Info
- Utilizzare la checkbox di selezione a fianco di ciascun documento per attivare le funzionalità di stampa, invio email, download nei formati disponibili del (i) record.
LC-NMR and other hyphenated NMR techniques [[electronic resource] ] : overview and applications / / Maria Victoria Silva Elipe
| LC-NMR and other hyphenated NMR techniques [[electronic resource] ] : overview and applications / / Maria Victoria Silva Elipe |
| Autore | Silva Elipe Maria V. <1963-> |
| Pubbl/distr/stampa | Hoboken, NJ : , : Wiley, , c2012 |
| Descrizione fisica | 1 online resource (240 p.) |
| Disciplina | 543/.66 |
| Collana | THEi Wiley ebooks |
| Soggetto topico |
Nuclear magnetic resonance spectroscopy - Industrial applications
Organic compounds - Analysis Drug development |
| ISBN |
1-283-33226-4
9786613332264 1-118-13538-5 1-118-13539-3 1-118-13536-9 |
| Classificazione | SCI078000 |
| Formato | Materiale a stampa  |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
LC-NMR and Other Hyphenated NMR Techniques: Overview and Applications; Contents; Preface; Abbreviations, Symbols, and Units; 1. Basic Concepts of NMR Spectroscopy; 1.1 Introduction; 1.2 Basic Knowledge Regarding the Physics of NMR Spectroscopy; 1.3 Basic Parameters for NMR Interpretation; 1.3.1 Chemical Shift; 1.3.2 Spin-Spin Coupling Constants; 1.3.3 Spin Systems; 1.3.4 Signal Intensities; 1.3.5 Bond Correlations; 1.3.6 Spatial Correlations; 1.3.7 Other Topics; 1.4 Conclusions; References; 2. Historical Development of NMR and LC-NMR; 2.1 Introduction; 2.2 Historical Development of NMR
2.3 Historical Development of LC-NMR2.4 Historical Development of Other Analytical Techniques Hyphenated with NMR; 2.5 Current Trends; References; 3. Basic Technical Aspects and Operation of LC-NMR and LC-MS-NMR; 3.1 Introduction; 3.2 Technical Considerations Regarding LC-NMR; 3.2.1 Solvent Compatibility; 3.2.2 Solvent Suppression; 3.2.3 NMR Flow Cell; 3.2.4 LC-NMR Sensitivity; 3.3 Technical Considerations Regarding LC-MS-NMR; 3.3.1 Deuterated Solvents; 3.4 Modes of Operation of LC-NMR; 3.4.1 On-Flow Mode; 3.4.2 Stop-Flow Mode; 3.4.3 Time-Sliced Mode; 3.4.4 Loop Collection Mode 3.5 Modes of Operation of LC-MS-NMR3.5.1 On-Flow Mode; 3.5.2 Stop-Flow Mode; 3.6 Other Modes of Operation; 3.7 Challenging Considerations; 3.7.1 Air Bubbles; 3.7.2 Carryover with and Without an Autosampler; 3.7.3 Sample Solubility and Precipitation; 3.7.4 Flow Cell and System Cleaning; 3.7.5 Flow Rate and Magnetic Susceptibility; 3.7.6 Quantitation; 3.8 Conclusions; References; 4. Applications of LC-NMR; 4.1 Introduction; 4.2 Applications of LC-NMR; 4.2.1 Natural Products; 4.2.2 Drug Metabolism; 4.2.3 Drug Discovery; 4.2.4 Impurity Characterization; 4.2.5 Degradation Products 4.2.6 Food Analysis4.2.7 Polymers; 4.2.8 Metabolomics and Metabonomics; 4.2.9 Isomers, Tautomers, and Chiral Compounds; 4.2.10 Others Areas; 4.3 Conclusions and Future Trends; References; 5. Applications of LC-MS-NMR; 5.1 Introduction; 5.2 Applications of LC-MS-NMR; 5.2.1 Natural Products; 5.2.2 Drug Metabolism; 5.2.3 Drug Discovery and Development; 5.2.4 Metabolomics and Metabonomics; 5.2.5 Others Areas; 5.3 Conclusions and Future Trends; References; 6. Hyphenation of