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Solid-state NMR spectroscopy : principles and applications / / edited by Melinda J. Duer
| Solid-state NMR spectroscopy : principles and applications / / edited by Melinda J. Duer |
| Pubbl/distr/stampa | Oxford : , : Blackwell Science, , [2002] |
| Descrizione fisica | 1 online resource (562 pages) |
| Disciplina |
543.0877
543/.0877 |
| Altri autori (Persone) | DuerMelinda J |
| Soggetto topico |
Nuclear magnetic resonance spectroscopy
Solid state chemistry |
| ISBN |
1-281-31276-2
9786611312763 0-470-99939-X 0-470-99938-1 |
| Formato | Materiale a stampa  |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Solid-State NMR Spectroscopy Principles and Applications; List of Contributors; Contents; Index; Preface; Acknowledgements; Part I The Theory of Solid-State NMR and its Experiments; 1 The Basics of Solid-State NMR; 1.1 The vector model of pulsed NMR; 1.1.1 Nuclei in a static, uniform magnetic field; 1.1.2 The effect of rf pulses; 1.2 The quantum mechanical picture: hamiltonians and the Schrödinger equation; Box 1.1 Quantum mechanics and NMR; 1.2.1 Nuclei in a static, uniform field; 1.2.2 The effect of rf pulses; Box 1.2 Exponential operators, rotation operators and rotations
1.3 The density matrix representation and coherences1.3.1 Coherences and populations; 1.3.2 The density operator at thermal equilibrium; 1.3.3 Time evolution of the density matrix; 1.4 Nuclear spin interactions; 1.4.1 The chemical shift and chemical shift anisotropy; 1.4.2 Dipole-dipole coupling; Box 1.3 Basis sets for multispin systems; 1.4.3 Quadrupolar coupling; 1.5 Calculating NMR powder patterns; 1.6 General features of NMR experiments; 1.6.1 Multidimensional NMR; 1.6.2 Phase cycling; 1.6.3 Quadrature detection; Box 1.4 The NMR spectrometer; References 2 Essential Techniques for Spin-1/2 Nuclei2.1 Introduction; 2.2 Magic-angle spinning (MAS); 2.2.1 Spinning sidebands; 2.2.2 Rotor or rotational echoes; 2.2.3 Removing spinning sidebands; 2.2.4 Magic-angle spinning for homonuclear dipolar couplings; 2.3 High-power decoupling; 2.4 Multiple pulse decoupling sequences; Box 2.1 Average hamiltonian theory and the toggling frame; 2.5 Cross-polarization; 2.5.1 Theory; 2.5.2 Experimental details; Box 2.2 Cross-polarization and magic-angle spinning; 2.6 Solid or quadrupole echo pulse sequence; References; 3 Dipolar Coupling: Its Measurement and Uses 3.1 IntroductionBox 3.1 The dipolar hamiltonian in terms of spherical tensor operators; 3.2 Techniques for measuring homonuclear dipolar couplings; 3.2.1 Recoupling pulse sequences; Box 3.2 Analysis of the DRAMA pulse sequence; 3.2.2 Double-quantum filtered experiments; 3.2.3 Rotational resonance; Box 3.3 Excitation of double-quantum coherence under magic-angle spinning; 3.3 Techniques for measuring heteronuclear dipolar couplings; Box 3.4 Analysis of the C7 pulse sequence for exciting double-quantum coherence in dipolar-coupled spin pairs; 3.3.1 Spin-echo double resonance Box 3.5 Theory of rotational resonance3.3.2 Rotational-echo double resonance; Box 3.6 Analysis of the REDOR experiment; 3.4 Techniques for dipolar-coupled quadrupolar (spin-1/2) pairs; 3.4.1 Transfer of population in double resonance; 3.4.2 Rotational echo, adiabatic passage, double resonance; 3.5 Techniques for measuring dipolar couplings between quadrupolar nuclei; 3.6 Correlation experiments; 3.6.1 Homonuclear correlation experiments for spin-systems; 3.6.2 Homonuclear correlation experiments for quadrupolar spin systems; 3.6.3 Heteronuclear correlation experiments for spin-1/2 3.7 Spin-counting experiments |
| Record Nr. | UNINA-9910145741203321 |
| Oxford : , : Blackwell Science, , [2002] | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Solid-state NMR spectroscopy : principles and applications / / edited by Melinda J. Duer
| Solid-state NMR spectroscopy : principles and applications / / edited by Melinda J. Duer |
| Edizione | [1st ed.] |
| Pubbl/distr/stampa | Oxford : , : Blackwell Science, , [2002] |
| Descrizione fisica | 1 online resource (562 pages) |
| Disciplina |
543.0877
543/.0877 |
| Altri autori (Persone) | DuerMelinda J |
| Soggetto topico |
Nuclear magnetic resonance spectroscopy
Solid state chemistry |
| ISBN |
1-281-31276-2
9786611312763 0-470-99939-X 0-470-99938-1 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Solid-State NMR Spectroscopy Principles and Applications; List of Contributors; Contents; Index; Preface; Acknowledgements; Part I The Theory of Solid-State NMR and its Experiments; 1 The Basics of Solid-State NMR; 1.1 The vector model of pulsed NMR; 1.1.1 Nuclei in a static, uniform magnetic field; 1.1.2 The effect of rf pulses; 1.2 The quantum mechanical picture: hamiltonians and the Schrödinger equation; Box 1.1 Quantum mechanics and NMR; 1.2.1 Nuclei in a static, uniform field; 1.2.2 The effect of rf pulses; Box 1.2 Exponential operators, rotation operators and rotations
1.3 The density matrix representation and coherences1.3.1 Coherences and populations; 1.3.2 The density operator at thermal equilibrium; 1.3.3 Time evolution of the density matrix; 1.4 Nuclear spin interactions; 1.4.1 The chemical shift and chemical shift anisotropy; 1.4.2 Dipole-dipole coupling; Box 1.3 Basis sets for multispin systems; 1.4.3 Quadrupolar coupling; 1.5 Calculating NMR powder patterns; 1.6 General features of NMR experiments; 1.6.1 Multidimensional NMR; 1.6.2 Phase cycling; 1.6.3 Quadrature detection; Box 1.4 The NMR spectrometer; References 2 Essential Techniques for Spin-1/2 Nuclei2.1 Introduction; 2.2 Magic-angle spinning (MAS); 2.2.1 Spinning sidebands; 2.2.2 Rotor or rotational echoes; 2.2.3 Removing spinning sidebands; 2.2.4 Magic-angle spinning for homonuclear dipolar couplings; 2.3 High-power decoupling; 2.4 Multiple pulse decoupling sequences; Box 2.1 Average hamiltonian theory and the toggling frame; 2.5 Cross-polarization; 2.5.1 Theory; 2.5.2 Experimental details; Box 2.2 Cross-polarization and magic-angle spinning; 2.6 Solid or quadrupole echo pulse sequence; References; 3 Dipolar Coupling: Its Measurement and Uses 3.1 IntroductionBox 3.1 The dipolar hamiltonian in terms of spherical tensor operators; 3.2 Techniques for measuring homonuclear dipolar couplings; 3.2.1 Recoupling pulse sequences; Box 3.2 Analysis of the DRAMA pulse sequence; 3.2.2 Double-quantum filtered experiments; 3.2.3 Rotational resonance; Box 3.3 Excitation of double-quantum coherence under magic-angle spinning; 3.3 Techniques for measuring heteronuclear dipolar couplings; Box 3.4 Analysis of the C7 pulse sequence for exciting double-quantum coherence in dipolar-coupled spin pairs; 3.3.1 Spin-echo double resonance Box 3.5 Theory of rotational resonance3.3.2 Rotational-echo double resonance; Box 3.6 Analysis of the REDOR experiment; 3.4 Techniques for dipolar-coupled quadrupolar (spin-1/2) pairs; 3.4.1 Transfer of population in double resonance; 3.4.2 Rotational echo, adiabatic passage, double resonance; 3.5 Techniques for measuring dipolar couplings between quadrupolar nuclei; 3.6 Correlation experiments; 3.6.1 Homonuclear correlation experiments for spin-systems; 3.6.2 Homonuclear correlation experiments for quadrupolar spin systems; 3.6.3 Heteronuclear correlation experiments for spin-1/2 3.7 Spin-counting experiments |
| Record Nr. | UNINA-9910815642603321 |
