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Industrial crystallization process monitoring and control [[electronic resource] /] / edited by Angelo Chianese and Herman J. M. Kramer
| Industrial crystallization process monitoring and control [[electronic resource] /] / edited by Angelo Chianese and Herman J. M. Kramer |
| Pubbl/distr/stampa | Weinheim, Germany, : Wiley-VCH, 2012 |
| Descrizione fisica | 1 online resource (253 p.) |
| Disciplina | 660.284298 |
| Altri autori (Persone) |
ChianeseAngelo
KramerHerman J. M |
| Soggetto topico |
Crystallization - Industrial applications
Crystallization |
| ISBN |
3-527-64517-9
1-280-66298-0 9786613639912 3-527-64520-9 3-527-64518-7 |
| Formato | Materiale a stampa  |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Industrial Crystallization Process Monitoring and Control; Contents; Preface; Scope of the Book; List of Contributors; 1 Characterization of Crystal Size Distribution; 1.1 Introduction; 1.2 Particle Size Distribution; 1.3 Particle Size Distribution Moments; 1.4 Particle Size Distribution Characterization on the Basis of Mass Distribution; References; 2 Forward Light Scattering; 2.1 Introduction; 2.2 Principles of Laser Diffraction; 2.3 Scatter Theory; 2.3.1 Generalized Lorenz-Mie Theory; 2.3.2 Anomalous Diffraction; 2.3.3 Fraunhofer Diffraction; 2.4 Deconvolution
2.4.1 Direct Inversion Using the Nonnegativity Constraint 2.4.2 Philips Twomey Inversion Method; 2.4.3 Iterative Methods; 2.5 The Effects of Shape; 2.6 Multiple Scattering; 2.7 Application of Laser Diffraction for Monitoring and Control of Industrial Crystallization Processes; 2.8 Conclusions; References; Further Reading; 3 Focused Beam Reflectance Measurement; 3.1 Measurement Principle; 3.2 Application Examples; 3.2.1 Solubility and Metastable Zone Width (MSZW); 3.2.2 Seed Effectiveness; 3.2.3 Polymorph Transformations; 3.2.4 Effect of Different Impurity Levels; 3.2.5 Nucleation Kinetics 3.2.6 Improved Downstream Processing 3.2.7 Process Control; 3.3 Advantages and Limitations; References; 4 Turbidimetry for the Estimation of Crystal Average Size; 4.1 Introduction; 4.2 Determination of Average Particle Size from Specific Turbidity; 4.3 Procedure to Evaluate Average Crystal Size by Turbidimetry for a High Solid Slurry Concentration; 4.4 Conclusion; References; Further Reading; 5 Imaging; 5.1 Introduction; 5.2 Literature Overview; 5.3 The Sensor Design; 5.3.1 Optics and Illumination; 5.3.2 The Camera System and the Resolution; 5.3.3 Image Analysis; 5.3.4 Statistics 5.4 Application of In Situ Imaging for Monitoring Crystallization Processes 5.4.1 Example 1; 5.4.2 Example 2; 5.5 Conclusions; References; Further Reading; 6 Turbidimetry and Nephelometry; 6.1 Introduction; 6.2 Measurement of Nucleation and Solubility Points; 6.3 The Developed Turbidimetric and Nephelometric Instruments; 6.4 The Examined Systems; 6.5 Obtained Results; References; 7 Speed of Sound; 7.1 Introduction; 7.2 In-Process Ultrasound Measurement; 7.3 Determining Solubility and Metastable Zone Width; 7.4 Measuring Crystal Growth Rates; 7.5 Detecting Phase Transitions with Ultrasound References 8 In-Line Process Refractometer for Concentration Measurement in Sugar Crystallizers; 8.1 Introduction; 8.2 Measurement Principle; 8.3 In-Line Instrument Features and Benefits; 8.3.1 Accuracy; 8.3.2 Concentration Determination; 8.3.3 Process Temperature Compensation Factor; 8.3.4 Process Sensor; 8.4 Features and Benefits; 8.5 Example of Application in the Crystallization; 8.5.1 Seeding Point and Supersaturation Control in Sugar Vacuum Pan; 8.6 Conclusion; References; 9 ATR-FTIR Spectroscopy; 9.1 Introduction; 9.2 Calibration; 9.3 Speciation Monitoring; 9.4 Co-Crystal Formation 9.5 Solubility Measurement |
| Record Nr. | UNINA-9910139693403321 |