NMR with Other Analytical Separation Techniques; 6.1 Introduction; 6.2 GC-NMR; 6.3 GPC-NMR; 6.4 SEC-NMR; 6.5 SFC-NMR 6.6 SFE-NMR6.7 CE-NMR; 6.8 CEC-NMR; 6.9 CZE-NMR; 6.10 cITP-NMR; 6.11 CapLC-NMR; 6.12 SPE-NMR; 6.13 SPE-MS-NMR; 6.14 Conclusions and Future Trends; References; 7. Special Topics and Applications Related to LC-NMR; 7.1 Introduction; 7.2 Off-Line Versus Online NMR for Structural Elucidation; 7.2.1 Cases Solved Off-Line; 7.2.2 Cases Solved Online; 7.3 Analysis of Chiral Molecules by NMR; 7.3.1 Classical Approach: Off-Line; 7.3.2 Nonclassical Approach: Online; 7.4 Monitoring Chemical Reactions In Situ; 7.4.1 Classical Approach: Off-Line; 7.4.2 Nonclassical Approach: Online 7.5 Analysis of Mixtures Off-Line, Online, and by Other NMR Methodologies |
| Record Nr. | UNINA-9910139558903321 |
Silva Elipe Maria V. <1963->
|
||
| Hoboken, NJ : , : Wiley, , c2012 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
LC-NMR and other hyphenated NMR techniques [[electronic resource] ] : overview and applications / / Maria Victoria Silva Elipe
| LC-NMR and other hyphenated NMR techniques [[electronic resource] ] : overview and applications / / Maria Victoria Silva Elipe |
| Autore | Silva Elipe Maria V. <1963-> |
| Pubbl/distr/stampa | Hoboken, NJ : , : Wiley, , c2012 |
| Descrizione fisica | 1 online resource (240 p.) |
| Disciplina | 543/.66 |
| Collana | THEi Wiley ebooks |
| Soggetto topico |
Nuclear magnetic resonance spectroscopy - Industrial applications
Organic compounds - Analysis Drug development |
| ISBN |
1-283-33226-4
9786613332264 1-118-13538-5 1-118-13539-3 1-118-13536-9 |
| Classificazione | SCI078000 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
LC-NMR and Other Hyphenated NMR Techniques: Overview and Applications; Contents; Preface; Abbreviations, Symbols, and Units; 1. Basic Concepts of NMR Spectroscopy; 1.1 Introduction; 1.2 Basic Knowledge Regarding the Physics of NMR Spectroscopy; 1.3 Basic Parameters for NMR Interpretation; 1.3.1 Chemical Shift; 1.3.2 Spin-Spin Coupling Constants; 1.3.3 Spin Systems; 1.3.4 Signal Intensities; 1.3.5 Bond Correlations; 1.3.6 Spatial Correlations; 1.3.7 Other Topics; 1.4 Conclusions; References; 2. Historical Development of NMR and LC-NMR; 2.1 Introduction; 2.2 Historical Development of NMR
2.3 Historical Development of LC-NMR2.4 Historical Development of Other Analytical Techniques Hyphenated with NMR; 2.5 Current Trends; References; 3. Basic Technical Aspects and Operation of LC-NMR and LC-MS-NMR; 3.1 Introduction; 3.2 Technical Considerations Regarding LC-NMR; 3.2.1 Solvent Compatibility; 3.2.2 Solvent Suppression; 3.2.3 NMR Flow Cell; 3.2.4 LC-NMR Sensitivity; 3.3 Technical Considerations Regarding LC-MS-NMR; 3.3.1 Deuterated Solvents; 3.4 Modes of Operation of LC-NMR; 3.4.1 On-Flow Mode; 3.4.2 Stop-Flow Mode; 3.4.3 Time-Sliced Mode; 3.4.4 Loop Collection Mode 3.5 Modes of Operation of LC-MS-NMR3.5.1 On-Flow Mode; 3.5.2 Stop-Flow Mode; 3.6 Other Modes of Operation; 3.7 Challenging Considerations; 3.7.1 Air Bubbles; 3.7.2 Carryover with and Without an Autosampler; 3.7.3 Sample Solubility and Precipitation; 3.7.4 Flow Cell and System Cleaning; 3.7.5 Flow Rate and Magnetic Susceptibility; 3.7.6 