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Sample preparation techniques in analytical chemistry [[electronic resource] /] / edited by Somenath Mitra
Sample preparation techniques in analytical chemistry [[electronic resource] /] / edited by Somenath Mitra
Pubbl/distr/stampa Hoboken, N.J., : J. Wiley, c2003
Descrizione fisica 1 online resource (480 p.)
Disciplina 543
543.02
Altri autori (Persone) MitraS <1959-> (Somenath)
Collana Chemical analysis
Soggetto topico Sampling
Analytical chemistry - Methodology
ISBN 1-280-36611-7
9786610366118
0-470-24730-4
0-471-45782-5
0-471-45781-7
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Sample Preparation Techniques in Analytical Chemistry; CONTENTS; CONTRIBUTORS; PREFACE; CHAPTER 1 SAMPLE PREPARATION: AN ANALYTICAL PERSPECTIVE; 1.1. The Measurement Process; 1.1.1. Qualitative and Quantitative Analysis; 1.1.2. Methods of Quantitation; 1.2. Errors in Quantitative Analysis: Accuracy and Precision; 1.2.1. Accuracy; 1.2.2. Precision; 1.2.3. Statistical Aspects of Sample Preparation; 1.3. Method Performance and Method Validation; 1.3.1. Sensitivity; 1.3.2. Detection Limit; 1.3.3. Range of Quantitation; 1.3.4. Other Important Parameters; 1.3.5. Method Validation
1.4. Preservation of Samples1.4.1. Volatilization; 1.4.2. Choice of Proper Containers; 1.4.3. Absorption of Gases from the Atmosphere; 1.4.4. Chemical Changes; 1.4.5. Preservation of Unstable Solids; 1.5. Postextraction Procedures; 1.5.1. Concentration of Sample Extracts; 1.5.2. Sample Cleanup; 1.6. Quality Assurance and Quality Control during Sample Preparation; 1.6.1. Determination of Accuracy and Precision; 1.6.2. Statistical Control; 1.6.3. Matrix Control; 1.6.4. Contamination Control; References; SECTION A EXTRACTION AND ENRICHMENT IN SAMPLE PREPARATION
CHAPTER 2 PRINCIPLES OF EXTRACTION AND THE EXTRACTION OF SEMIVOLATILE ORGANICS FROM LIQUIDS2.1. Principles of Extraction; 2.1.1. Volatilization; 2.1.2. Hydrophobicity; 2.1.3. Acid-Base Equilibria; 2.1.4. Distribution of Hydrophobic Ionogenic Organic Compounds; 2.2. Liquid-Liquid Extraction; 2.2.1. Recovery; 2.2.2. Methodology; 2.2.3. Procedures; 2.2.4. Recent Advances in Techniques; 2.3. Liquid-Solid Extraction; 2.3.1. Sorption; 2.4. Solid-Phase Extraction; 2.4.1. Sorbents in SPE; 2.4.2. Sorbent Selection; 2.4.3. Recovery; 2.4.4. Methodology; 2.4.5. Procedures; 2.4.6. Recent Advances in SPE
2.5. Solid-Phase Microextraction2.5.1. Sorbents; 2.5.2. Sorbent Selection; 2.5.3. Methodology; 2.5.4. Recent Advances in Techniques; 2.6. Stir Bar Sorptive Extraction; 2.6.1. Sorbent and Analyte Recovery; 2.6.2. Methodology; 2.6.3. Recent Advances in Techniques; 2.7. Method Comparison; References; CHAPTER 3 EXTRACTION OF SEMIVOLATILE ORGANIC COMPOUNDS FROM SOLID MATRICES; 3.1. Introduction; 3.1.1. Extraction Mechanism; 3.1.2. Preextraction Procedures; 3.1.3. Postextraction Procedures; 3.2. Soxhlet and Automated Soxhlet; 3.2.1. Soxhlet Extraction; 3.2.2. Automated Soxhlet Extraction
3.2.3. Comparison between Soxtec and Soxhlet3.3. Ultrasonic Extraction; 3.3.1. Selected Applications and Comparison with Soxhlet; 3.4. Supercritical Fluid Extraction; 3.4.1. Theoretical Considerations; 3.4.2. Instrumentation; 3.4.3. Operational Procedures; 3.4.4. Advantages/Disadvantages and Applications of SFE; 3.5. Accelerated Solvent Extraction; 3.5.1. Theoretical Considerations; 3.5.2. Instrumentation; 3.5.3. Operational Procedures; 3.5.4. Process Parameters; 3.5.5. Advantages and Applications of ASE; 3.6. Microwave-Assisted Extraction; 3.6.1. Theoretical Considerations
3.6.2. Instrumentation
Record Nr. UNINA-9910143196903321
Hoboken, N.J., : J. Wiley, c2003
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Sample preparation techniques in analytical chemistry [[electronic resource] /] / edited by Somenath Mitra
Sample preparation techniques in analytical chemistry [[electronic resource] /] / edited by Somenath Mitra
Pubbl/distr/stampa Hoboken, N.J., : J. Wiley, c2003
Descrizione fisica 1 online resource (480 p.)