| Weinheim, Germany, : Wiley-VCH, 2012 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Industrial crystallization process monitoring and control / / edited by Angelo Chianese and Herman J. M. Kramer
| Industrial crystallization process monitoring and control / / edited by Angelo Chianese and Herman J. M. Kramer |
| Edizione | [1st ed.] |
| Pubbl/distr/stampa | Weinheim, Germany, : Wiley-VCH, 2012 |
| Descrizione fisica | 1 online resource (253 p.) |
| Disciplina | 660.284298 |
| Altri autori (Persone) |
ChianeseAngelo
KramerHerman J. M |
| Soggetto topico |
Crystallization - Industrial applications
Crystallization |
| ISBN |
9786613639912
9783527645176 3527645179 9781280662980 1280662980 9783527645206 3527645209 9783527645183 3527645187 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Industrial Crystallization Process Monitoring and Control; Contents; Preface; Scope of the Book; List of Contributors; 1 Characterization of Crystal Size Distribution; 1.1 Introduction; 1.2 Particle Size Distribution; 1.3 Particle Size Distribution Moments; 1.4 Particle Size Distribution Characterization on the Basis of Mass Distribution; References; 2 Forward Light Scattering; 2.1 Introduction; 2.2 Principles of Laser Diffraction; 2.3 Scatter Theory; 2.3.1 Generalized Lorenz-Mie Theory; 2.3.2 Anomalous Diffraction; 2.3.3 Fraunhofer Diffraction; 2.4 Deconvolution
2.4.1 Direct Inversion Using the Nonnegativity Constraint 2.4.2 Philips Twomey Inversion Method; 2.4.3 Iterative Methods; 2.5 The Effects of Shape; 2.6 Multiple Scattering; 2.7 Application of Laser Diffraction for Monitoring and Control of Industrial Crystallization Processes; 2.8 Conclusions; References; Further Reading; 3 Focused Beam Reflectance Measurement; 3.1 Measurement Principle; 3.2 Application Examples; 3.2.1 Solubility and Metastable Zone Width (MSZW); 3.2.2 Seed Effectiveness; 3.2.3 Polymorph Transformations; 3.2.4 Effect of Different Impurity Levels; 3.2.5 Nucleation Kinetics 3.2.6 Improved Downstream Processing 3.2.7 Process Control; 3.3 Advantages and Limitations; References; 4 Turbidimetry for the Estimation of Crystal Average Size; 4.1 Introduction; 4.2 Determination of Average Particle Size from Specific Turbidity; 4.3 Procedure to Evaluate Average Crystal Size by Turbidimetry for a High Solid Slurry Concentration; 4.4 Conclusion; References; Further Reading; 5 Imaging; 5.1 Introduction; 5.2 Literature Overview; 5.3 The Sensor Design; 5.3.1 Optics and Illumination; 5.3.2 The Camera System and the Resolution; 5.3.3 Image Analysis; 5.3.4 Statistics 5.4 Application of In Situ Imaging for Monitoring Crystallization Processes 5.4.1 Example 1; 5.4.2 Example 2; 5.5 Conclusions; References; Further Reading; 6 Turbidimetry and Nephelometry; 6.1 Introduction; 6.2 Measurement of Nucleation and Solubility Points; 6.3 The Developed Turbidimetric and Nephelometric Instruments; 6.4 The Examined Systems; 6.5 Obtained Results; References; 7 Speed of Sound; 7.1 Introduction; 7.2 In-Process Ultrasound Measurement; 7.3 Determining Solubility and Metastable Zone Width; 7.4 Measuring Crystal Growth Rates; 7.5 Detecting Phase Transitions with Ultrasound References 8 In-Line Process Refractometer for Concentration Measurement in Sugar Crystallizers; 8.1 Introduction; 8.2 Measurement Principle; 8.3 In-Line Instrument Features and Benefits; 8.3.1 Accuracy; 8.3.2 Concentration Determination; 8.3.3 Process Temperature Compensation Factor; 8.3.4 Process Sensor; 8.4 Features and Benefits; 8.5 Example of Application in the Crystallization; 8.5.1 Seeding Point and Supersaturation Control in Sugar Vacuum Pan; 8.6 Conclusion; References; 9 ATR-FTIR Spectroscopy; 9.1 Introduction; 9.2 Calibration; 9.3 Speciation Monitoring; 9.4 Co-Crystal Formation 9.5 Solubility Measurement |
| Record Nr. | UNINA-9910815012703321 |
| Weinheim, Germany, : Wiley-VCH, 2012 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||