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Chemical synthesis using supercritical fluids [[electronic resource] /] / edited by Philip G. Jessop and Walter Leitner
| Chemical synthesis using supercritical fluids [[electronic resource] /] / edited by Philip G. Jessop and Walter Leitner |
| Pubbl/distr/stampa | Weinheim ; ; New York, : Wiley-VCH, c1999 |
| Descrizione fisica | 1 online resource (503 p.) |
| Disciplina |
541.3
541.39 |
| Altri autori (Persone) |
JessopPhilip G
LeitnerWalter |
| Soggetto topico |
High pressure chemistry
Organic compounds - Synthesis Supercritical fluids |
| Soggetto genere / forma | Electronic books. |
| ISBN |
1-281-76423-X
9786611764234 3-527-61368-4 3-527-61369-2 |
| Formato | Materiale a stampa  |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Chemical Synthesis Using Supercritical Fluids; Preface; Contents; Contents; List of Contributors; 1 Introduction; 1.1 Supercritical Fluids as Media for Chemical Reactions; 1.1.1 What is a Supercritical Fluid (SCF)?; 1.1.2 Practical Aspects of Reactions in Supercritical Fluids (SFRs); 1.1.3 Motivation for Use of SCFs in Modern Chemical Synthesis; 1.1.4 A Brief History of Chemical Synthesis in SCFs; 1.1.4.1 Discovery of SCFs and their Use as Solvents; 1.1.4.2 Early Examples of Chemical Reactions in SCFs; 1.1.4.3 Industrial Use of SCFs as Reaction Media; References
1.2 Phase Behavior and Solubility1.2.1 Basic Physical Properties of Supercritical Fluids; 1.2.2 Phase Behavior in High Pressure Systems; 1.2.2.1 Types of Binary Phase Diagrams; 1.2.2.2 Asymmetric Binary Mixtures; 1.2.3 Factors Affecting Solubility in Supercritical Fluids; 1.2.3.1 SCF Solvent; 1.2.3.2 Chemical Functionality of the Solute; 1.2.3.3 Temperature and Pressure Effects; References; 1.3 Physical Properties as Related to Chemical Reactions; 1.3.1 Behavior of Diffusion Coefficients; 1.3.2 Diffusional Effects on Reactions; 1.3.3 Transition-state Theory Applied to SCFs 1.3.4 Density Dependence of Two Competing Reactions1.3.5 Solvation Effects on Reactions; 1.3.6 Conclusions; References; 2 Experimental Techniques; 2.1 High-pressure Reaction Equipment Design; 2.1.1 Introduction; 2.1.2 Basic Equipment and Components; 2.1.2.1 Design of Thick-Walled Vessels; 2.1.2.2 Closures and Connectors; 2.1.2.3 Tubing and Fittings; 2.1.2.4 Valves; 2.1.2.5 Compressors and Pumps; 2.1.2.6 Stirring and Mixing; 2.1.2.7 Optical Windows; 2.1.3 High Pressure Systems; 2.1.3.1 Single-batch High-pressure Reactors; 2.1.3.2 View Cells; 2.1.3.3 Systems for Continuous Processing 2.1.4 SummaryReferences; 2.2 Extraction and Related Separation Techniques; 2.2.1 General Aspects of Supercritical Fluids as Mass Separating Agents; 2.2.2 Extraction from Solids; 2.2.2.1 Basic Process Design; 2.2.2.2 Process Parameters; 2.2.2.3 Modeling the Extraction; 2.2.2.4 Solids in Multiple Stages and Countercurrent Operation in SFE; 2.2.2.5 Continuous Extraction of Contaminated Soil with Supercritical Water; 2.2.3 Countercurrent Multistage Extraction; 2.2.3.1 Basic Process Design; 2.2.3.2 Phase Equilibria; 2.2.3.3 Separation Analysis with Respect to Theoretical Stages 2.2.3.4 Multicomponent Process Simulation2.2.3.5 Determination of the Height (Length) of a Theoretical Stage; 2.2.3.6 Determination of Column Diameter; 2.2.4 Chromatographic Separation with Supercritical Fluids; 2.2.4.1 Design of SFC Apparatus; 2.2.4.2 Methods for Scale-up of Chromatography; 2.2.5 Conclusion; References; 2.3 Precipitation and Crystallization Techniques; 2.3.1 Introduction; 2.3.2 Thermodynamics and Phase Equilibria; 2.3.2.1 CSS, PGSS and RESS; 2.3.2.2 GASP; 2.3.3 Process Basics and Reference Schemes; 2.3.3.1 Crystallization from a Supercritical Solution (CSS) 2.3.3.2 Formation of Particles from Gas Saturated Solution (PGSS) |
| Record Nr. | UNINA-9910144282503321 |
