High-performance liquid chromatography and mass spectrometry of porphyrins, chlorophylls and bilins [[electronic resource] /] / Chang Kee Lim |
Autore | Lim Chang Kee |
Pubbl/distr/stampa | River Edge, N.J., : World Scientific, 2010 |
Descrizione fisica | 1 online resource (245 p.) |
Disciplina | 547/.593 |
Collana | Methods in chromatography |
Soggetto topico |
Porphyrins
Chlorophyll Tetrapyrroles High performance liquid chromatography Mass spectrometry |
Soggetto genere / forma | Electronic books. |
ISBN |
1-282-75824-1
9786612758249 981-4277-19-3 |
Formato | Materiale a stampa |
Livello bibliografico | Monografia |
Lingua di pubblicazione | eng |
Nota di contenuto |
Contents; Preface; Chapter 1. Structure, Distribution, Biosynthesis and Function; 1.1. Introduction; 1.2. Nomenclature; 1.3. Biosynthesis of Porphyrins, Haem and Chlorophyll; 1.4. Biosynthesis of Bilins in Animals and Plants; 1.4.1. Degradation of haem to bile pigments; 1.4.2. Biosynthesis of bilins in plants, algae and cyanobacteria; 1.4.3. Degradation of chlorophyll in senescent higher plants; 1.5. Function of Porphyrins and Other Tetrapyrroles; References; Chapter 2. High-Performance Liquid Chromatography of Porphyrins; 2.1. Introduction; 2.2. HPLC of Porphyrin Methyl Esters
2.3. HPLC of Porphyrin Free Acids2.3.1. Stationary phases for reversed-phase HPLC of porphyrins; 2.3.2. Mobile phases for reversed-phase HPLC of porphyrins; 2.3.3. Procedure for optimisation of porphyrin separation by reversed-phase HPLC; 2.3.4. Retention behaviour of porphyrins in reversed-phase HPLC; 2.4 HPLC of Porphyrinogens; References; Chapter 3. Mass Spectrometry of Porphyrins; 3.1. Introduction; 3.2. Fast Atom Bombardment (FAB) Mass Spectrometry of Porphyrins; 3.3. Laser Desorption/Ionisation Time-of-Flight (LDI-TOF) Mass Spectrometry of Porphyrins 3.4 Electrospray Ionisation Mass Spectrometry (ESI-MS) and HPLC/ESI-MS of Porphyrins3.4.1. HPLC/ESI-MS of porphyrins; 3.4.2. ESI-MS/MS fragmentation of porphyrins; 3.4.2.1. ESI-MS/MS product ion spectrum and fragmentation pathways of uroporphyrin; 3.4.3. ESI-MS/MS fragmentation of hydroxyuroporphyrins; 3.4.3.1. ESI-MS/MS product ion spectrum and fragmentation pathways of meso-hydroxyuroporphyrin; 3.4.3.2. ESI-MS/MS product ion spectrum of hydroxyacetic acid uroporphyrin; 3.4.3.3. ESI-MS/MS product ion spectrum of α-hydroxypropionic acid uroporphyrin 3.4.3.4. ESI-MS/MS product ion spectrum and fragmentation pathways of β-hydroxypropionic acid uroporphyrin3.4.3.5. ESI-MS/MS product ion spectra and fragmentation pathways of cis- and transhydroxyspirolactoneurochlorins; 3.4.3.6. ESI-MS/MS product ion spectra and fragmentation pathways of cis- and transdihydroxyurochlorins; 3.4.3.7. Characteristic ESI-MS/MS product ions of hydroxyuroporphyrins; 3.4.4. ESI-MS/MS product ion spectra of ketoacid uroporphyrins; 3.4.5. ESI-MS/MS of heptacarboxylic porphyrin; 3.4.6. ESI-MS/MS of hydroxyheptacarboxylic porphyrins 3.4.7. ESI-MS/MS of ketoacid heptacarboxylic porphyrins and formyl heptacarboxylic porphyrin3.4.8. ESI-MS/MS product ion spectrum and fragmentation pattern of coproporphyrin; 3.4.9. ESI-MS/MS of hydroxymethylcoproporphyrin; 3.4.10. ESI-MS/MS of β-ketopropionic acid coproporphyrin and formylcoproporphyrin; 3.4.11. ESI-MS/MS product ion spectrum and fragmentation pattern of protoporphyrin; 3.4.12. HPLC/ESI-MS and MS/MS of meso-tetraphenylporphyrin derivatives; References; Chapter 4. Porphyrin Profiles in Blood, Urine and Faeces by HPLC and HPLC/ESI-MS; 4.1. Introduction 4.2. Sample Collection and Preparation |
Record Nr. | UNINA-9910455867903321 |
Lim Chang Kee | ||
River Edge, N.J., : World Scientific, 2010 | ||
Materiale a stampa | ||
