Principles and case studies of simultaneous design [[electronic resource] /] / William L. Luyben
Principles and case studies of simultaneous design [[electronic resource] /] / William L. Luyben
Autore Luyben William L
Pubbl/distr/stampa Hoboken, N.J., : John Wiley, c2011
Descrizione fisica 1 online resource (342 p.)
Disciplina 660.2812
660/.2812
Soggetto topico Chemical engineering
Engineering design
Soggetto genere / forma Electronic books.
ISBN 1-283-92758-6
1-118-00164-8
1-118-00165-6
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto PRINCIPLES ANDCASE STUDIES OFSIMULTANEOUS DESIGN; PREFACE; 1 INTRODUCTION; 1.1 Overview; 1.2 History; 1.3 Books; 1.4 Tools; Reference Textbooks; 2 PRINCIPLES OF REACTOR DESIGN AND CONTROL; 2.1 Background; 2.2 Principles Derived from Chemistry; 2.2.1 Heat of Reaction; 2.2.2 Reversible and Irreversible Reactions; 2.2.3 Multiple Reactions; 2.3 Principles Derived from Phase of Reaction; 2.4 Determining Kinetic Parameters; 2.4.1 Thermodynamic Constraints; 2.4.2 Kinetic Parameters from Plant Data; 2.5 Principles of Reactor Heat Exchange; 2.5.1 Continuous Stirred-Tank Reactors
2.5.2 Tubular Reactors2.5.3 Feed-Effluent Heat Exchangers; 2.6 Heuristic Design of Reactor/Separation Processes; 2.6.1 Introduction; 2.6.2 Process Studied; 2.6.3 Economic Optimization; 2.6.4 Other Cases; 2.6.5 Real Example; 2.7 Conclusion; References; 3 PRINCIPLES OF DISTILLATION DESIGN AND CONTROL; 3.1 Principles of Economic Distillation Design; 3.1.1 Operating Pressure; 3.1.2 Heuristic Optimization; 3.1.3 Rigorous Optimization; 3.1.4 Feed Preheating and Intermediate Reboilers and Condensers; 3.1.5 Heat Integration; 3.2 Principles of Distillation Control; 3.2.1 Single-End Control
3.2.2 Dual-End Control3.2.3 Alternative Control Structures; 3.3 Conclusion; References; 4 PRINCIPLES OF PLANTWIDE CONTROL; 4.1 History; 4.2 Effects of Recycle; 4.2.1 Time Constants of Integrated Plant with Recycle; 4.2.2 Recycle Snowball Effect; 4.3 Management of Fresh Feed Streams; 4.3.1 Fundamentals; 4.3.2 Process with Two Recycles and Two Fresh Feeds; 4.4 Conclusion; 5 ECONOMIC BASIS; 5.1 Level of Accuracy; 5.2 Sizing Equipment; 5.2.1 Vessels; 5.2.2 Heat Exchangers; 5.2.3 Compressors; 5.2.4 Pumps, Valves, and Piping; 5.3 Equipment Capital Cost; 5.3.1 Vessels (diameter and length in meters)
5.3.2 Heat Exchangers (area in square meters)5.3.3 Compressors (work in horsepower); 5.4 Energy Costs; 5.5 Chemical Costs; References; 6 DESIGN AND CONTROL OF THE ACETONE PROCESS VIA DEHYDROGENATION OF ISOPROPANOL; 6.1 Process Description; 6.1.1 Reaction Kinetics; 6.1.2 Phase Equilibrium; 6.2 Turton Flowsheet; 6.2.1 Vaporizer; 6.2.2 Reactor; 6.2.3 Heat Exchangers, Flash Tank, and Absorber; 6.2.4 Acetone Column C1; 6.2.5 Water Column C2; 6.3 Revised Flowsheet; 6.3.1 Effect of Absorber Pressure; 6.3.2 Effect of Water Solvent and Absorber Stages; 6.3.3 Effect of Reactor Size
6.3.4 Optimum Distillation Design6.4 Economic Comparison; 6.5 Plantwide Control; 6.5.1 Control Structure; 6.5.2 Column Control Structure Selection; 6.5.3 Dynamic Performance Results; 6.6 Conclusion; References; 7 DESIGN AND CONTROL OF AN AUTO-REFRIGERATED ALKYLATION PROCESS; 7.1 Introduction; 7.2 Process Description; 7.2.1 Reaction Kinetics; 7.2.2 Phase Equilibrium; 7.2.3 Flowsheet; 7.2.4 Design Optimization Variables; 7.3 Design of Distillation Columns; 7.3.1 Depropanizer; 7.3.2 Deisobutanizer; 7.4 Economic Optimization of Entire Process; 7.4.1 Flowsheet Convergence; 7.4.2 Yield
7.4.3 Effect of Reactor Size
Record Nr. UNINA-9910141234903321
Luyben William L  
Hoboken, N.J., : John Wiley, c2011
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Principles and case studies of simultaneous design [[electronic resource] /] / William L. Luyben
Principles and case studies of simultaneous design [[electronic resource] /] / William L. Luyben
Autore Luyben William L
Pubbl/distr/stampa Hoboken, N.J., : John Wiley, c2011
Descrizione fisica 1 online resource (342 p.)
