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Columns for gas chromatography [[electronic resource] ] : performance and selection / / Eugene F. Barry, Robert L. Grob
| Columns for gas chromatography [[electronic resource] ] : performance and selection / / Eugene F. Barry, Robert L. Grob |
| Autore | Barry Eugene F |
| Pubbl/distr/stampa | Hoboken, N.J., : Wiley-Interscience, c2007 |
| Descrizione fisica | 1 online resource (314 p.) |
| Disciplina |
543.85
543/.85 |
| Altri autori (Persone) | GrobRobert Lee |
| Soggetto topico |
Gas chromatography
Chromatographic analysis |
| ISBN |
1-280-82679-7
9786610826797 0-470-11418-5 0-470-11417-7 |
| Formato | Materiale a stampa  |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
COLUMNS FOR GAS CHROMATOGRAPHY; CONTENTS; Preface; Acknowledgments; 1 Introduction; 1.1 Evolution of Gas Chromatographic Columns; 1.2 Central Role Played by the Column; 1.3 Justification for Column Selection and Care; 1.4 Literature on Gas Chromatographic Columns; 1.5 Gas Chromatographic Resources on the Internet; References; 2 Packed Column Gas Chromatography; 2.1 Introduction; 2.2 Solid Supports and Adsorbents; Supports for Gas-Liquid Chromatography; Adsorbents for Gas-Solid Chromatography; 2.3 Stationary Phases; Requirements of a Stationary Phase; USP Designation of Stationary Phases
Kovats Retention IndexMcReynolds and Rohrschneider Classifications of Stationary Phases; Evaluation of Column Operation; Optimization of Packed Column Separations; 2.4 Column Preparation; Coating Methods; Tubing Materials and Dimensions; Glass Wool Plugs and Column Fittings; Filling the Column; Conditioning the Column and Column Care; 2.5 United States Pharmacopeia and National Formulary Chromatographic Methods; References; 3 Capillary Column Gas Chromatography; 3.1 Introduction; Significance and Impact of Capillary Gas Chromatography Chronology of Achievements in Capillary Gas ChromatographyComparison of Packed and Capillary Columns; 3.2 Capillary Column Technology; Capillary Column Materials; Fused Silica and Other Glasses; Extrusion of a Fused-Silica Capillary Column; Aluminum-Clad Fused-Silica Capillary Columns; Fused-Silica-Lined Stainless Steel Capillary Columns; 3.3 Preparation of Fused-Silica Capillary Columns; Silanol Deactivation Procedures; Static Coating of Capillary Columns; Capillary Cages; Test Mixtures for Monitoring Column Performance; Diagnostic Role Played by Components of Test Mixtures 3.4 Chromatographic Performance of Capillary ColumnsGolay Equation Versus the van Deemter Expression; Choice of Carrier Gas; Measurement of Linear Velocity and Flow Rate; Effect of Carrier Gas Viscosity on Linear Velocity; Phase Ratio; Coating Efficiency; 3.5 Stationary-Phase Selection for Capillary Gas Chromatography; Requirements; History; Comparison of Columns from Manufacturers; Polysiloxane Phases; Polyethylene Glycol Phases; Cross-Linked Versus Chemically Bonded Phase; Chemical Bonding; MS-Grade Phases Versus Polysilarylene or Polysilphenylene Phases; Sol-Gel Stationary Phases Phenylpolycarborane-Siloxane Phases3.6 Specialty Columns; EPA Methods; Chiral Stationary Phases; Gas-Solid Adsorption Capillary Columns: PLOT Columns; 3.7 Capillary Column Selection; Practical Considerations of Column Diameter, Film Thickness, and Column Length; Capillary Columns of 0.53 mm i.d.: Megabore Columns; Correlation of Column Dimensions and Film Thickness with Parameters in the Fundamental Resolution Equation; Column Selection for Gas Chromatography by Specifications; 3.8 Column Installation and Care; Carrier Gas Purifiers; Ferrule Materials and Fittings; Column Installation Column Conditioning |
| Record Nr. | UNINA-9910143414203321 |
Barry Eugene F
|
||
| Hoboken, N.J., : Wiley-Interscience, c2007 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Columns for gas chromatography [[electronic resource] ] : performance and selection / / Eugene F. Barry, Robert L. Grob
| Columns for gas chromatography [[electronic resource] ] : performance and selection / / Eugene F. Barry, Robert L. Grob |
| Autore | Barry Eugene F |
| Pubbl/distr/stampa | Hoboken, N.J., : Wiley-Interscience, c2007 |
| Descrizione fisica | 1 online resource (314 p.) |
| Disciplina |
543.85
543/.85 |
| Altri autori (Persone) | GrobRobert Lee |
| Soggetto topico |
Gas chromatography
Chromatographic analysis |
| ISBN |
1-280-82679-7
9786610826797 0-470-11418-5 0-470-11417-7 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
COLUMNS FOR GAS CHROMATOGRAPHY; CONTENTS; Preface; Acknowledgments; 1 Introduction; 1.1 Evolution of Gas Chromatographic Columns; 1.2 Central Role Played by the Column; 1.3 Justification for Column Selection and Care; 1.4 Literature on Gas Chromatographic Columns; 1.5 Gas Chromatographic Resources on the Internet; References; 2 Packed Column Gas Chromatography; 2.1 Introduction; 2.2 Solid Supports and Adsorbents; Supports for Gas-Liquid Chromatography; Adsorbents for Gas-Solid Chromatography; 2.3 Stationary Phases; Requirements of a Stationary Phase; USP Designation of Stationary Phases
Kovats Retention IndexMcReynolds and Rohrschneider Classifications of Stationary Phases; Evaluation of Column Operation; Optimization of Packed Column Separations; 2.4 Column Preparation; Coating Methods; Tubing Materials and Dimensions; Glass Wool Plugs and Column Fittings; Filling the Column; Conditioning the Column and Column Care; 2.5 United States Pharmacopeia and National Formulary Chromatographic Methods; References; 3 Capillary Column Gas Chromatography; 3.1 Introduction; Significance and Impact of Capillary Gas Chromatography Chronology of Achievements in Capillary Gas ChromatographyComparison of Packed and Capillary Columns; 3.2 Capillary Column Technology; Capillary Column Materials; Fused Silica and Other Glasses; Extrusion of a Fused-Silica Capillary Column; Aluminum-Clad Fused-Silica Capillary Columns; Fused-Silica-Lined Stainless Steel Capillary Columns; 3.3 Preparation of Fused-Silica Capillary Columns; Silanol Deactivation Procedures; Static Coating of Capillary Columns; Capillary Cages; Test Mixtures for Monitoring Column Performance; Diagnostic Role Played by Components of Test Mixtures 3.4 Chromatographic Performance of Capillary ColumnsGolay Equation Versus the van Deemter Expression; Choice of Carrier Gas; Measurement of Linear Velocity and Flow Rate; Effect of Carrier Gas Viscosity on Linear Velocity; Phase Ratio; Coating Efficiency; 3.5 Stationary-Phase Selection for Capillary Gas Chromatography; Requirements; History; Comparison of Columns from Manufacturers; Polysiloxane Phases; Polyethylene Glycol Phases; Cross-Linked Versus Chemically Bonded Phase; Chemical Bonding; MS-Grade Phases Versus Polysilarylene or Polysilphenylene Phases; Sol-Gel Stationary Phases Phenylpolycarborane-Siloxane Phases3.6 Specialty Columns; EPA Methods; Chiral Stationary Phases; Gas-Solid Adsorption Capillary Columns: PLOT Columns; 3.7 Capillary Column Selection; Practical Considerations of Column Diameter, Film Thickness, and Column Length; Capillary Columns of 0.53 mm i.d.: Megabore Columns; Correlation of Column Dimensions and Film Thickness with Parameters in the Fundamental Resolution Equation; Column Selection for Gas Chromatography by Specifications; 3.8 Column Installation and Care; Carrier Gas Purifiers; Ferrule Materials and Fittings; Column Installation Column Conditioning |
| Record Nr. | UNINA-9910830531803321 |
|
Barry Eugene F
|
||