Disciplina 543
543.02
Altri autori (Persone) MitraS <1959-> (Somenath)
Collana Chemical analysis
Soggetto topico Sampling
Analytical chemistry - Methodology
ISBN 1-280-36611-7
9786610366118
0-470-24730-4
0-471-45782-5
0-471-45781-7
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Sample Preparation Techniques in Analytical Chemistry; CONTENTS; CONTRIBUTORS; PREFACE; CHAPTER 1 SAMPLE PREPARATION: AN ANALYTICAL PERSPECTIVE; 1.1. The Measurement Process; 1.1.1. Qualitative and Quantitative Analysis; 1.1.2. Methods of Quantitation; 1.2. Errors in Quantitative Analysis: Accuracy and Precision; 1.2.1. Accuracy; 1.2.2. Precision; 1.2.3. Statistical Aspects of Sample Preparation; 1.3. Method Performance and Method Validation; 1.3.1. Sensitivity; 1.3.2. Detection Limit; 1.3.3. Range of Quantitation; 1.3.4. Other Important Parameters; 1.3.5. Method Validation
1.4. Preservation of Samples1.4.1. Volatilization; 1.4.2. Choice of Proper Containers; 1.4.3. Absorption of Gases from the Atmosphere; 1.4.4. Chemical Changes; 1.4.5. Preservation of Unstable Solids; 1.5. Postextraction Procedures; 1.5.1. Concentration of Sample Extracts; 1.5.2. Sample Cleanup; 1.6. Quality Assurance and Quality Control during Sample Preparation; 1.6.1. Determination of Accuracy and Precision; 1.6.2. Statistical Control; 1.6.3. Matrix Control; 1.6.4. Contamination Control; References; SECTION A EXTRACTION AND ENRICHMENT IN SAMPLE PREPARATION
CHAPTER 2 PRINCIPLES OF EXTRACTION AND THE EXTRACTION OF SEMIVOLATILE ORGANICS FROM LIQUIDS2.1. Principles of Extraction; 2.1.1. Volatilization; 2.1.2. Hydrophobicity; 2.1.3. Acid-Base Equilibria; 2.1.4. Distribution of Hydrophobic Ionogenic Organic Compounds; 2.2. Liquid-Liquid Extraction; 2.2.1. Recovery; 2.2.2. Methodology; 2.2.3. Procedures; 2.2.4. Recent Advances in Techniques; 2.3. Liquid-Solid Extraction; 2.3.1. Sorption; 2.4. Solid-Phase Extraction; 2.4.1. Sorbents in SPE; 2.4.2. Sorbent Selection; 2.4.3. Recovery; 2.4.4. Methodology; 2.4.5. Procedures; 2.4.6. Recent Advances in SPE
2.5. Solid-Phase Microextraction2.5.1. Sorbents; 2.5.2. Sorbent Selection; 2.5.3. Methodology; 2.5.4. Recent Advances in Techniques; 2.6. Stir Bar Sorptive Extraction; 2.6.1. Sorbent and Analyte Recovery; 2.6.2. Methodology; 2.6.3. Recent Advances in Techniques; 2.7. Method Comparison; References; CHAPTER 3 EXTRACTION OF SEMIVOLATILE ORGANIC COMPOUNDS FROM SOLID MATRICES; 3.1. Introduction; 3.1.1. Extraction Mechanism; 3.1.2. Preextraction Procedures; 3.1.3. Postextraction Procedures; 3.2. Soxhlet and Automated Soxhlet; 3.2.1. Soxhlet Extraction; 3.2.2. Automated Soxhlet Extraction
3.2.3. Comparison between Soxtec and Soxhlet3.3. Ultrasonic Extraction; 3.3.1. Selected Applications and Comparison with Soxhlet; 3.4. Supercritical Fluid Extraction; 3.4.1. Theoretical Considerations; 3.4.2. Instrumentation; 3.4.3. Operational Procedures; 3.4.4. Advantages/Disadvantages and Applications of SFE; 3.5. Accelerated Solvent Extraction; 3.5.1. Theoretical Considerations; 3.5.2. Instrumentation; 3.5.3. Operational Procedures; 3.5.4. Process Parameters; 3.5.5. Advantages and Applications of ASE; 3.6. Microwave-Assisted Extraction; 3.6.1. Theoretical Considerations
3.6.2. Instrumentation
Record Nr. UNINA-9910830239503321
Hoboken, N.J., : J. Wiley, c2003
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Sample preparation techniques in analytical chemistry [[electronic resource] /] / edited by Somenath Mitra
Sample preparation techniques in analytical chemistry [[electronic resource] /] / edited by Somenath Mitra
Pubbl/distr/stampa Hoboken, N.J., : J. Wiley, c2003
Descrizione fisica 1 online resource (480 p.)
Disciplina 543
543.02
Altri autori (Persone) MitraS <1959-> (Somenath)
Collana Chemical analysis
Soggetto topico Sampling
Analytical chemistry - Methodology
ISBN 1-280-36611-7
9786610366118
0-470-24730-4
0-471-45782-5
0-471-45781-7
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Sample Preparation Techniques in Analytical Chemistry; CONTENTS; CONTRIBUTORS; PREFACE; CHAPTER 1 SAMPLE PREPARATION: AN ANALYTICAL PERSPECTIVE; 1.1. The Measurement Process; 1.1.1. Qualitative and Quantitative Analysis; 1.1.2. Methods of Quantitation; 1.2. Errors in Quantitative Analysis: Accuracy and Precision; 1.2.1. Accuracy; 1.2.2. Precision; 1.2.3. Statistical Aspects of Sample Preparation; 1.3. Method Performance and Method Validation; 1.3.1. Sensitivity; 1.3.2. Detection Limit; 1.3.3. Range of Quantitation; 1.3.4. Other Important Parameters; 1.3.5. Method Validation
1.4. Preservation of Samples1.4.1. Volatilization; 1.4.2. Choice of Proper Containers; 1.4.3. Absorption of Gases from the Atmosphere; 1.4.4. Chemical Changes; 1.4.5. Preservation of Unstable Solids; 1.5. Postextraction Procedures; 1.5.1. Concentration of Sample Extracts; 1.5.2. Sample Cleanup; 1.6. Quality Assurance and Quality Control during Sample Preparation; 1.6.1. Determination of Accuracy and Precision; 1.6.2. Statistical Control; 1.6.3. Matrix Control; 1.6.4. Contamination Control; References; SECTION A EXTRACTION AND ENRICHMENT IN SAMPLE PREPARATION
CHAPTER 2 PRINCIPLES OF EXTRACTION AND THE EXTRACTION OF SEMIVOLATILE ORGANICS FROM LIQUIDS2.1. Principles of Extraction; 2.1.1. Volatilization; 2.1.2. Hydrophobicity; 2.1.3. Acid-Base Equilibria; 2.1.4. Distribution of Hydrophobic Ionogenic Organic Compounds; 2.2. Liquid-Liquid Extraction; 2.2.1. Recovery; 2.2.2. Methodology; 2.2.3. Procedures; 2.2.4. Recent Advances in Techniques; 2.3. Liquid-Solid Extraction; 2.3.1. Sorption; 2.4. Solid-Phase Extraction; 2.4.1. Sorbents in SPE; 2.4.2. Sorbent Selection; 2.4.3. Recovery; 2.4.4. Methodology; 2.4.5. Procedures; 2.4.6. Recent Advances in SPE