Disciplina 660.2812
660/.2812
Soggetto topico Chemical engineering
Engineering design
ISBN 1-283-92758-6
1-118-00164-8
1-118-00165-6
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto PRINCIPLES ANDCASE STUDIES OFSIMULTANEOUS DESIGN; PREFACE; 1 INTRODUCTION; 1.1 Overview; 1.2 History; 1.3 Books; 1.4 Tools; Reference Textbooks; 2 PRINCIPLES OF REACTOR DESIGN AND CONTROL; 2.1 Background; 2.2 Principles Derived from Chemistry; 2.2.1 Heat of Reaction; 2.2.2 Reversible and Irreversible Reactions; 2.2.3 Multiple Reactions; 2.3 Principles Derived from Phase of Reaction; 2.4 Determining Kinetic Parameters; 2.4.1 Thermodynamic Constraints; 2.4.2 Kinetic Parameters from Plant Data; 2.5 Principles of Reactor Heat Exchange; 2.5.1 Continuous Stirred-Tank Reactors
2.5.2 Tubular Reactors2.5.3 Feed-Effluent Heat Exchangers; 2.6 Heuristic Design of Reactor/Separation Processes; 2.6.1 Introduction; 2.6.2 Process Studied; 2.6.3 Economic Optimization; 2.6.4 Other Cases; 2.6.5 Real Example; 2.7 Conclusion; References; 3 PRINCIPLES OF DISTILLATION DESIGN AND CONTROL; 3.1 Principles of Economic Distillation Design; 3.1.1 Operating Pressure; 3.1.2 Heuristic Optimization; 3.1.3 Rigorous Optimization; 3.1.4 Feed Preheating and Intermediate Reboilers and Condensers; 3.1.5 Heat Integration; 3.2 Principles of Distillation Control; 3.2.1 Single-End Control
3.2.2 Dual-End Control3.2.3 Alternative Control Structures; 3.3 Conclusion; References; 4 PRINCIPLES OF PLANTWIDE CONTROL; 4.1 History; 4.2 Effects of Recycle; 4.2.1 Time Constants of Integrated Plant with Recycle; 4.2.2 Recycle Snowball Effect; 4.3 Management of Fresh Feed Streams; 4.3.1 Fundamentals; 4.3.2 Process with Two Recycles and Two Fresh Feeds; 4.4 Conclusion; 5 ECONOMIC BASIS; 5.1 Level of Accuracy; 5.2 Sizing Equipment; 5.2.1 Vessels; 5.2.2 Heat Exchangers; 5.2.3 Compressors; 5.2.4 Pumps, Valves, and Piping; 5.3 Equipment Capital Cost; 5.3.1 Vessels (diameter and length in meters)
5.3.2 Heat Exchangers (area in square meters)5.3.3 Compressors (work in horsepower); 5.4 Energy Costs; 5.5 Chemical Costs; References; 6 DESIGN AND CONTROL OF THE ACETONE PROCESS VIA DEHYDROGENATION OF ISOPROPANOL; 6.1 Process Description; 6.1.1 Reaction Kinetics; 6.1.2 Phase Equilibrium; 6.2 Turton Flowsheet; 6.2.1 Vaporizer; 6.2.2 Reactor; 6.2.3 Heat Exchangers, Flash Tank, and Absorber; 6.2.4 Acetone Column C1; 6.2.5 Water Column C2; 6.3 Revised Flowsheet; 6.3.1 Effect of Absorber Pressure; 6.3.2 Effect of Water Solvent and Absorber Stages; 6.3.3 Effect of Reactor Size
6.3.4 Optimum Distillation Design6.4 Economic Comparison; 6.5 Plantwide Control; 6.5.1 Control Structure; 6.5.2 Column Control Structure Selection; 6.5.3 Dynamic Performance Results; 6.6 Conclusion; References; 7 DESIGN AND CONTROL OF AN AUTO-REFRIGERATED ALKYLATION PROCESS; 7.1 Introduction; 7.2 Process Description; 7.2.1 Reaction Kinetics; 7.2.2 Phase Equilibrium; 7.2.3 Flowsheet; 7.2.4 Design Optimization Variables; 7.3 Design of Distillation Columns; 7.3.1 Depropanizer; 7.3.2 Deisobutanizer; 7.4 Economic Optimization of Entire Process; 7.4.1 Flowsheet Convergence; 7.4.2 Yield
7.4.3 Effect of Reactor Size
Record Nr. UNINA-9910830583403321
Luyben William L  
Hoboken, N.J., : John Wiley, c2011
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Principles and case studies of simultaneous design [[electronic resource] /] / William L. Luyben
Principles and case studies of simultaneous design [[electronic resource] /] / William L. Luyben
Autore Luyben William L
Pubbl/distr/stampa Hoboken, N.J., : John Wiley, c2011
Descrizione fisica 1 online resource (342 p.)
Disciplina 660.2812
660/.2812
Soggetto topico Chemical engineering
Engineering design
ISBN 1-283-92758-6
1-118-00164-8
1-118-00165-6
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto PRINCIPLES ANDCASE STUDIES OFSIMULTANEOUS DESIGN; PREFACE; 1 INTRODUCTION; 1.1 Overview; 1.2 History; 1.3 Books; 1.4 Tools; Reference Textbooks; 2 PRINCIPLES OF REACTOR DESIGN AND CONTROL; 2.1 Background; 2.2 Principles Derived from Chemistry; 2.2.1 Heat of Reaction; 2.2.2 Reversible and Irreversible Reactions; 2.2.3 Multiple Reactions; 2.3 Principles Derived from Phase of Reaction; 2.4 Determining Kinetic Parameters; 2.4.1 Thermodynamic Constraints; 2.4.2 Kinetic Parameters from Plant Data; 2.5 Principles of Reactor Heat Exchange; 2.5.1 Continuous Stirred-Tank Reactors
2.5.2 Tubular Reactors2.5.3 Feed-Effluent Heat Exchangers; 2.6 Heuristic Design of Reactor/Separation Processes; 2.6.1 Introduction; 2.6.2 Process Studied; 2.6.3 Economic Optimization; 2.6.4 Other Cases; 2.6.5 Real Example; 2.7 Conclusion; References; 3 PRINCIPLES OF DISTILLATION DESIGN AND CONTROL; 3.1 Principles of Economic Distillation Design; 3.1.1 Operating Pressure; 3.1.2 Heuristic Optimization; 3.1.3 Rigorous Optimization; 3.1.4 Feed Preheating and Intermediate Reboilers and Condensers; 3.1.5 Heat Integration; 3.2 Principles of Distillation Control; 3.2.1 Single-End Control