| Hoboken, N.J., : Wiley-Interscience, c2007 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Columns for gas chromatography [[electronic resource] ] : performance and selection / / Eugene F. Barry, Robert L. Grob
| Columns for gas chromatography [[electronic resource] ] : performance and selection / / Eugene F. Barry, Robert L. Grob |
| Autore | Barry Eugene F |
| Pubbl/distr/stampa | Hoboken, N.J., : Wiley-Interscience, c2007 |
| Descrizione fisica | 1 online resource (314 p.) |
| Disciplina |
543.85
543/.85 |
| Altri autori (Persone) | GrobRobert Lee |
| Soggetto topico |
Gas chromatography
Chromatographic analysis |
| ISBN |
1-280-82679-7
9786610826797 0-470-11418-5 0-470-11417-7 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
COLUMNS FOR GAS CHROMATOGRAPHY; CONTENTS; Preface; Acknowledgments; 1 Introduction; 1.1 Evolution of Gas Chromatographic Columns; 1.2 Central Role Played by the Column; 1.3 Justification for Column Selection and Care; 1.4 Literature on Gas Chromatographic Columns; 1.5 Gas Chromatographic Resources on the Internet; References; 2 Packed Column Gas Chromatography; 2.1 Introduction; 2.2 Solid Supports and Adsorbents; Supports for Gas-Liquid Chromatography; Adsorbents for Gas-Solid Chromatography; 2.3 Stationary Phases; Requirements of a Stationary Phase; USP Designation of Stationary Phases
Kovats Retention IndexMcReynolds and Rohrschneider Classifications of Stationary Phases; Evaluation of Column Operation; Optimization of Packed Column Separations; 2.4 Column Preparation; Coating Methods; Tubing Materials and Dimensions; Glass Wool Plugs and Column Fittings; Filling the Column; Conditioning the Column and Column Care; 2.5 United States Pharmacopeia and National Formulary Chromatographic Methods; References; 3 Capillary Column Gas Chromatography; 3.1 Introduction; Significance and Impact of Capillary Gas Chromatography Chronology of Achievements in Capillary Gas ChromatographyComparison of Packed and Capillary Columns; 3.2 Capillary Column Technology; Capillary Column Materials; Fused Silica and Other Glasses; Extrusion of a Fused-Silica Capillary Column; Aluminum-Clad Fused-Silica Capillary Columns; Fused-Silica-Lined Stainless Steel Capillary Columns; 3.3 Preparation of Fused-Silica Capillary Columns; Silanol Deactivation Procedures; Static Coating of Capillary Columns; Capillary Cages; Test Mixtures for Monitoring Column Performance; Diagnostic Role Played by Components of Test Mixtures 3.4 Chromatographic Performance of Capillary ColumnsGolay Equation Versus the van Deemter Expression; Choice of Carrier Gas; Measurement of Linear Velocity and Flow Rate; Effect of Carrier Gas Viscosity on Linear Velocity; Phase Ratio; Coating Efficiency; 3.5 Stationary-Phase Selection for Capillary Gas Chromatography; Requirements; History; Comparison of Columns from Manufacturers; Polysiloxane Phases; Polyethylene Glycol Phases; Cross-Linked Versus Chemically Bonded Phase; Chemical Bonding; MS-Grade Phases Versus Polysilarylene or Polysilphenylene Phases; Sol-Gel Stationary Phases Phenylpolycarborane-Siloxane Phases3.6 Specialty Columns; EPA Methods; Chiral Stationary Phases; Gas-Solid Adsorption Capillary Columns: PLOT Columns; 3.7 Capillary Column Selection; Practical Considerations of Column Diameter, Film Thickness, and Column Length; Capillary Columns of 0.53 mm i.d.: Megabore Columns; Correlation of Column Dimensions and Film Thickness with Parameters in the Fundamental Resolution Equation; Column Selection for Gas Chromatography by Specifications; 3.8 Column Installation and Care; Carrier Gas Purifiers; Ferrule Materials and Fittings; Column Installation Column Conditioning |
| Record Nr. | UNINA-9910840728003321 |
|
Barry Eugene F
|
||
| Hoboken, N.J., : Wiley-Interscience, c2007 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||