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Micro instrumentation [[electronic resource] ] : for high throughput experimentation and process intensification - a tool for PAT / / edited by Melvin V. Koch, Kurt M. Vandenbussche, and Ray W. Chrisman
Micro instrumentation [[electronic resource] ] : for high throughput experimentation and process intensification - a tool for PAT / / edited by Melvin V. Koch, Kurt M. Vandenbussche, and Ray W. Chrisman
Pubbl/distr/stampa Weinheim, : Wiley-VCH
Descrizione fisica 1 online resource (523 p.)
Disciplina 660.281
Altri autori (Persone) KochMelvin V
VandenbusscheKurt M
ChrismanRay W
Soggetto topico Chemical engineering - Equipment and supplies
Chemical processes
Soggetto genere / forma Electronic books.
ISBN 1-280-92157-9
9786610921577
3-527-61062-6
3-527-61061-8
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Micro Instrumentation; Contents; Preface; List of Contributors; Part I Introducing the Concepts; 1 Introduction; 1.1 Background; 1.2 Analytical Tools for use in PAT; 1.3 The Center for Process Analytical Chemistry (CPAC) and the Summer Institute; 1.4 Topics covered by Previous CPAC Summer Institutes; 1.5 Recent Emphasis of CPAC Summer Institutes: High Throughput Experimentation and Process Intensification; 1.6 Conclusion; References; 2 Macro to Micro ... The Evolution of Process Analytical Systems; 2.1 Introduction; 2.1.2 Early Developments; 2.1.3 Developments since 1980; 2.1.4 Sampling Systems
2.1.4.1 Filtration2.1.4.2 The Fast Loop-Analytical Loop Strategy; 2.1.4.3 NeSSI; 2.1.5 General Reviews; 2.2 Chromatography; 2.2.1 Gas Chromatography; 2.2.2 Liquid Chromatography; 2.2.3 On-line Spectroscopy; 2.2.4 On-line Mass Spectrometry; 2.2.5 Microflow Techniques; References; 3 Process Intensification; 3.1 Introduction, Scope and Definitions; 3.2 Process Intensification in the Field of Reaction Engineering; 3.3 Process Intensification through Micro-structured Unit Operations; 3.3.1 Gas Phase Mass Transfer; 3.3.2 Liquid-Liquid Mass Transfer: Mixing and Emulsions
3.3.3 Gas-Liquid Mass Transfer3.3.4 Mass Transfer in Gas-Solid Systems; 3.3.5 Heat Transfer; 3.4 Case Studies; 3.4.1 Distributed Production of Methanol; 3.4.2 Distributed Production of Hydrogen; 3.5 Conclusions; References; 4 High Throughput Research; 4.1 Introduction; 4.2 Description of Terms; 4.3 Concept of a Research Process; 4.4 High Throughput Analytical; 4.5 Extracting Information from the Process; 4.6 Process Development becomes the Next Bottleneck; 4.7 Use of High Throughput Concepts for Process Development; 4.8 Microreactors for Process Development
4.9 Current Barriers and Limitations to Microscale Reaction Characterization4.10 Conclusion; References; Part II Technology Developments and Case Studies; 5 Introduction; 6 Microreactor Concepts and Processing; 6.1 Introduction; 6.2 Microreactor Technology - Interfacing and Discipline Cross-boundary Research; 6.3 Microstructured Mixer-reactors for Pilot and Production Range and Scale-out Issues; 6.3.1 Caterpillar Microstructured Mixer-reactors; 6.3.2 StarLam Microstructured Mixer-reactors; 6.3.3 Microstructured Heat Exchanger-reactors; 6.4 Fine-chemical Microreactor Plants
6.4.1 Laboratory-range Plants6.4.2 Pilot-range Plants; 6.5 Industrial Microreactor Process Development for Fine and Functional Chemistry; 6.5.1 Phenyl Boronic Acid Synthesis (Scheme 6.1) (Clariant/Frankfurt + IMM); 6.5.1.1 Process Development Issue; 6.5.1.2 Microreactor Plant and Processing Solution; 6.5.2 Azo Pigment Yellow 12 Manufacture (Scheme 6.2) (Trust Chem/Hangzhou + IMM); 6.5.2.1 Process Development Issue; 6.5.2.2 Microreactor Plant and Processing Solution; 6.5.3 Hydrogen Peroxide Synthesis (UOP/Chicago + IMM); 6.5.3.1 Process Development Issues
6.5.3.2 Microreactor Plant and Processing Solution
Record Nr. UNINA-9910144003303321
Weinheim, : Wiley-VCH
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Micro instrumentation [[electronic resource] ] : for high throughput experimentation and process intensification - a tool for PAT / / edited by Melvin V. Koch, Kurt M. Vandenbussche, and Ray W. Chrisman
Micro instrumentation [[electronic resource] ] : for high throughput experimentation and process intensification - a tool for PAT / / edited by Melvin V. Koch, Kurt M. Vandenbussche, and Ray W. Chrisman
Pubbl/distr/stampa Weinheim, : Wiley-VCH
Descrizione fisica 1 online resource (523 p.)
