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Quality assurance in analytical chemistry [[electronic resource] ] : applications in environmental, food, and materials analysis, biotechnology, and medical engineering / / Werner Funk, Vera Dammann, Gerhild Donnevert
| Quality assurance in analytical chemistry [[electronic resource] ] : applications in environmental, food, and materials analysis, biotechnology, and medical engineering / / Werner Funk, Vera Dammann, Gerhild Donnevert |
| Autore | Funk Werner <1944-1996.> |
| Edizione | [2nd ed.] |
| Pubbl/distr/stampa | Weinheim, : Wiley-VCH, c2007 |
| Descrizione fisica | 1 online resource (303 p.) |
| Disciplina |
540
543.0685 |
| Altri autori (Persone) |
DammannVera
DonnevertGerhild |
| Soggetto topico |
Chemical laboratories - Quality control
Chemistry, Analytic - Quality control Chemistry, Analytic - Technique |
| ISBN |
1-281-08789-0
9786611087890 3-527-60944-X 3-527-60930-X |
| Formato | Materiale a stampa  |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Quality Assurance in Analytical Chemistry; Contents; Preface to the Second Edition; Preface to the First Edition; List of Symbols; 0 Introduction; 0.1 General Differentiation of Analytical Processes; 0.2 Quality of Analytical Processes and Results; 0.3 The System of Analytical Quality Assurance; 0.4 The Four-Phase Model of Analytical Quality Assurance; 1 Phase I: Establishing a New Analytical Procedure; 1.1 Introduction; 1.1.1 Objectives of Phase I; 1.1.2 When Are Characteristic Data Obtained?; 1.1.3 The Progression of Phase I; 1.1.4 Results of Phase I; Statistical Data
1.2 Calibration of the Fundamental Analytical Procedure (Fundamental Calibration)1.2.1 Establishment of an Analytical Range; 1.2.2 Preparation of Standard Samples; 1.2.3 Determination of the Calibration Function and Process Data; 1.2.3.1 Process Data for the Linear Calibration Function; 1.2.3.2 Process Data for the Second-Order Calibration Function; 1.2.3.3 Calculating Analytical Results with the Aid of the Calibration Function; 1.2.4 Verification of the Fundamental Calibration; 1.2.4.1 Verification of Linearity; 1.2.4.2 Verification of Precision; 1.3 Analyses at Very Low Concentrations 1.3.1 Decision Limit [34, 120, 132]1.3.2 Determining the Minimum Detectable Value [34, 120]; 1.3.2.1 Minimum Detectable Value, Determined Using the Distribution of Blank Values; 1.3.2.2 Minimum Detectable Value, Obtained Using the Calibration Function; 1.3.3 Limit of Quantification [34]; 1.3.4 Quick Estimation; 1.3.5 Estimation of the Decision Limit and Limit of Quantification Using the S/N Ratio; 1.4 Validation of Individual Process Steps and Examination of Matrix Influences; 1.4.1 Systematic Errors; 1.4.1.1 Constant Systematic Errors, Additive Deviations 1.4.1.2 Proportional Systematic Errors, Multiplicative Deviations1.4.2 Establishment and Assessment of the Recovery Function; 1.4.2.1 Prerequisites for the Interpretation of the Recovery Function; 1.4.2.2 Testing for Systematic Errors; 1.4.3 Application of the Recovery Function; 1.4.3.1 Checking Individual Process Steps; 1.4.3.2 Determination of the Recovery Function to Prove the Influence of a Matrix; 1.5 Additional Statistical Methods; 1.6 Use of Internal Standards [50]; 1.6.1 Definition, Purpose; 1.6.2 Conditions and Limitations of the Use of Internal Standards; 1.6.3 Procedure 1.7 Preparing for Routine Analysis1.7.1 Examination of the Time Dependency of Measured Values; 1.7.1.1 Comparison of the "Within Batch" Standard Deviation (s(w)) with the "Between Batches" Standard Deviation (s(b)) [215]; 1.7.1.2 Determining the Need for Daily Adjustment of Analytical Equipment; 1.7.1.3 The Trend Test; 1.8 Summary of the Results of Phase I (Process Development): Documentation; 2 Phase II: An Analytical Process Becomes Routine; Preparative Quality Assurance; 2.1 Introduction; 2.1.1 Objective of Phase II; 2.1.2 Execution of Phase II; 2.1.3 Progression of Phase II 2.1.4 Results of Phase II |
| Record Nr. | UNINA-9910142572403321 |
Funk Werner <1944-1996.>
|
||