| Weinheim ; ; New York, : Wiley-VCH, c1999 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Chemical synthesis using supercritical fluids [[electronic resource] /] / edited by Philip G. Jessop and Walter Leitner
| Chemical synthesis using supercritical fluids [[electronic resource] /] / edited by Philip G. Jessop and Walter Leitner |
| Pubbl/distr/stampa | Weinheim ; ; New York, : Wiley-VCH, c1999 |
| Descrizione fisica | 1 online resource (503 p.) |
| Disciplina |
541.3
541.39 |
| Altri autori (Persone) |
JessopPhilip G
LeitnerWalter |
| Soggetto topico |
High pressure chemistry
Organic compounds - Synthesis Supercritical fluids |
| ISBN |
1-281-76423-X
9786611764234 3-527-61368-4 3-527-61369-2 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Chemical Synthesis Using Supercritical Fluids; Preface; Contents; Contents; List of Contributors; 1 Introduction; 1.1 Supercritical Fluids as Media for Chemical Reactions; 1.1.1 What is a Supercritical Fluid (SCF)?; 1.1.2 Practical Aspects of Reactions in Supercritical Fluids (SFRs); 1.1.3 Motivation for Use of SCFs in Modern Chemical Synthesis; 1.1.4 A Brief History of Chemical Synthesis in SCFs; 1.1.4.1 Discovery of SCFs and their Use as Solvents; 1.1.4.2 Early Examples of Chemical Reactions in SCFs; 1.1.4.3 Industrial Use of SCFs as Reaction Media; References
1.2 Phase Behavior and Solubility1.2.1 Basic Physical Properties of Supercritical Fluids; 1.2.2 Phase Behavior in High Pressure Systems; 1.2.2.1 Types of Binary Phase Diagrams; 1.2.2.2 Asymmetric Binary Mixtures; 1.2.3 Factors Affecting Solubility in Supercritical Fluids; 1.2.3.1 SCF Solvent; 1.2.3.2 Chemical Functionality of the Solute; 1.2.3.3 Temperature and Pressure Effects; References; 1.3 Physical Properties as Related to Chemical Reactions; 1.3.1 Behavior of Diffusion Coefficients; 1.3.2 Diffusional Effects on Reactions; 1.3.3 Transition-state Theory Applied to SCFs 1.3.4 Density Dependence of Two Competing Reactions1.3.5 Solvation Effects on Reactions; 1.3.6 Conclusions; References; 2 Experimental Techniques; 2.1 High-pressure Reaction Equipment Design; 2.1.1 Introduction; 2.1.2 Basic Equipment and Components; 2.1.2.1 Design of Thick-Walled Vessels; 2.1.2.2 Closures and Connectors; 2.1.2.3 Tubing and Fittings; 2.1.2.4 Valves; 2.1.2.5 Compressors and Pumps; 2.1.2.6 Stirring and Mixing; 2.1.2.7 Optical Windows; 2.1.3 High Pressure Systems; 2.1.3.1 Single-batch High-pressure Reactors; 2.1.3.2 View Cells; 2.1.3.3 Systems for Continuous Processing 2.1.4 SummaryReferences; 2.2 Extraction and Related Separation Techniques; 2.2.1 General Aspects of Supercritical Fluids as Mass Separating Agents; 2.2.2 Extraction from Solids; 2.2.2.1 Basic Process Design; 2.2.2.2 Process Parameters; 2.2.2.3 Modeling the Extraction; 2.2.2.4 Solids in Multiple Stages and Countercurrent Operation in SFE; 2.2.2.5 Continuous Extraction of Contaminated Soil with Supercritical Water; 2.2.3 Countercurrent Multistage Extraction; 2.2.3.1 Basic Process Design; 2.2.3.2 Phase Equilibria; 2.2.3.3 Separation Analysis with Respect to Theoretical Stages 2.2.3.4 Multicomponent Process Simulation2.2.3.5 Determination of the Height (Length) of a Theoretical Stage; 2.2.3.6 Determination of Column Diameter; 2.2.4 Chromatographic Separation with Supercritical Fluids; 2.2.4.1 Design of SFC Apparatus; 2.2.4.2 Methods for Scale-up of Chromatography; 2.2.5 Conclusion; References; 2.3 Precipitation and Crystallization Techniques; 2.3.1 Introduction; 2.3.2 Thermodynamics and Phase Equilibria; 2.3.2.1 CSS, PGSS and RESS; 2.3.2.2 GASP; 2.3.3 Process Basics and Reference Schemes; 2.3.3.1 Crystallization from a Supercritical Solution (CSS) 2.3.3.2 Formation of Particles from Gas Saturated Solution (PGSS) |
| Record Nr. | UNINA-9910830740303321 |