2.5. Solid-Phase Microextraction2.5.1. Sorbents; 2.5.2. Sorbent Selection; 2.5.3. Methodology; 2.5.4. Recent Advances in Techniques; 2.6. Stir Bar Sorptive Extraction; 2.6.1. Sorbent and Analyte Recovery; 2.6.2. Methodology; 2.6.3. Recent Advances in Techniques; 2.7. Method Comparison; References; CHAPTER 3 EXTRACTION OF SEMIVOLATILE ORGANIC COMPOUNDS FROM SOLID MATRICES; 3.1. Introduction; 3.1.1. Extraction Mechanism; 3.1.2. Preextraction Procedures; 3.1.3. Postextraction Procedures; 3.2. Soxhlet and Automated Soxhlet; 3.2.1. Soxhlet Extraction; 3.2.2. Automated Soxhlet Extraction
3.2.3. Comparison between Soxtec and Soxhlet3.3. Ultrasonic Extraction; 3.3.1. Selected Applications and Comparison with Soxhlet; 3.4. Supercritical Fluid Extraction; 3.4.1. Theoretical Considerations; 3.4.2. Instrumentation; 3.4.3. Operational Procedures; 3.4.4. Advantages/Disadvantages and Applications of SFE; 3.5. Accelerated Solvent Extraction; 3.5.1. Theoretical Considerations; 3.5.2. Instrumentation; 3.5.3. Operational Procedures; 3.5.4. Process Parameters; 3.5.5. Advantages and Applications of ASE; 3.6. Microwave-Assisted Extraction; 3.6.1. Theoretical Considerations
3.6.2. Instrumentation
Record Nr. UNINA-9910840634303321
Hoboken, N.J., : J. Wiley, c2003
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Sampling techniques / W.G. Cochran
Sampling techniques / W.G. Cochran
Autore Cochran, William Gemmell
Pubbl/distr/stampa New York : John Wiley & Sons, 1977
Descrizione fisica xvi, 428 p. : ill. ; 24 cm.
Soggetto topico Sampling
ISBN 9780471162407
Classificazione 001.4'222
510(022:076)
510.60
510.62
QA276
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Record Nr. UNISALENTO-991001224579707536
Cochran, William Gemmell  
New York : John Wiley & Sons, 1977
Materiale a stampa
Lo trovi qui: Univ. del Salento
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Statistical methods for rates and proportions / Joseph L. Fleiss
Statistical methods for rates and proportions / Joseph L. Fleiss
Autore Fleiss, Joseph L.
Edizione [2d ed]
Descrizione fisica xviii, 321 p. ; 24 cm
Disciplina 519.5352
Collana Wiley series in probability and mathematical statistics. Applied Probability and Statistics, 0271-6353
Soggetto topico Analysis of variance
Biometry
Sampling
Statistics
ISBN 0471064289
Classificazione AMS 62-01
AMS 62-XX
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Record Nr. UNISALENTO-991001373759707536
Fleiss, Joseph L.  