Lo trovi qui: Univ. Federico II | ||
|
High-performance liquid chromatography and mass spectrometry of porphyrins, chlorophylls and bilins [[electronic resource] /] / Chang Kee Lim |
Autore | Lim Chang Kee |
Pubbl/distr/stampa | River Edge, N.J., : World Scientific, 2010 |
Descrizione fisica | 1 online resource (245 p.) |
Disciplina | 547/.593 |
Collana | Methods in chromatography |
Soggetto topico |
Porphyrins
Chlorophyll Tetrapyrroles High performance liquid chromatography Mass spectrometry |
ISBN |
1-282-75824-1
9786612758249 981-4277-19-3 |
Formato | Materiale a stampa |
Livello bibliografico | Monografia |
Lingua di pubblicazione | eng |
Nota di contenuto |
Contents; Preface; Chapter 1. Structure, Distribution, Biosynthesis and Function; 1.1. Introduction; 1.2. Nomenclature; 1.3. Biosynthesis of Porphyrins, Haem and Chlorophyll; 1.4. Biosynthesis of Bilins in Animals and Plants; 1.4.1. Degradation of haem to bile pigments; 1.4.2. Biosynthesis of bilins in plants, algae and cyanobacteria; 1.4.3. Degradation of chlorophyll in senescent higher plants; 1.5. Function of Porphyrins and Other Tetrapyrroles; References; Chapter 2. High-Performance Liquid Chromatography of Porphyrins; 2.1. Introduction; 2.2. HPLC of Porphyrin Methyl Esters
2.3. HPLC of Porphyrin Free Acids2.3.1. Stationary phases for reversed-phase HPLC of porphyrins; 2.3.2. Mobile phases for reversed-phase HPLC of porphyrins; 2.3.3. Procedure for optimisation of porphyrin separation by reversed-phase HPLC; 2.3.4. Retention behaviour of porphyrins in reversed-phase HPLC; 2.4 HPLC of Porphyrinogens; References; Chapter 3. Mass Spectrometry of Porphyrins; 3.1. Introduction; 3.2. Fast Atom Bombardment (FAB) Mass Spectrometry of Porphyrins; 3.3. Laser Desorption/Ionisation Time-of-Flight (LDI-TOF) Mass Spectrometry of Porphyrins 3.4 Electrospray Ionisation Mass Spectrometry (ESI-MS) and HPLC/ESI-MS of Porphyrins3.4.1. HPLC/ESI-MS of porphyrins; 3.4.2. ESI-MS/MS fragmentation of porphyrins; 3.4.2.1. ESI-MS/MS product ion spectrum and fragmentation pathways of uroporphyrin; 3.4.3. ESI-MS/MS fragmentation of hydroxyuroporphyrins; 3.4.3.1. ESI-MS/MS product ion spectrum and fragmentation pathways of meso-hydroxyuroporphyrin; 3.4.3.2. ESI-MS/MS product ion spectrum of hydroxyacetic acid uroporphyrin; 3.4.3.3. ESI-MS/MS product ion spectrum of α-hydroxypropionic acid uroporphyrin 3.4.3.4. ESI-MS/MS product ion spectrum and fragmentation pathways of β-hydroxypropionic acid uroporphyrin3.4.3.5. ESI-MS/MS product ion spectra and fragmentation pathways of cis- and transhydroxyspirolactoneurochlorins; 3.4.3.6. ESI-MS/MS product ion spectra and fragmentation pathways of cis- and transdihydroxyurochlorins; 3.4.3.7. Characteristic ESI-MS/MS product ions of hydroxyuroporphyrins; 3.4.4. ESI-MS/MS product ion spectra of ketoacid uroporphyrins; 3.4.5. ESI-MS/MS of heptacarboxylic porphyrin; 3.4.6. ESI-MS/MS of hydroxyheptacarboxylic porphyrins 3.4.7. ESI-MS/MS of ketoacid heptacarboxylic porphyrins and formyl heptacarboxylic porphyrin3.4.8. ESI-MS/MS product ion spectrum and fragmentation pattern of coproporphyrin; 3.4.9. ESI-MS/MS of hydroxymethylcoproporphyrin; 3.4.10. ESI-MS/MS of β-ketopropionic acid coproporphyrin and formylcoproporphyrin; 3.4.11. ESI-MS/MS product ion spectrum and fragmentation pattern of protoporphyrin; 3.4.12. HPLC/ESI-MS and MS/MS of meso-tetraphenylporphyrin derivatives; References; Chapter 4. Porphyrin Profiles in Blood, Urine and Faeces by HPLC and HPLC/ESI-MS; 4.1. Introduction 4.2. Sample Collection and Preparation |
Record Nr. | UNINA-9910780728103321 |
Lim Chang Kee | ||
River Edge, N.J., : World Scientific, 2010 | ||
Materiale a stampa | ||
Lo trovi qui: Univ. Federico II | ||
|
High-performance liquid chromatography and mass spectrometry of porphyrins, chlorophylls and bilins / / Chang Kee Lim |
Autore | Lim Chang Kee |
Edizione | [1st ed.] |
Pubbl/distr/stampa | River Edge, N.J., : World Scientific, 2010 |
Descrizione fisica | 1 online resource (245 p.) |
Disciplina | 547/.593 |
Collana | Methods in chromatography |
Soggetto topico |
Porphyrins
Chlorophyll Tetrapyrroles High performance liquid chromatography Mass spectrometry |
ISBN |
1-282-75824-1
9786612758249 981-4277-19-3 |
Formato | Materiale a stampa |
Livello bibliografico | Monografia |
Lingua di pubblicazione | eng |
Nota di contenuto |
Contents; Preface; Chapter 1. Structure, Distribution, Biosynthesis and Function; 1.1. Introduction; 1.2. Nomenclature; 1.3. Biosynthesis of Porphyrins, Haem and Chlorophyll; 1.4. Biosynthesis of Bilins in Animals and Plants; 1.4.1. Degradation of haem to bile pigments; 1.4.2. Biosynthesis of bilins in plants, algae and cyanobacteria; 1.4.3. Degradation of chlorophyll in senescent higher plants; 1.5. Function of Porphyrins and Other Tetrapyrroles; References; Chapter 2. High-Performance Liquid Chromatography of Porphyrins; 2.1. Introduction; 2.2. HPLC of Porphyrin Methyl Esters
2.3. HPLC of Porphyrin Free Acids2.3.1. Stationary phases for reversed-phase HPLC of porphyrins; 2.3.2. Mobile phases for reversed-phase HPLC of porphyrins; 2.3.3. Procedure for optimisation of porphyrin separation by reversed-phase HPLC; 2.3.4. Retention behaviour of porphyrins in reversed-phase HPLC; 2.4 HPLC of Porphyrinogens; References; Chapter 3. Mass Spectrometry of Porphyrins; 3.1. Introduction; 3.2. Fast Atom Bombardment (FAB) Mass Spectrometry of Porphyrins; 3.3. Laser Desorption/Ionisation Time-of-Flight (LDI-TOF) Mass Spectrometry of Porphyrins 3.4 Electrospray Ionisation Mass Spectrometry (ESI-MS) and HPLC/ESI-MS of Porphyrins3.4.1. HPLC/ESI-MS of porphyrins; 3.4.2. ESI-MS/MS fragmentation of porphyrins; 3.4.2.1. ESI-MS/MS product ion spectrum and fragmentation pathways of uroporphyrin; 3.4.3. ESI-MS/MS fragmentation of hydroxyuroporphyrins; 3.4.3.1. ESI-MS/MS product ion spectrum and fragmentation pathways of meso-hydroxyuroporphyrin; 3.4.3.2. ESI-MS/MS product ion spectrum of hydroxyacetic acid uroporphyrin; 3.4.3.3. ESI-MS/MS product ion spectrum of α-hydroxypropionic acid uroporphyrin 3.4.3.4. ESI-MS/MS product ion spectrum and fragmentation pathways of β-hydroxypropionic acid uroporphyrin3.4.3.5. ESI-MS/MS product ion spectra and fragmentation pathways of cis- and transhydroxyspirolactoneurochlorins; 3.4.3.6. ESI-MS/MS product ion spectra and fragmentation pathways of cis- and transdihydroxyurochlorins; 3.4.3.7. Characteristic ESI-MS/MS product ions of hydroxyuroporphyrins; 3.4.4. ESI-MS/MS product ion spectra of ketoacid uroporphyrins; 3.4.5. ESI-MS/MS of heptacarboxylic porphyrin; 3.4.6. ESI-MS/MS of hydroxyheptacarboxylic porphyrins 3.4.7. ESI-MS/MS of ketoacid heptacarboxylic porphyrins and formyl heptacarboxylic porphyrin3.4.8. ESI-MS/MS product ion spectrum and fragmentation pattern of coproporphyrin; 3.4.9. ESI-MS/MS of hydroxymethylcoproporphyrin; 3.4.10. ESI-MS/MS of β-ketopropionic acid coproporphyrin and formylcoproporphyrin; 3.4.11. ESI-MS/MS product ion spectrum and fragmentation pattern of protoporphyrin; 3.4.12. HPLC/ESI-MS and MS/MS of meso-tetraphenylporphyrin derivatives; References; Chapter 4. Porphyrin Profiles in Blood, Urine and Faeces by HPLC and HPLC/ESI-MS; 4.1. Introduction 4.2. Sample Collection and Preparation |
Record Nr. | UNINA-9910825593303321 |
Lim Chang Kee | ||
River Edge, N.J., : World Scientific, 2010 | ||
Materiale a stampa | ||
Lo trovi qui: Univ. Federico II | ||
|