| Weinheim, : Wiley-VCH, c2007 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Quality assurance in analytical chemistry [[electronic resource] ] : applications in environmental, food, and materials analysis, biotechnology, and medical engineering / / Werner Funk, Vera Dammann, Gerhild Donnevert
| Quality assurance in analytical chemistry [[electronic resource] ] : applications in environmental, food, and materials analysis, biotechnology, and medical engineering / / Werner Funk, Vera Dammann, Gerhild Donnevert |
| Autore | Funk Werner <1944-1996.> |
| Edizione | [2nd ed.] |
| Pubbl/distr/stampa | Weinheim, : Wiley-VCH, c2007 |
| Descrizione fisica | 1 online resource (303 p.) |
| Disciplina |
540
543.0685 |
| Altri autori (Persone) |
DammannVera
DonnevertGerhild |
| Soggetto topico |
Chemical laboratories - Quality control
Chemistry, Analytic - Quality control Chemistry, Analytic - Technique |
| ISBN |
1-281-08789-0
9786611087890 3-527-60944-X 3-527-60930-X |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Quality Assurance in Analytical Chemistry; Contents; Preface to the Second Edition; Preface to the First Edition; List of Symbols; 0 Introduction; 0.1 General Differentiation of Analytical Processes; 0.2 Quality of Analytical Processes and Results; 0.3 The System of Analytical Quality Assurance; 0.4 The Four-Phase Model of Analytical Quality Assurance; 1 Phase I: Establishing a New Analytical Procedure; 1.1 Introduction; 1.1.1 Objectives of Phase I; 1.1.2 When Are Characteristic Data Obtained?; 1.1.3 The Progression of Phase I; 1.1.4 Results of Phase I; Statistical Data
1.2 Calibration of the Fundamental Analytical Procedure (Fundamental Calibration)1.2.1 Establishment of an Analytical Range; 1.2.2 Preparation of Standard Samples; 1.2.3 Determination of the Calibration Function and Process Data; 1.2.3.1 Process Data for the Linear Calibration Function; 1.2.3.2 Process Data for the Second-Order Calibration Function; 1.2.3.3 Calculating Analytical Results with the Aid of the Calibration Function; 1.2.4 Verification of the Fundamental Calibration; 1.2.4.1 Verification of Linearity; 1.2.4.2 Verification of Precision; 1.3 Analyses at Very Low Concentrations 1.3.1 Decision Limit [34, 120, 132]1.3.2 Determining the Minimum Detectable Value [34, 120]; 1.3.2.1 Minimum Detectable Value, Determined Using the Distribution of Blank Values; 1.3.2.2 Minimum Detectable Value, Obtained Using the Calibration Function; 1.3.3 Limit of Quantification [34]; 1.3.4 Quick Estimation; 1.3.5 Estimation of the Decision Limit and Limit of Quantification Using the S/N Ratio; 1.4 Validation of Individual Process Steps and Examination of Matrix Influences; 1.4.1 Systematic Errors; 1.4.1.1 Constant Systematic Errors, Additive Deviations 1.4.1.2 Proportional Systematic Errors, Multiplicative Deviations1.4.2 Establishment and Assessment of the Recovery Function; 1.4.2.1 Prerequisites for the Interpretation of the Recovery Function; 1.4.2.2 Testing for Systematic Errors; 1.4.3 Application of the Recovery Function; 1.4.3.1 Checking Individual Process Steps; 1.4.3.2 Determination of the Recovery Function to Prove the Influence of a Matrix; 1.5 Additional Statistical Methods; 1.6 Use of Internal Standards [50]; 1.6.1 Definition, Purpose; 1.6.2 Conditions and Limitations of the Use of Internal Standards; 1.6.3 Procedure 1.7 Preparing for Routine Analysis1.7.1 Examination of the Time Dependency of Measured Values; 1.7.1.1 Comparison of the "Within Batch" Standard Deviation (s(w)) with the "Between Batches" Standard Deviation (s(b)) [215]; 1.7.1.2 Determining the Need for Daily Adjustment of Analytical Equipment; 1.7.1.3 The Trend Test; 1.8 Summary of the Results of Phase I (Process Development): Documentation; 2 Phase II: An Analytical Process Becomes Routine; Preparative Quality Assurance; 2.1 Introduction; 2.1.1 Objective of Phase II; 2.1.2 Execution of Phase II; 2.1.3 Progression of Phase II 2.1.4 Results of Phase II |
| Record Nr. | UNINA-9910829881303321 |
|
Funk Werner <1944-1996.>
|
||
| Weinheim, : Wiley-VCH, c2007 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Quality assurance in analytical chemistry : applications in environmental, food, and materials analysis, biotechnology, and medical engineering / / Werner Funk, Vera Dammann, Gerhild Donnevert
| Quality assurance in analytical chemistry : applications in environmental, food, and materials analysis, biotechnology, and medical engineering / / Werner Funk, Vera Dammann, Gerhild Donnevert |
| Autore | Funk Werner <1944-1996.> |
| Edizione | [2nd ed.] |
| Pubbl/distr/stampa | Weinheim, : Wiley-VCH, c2007 |
| Descrizione fisica | 1 online resource (303 p.) |
| Disciplina |
540
543.0685 |
| Altri autori (Persone) |
DammannVera
DonnevertGerhild |
| Soggetto topico |
Chemical laboratories - Quality control
Analytical chemistry - Quality control Analytical chemistry - Technique |
| ISBN |
1-281-08789-0
9786611087890 3-527-60944-X 3-527-60930-X |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Quality Assurance in Analytical Chemistry; Contents; Preface to the Second Edition; Preface to the First Edition; List of Symbols; 0 Introduction; 0.1 General Differentiation of Analytical Processes; 0.2 Quality of Analytical Processes and Results; 0.3 The System of Analytical Quality Assurance; 0.4 The Four-Phase Model of Analytical Quality Assurance; 1 Phase I: Establishing a New Analytical Procedure; 1.1 Introduction; 1.1.1 Objectives of Phase I; 1.1.2 When Are Characteristic Data Obtained?; 1.1.3 The Progression of Phase I; 1.1.4 Results of Phase I; Statistical Data
1.2 Calibration of the Fundamental Analytical Procedure (Fundamental Calibration)1.2.1 Establishment of an Analytical Range; 1.2.2 Preparation of Standard Samples; 1.2.3 Determination of the Calibration Function and Process Data; 1.2.3.1 Process Data for the Linear Calibration Function; 1.2.3.2 Process Data for the Second-Order Calibration Function; 1.2.3.3 Calculating Analytical Results with the Aid of the Calibration Function; 1.2.4 Verification of the Fundamental Calibration; 1.2.4.1 Verification of Linearity; 1.2.4.2 Verification of Precision; 1.3 Analyses at Very Low Concentrations 1.3.1 Decision Limit [34, 120, 132]1.3.2 Determining the Minimum Detectable Value [34, 120]; 1.3.2.1 Minimum Detectable Value, Determined Using the Distribution of Blank Values; 1.3.2.2 Minimum Detectable Value, Obtained Using the Calibration Function; 1.3.3 Limit of Quantification [34]; 1.3.4 Quick Estimation; 1.3.5 Estimation of the Decision Limit and Limit of Quantification Using the S/N Ratio; 1.4 Validation of Individual Process Steps and Examination of Matrix Influences; 1.4.1 Systematic Errors; 1.4.1.1 Constant Systematic Errors, Additive Deviations 1.4.1.2 Proportional Systematic Errors, Multiplicative Deviations1.4.2 Establishment and Assessment of the Recovery Function; 1.4.2.1 Prerequisites for the Interpretation of the Recovery Function; 1.4.2.2 Testing for Systematic Errors; 1.4.3 Application of the Recovery Function; 1.4.3.1 Checking Individual Process Steps; 1.4.3.2 Determination of the Recovery Function to Prove the Influence of a Matrix; 1.5 Additional Statistical Methods; 1.6 Use of Internal Standards [50]; 1.6.1 Definition, Purpose; 1.6.2 Conditions and Limitations of the Use of Internal Standards; 1.6.3 Procedure 1.7 Preparing for Routine Analysis1.7.1 Examination of the Time Dependency of Measured Values; 1.7.1.1 Comparison of the "Within Batch" Standard Deviation (s(w)) with the "Between Batches" Standard Deviation (s(b)) [215]; 1.7.1.2 Determining the Need for Daily Adjustment of Analytical Equipment; 1.7.1.3 The Trend Test; 1.8 Summary of the Results of Phase I (Process Development): Documentation; 2 Phase II: An Analytical Process Becomes Routine; Preparative Quality Assurance; 2.1 Introduction; 2.1.1 Objective of Phase II; 2.1.2 Execution of Phase II; 2.1.3 Progression of Phase II 2.1.4 Results of Phase II |
| Record Nr. | UNINA-9910876565703321 |
|
Funk Werner <1944-1996.>
|
||
| Weinheim, : Wiley-VCH, c2007 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||