Materiale a stampa
Lo trovi qui: Univ. del Salento
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Statistical multiple integration : proceedings of the AMS-IMS-SIAM Joint Summer Research Conference held June 17-23, 1989 / Nancy Flournoy and Robert K. Tsutakawa, editors
Statistical multiple integration : proceedings of the AMS-IMS-SIAM Joint Summer Research Conference held June 17-23, 1989 / Nancy Flournoy and Robert K. Tsutakawa, editors
Autore AMS-IMS-SIAM Joint Summer research conference on statistical multiple integration <1989 ; Humboldt University>
Pubbl/distr/stampa Providence, R.I. : American Mathematical Society, c1991
Descrizione fisica xii, 276 p. : ill. ; 26 cm
Disciplina 519.5
Altri autori (Persone) Flournoy, Nancyauthor
Tsutakawa, Robert K.
Collana Contemporary mathematics, 0271-4132 ; 115
Soggetto topico Bayesian statistical decision theory
Multivariate analysis
Numerical integration
Sampling
ISBN 0821851225
Classificazione AMS 62-06
QA276.7.A47
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Record Nr. UNISALENTO-991001374019707536
AMS-IMS-SIAM Joint Summer research conference on statistical multiple integration <1989 ; Humboldt University>  
Providence, R.I. : American Mathematical Society, c1991
Materiale a stampa
Lo trovi qui: Univ. del Salento
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Statistical theory of sampling inspection by attributes / A. Hald
Statistical theory of sampling inspection by attributes / A. Hald
Autore Hald, Anders
Pubbl/distr/stampa London ; New York : Academic Press, 1981
Descrizione fisica xiv, 515 p. : ill. ; 24 cm.
Disciplina 519.5
Collana Probability and mathematical statistics. A series of monographs and textbooks
Soggetto topico Acceptance sampling
Sampling
ISBN 0123183502
Classificazione AMS 62D05
QA276.6
TS156.4
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Record Nr. UNISALENTO-991001374409707536
Hald, Anders  
London ; New York : Academic Press, 1981
Materiale a stampa
Lo trovi qui: Univ. del Salento
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Statistics of directional data / K. V. Mardia
Statistics of directional data / K. V. Mardia
Autore Mardia, K. V.
Pubbl/distr/stampa London : Academic Press, 1972
Descrizione fisica xx, 357 p. : ill. ; 24 cm.
Disciplina 519.53
Collana Probability and mathematical statistics. A series of monographs and textbooks ; 13
Soggetto topico Distributions
Mathematical statistics
Sampling
Statistics
ISBN 0124711502
Classificazione AMS 62-01
AMS 62-XX
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Record Nr. UNISALENTO-991001375059707536
Mardia, K. V.  
London : Academic Press, 1972
Materiale a stampa
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Symposium on Bulk Sampling
Symposium on Bulk Sampling
Pubbl/distr/stampa [Place of publication not identified], : American Society for Testing & Materials, 1952
Descrizione fisica 1 online resource (65 pages) : illustrations
Disciplina 620.1123
Collana ASTM special technical publication
Soggetto topico Sampling
ISBN 0-8031-5915-3
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Record Nr. UNINA-9910164326403321
[Place of publication not identified], : American Society for Testing & Materials, 1952
Materiale a stampa
Lo trovi qui: Univ. Federico II
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Weak convergence and empirical processes : with applications to statistics / Aad W. van der Vaart, Jon A. Wellner
Weak convergence and empirical processes : with applications to statistics / Aad W. van der Vaart, Jon A. Wellner
Autore Vaart, Aad W. van der
Pubbl/distr/stampa New York : Springer-Verlag, c1996
Descrizione fisica xvi, 508 p. : ill. ; 24 cm.
Disciplina 519.2
Altri autori (Persone) Wellner, Jon A.
Collana Springer series in statistics
Soggetto topico Convergence
Distributions
Sampling
Stochastic processes
ISBN 0387946403
Classificazione AMS 60B10
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Record Nr. UNISALENTO-991001484679707536
Vaart, Aad W. van der  
New York : Springer-Verlag, c1996
Materiale a stampa
Lo trovi qui: Univ. del Salento
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