3.2.2 Dual-End Control3.2.3 Alternative Control Structures; 3.3 Conclusion; References; 4 PRINCIPLES OF PLANTWIDE CONTROL; 4.1 History; 4.2 Effects of Recycle; 4.2.1 Time Constants of Integrated Plant with Recycle; 4.2.2 Recycle Snowball Effect; 4.3 Management of Fresh Feed Streams; 4.3.1 Fundamentals; 4.3.2 Process with Two Recycles and Two Fresh Feeds; 4.4 Conclusion; 5 ECONOMIC BASIS; 5.1 Level of Accuracy; 5.2 Sizing Equipment; 5.2.1 Vessels; 5.2.2 Heat Exchangers; 5.2.3 Compressors; 5.2.4 Pumps, Valves, and Piping; 5.3 Equipment Capital Cost; 5.3.1 Vessels (diameter and length in meters)
5.3.2 Heat Exchangers (area in square meters)5.3.3 Compressors (work in horsepower); 5.4 Energy Costs; 5.5 Chemical Costs; References; 6 DESIGN AND CONTROL OF THE ACETONE PROCESS VIA DEHYDROGENATION OF ISOPROPANOL; 6.1 Process Description; 6.1.1 Reaction Kinetics; 6.1.2 Phase Equilibrium; 6.2 Turton Flowsheet; 6.2.1 Vaporizer; 6.2.2 Reactor; 6.2.3 Heat Exchangers, Flash Tank, and Absorber; 6.2.4 Acetone Column C1; 6.2.5 Water Column C2; 6.3 Revised Flowsheet; 6.3.1 Effect of Absorber Pressure; 6.3.2 Effect of Water Solvent and Absorber Stages; 6.3.3 Effect of Reactor Size
6.3.4 Optimum Distillation Design6.4 Economic Comparison; 6.5 Plantwide Control; 6.5.1 Control Structure; 6.5.2 Column Control Structure Selection; 6.5.3 Dynamic Performance Results; 6.6 Conclusion; References; 7 DESIGN AND CONTROL OF AN AUTO-REFRIGERATED ALKYLATION PROCESS; 7.1 Introduction; 7.2 Process Description; 7.2.1 Reaction Kinetics; 7.2.2 Phase Equilibrium; 7.2.3 Flowsheet; 7.2.4 Design Optimization Variables; 7.3 Design of Distillation Columns; 7.3.1 Depropanizer; 7.3.2 Deisobutanizer; 7.4 Economic Optimization of Entire Process; 7.4.1 Flowsheet Convergence; 7.4.2 Yield
7.4.3 Effect of Reactor Size
Record Nr. UNINA-9910840804103321
Luyben William L  
Hoboken, N.J., : John Wiley, c2011
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Reactive distillation design and control [[electronic resource] /] / William L. Luyben, Cheng-Ching Yu
Reactive distillation design and control [[electronic resource] /] / William L. Luyben, Cheng-Ching Yu
Autore Luyben William L
Pubbl/distr/stampa Hoboken, NJ, : John Wiley, c2008
Descrizione fisica 1 online resource (598 p.)