Quantitation; 3.8 Conclusions; References; 4. Applications of LC-NMR; 4.1 Introduction; 4.2 Applications of LC-NMR; 4.2.1 Natural Products; 4.2.2 Drug Metabolism; 4.2.3 Drug Discovery; 4.2.4 Impurity Characterization; 4.2.5 Degradation Products 4.2.6 Food Analysis4.2.7 Polymers; 4.2.8 Metabolomics and Metabonomics; 4.2.9 Isomers, Tautomers, and Chiral Compounds; 4.2.10 Others Areas; 4.3 Conclusions and Future Trends; References; 5. Applications of LC-MS-NMR; 5.1 Introduction; 5.2 Applications of LC-MS-NMR; 5.2.1 Natural Products; 5.2.2 Drug Metabolism; 5.2.3 Drug Discovery and Development; 5.2.4 Metabolomics and Metabonomics; 5.2.5 Others Areas; 5.3 Conclusions and Future Trends; References; 6. Hyphenation of NMR with Other Analytical Separation Techniques; 6.1 Introduction; 6.2 GC-NMR; 6.3 GPC-NMR; 6.4 SEC-NMR; 6.5 SFC-NMR 6.6 SFE-NMR6.7 CE-NMR; 6.8 CEC-NMR; 6.9 CZE-NMR; 6.10 cITP-NMR; 6.11 CapLC-NMR; 6.12 SPE-NMR; 6.13 SPE-MS-NMR; 6.14 Conclusions and Future Trends; References; 7. Special Topics and Applications Related to LC-NMR; 7.1 Introduction; 7.2 Off-Line Versus Online NMR for Structural Elucidation; 7.2.1 Cases Solved Off-Line; 7.2.2 Cases Solved Online; 7.3 Analysis of Chiral Molecules by NMR; 7.3.1 Classical Approach: Off-Line; 7.3.2 Nonclassical Approach: Online; 7.4 Monitoring Chemical Reactions In Situ; 7.4.1 Classical Approach: Off-Line; 7.4.2 Nonclassical Approach: Online 7.5 Analysis of Mixtures Off-Line, Online, and by Other NMR Methodologies |
| Record Nr. | UNINA-9910829093403321 |
|
Silva Elipe Maria V. <1963->
|
||
| Hoboken, NJ : , : Wiley, , c2012 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Die Linalool-Dehydratase-Isomerase aus dem nitratreduzierenden Betaproteobakterium Castellaniella defragrans 65Phen / / Danny Brodkorb
| Die Linalool-Dehydratase-Isomerase aus dem nitratreduzierenden Betaproteobakterium Castellaniella defragrans 65Phen / / Danny Brodkorb |
| Autore | Brodkorb Danny |
| Edizione | [1. Auflage.] |
| Pubbl/distr/stampa | Göttingen, [Germany] : , : Cuvillier Verlag, , 2009 |
| Descrizione fisica | 1 online resource (115 pages) : illustrations, photographs |
| Disciplina | 547.122 |
| Soggetto topico | Organic compounds - Analysis |
| ISBN | 3-7369-3213-8 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | ger |
| Record Nr. | UNINA-9910795092803321 |
|
Brodkorb Danny
|
||
| Göttingen, [Germany] : , : Cuvillier Verlag, , 2009 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Die Linalool-Dehydratase-Isomerase aus dem nitratreduzierenden Betaproteobakterium Castellaniella defragrans 65Phen / / Danny Brodkorb
| Die Linalool-Dehydratase-Isomerase aus dem nitratreduzierenden Betaproteobakterium Castellaniella defragrans 65Phen / / Danny Brodkorb |
| Autore | Brodkorb Danny |
| Edizione | [1. Auflage.] |
| Pubbl/distr/stampa | Göttingen, [Germany] : , : Cuvillier Verlag, , 2009 |
| Descrizione fisica | 1 online resource (115 pages) : illustrations, photographs |
| Disciplina | 547.122 |
| Soggetto topico | Organic compounds - Analysis |
| ISBN | 3-7369-3213-8 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | ger |
| Record Nr. | UNINA-9910818545803321 |
|
Brodkorb Danny
|
||
| Göttingen, [Germany] : , : Cuvillier Verlag, , 2009 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Metodi spettroscopici nella chimica organica / Manfred Hess, Herbert Meier, Bernd Zeeh
| Metodi spettroscopici nella chimica organica / Manfred Hess, Herbert Meier, Bernd Zeeh |
| Autore | Hesse, Manfred |
| Edizione | [2nd ed. italiana / a cura di Giorgio Abbiati, Elena Pini, Elisabetta Rossi] |
| Pubbl/distr/stampa | Napoli : EdiSES, 2010 |
| Descrizione fisica | ix, 453 p. : ill. ; cm |
| Disciplina | 547.3 |
| Altri autori (Persone) |
Meier, H.
Zeeh, Berndauthor |
| Soggetto topico |
Spectrum analysis
Organic compounds - Analysis |
| ISBN | 9788879596626 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | ita |
| Record Nr. | UNISALENTO-991002448859707536 |
|
Hesse, Manfred
|
||
| Napoli : EdiSES, 2010 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. del Salento | ||
| ||
Organic compounds in natural waters : analysis and determination / / T. Roy Crompton, retired, UK Rivers Authority, UK
| Organic compounds in natural waters : analysis and determination / / T. Roy Crompton, retired, UK Rivers Authority, UK |
| Autore | Crompton T. R (Thomas Roy) |
| Edizione | [1st edition] |
| Pubbl/distr/stampa | Leiden, The Netherlands : , : CRC Press/Balkema, an imprint of the Taylor & Francis Group, , [2014] |
| Descrizione fisica | 1 online resource (305 p.) |
| Disciplina |
628.1/68
628.168 |
| Soggetto topico |
Organic compounds - Environmental aspects
Water - Pollution Organic compounds - Analysis Saline waters - Analysis Fresh water - Analysis Water - Pollution - Measurement Water chemistry |
| ISBN |
1-138-07484-5
0-429-22782-5 1-315-86300-6 |
| Classificazione | SCI013000SCI026000TEC010030 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto | Hydrocarbons in non-saline waters -- Oxygen containing compounds in non-saline waters -- Halogen containing compounds in non-saline waters -- Nitrogen compounds in non-saline waters -- Phosphorus contianing compounds in non-saline waters -- Sulphur containing compounds in non-saline waters -- Surface active agents in non-saline waters -- Volatile organic compounds -- Multiorganics in non-saline waters -- Pesticides and herbicides -- Organic compounds in saline waters -- Miscellaneous organic compounds -- Organometallic compounds -- Organic compounds aqueous precipitation. |
| Record Nr. | UNINA-9910790604103321 |
|
Crompton T. R (Thomas Roy)
|
||
| Leiden, The Netherlands : , : CRC Press/Balkema, an imprint of the Taylor & Francis Group, , [2014] | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Organic compounds in natural waters : analysis and determination / / T. Roy Crompton, retired, UK Rivers Authority, UK
| Organic compounds in natural waters : analysis and determination / / T. Roy Crompton, retired, UK Rivers Authority, UK |
| Autore | Crompton T. R (Thomas Roy) |
| Edizione | [1st edition] |
| Pubbl/distr/stampa | Leiden, The Netherlands : , : CRC Press/Balkema, an imprint of the Taylor & Francis Group, , [2014] |
| Descrizione fisica | 1 online resource (305 p.) |
| Disciplina |
628.1/68
628.168 |
| Soggetto topico |
Organic compounds - Environmental aspects