Disciplina 660.281
Altri autori (Persone) KochMelvin V
VandenbusscheKurt M
ChrismanRay W
Soggetto topico Chemical engineering - Equipment and supplies
Chemical processes
ISBN 1-280-92157-9
9786610921577
3-527-61062-6
3-527-61061-8
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Micro Instrumentation; Contents; Preface; List of Contributors; Part I Introducing the Concepts; 1 Introduction; 1.1 Background; 1.2 Analytical Tools for use in PAT; 1.3 The Center for Process Analytical Chemistry (CPAC) and the Summer Institute; 1.4 Topics covered by Previous CPAC Summer Institutes; 1.5 Recent Emphasis of CPAC Summer Institutes: High Throughput Experimentation and Process Intensification; 1.6 Conclusion; References; 2 Macro to Micro ... The Evolution of Process Analytical Systems; 2.1 Introduction; 2.1.2 Early Developments; 2.1.3 Developments since 1980; 2.1.4 Sampling Systems
2.1.4.1 Filtration2.1.4.2 The Fast Loop-Analytical Loop Strategy; 2.1.4.3 NeSSI; 2.1.5 General Reviews; 2.2 Chromatography; 2.2.1 Gas Chromatography; 2.2.2 Liquid Chromatography; 2.2.3 On-line Spectroscopy; 2.2.4 On-line Mass Spectrometry; 2.2.5 Microflow Techniques; References; 3 Process Intensification; 3.1 Introduction, Scope and Definitions; 3.2 Process Intensification in the Field of Reaction Engineering; 3.3 Process Intensification through Micro-structured Unit Operations; 3.3.1 Gas Phase Mass Transfer; 3.3.2 Liquid-Liquid Mass Transfer: Mixing and Emulsions
3.3.3 Gas-Liquid Mass Transfer3.3.4 Mass Transfer in Gas-Solid Systems; 3.3.5 Heat Transfer; 3.4 Case Studies; 3.4.1 Distributed Production of Methanol; 3.4.2 Distributed Production of Hydrogen; 3.5 Conclusions; References; 4 High Throughput Research; 4.1 Introduction; 4.2 Description of Terms; 4.3 Concept of a Research Process; 4.4 High Throughput Analytical; 4.5 Extracting Information from the Process; 4.6 Process Development becomes the Next Bottleneck; 4.7 Use of High Throughput Concepts for Process Development; 4.8 Microreactors for Process Development
4.9 Current Barriers and Limitations to Microscale Reaction Characterization4.10 Conclusion; References; Part II Technology Developments and Case Studies; 5 Introduction; 6 Microreactor Concepts and Processing; 6.1 Introduction; 6.2 Microreactor Technology - Interfacing and Discipline Cross-boundary Research; 6.3 Microstructured Mixer-reactors for Pilot and Production Range and Scale-out Issues; 6.3.1 Caterpillar Microstructured Mixer-reactors; 6.3.2 StarLam Microstructured Mixer-reactors; 6.3.3 Microstructured Heat Exchanger-reactors; 6.4 Fine-chemical Microreactor Plants
6.4.1 Laboratory-range Plants6.4.2 Pilot-range Plants; 6.5 Industrial Microreactor Process Development for Fine and Functional Chemistry; 6.5.1 Phenyl Boronic Acid Synthesis (Scheme 6.1) (Clariant/Frankfurt + IMM); 6.5.1.1 Process Development Issue; 6.5.1.2 Microreactor Plant and Processing Solution; 6.5.2 Azo Pigment Yellow 12 Manufacture (Scheme 6.2) (Trust Chem/Hangzhou + IMM); 6.5.2.1 Process Development Issue; 6.5.2.2 Microreactor Plant and Processing Solution; 6.5.3 Hydrogen Peroxide Synthesis (UOP/Chicago + IMM); 6.5.3.1 Process Development Issues
6.5.3.2 Microreactor Plant and Processing Solution
Record Nr. UNINA-9910830529303321
Weinheim, : Wiley-VCH
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Micro instrumentation : for high throughput experimentation and process intensification - a tool for PAT / / edited by Melvin V. Koch, Kurt M. Vandenbussche, and Ray W. Chrisman
Micro instrumentation : for high throughput experimentation and process intensification - a tool for PAT / / edited by Melvin V. Koch, Kurt M. Vandenbussche, and Ray W. Chrisman
Pubbl/distr/stampa Weinheim, : Wiley-VCH
Descrizione fisica 1 online resource (523 p.)