Disciplina 660
660.28425
660/.28425
Altri autori (Persone) YuCheng-Ching <1956->
Soggetto topico Distillation apparatus - Design and construction
Chemical process control
Distillation
Reactivity (Chemistry)
ISBN 1-282-11265-1
9786612112652
0-470-37774-7
0-470-37779-8
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto REACTIVE DISTILLATION DESIGN AND CONTROL; CONTENTS; PREFACE; 1 INTRODUCTION; 1.1 History; 1.2 Basics of Reactive Distillation; 1.3 Neat Operation Versus Excess Reactant; 1.4 Limitations; 1.4.1 Temperature Mismatch; 1.4.2 Unfavorable Volatilities; 1.4.3 Slow Reaction Rates; 1.4.4 Other Restrictions; 1.5 Scope; 1.6 Computational Methods; 1.6.1 Matlab Programs for Steady-State Design; 1.6.2 Aspen Simulations; 1.7 Reference Materials; PART I STEADY-STATE DESIGN OF IDEAL QUATERNARY SYSTEM; 2 PARAMETER EFFECTS; 2.1 Effect of Holdup on Reactive Trays; 2.2 Effect of Number of Reactive Trays
2.3 Effect of Pressure2.4 Effect of Chemical Equilibrium Constant; 2.5 Effect of Relative Volatilities; 2.5.1 Constant Relative Volatilities; 2.5.2 Temperature-Dependent Relative Volatilities; 2.6 Effect of Number of Stripping and Rectifying Trays; 2.7 Effect of Reactant Feed Location; 2.7.1 Reactant A Feed Location (N(FA)); 2.7.2 Reactant B Feed Location (N(FB)); 2.8 Conclusion; 3 ECONOMIC COMPARISON OF REACTIVE DISTILLATION WITH A CONVENTIONAL PROCESS; 3.1 Conventional Multiunit Process; 3.1.1 Assumptions and Specifications; 3.1.2 Steady-State Design Procedure
3.1.3 Sizing and Economic Equations3.2 Reactive Distillation Design; 3.2.1 Assumptions and Specifications; 3.2.2 Steady-State Design Procedure; 3.3 Results for Different Chemical Equilibrium Constants; 3.3.1 Conventional Process; 3.3.2 Reactive Distillation Process; 3.3.3 Comparisons; 3.4 Results for Temperature-Dependent Relative Volatilities; 3.4.1 Relative Volatilities; 3.4.2 Optimum Steady-State Designs; 3.4.3 Real Chemical Systems; 3.5 Conclusion; 4 NEAT OPERATION VERSUS USING EXCESS REACTANT; 4.1 Introduction; 4.2 Neat Reactive Column; 4.3 Two-Column System with Excess B
4.3.1 20% Excess B Case4.3.2 10% Excess B Case; 4.4 Two-Column System with 20% Excess of A; 4.5 Economic Comparison; 4.6 Conclusion; PART II STEADY-STATE DESIGN OF OTHER IDEAL SYSTEMS; 5 TERNARY REACTIVE DISTILLATION SYSTEMS; 5.1 Ternary System Without Inerts; 5.1.1 Column Configuration; 5.1.2 Chemistry and Phase Equilibrium Parameters; 5.1.3 Design Parameters and Procedure; 5.1.4 Effect of Pressure; 5.1.5 Holdup on Reactive Trays; 5.1.6 Number of Reactive Trays; 5.1.7 Number of Stripping Trays; 5.2 Ternary System With Inerts; 5.2.1 Column Configuration
5.2.2 Chemistry and Phase Equilibrium Parameters5.2.3 Design Parameters and Procedure; 5.2.4 Effect of Pressure; 5.2.5 Control Tray Composition; 5.2.6 Reactive Tray Holdup; 5.2.7 Effect of Reflux; 5.2.8 Chemical Equilibrium Constant; 5.2.9 Feed Composition; 5.2.10 Number of Reactive Trays; 5.2.11 Number of Rectifying and Stripping Trays; 5.3 Conclusion; 6 TERNARY DECOMPOSITION REACTION; 6.1 Ternary Decomposition Reaction: Intermediate-Boiling Reactant; 6.1.1 Column Configuration; 6.1.2 Chemistry and Phase Equilibrium Parameters; 6.1.3 Design Parameters and Procedure
6.1.4 Holdup on Reactive Trays
Record Nr. UNINA-9910145955003321
Luyben William L  
Hoboken, NJ, : John Wiley, c2008
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Reactive distillation design and control [[electronic resource] /] / William L. Luyben, Cheng-Ching Yu
Reactive distillation design and control [[electronic resource] /] / William L. Luyben, Cheng-Ching Yu
Autore Luyben William L
Pubbl/distr/stampa Hoboken, NJ, : John Wiley, c2008
Descrizione fisica 1 online resource (598 p.)