| Oxford : , : Blackwell Science, , [2002] | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Solid-state NMR spectroscopy : principles and applications / / edited by Melinda J. Duer
| Solid-state NMR spectroscopy : principles and applications / / edited by Melinda J. Duer |
| Edizione | [1st ed.] |
| Pubbl/distr/stampa | Oxford : , : Blackwell Science, , [2002] |
| Descrizione fisica | 1 online resource (562 pages) |
| Disciplina |
543.0877
543/.0877 |
| Altri autori (Persone) | DuerMelinda J |
| Soggetto topico |
Nuclear magnetic resonance spectroscopy
Solid state chemistry |
| ISBN |
1-281-31276-2
9786611312763 0-470-99939-X 0-470-99938-1 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Solid-State NMR Spectroscopy Principles and Applications; List of Contributors; Contents; Index; Preface; Acknowledgements; Part I The Theory of Solid-State NMR and its Experiments; 1 The Basics of Solid-State NMR; 1.1 The vector model of pulsed NMR; 1.1.1 Nuclei in a static, uniform magnetic field; 1.1.2 The effect of rf pulses; 1.2 The quantum mechanical picture: hamiltonians and the Schrödinger equation; Box 1.1 Quantum mechanics and NMR; 1.2.1 Nuclei in a static, uniform field; 1.2.2 The effect of rf pulses; Box 1.2 Exponential operators, rotation operators and rotations
1.3 The density matrix representation and coherences1.3.1 Coherences and populations; 1.3.2 The density operator at thermal equilibrium; 1.3.3 Time evolution of the density matrix; 1.4 Nuclear spin interactions; 1.4.1 The chemical shift and chemical shift anisotropy; 1.4.2 Dipole-dipole coupling; Box 1.3 Basis sets for multispin systems; 1.4.3 Quadrupolar coupling; 1.5 Calculating NMR powder patterns; 1.6 General features of NMR experiments; 1.6.1 Multidimensional NMR; 1.6.2 Phase cycling; 1.6.3 Quadrature detection; Box 1.4 The NMR spectrometer; References 2 Essential Techniques for Spin-1/2 Nuclei2.1 Introduction; 2.2 Magic-angle spinning (MAS); 2.2.1 Spinning sidebands; 2.2.2 Rotor or rotational echoes; 2.2.3 Removing spinning sidebands; 2.2.4 Magic-angle spinning for homonuclear dipolar couplings; 2.3 High-power decoupling; 2.4 Multiple pulse decoupling sequences; Box 2.1 Average hamiltonian theory and the toggling frame; 2.5 Cross-polarization; 2.5.1 Theory; 2.5.2 Experimental details; Box 2.2 Cross-polarization and magic-angle spinning; 2.6 Solid or quadrupole echo pulse sequence; References; 3 Dipolar Coupling: Its Measurement and Uses 3.1 IntroductionBox 3.1 The dipolar hamiltonian in terms of spherical tensor operators; 3.2 Techniques for measuring homonuclear dipolar couplings; 3.2.1 Recoupling pulse sequences; Box 3.2 Analysis of the DRAMA pulse sequence; 3.2.2 Double-quantum filtered experiments; 3.2.3 Rotational resonance; Box 3.3 Excitation of double-quantum coherence under magic-angle spinning; 3.3 Techniques for measuring heteronuclear dipolar couplings; Box 3.4 Analysis of the C7 pulse sequence for exciting double-quantum coherence in dipolar-coupled spin pairs; 3.3.1 Spin-echo double resonance Box 3.5 Theory of rotational resonance3.3.2 Rotational-echo double resonance; Box 3.6 Analysis of the REDOR experiment; 3.4 Techniques for dipolar-coupled quadrupolar (spin-1/2) pairs; 3.4.1 Transfer of population in double resonance; 3.4.2 Rotational echo, adiabatic passage, double resonance; 3.5 Techniques for measuring dipolar couplings between quadrupolar nuclei; 3.6 Correlation experiments; 3.6.1 Homonuclear correlation experiments for spin-systems; 3.6.2 Homonuclear correlation experiments for quadrupolar spin systems; 3.6.3 Heteronuclear correlation experiments for spin-1/2 3.7 Spin-counting experiments |
| Record Nr. | UNISA-996202095403316 |
| Oxford : , : Blackwell Science, , [2002] | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. di Salerno | ||
| ||