Water - Pollution Organic compounds - Analysis Saline waters - Analysis Fresh water - Analysis Water - Pollution - Measurement Water chemistry |
| ISBN |
1-317-95039-9
1-138-07484-5 0-429-22782-5 1-315-86300-6 |
| Classificazione | SCI013000SCI026000TEC010030 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto | Hydrocarbons in non-saline waters -- Oxygen containing compounds in non-saline waters -- Halogen containing compounds in non-saline waters -- Nitrogen compounds in non-saline waters -- Phosphorus contianing compounds in non-saline waters -- Sulphur containing compounds in non-saline waters -- Surface active agents in non-saline waters -- Volatile organic compounds -- Multiorganics in non-saline waters -- Pesticides and herbicides -- Organic compounds in saline waters -- Miscellaneous organic compounds -- Organometallic compounds -- Organic compounds aqueous precipitation. |
| Record Nr. | UNINA-9910824951403321 |
|
Crompton T. R (Thomas Roy)
|
||
| Leiden, The Netherlands : , : CRC Press/Balkema, an imprint of the Taylor & Francis Group, , [2014] | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Organic mass spectrometry in art and archaeology [[electronic resource] /] / edited by Maria Perla Colombini and Francesca Modugno
| Organic mass spectrometry in art and archaeology [[electronic resource] /] / edited by Maria Perla Colombini and Francesca Modugno |
| Pubbl/distr/stampa | Chichester, West Sussex, U.K. ; ; Hoboken, N.J., : Wiley, 2009 |
| Descrizione fisica | 1 online resource (517 p.) |
| Disciplina |
702.88
708.87 |
| Altri autori (Persone) |
ColombiniMaria Perla
ModugnoFrancesca |
| Soggetto topico |
Mass spectrometry
Organic compounds - Analysis |
| Soggetto genere / forma | Electronic books. |
| ISBN |
1-282-25938-5
9786612259388 0-470-74191-0 0-470-74192-9 |
| Classificazione | 20.15 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Organic Mass Spectrometry in Art and Archaeology; Contents; List of Contributors; Acknowledgements; Preface; Part I Introduction; 1 Organic Materials in Art and Archaeology; 2 Overview of Mass Spectrometric Based Techniques Applied in the Cultural Heritage Field; PART II DIRECT MASS SPECTROMETRIC ANALYSIS; 3 Direct Mass Spectrometric Techniques: Versatile Tools to Characterise Resinous Materials; 4 Direct Mass Spectrometry to Characterise Wax and Lipid Materials; 5 GALDI-MS Applied to Characterise Natural Varnishes and Binders; 6 MALDI-MS Applied to the Analysis of Protein Paint Binders
PART III GAS CHROMATOGRAPHY/MASS SPECTROMETRY7 GC/MS in the Characterization of Lipids; 8 GC/MS in the Characterisation of Resinous Materials; 9 GC/MS in the Characterisation of Protein Paint Binders; 10 SPME/GC-MS in the Characterisation of Terpenic Resins; 11 Py-GC/MS of Organic Paint Binders; 12 Py-GC/MS of Natural and Synthetic Resins; PART IV LIQUID CHROMATOGRAPHY/MASS SPECTROMETRY; 13 Characterization of Organic Natural Dyes by Electrospray Mass Spectrometry Coupled with HPLC and/or Capillary Electrophoresis; PART V OTHER MS-BASED TECHNIQUES 14 Compound-specific Stable Isotopes in Organic Residue Analysis in Archaeology15 ToF-SIMS Study of Organic Materials in Cultural Heritage: Identification and Chemical Imaging; 16 Accelerator Mass Spectrometry for 14C Dating; Index; Colour Plates |