Disciplina 660.283
Altri autori (Persone) KochMelvin V
VandenbusscheKurt M
ChrismanRay W
Soggetto topico Chemical engineering - Equipment and supplies
Chemical processes
ISBN 1-280-92157-9
9786610921577
3-527-61062-6
3-527-61061-8
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Micro Instrumentation; Contents; Preface; List of Contributors; Part I Introducing the Concepts; 1 Introduction; 1.1 Background; 1.2 Analytical Tools for use in PAT; 1.3 The Center for Process Analytical Chemistry (CPAC) and the Summer Institute; 1.4 Topics covered by Previous CPAC Summer Institutes; 1.5 Recent Emphasis of CPAC Summer Institutes: High Throughput Experimentation and Process Intensification; 1.6 Conclusion; References; 2 Macro to Micro ... The Evolution of Process Analytical Systems; 2.1 Introduction; 2.1.2 Early Developments; 2.1.3 Developments since 1980; 2.1.4 Sampling Systems
2.1.4.1 Filtration2.1.4.2 The Fast Loop-Analytical Loop Strategy; 2.1.4.3 NeSSI; 2.1.5 General Reviews; 2.2 Chromatography; 2.2.1 Gas Chromatography; 2.2.2 Liquid Chromatography; 2.2.3 On-line Spectroscopy; 2.2.4 On-line Mass Spectrometry; 2.2.5 Microflow Techniques; References; 3 Process Intensification; 3.1 Introduction, Scope and Definitions; 3.2 Process Intensification in the Field of Reaction Engineering; 3.3 Process Intensification through Micro-structured Unit Operations; 3.3.1 Gas Phase Mass Transfer; 3.3.2 Liquid-Liquid Mass Transfer: Mixing and Emulsions
3.3.3 Gas-Liquid Mass Transfer3.3.4 Mass Transfer in Gas-Solid Systems; 3.3.5 Heat Transfer; 3.4 Case Studies; 3.4.1 Distributed Production of Methanol; 3.4.2 Distributed Production of Hydrogen; 3.5 Conclusions; References; 4 High Throughput Research; 4.1 Introduction; 4.2 Description of Terms; 4.3 Concept of a Research Process; 4.4 High Throughput Analytical; 4.5 Extracting Information from the Process; 4.6 Process Development becomes the Next Bottleneck; 4.7 Use of High Throughput Concepts for Process Development; 4.8 Microreactors for Process Development
4.9 Current Barriers and Limitations to Microscale Reaction Characterization4.10 Conclusion; References; Part II Technology Developments and Case Studies; 5 Introduction; 6 Microreactor Concepts and Processing; 6.1 Introduction; 6.2 Microreactor Technology - Interfacing and Discipline Cross-boundary Research; 6.3 Microstructured Mixer-reactors for Pilot and Production Range and Scale-out Issues; 6.3.1 Caterpillar Microstructured Mixer-reactors; 6.3.2 StarLam Microstructured Mixer-reactors; 6.3.3 Microstructured Heat Exchanger-reactors; 6.4 Fine-chemical Microreactor Plants
6.4.1 Laboratory-range Plants6.4.2 Pilot-range Plants; 6.5 Industrial Microreactor Process Development for Fine and Functional Chemistry; 6.5.1 Phenyl Boronic Acid Synthesis (Scheme 6.1) (Clariant/Frankfurt + IMM); 6.5.1.1 Process Development Issue; 6.5.1.2 Microreactor Plant and Processing Solution; 6.5.2 Azo Pigment Yellow 12 Manufacture (Scheme 6.2) (Trust Chem/Hangzhou + IMM); 6.5.2.1 Process Development Issue; 6.5.2.2 Microreactor Plant and Processing Solution; 6.5.3 Hydrogen Peroxide Synthesis (UOP/Chicago + IMM); 6.5.3.1 Process Development Issues
6.5.3.2 Microreactor Plant and Processing Solution
Record Nr. UNINA-9910877238903321
Weinheim, : Wiley-VCH
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui