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Basic 1H- and 13C-NMR spectroscopy [[electronic resource] /] / Metin Balcıi
| Basic 1H- and 13C-NMR spectroscopy [[electronic resource] /] / Metin Balcıi |
| Autore | Balcıi Metin |
| Edizione | [1st ed.] |
| Pubbl/distr/stampa | Amsterdam ; ; Boston, : Elsevier, 2005 |
| Descrizione fisica | 1 online resource (441 p.) |
| Disciplina | 543.66 |
| Soggetto topico |
Nuclear magnetic resonance spectroscopy
Spectrum analysis |
| Soggetto genere / forma | Electronic books. |
| ISBN |
1-281-02542-9
9786611025427 0-08-052553-9 |
| Formato | Materiale a stampa  |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Front Cover; Basic 1H- and 13C-NMR Spectroscopy; Copyright Page; Preface; Contents; Part I: 1H-NMR Spectroscopy; Chapter 1. Introduction; 1.1 Structure Elucidation and NMR; 1.2 Development of NMR Spectroscopy; Chapter 2. Resonance Phenomena; 2.1 Magnetic Properties of Atomic Nuclei; 2.2 Spin Quantum Numbers of Elements; 2.3 Behavior of an Atomic Nucleus in a Magnetic Field; 2.4 Relaxation; 2.5 NMR Instrumentation; Chapter 3. Chemical shift; 3.1 Local Magnetic Fields Around a Nucleus; 3.2 The Unit of the Chemical Shift; 3.3 Sample Preparation; 3.4 Factors Influencing the Chemical Shift
3.5 Exercises 1-30 Chapter 4. Spin-Spin Splitting in 1H-NMR Spectra; 4.1 Explanation of Spin-Spin Splitting; 4.2 Spin-Spin Coupling Mechanism; 4.3 Factors Influencing Spin-Spin Coupling Constants; Chapter 5. Spin-Spin Splitting to Different Protons; 5.1 General Rules; 5.2 Examples of Coupling with Different Protons; 5.3 Exercises 31-60; Chapter 6. Spin Systems: Analysis of the 1H-NMR Spectra; 6.1 Second-order Spectra; 6.2 Two-spin Systems; Chapter 7. NMR Shift Reagents and Double Resonance Experiments: Simplification of the NMR Spectra; 7.1 Shift Reagents; 7.2 Double Resonance Experiments Chapter 8. Dynamic NMR Spectroscopy 8.1 Basic Theories; 8.2 Exercises 61-101; Part II: 13C-NMR Spectroscopy; Chapter 9. Introduction; 9.1 Development of 13C-NMR Spectroscopy; 9.2 Comparison of the 'H and 13C Nucleus; 9.3 The Factors Influencing The Sensitivity Of The 13c Nucleus; 9.4 The Factors Increasing the Sensitivity In 13C-NMR Spectroscopy; Chapter 10. Absorption and Resonance; 10.1 Classical Treatment of Absorption and Resonance; 10.2 Relaxation Processes; Chapter 11. Pulse NMR Spectroscopy; 11.1 Introduction to the Pulse NMR Spectroscopy; 11.2 CW and FT Spectroscopy 11.3 Interaction of a Monochromatic Radio frequency With the Sample 11.4 Fourier Transformation; 11.5 Routine Pulsed 13C-NMR Measurement Techniques; 11.6 Broadband Decoupling; 11.7 Nuclear Overhauser Effect; 11.8 Measurements of NOE Enhanced Coupled 13C-NMR Spectra: Gated Decoupling; 11.9 Off Resonance 1H Decoupled and Selective Decoupled Experiments; 11.10 Inverse Gated Decoupling; 11.11 Sample Preparation and Solvents; Chapter 12. Chemical Shift; 12.1 Diamagnetic and Paramagnetic Shielding on Proton and Carbon Atoms; 12.2 Factors which Influence the Chemical Shifts Chapter 13. 13C Chemical Shifts of Organic Compounds 13.1 Alkanes; 13.2 Substituted Alkanes; 13.3 Cycloalkanes; 13.4 Alkenes; 13.5 Aromatic Compounds; 13.6 Carbonyl Compounds; 13.7 Heterocyclic Compounds; Chapter 14. Spin-Spin Coupling; 14.1 Couplings Over One Bond (1JCH); 14.2 Couplings Over Two Bonds (2JcH) (Geminal Coupling); 14.3 Couplings Over Three Bonds (3JcH) (Vicinal Coupling); 14.4 Carbon-Deuterium Coupling (1JcD); Chapter 15. Multiple-Pulse NMR Experiments; 15.1 Measurements of Relaxation Times; 15.2 J-Modulated Spin-echo Experiments 15.3 Signal Enhancement by Population Transfer: Selective Population Transfer and Selective Population Inversion |
| Record Nr. | UNINA-9910457297003321 |
Balcıi Metin
|
||
| Amsterdam ; ; Boston, : Elsevier, 2005 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Basic 1H- and 13C-NMR spectroscopy [[electronic resource] /] / Metin Balcıi
| Basic 1H- and 13C-NMR spectroscopy [[electronic resource] /] / Metin Balcıi |
| Autore | Balcıi Metin |
| Edizione | [1st ed.] |
| Pubbl/distr/stampa | Amsterdam ; ; Boston, : Elsevier, 2005 |
| Descrizione fisica | 1 online resource (441 p.) |
| Disciplina | 543.66 |
| Soggetto topico |
Nuclear magnetic resonance spectroscopy
Spectrum analysis |
| ISBN |
1-281-02542-9
9786611025427 0-08-052553-9 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Front Cover; Basic 1H- and 13C-NMR Spectroscopy; Copyright Page; Preface; Contents; Part I: 1H-NMR Spectroscopy; Chapter 1. Introduction; 1.1 Structure Elucidation and NMR; 1.2 Development of NMR Spectroscopy; Chapter 2. Resonance Phenomena; 2.1 Magnetic Properties of Atomic Nuclei; 2.2 Spin Quantum Numbers of Elements; 2.3 Behavior of an Atomic Nucleus in a Magnetic Field; 2.4 Relaxation; 2.5 NMR Instrumentation; Chapter 3. Chemical shift; 3.1 Local Magnetic Fields Around a Nucleus; 3.2 The Unit of the Chemical Shift; 3.3 Sample Preparation; 3.4 Factors Influencing the Chemical Shift
3.5 Exercises 1-30 Chapter 4. Spin-Spin Splitting in 1H-NMR Spectra; 4.1 Explanation of Spin-Spin Splitting; 4.2 Spin-Spin Coupling Mechanism; 4.3 Factors Influencing Spin-Spin Coupling Constants; Chapter 5. Spin-Spin Splitting to Different Protons; 5.1 General Rules; 5.2 Examples of Coupling with Different Protons; 5.3 Exercises 31-60; Chapter 6. Spin Systems: Analysis of the 1H-NMR Spectra; 6.1 Second-order Spectra; 6.2 Two-spin Systems; Chapter 7. NMR Shift Reagents and Double Resonance Experiments: Simplification of the NMR Spectra; 7.1 Shift Reagents; 7.2 Double Resonance Experiments Chapter 8. Dynamic NMR Spectroscopy 8.1 Basic Theories; 8.2 Exercises 61-101; Part II: 13C-NMR Spectroscopy; Chapter 9. Introduction; 9.1 Development of 13C-NMR Spectroscopy; 9.2 Comparison of the 'H and 13C Nucleus; 9.3 The Factors Influencing The Sensitivity Of The 13c Nucleus; 9.4 The Factors Increasing the Sensitivity In 13C-NMR Spectroscopy; Chapter 10. Absorption and Resonance; 10.1 Classical Treatment of Absorption and Resonance; 10.2 Relaxation Processes; Chapter 11. Pulse NMR Spectroscopy; 11.1 Introduction to the Pulse NMR Spectroscopy; 11.2 CW and FT Spectroscopy 11.3 Interaction of a Monochromatic Radio frequency With the Sample 11.4 Fourier Transformation; 11.5 Routine Pulsed 13C-NMR Measurement Techniques; 11.6 Broadband Decoupling; 11.7 Nuclear Overhauser Effect; 11.8 Measurements of NOE Enhanced Coupled 13C-NMR Spectra: Gated Decoupling; 11.9 Off Resonance 1H Decoupled and Selective Decoupled Experiments; 11.10 Inverse Gated Decoupling; 11.11 Sample Preparation and Solvents; Chapter 12. Chemical Shift; 12.1 Diamagnetic and Paramagnetic Shielding on Proton and Carbon Atoms; 12.2 Factors which Influence the Chemical Shifts Chapter 13. 13C Chemical Shifts of Organic Compounds 13.1 Alkanes; 13.2 Substituted Alkanes; 13.3 Cycloalkanes; 13.4 Alkenes; 13.5 Aromatic Compounds; 13.6 Carbonyl Compounds; 13.7 Heterocyclic Compounds; Chapter 14. Spin-Spin Coupling; 14.1 Couplings Over One Bond (1JCH); 14.2 Couplings Over Two Bonds (2JcH) (Geminal Coupling); 14.3 Couplings Over Three Bonds (3JcH) (Vicinal Coupling); 14.4 Carbon-Deuterium Coupling (1JcD); Chapter 15. Multiple-Pulse NMR Experiments; 15.1 Measurements of Relaxation Times; 15.2 J-Modulated Spin-echo Experiments 15.3 Signal Enhancement by Population Transfer: Selective Population Transfer and Selective Population Inversion |
| Record Nr. | UNINA-9910784592503321 |
|
Balcıi Metin
|
||
| Amsterdam ; ; Boston, : Elsevier, 2005 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Basic 1H- and 13C-NMR spectroscopy / / Metin Balcıi
| Basic 1H- and 13C-NMR spectroscopy / / Metin Balcıi |
| Autore | Balcıi Metin |
| Edizione | [1st ed.] |
| Pubbl/distr/stampa | Amsterdam ; ; Boston, : Elsevier, 2005 |
| Descrizione fisica | 1 online resource (441 p.) |
| Disciplina | 543.66 |
| Soggetto topico |
Nuclear magnetic resonance spectroscopy
Spectrum analysis |
| ISBN |
1-281-02542-9
9786611025427 0-08-052553-9 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Front Cover; Basic 1H- and 13C-NMR Spectroscopy; Copyright Page; Preface; Contents; Part I: 1H-NMR Spectroscopy; Chapter 1. Introduction; 1.1 Structure Elucidation and NMR; 1.2 Development of NMR Spectroscopy; Chapter 2. Resonance Phenomena; 2.1 Magnetic Properties of Atomic Nuclei; 2.2 Spin Quantum Numbers of Elements; 2.3 Behavior of an Atomic Nucleus in a Magnetic Field; 2.4 Relaxation; 2.5 NMR Instrumentation; Chapter 3. Chemical shift; 3.1 Local Magnetic Fields Around a Nucleus; 3.2 The Unit of the Chemical Shift; 3.3 Sample Preparation; 3.4 Factors Influencing the Chemical Shift
3.5 Exercises 1-30 Chapter 4. Spin-Spin Splitting in 1H-NMR Spectra; 4.1 Explanation of Spin-Spin Splitting; 4.2 Spin-Spin Coupling Mechanism; 4.3 Factors Influencing Spin-Spin Coupling Constants; Chapter 5. Spin-Spin Splitting to Different Protons; 5.1 General Rules; 5.2 Examples of Coupling with Different Protons; 5.3 Exercises 31-60; Chapter 6. Spin Systems: Analysis of the 1H-NMR Spectra; 6.1 Second-order Spectra; 6.2 Two-spin Systems; Chapter 7. NMR Shift Reagents and Double Resonance Experiments: Simplification of the NMR Spectra; 7.1 Shift Reagents; 7.2 Double Resonance Experiments Chapter 8. Dynamic NMR Spectroscopy 8.1 Basic Theories; 8.2 Exercises 61-101; Part II: 13C-NMR Spectroscopy; Chapter 9. Introduction; 9.1 Development of 13C-NMR Spectroscopy; 9.2 Comparison of the 'H and 13C Nucleus; 9.3 The Factors Influencing The Sensitivity Of The 13c Nucleus; 9.4 The Factors Increasing the Sensitivity In 13C-NMR Spectroscopy; Chapter 10. Absorption and Resonance; 10.1 Classical Treatment of Absorption and Resonance; 10.2 Relaxation Processes; Chapter 11. Pulse NMR Spectroscopy; 11.1 Introduction to the Pulse NMR Spectroscopy; 11.2 CW and FT Spectroscopy 11.3 Interaction of a Monochromatic Radio frequency With the Sample 11.4 Fourier Transformation; 11.5 Routine Pulsed 13C-NMR Measurement Techniques; 11.6 Broadband Decoupling; 11.7 Nuclear Overhauser Effect; 11.8 Measurements of NOE Enhanced Coupled 13C-NMR Spectra: Gated Decoupling; 11.9 Off Resonance 1H Decoupled and Selective Decoupled Experiments; 11.10 Inverse Gated Decoupling; 11.11 Sample Preparation and Solvents; Chapter 12. Chemical Shift; 12.1 Diamagnetic and Paramagnetic Shielding on Proton and Carbon Atoms; 12.2 Factors which Influence the Chemical Shifts Chapter 13. 13C Chemical Shifts of Organic Compounds 13.1 Alkanes; 13.2 Substituted Alkanes; 13.3 Cycloalkanes; 13.4 Alkenes; 13.5 Aromatic Compounds; 13.6 Carbonyl Compounds; 13.7 Heterocyclic Compounds; Chapter 14. Spin-Spin Coupling; 14.1 Couplings Over One Bond (1JCH); 14.2 Couplings Over Two Bonds (2JcH) (Geminal Coupling); 14.3 Couplings Over Three Bonds (3JcH) (Vicinal Coupling); 14.4 Carbon-Deuterium Coupling (1JcD); Chapter 15. Multiple-Pulse NMR Experiments; 15.1 Measurements of Relaxation Times; 15.2 J-Modulated Spin-echo Experiments 15.3 Signal Enhancement by Population Transfer: Selective Population Transfer and Selective Population Inversion |
| Record Nr. | UNINA-9910808892603321 |
|
Balcıi Metin
|
||
| Amsterdam ; ; Boston, : Elsevier, 2005 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||