| Weinheim ; ; New York, : Wiley-VCH, c1999 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Chemical synthesis using supercritical fluids / / edited by Philip G. Jessop and Walter Leitner
| Chemical synthesis using supercritical fluids / / edited by Philip G. Jessop and Walter Leitner |
| Pubbl/distr/stampa | Weinheim ; ; New York, : Wiley-VCH, c1999 |
| Descrizione fisica | 1 online resource (503 p.) |
| Disciplina |
541.3
541.39 |
| Altri autori (Persone) |
JessopPhilip G
LeitnerWalter |
| Soggetto topico |
High pressure chemistry
Organic compounds - Synthesis Supercritical fluids |
| ISBN |
1-281-76423-X
9786611764234 3-527-61368-4 3-527-61369-2 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Chemical Synthesis Using Supercritical Fluids; Preface; Contents; Contents; List of Contributors; 1 Introduction; 1.1 Supercritical Fluids as Media for Chemical Reactions; 1.1.1 What is a Supercritical Fluid (SCF)?; 1.1.2 Practical Aspects of Reactions in Supercritical Fluids (SFRs); 1.1.3 Motivation for Use of SCFs in Modern Chemical Synthesis; 1.1.4 A Brief History of Chemical Synthesis in SCFs; 1.1.4.1 Discovery of SCFs and their Use as Solvents; 1.1.4.2 Early Examples of Chemical Reactions in SCFs; 1.1.4.3 Industrial Use of SCFs as Reaction Media; References
1.2 Phase Behavior and Solubility1.2.1 Basic Physical Properties of Supercritical Fluids; 1.2.2 Phase Behavior in High Pressure Systems; 1.2.2.1 Types of Binary Phase Diagrams; 1.2.2.2 Asymmetric Binary Mixtures; 1.2.3 Factors Affecting Solubility in Supercritical Fluids; 1.2.3.1 SCF Solvent; 1.2.3.2 Chemical Functionality of the Solute; 1.2.3.3 Temperature and Pressure Effects; References; 1.3 Physical Properties as Related to Chemical Reactions; 1.3.1 Behavior of Diffusion Coefficients; 1.3.2 Diffusional Effects on Reactions; 1.3.3 Transition-state Theory Applied to SCFs 1.3.4 Density Dependence of Two Competing Reactions1.3.5 Solvation Effects on Reactions; 1.3.6 Conclusions; References; 2 Experimental Techniques; 2.1 High-pressure Reaction Equipment Design; 2.1.1 Introduction; 2.1.2 Basic Equipment and Components; 2.1.2.1 Design of Thick-Walled Vessels; 2.1.2.2 Closures and Connectors; 2.1.2.3 Tubing and Fittings; 2.1.2.4 Valves; 2.1.2.5 Compressors and Pumps; 2.1.2.6 Stirring and Mixing; 2.1.2.7 Optical Windows; 2.1.3 High Pressure Systems; 2.1.3.1 Single-batch High-pressure Reactors; 2.1.3.2 View Cells; 2.1.3.3 Systems for Continuous Processing 2.1.4 SummaryReferences; 2.2 Extraction and Related Separation Techniques; 2.2.1 General Aspects of Supercritical Fluids as Mass Separating Agents; 2.2.2 Extraction from Solids; 2.2.2.1 Basic Process Design; 2.2.2.2 Process Parameters; 2.2.2.3 Modeling the Extraction; 2.2.2.4 Solids in Multiple Stages and Countercurrent Operation in SFE; 2.2.2.5 Continuous Extraction of Contaminated Soil with Supercritical Water; 2.2.3 Countercurrent Multistage Extraction; 2.2.3.1 Basic Process Design; 2.2.3.2 Phase Equilibria; 2.2.3.3 Separation Analysis with Respect to Theoretical Stages 2.2.3.4 Multicomponent Process Simulation2.2.3.5 Determination of the Height (Length) of a Theoretical Stage; 2.2.3.6 Determination of Column Diameter; 2.2.4 Chromatographic Separation with Supercritical Fluids; 2.2.4.1 Design of SFC Apparatus; 2.2.4.2 Methods for Scale-up of Chromatography; 2.2.5 Conclusion; References; 2.3 Precipitation and Crystallization Techniques; 2.3.1 Introduction; 2.3.2 Thermodynamics and Phase Equilibria; 2.3.2.1 CSS, PGSS and RESS; 2.3.2.2 GASP; 2.3.3 Process Basics and Reference Schemes; 2.3.3.1 Crystallization from a Supercritical Solution (CSS) 2.3.3.2 Formation of Particles from Gas Saturated Solution (PGSS) |
| Record Nr. | UNINA-9910877316203321 |
| Weinheim ; ; New York, : Wiley-VCH, c1999 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||