| Record Nr. | UNINA-9910139922603321 |
| Chichester, West Sussex, U.K. ; ; Hoboken, N.J., : Wiley, 2009 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Organic mass spectrometry in art and archaeology / Maria Perla Colombini, Francesca Modugno
| Organic mass spectrometry in art and archaeology / Maria Perla Colombini, Francesca Modugno |
| Pubbl/distr/stampa | Chichester, West Sussex ; Hoboken, N. J. : Wiley, 2009 |
| Descrizione fisica | xiii, 493 p. : ill. ; 25 cm |
| Disciplina | 543.5 |
| Altri autori (Persone) |
Colombini, Maria Perlaauthor
Modugno, Francescaauthor |
| Soggetto topico |
Mass spectrometry
Organic compounds - Analysis |
| ISBN | 9780470517031 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Record Nr. | UNISALENTO-991000428339707536 |
| Chichester, West Sussex ; Hoboken, N. J. : Wiley, 2009 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. del Salento | ||
| ||
Organic mass spectrometry in art and archaeology [[electronic resource] /] / edited by Maria Perla Colombini and Francesca Modugno
| Organic mass spectrometry in art and archaeology [[electronic resource] /] / edited by Maria Perla Colombini and Francesca Modugno |
| Pubbl/distr/stampa | Chichester, West Sussex, U.K. ; ; Hoboken, N.J., : Wiley, 2009 |
| Descrizione fisica | 1 online resource (517 p.) |
| Disciplina |
702.88
708.87 |
| Altri autori (Persone) |
ColombiniMaria Perla
ModugnoFrancesca |
| Soggetto topico |
Mass spectrometry
Organic compounds - Analysis |
| ISBN |
1-282-25938-5
9786612259388 0-470-74191-0 0-470-74192-9 |
| Classificazione | 20.15 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Organic Mass Spectrometry in Art and Archaeology; Contents; List of Contributors; Acknowledgements; Preface; Part I Introduction; 1 Organic Materials in Art and Archaeology; 2 Overview of Mass Spectrometric Based Techniques Applied in the Cultural Heritage Field; PART II DIRECT MASS SPECTROMETRIC ANALYSIS; 3 Direct Mass Spectrometric Techniques: Versatile Tools to Characterise Resinous Materials; 4 Direct Mass Spectrometry to Characterise Wax and Lipid Materials; 5 GALDI-MS Applied to Characterise Natural Varnishes and Binders; 6 MALDI-MS Applied to the Analysis of Protein Paint Binders
PART III GAS CHROMATOGRAPHY/MASS SPECTROMETRY7 GC/MS in the Characterization of Lipids; 8 GC/MS in the Characterisation of Resinous Materials; 9 GC/MS in the Characterisation of Protein Paint Binders; 10 SPME/GC-MS in the Characterisation of Terpenic Resins; 11 Py-GC/MS of Organic Paint Binders; 12 Py-GC/MS of Natural and Synthetic Resins; PART IV LIQUID CHROMATOGRAPHY/MASS SPECTROMETRY; 13 Characterization of Organic Natural Dyes by Electrospray Mass Spectrometry Coupled with HPLC and/or Capillary Electrophoresis; PART V OTHER MS-BASED TECHNIQUES 14 Compound-specific Stable Isotopes in Organic Residue Analysis in Archaeology15 ToF-SIMS Study of Organic Materials in Cultural Heritage: Identification and Chemical Imaging; 16 Accelerator Mass Spectrometry for 14C Dating; Index; Colour Plates |
| Record Nr. | UNINA-9910831070503321 |
| Chichester, West Sussex, U.K. ; ; Hoboken, N.J., : Wiley, 2009 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