Disciplina 660
660.28425
660/.28425
Altri autori (Persone) YuCheng-Ching <1956->
Soggetto topico Distillation apparatus - Design and construction
Chemical process control
Distillation
Reactivity (Chemistry)
ISBN 1-282-11265-1
9786612112652
0-470-37774-7
0-470-37779-8
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto REACTIVE DISTILLATION DESIGN AND CONTROL; CONTENTS; PREFACE; 1 INTRODUCTION; 1.1 History; 1.2 Basics of Reactive Distillation; 1.3 Neat Operation Versus Excess Reactant; 1.4 Limitations; 1.4.1 Temperature Mismatch; 1.4.2 Unfavorable Volatilities; 1.4.3 Slow Reaction Rates; 1.4.4 Other Restrictions; 1.5 Scope; 1.6 Computational Methods; 1.6.1 Matlab Programs for Steady-State Design; 1.6.2 Aspen Simulations; 1.7 Reference Materials; PART I STEADY-STATE DESIGN OF IDEAL QUATERNARY SYSTEM; 2 PARAMETER EFFECTS; 2.1 Effect of Holdup on Reactive Trays; 2.2 Effect of Number of Reactive Trays
2.3 Effect of Pressure2.4 Effect of Chemical Equilibrium Constant; 2.5 Effect of Relative Volatilities; 2.5.1 Constant Relative Volatilities; 2.5.2 Temperature-Dependent Relative Volatilities; 2.6 Effect of Number of Stripping and Rectifying Trays; 2.7 Effect of Reactant Feed Location; 2.7.1 Reactant A Feed Location (N(FA)); 2.7.2 Reactant B Feed Location (N(FB)); 2.8 Conclusion; 3 ECONOMIC COMPARISON OF REACTIVE DISTILLATION WITH A CONVENTIONAL PROCESS; 3.1 Conventional Multiunit Process; 3.1.1 Assumptions and Specifications; 3.1.2 Steady-State Design Procedure
3.1.3 Sizing and Economic Equations3.2 Reactive Distillation Design; 3.2.1 Assumptions and Specifications; 3.2.2 Steady-State Design Procedure; 3.3 Results for Different Chemical Equilibrium Constants; 3.3.1 Conventional Process; 3.3.2 Reactive Distillation Process; 3.3.3 Comparisons; 3.4 Results for Temperature-Dependent Relative Volatilities; 3.4.1 Relative Volatilities; 3.4.2 Optimum Steady-State Designs; 3.4.3 Real Chemical Systems; 3.5 Conclusion; 4 NEAT OPERATION VERSUS USING EXCESS REACTANT; 4.1 Introduction; 4.2 Neat Reactive Column; 4.3 Two-Column System with Excess B
4.3.1 20% Excess B Case4.3.2 10% Excess B Case; 4.4 Two-Column System with 20% Excess of A; 4.5 Economic Comparison; 4.6 Conclusion; PART II STEADY-STATE DESIGN OF OTHER IDEAL SYSTEMS; 5 TERNARY REACTIVE DISTILLATION SYSTEMS; 5.1 Ternary System Without Inerts; 5.1.1 Column Configuration; 5.1.2 Chemistry and Phase Equilibrium Parameters; 5.1.3 Design Parameters and Procedure; 5.1.4 Effect of Pressure; 5.1.5 Holdup on Reactive Trays; 5.1.6 Number of Reactive Trays; 5.1.7 Number of Stripping Trays; 5.2 Ternary System With Inerts; 5.2.1 Column Configuration
5.2.2 Chemistry and Phase Equilibrium Parameters5.2.3 Design Parameters and Procedure; 5.2.4 Effect of Pressure; 5.2.5 Control Tray Composition; 5.2.6 Reactive Tray Holdup; 5.2.7 Effect of Reflux; 5.2.8 Chemical Equilibrium Constant; 5.2.9 Feed Composition; 5.2.10 Number of Reactive Trays; 5.2.11 Number of Rectifying and Stripping Trays; 5.3 Conclusion; 6 TERNARY DECOMPOSITION REACTION; 6.1 Ternary Decomposition Reaction: Intermediate-Boiling Reactant; 6.1.1 Column Configuration; 6.1.2 Chemistry and Phase Equilibrium Parameters; 6.1.3 Design Parameters and Procedure
6.1.4 Holdup on Reactive Trays
Record Nr. UNINA-9910830370703321
Luyben William L  
Hoboken, NJ, : John Wiley, c2008
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui