Info
- Utilizzare la checkbox di selezione a fianco di ciascun documento per attivare le funzionalità di stampa, invio email, download nei formati disponibili del (i) record.
Gas chromatography and mass spectrometry [[electronic resource] ] : a practical guide / / Fulton G. Kitson, Barbara S. Larsen, Charles N. McEwen
| Gas chromatography and mass spectrometry [[electronic resource] ] : a practical guide / / Fulton G. Kitson, Barbara S. Larsen, Charles N. McEwen |
| Autore | Kitson Fulton G |
| Pubbl/distr/stampa | San Diego, : Academic Press, c1996 |
| Descrizione fisica | 1 online resource (xii, 381 pages) : illustrations |
| Disciplina | 543/.0873 |
| Altri autori (Persone) |
LarsenBarbara Seliger
McEwenCharles N. <1942-> |
| Soggetto topico |
Gas chromatography
Mass spectrometry |
| ISBN |
1-281-01886-4
9786611018863 0-08-053232-2 |
| Formato | Materiale a stampa  |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Part I: The Fundamentals of GC/MS; Chapter 1. What Is GC/MS?; Chapter 2. Interpretation of Mass Spectra; Chapter 3. Quantitative GC/MS; Part II: GC Conditions, Derivatization, and Mass Spectral Interpretation of Specific Compound Types; Chapter 4. Acids; Chapter 5. Alcohols; Chapter 6. Aldehydes; Chapter 7. Amides; Chapter 8. Amines; Chapter 9. Amino Acids; Chapter 10. Common Contaminants; Chapter 11. Drugs and Their Metabolites; Chapter 12. Esters; Chapter 13. Ethers
Chapter 14. Fluorinated CompoundsChapter 15. Gases; Chapter 16. Glycols; Chapter 17. Halogenated Compounds (Other Than Fluorinated); Chapter 18. Hydrocarbons; Chapter 19. Isocyanates; Chapter 20. Ketones; Chapter 21. Nitriles; Chapter 22. Nitroaromatics; Chapter 23. Nitrogen-Containing Heterocyclics; Chapter 24. Nucleosides (TMS Derivatives); Chapter 25. Pesticides; Chapter 26. Phenols; Chapter 27. Phosphorus Compounds; Chapter 28. Plasticizers and Other Polymer Additives (Including Phthalates); Chapter 29. Prostaglandins (MO-TMS Derivatives); Chapter 30. Solvents and Their Impurities Chapter 31. SteroidsChapter 32. Sugars (Monosaccharides); Chapter 33. Sulfur Compounds; Part III: Ions for Determining Unknown Structures; Part IV: Appendices; Appendix 1. Definitions of Terms Related to Gas Chromatography; Appendix 2. Tips for Gas Chromatography; Appendix 3. Derivatives Found Useful in GC/MS; Appendix 4. Cross-Index Chart for GC Phases; Appendix 5. McReynolds' Constants; Appendix 6. Simple GC Troubleshooting; Appendix 7. Definitions of Terms Related to Mass Spectrometry; Appendix 8. Tips and Troubleshooting for Mass Spectrometers Appendix 9. Atomic Masses and Isotope AbundancesAppendix 10. Structurally Significant McLafferty Rearrangement Ions; Appendix 11. Isotope Patterns for Chlorine and Bromine; Appendix 12. Mixtures for Determining Mass Spectral Resolution; Index |
| Record Nr. | UNINA-9910784534603321 |
Kitson Fulton G
|
||
| San Diego, : Academic Press, c1996 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Gas chromatography and mass spectrometry : a practical guide / / Fulton G. Kitson, Barbara S. Larsen, Charles N. McEwen
| Gas chromatography and mass spectrometry : a practical guide / / Fulton G. Kitson, Barbara S. Larsen, Charles N. McEwen |
| Autore | Kitson Fulton G |
| Edizione | [1st ed.] |
| Pubbl/distr/stampa | San Diego, : Academic Press, c1996 |
| Descrizione fisica | 1 online resource (xii, 381 pages) : illustrations |
| Disciplina |
543/.0873
543.0873 |
| Altri autori (Persone) |
LarsenBarbara Seliger
McEwenCharles N. <1942-> |
| Soggetto topico |
Gas chromatography
Mass spectrometry |
| ISBN |
1-281-01886-4
9786611018863 0-08-053232-2 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Part I: The Fundamentals of GC/MS; Chapter 1. What Is GC/MS?; Chapter 2. Interpretation of Mass Spectra; Chapter 3. Quantitative GC/MS; Part II: GC Conditions, Derivatization, and Mass Spectral Interpretation of Specific Compound Types; Chapter 4. Acids; Chapter 5. Alcohols; Chapter 6. Aldehydes; Chapter 7. Amides; Chapter 8. Amines; Chapter 9. Amino Acids; Chapter 10. Common Contaminants; Chapter 11. Drugs and Their Metabolites; Chapter 12. Esters; Chapter 13. Ethers
Chapter 14. Fluorinated CompoundsChapter 15. Gases; Chapter 16. Glycols; Chapter 17. Halogenated Compounds (Other Than Fluorinated); Chapter 18. Hydrocarbons; Chapter 19. Isocyanates; Chapter 20. Ketones; Chapter 21. Nitriles; Chapter 22. Nitroaromatics; Chapter 23. Nitrogen-Containing Heterocyclics; Chapter 24. Nucleosides (TMS Derivatives); Chapter 25. Pesticides; Chapter 26. Phenols; Chapter 27. Phosphorus Compounds; Chapter 28. Plasticizers and Other Polymer Additives (Including Phthalates); Chapter 29. Prostaglandins (MO-TMS Derivatives); Chapter 30. Solvents and Their Impurities Chapter 31. SteroidsChapter 32. Sugars (Monosaccharides); Chapter 33. Sulfur Compounds; Part III: Ions for Determining Unknown Structures; Part IV: Appendices; Appendix 1. Definitions of Terms Related to Gas Chromatography; Appendix 2. Tips for Gas Chromatography; Appendix 3. Derivatives Found Useful in GC/MS; Appendix 4. Cross-Index Chart for GC Phases; Appendix 5. McReynolds' Constants; Appendix 6. Simple GC Troubleshooting; Appendix 7. Definitions of Terms Related to Mass Spectrometry; Appendix 8. Tips and Troubleshooting for Mass Spectrometers Appendix 9. Atomic Masses and Isotope AbundancesAppendix 10. Structurally Significant McLafferty Rearrangement Ions; Appendix 11. Isotope Patterns for Chlorine and Bromine; Appendix 12. Mixtures for Determining Mass Spectral Resolution; Index |
| Record Nr. | UNINA-9910827538403321 |
|
Kitson Fulton G
|
||
| San Diego, : Academic Press, c1996 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Gas chromatography and mass spectrometry [[electronic resource] ] : a practical guide / / O. David Sparkman, Zelda E. Penton, Fulton G. Kitson
| Gas chromatography and mass spectrometry [[electronic resource] ] : a practical guide / / O. David Sparkman, Zelda E. Penton, Fulton G. Kitson |
| Autore | Sparkman O. David (Orrin David), <1942-> |
| Edizione | [2nd ed.] |
| Pubbl/distr/stampa | Boston, : Elsevier, 2011 |
| Descrizione fisica | 1 online resource (633 p.) |
| Disciplina | 543/.85 |
| Altri autori (Persone) |
PentonZelda
KitsonFulton G |
| Soggetto topico |
Gas chromatography
Mass spectrometry |
| Soggetto genere / forma | Electronic books. |
| ISBN |
1-283-17107-4
9786613171078 0-08-092015-2 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto | The fundamentals of GC/MS -- Introduction and history -- Gas chromatography -- The gc/ms interface -- Mass spectrometry instrumentation -- Mass spectral data interpretation -- Quantitation with GC/MS -- GC conditions, derivatization, and mass spectral interpretation -- Of specific compound types -- Acids -- Alcohols -- Aldehydes -- Amides -- Amines -- Amino acid -- Common contaminants -- Drugs and their metabolites -- Esters -- Ethers -- Fluorinated compounds -- Gases -- Glycols -- Halogenated compounds (other than fluorinated) -- Hydrocarbons -- Isocyanates -- Ketones -- Nitriles -- Nitroaromatics -- Nitrogen-containing heterocyclics -- Nucleosides (TMS derivatives) -- Pesticides -- Phenols -- Phosphorus compounds -- Plasticizers and other polymer additives (including phthalates) -- Prostaglandins (MO-TMS derivatives) -- Solvents and their impurities -- Steroids -- Sugars (monosaccharides) -- Sulfur compounds -- Appendices -- A definitions of terms related to gas chromatography -- B definitions of terms related to mass spectrometry -- C atomic masses and isotope abundances -- X+1 and x+2 values for ions containing atoms of C and H based on -- Isotope contributions -- E isotope peak patterns for ions containing atoms of Cl and/or Br -- F steps to follow in the determination of an elemental composition -- Based on isotope peak intensity ratios -- G derivatization in GC/MS -- H points of comparison of LC/MS vs GC/MS -- I list of available EI mass spectral databases -- J information required for reporting a GC/MS analysis -- K third-party software for use with GC/MS -- GC installation and maintenance -- Troubleshooting common GC problems -- N maintenance, operating tips, and troubleshooting for mass spectrometers -- O mixtures for determining mass spectral resolution -- P cross-index chart for GC stationary phases -- Q ions for determining unknown structures. |
| Record Nr. | UNINA-9910459616903321 |
|
Sparkman O. David (Orrin David), <1942->
|
||
| Boston, : Elsevier, 2011 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Gas chromatography and mass spectrometry [[electronic resource] ] : a practical guide / / O. David Sparkman, Zelda E. Penton, Fulton G. Kitson
| Gas chromatography and mass spectrometry [[electronic resource] ] : a practical guide / / O. David Sparkman, Zelda E. Penton, Fulton G. Kitson |
| Autore | Sparkman O. David (Orrin David), <1942-> |
| Edizione | [2nd ed.] |
| Pubbl/distr/stampa | Boston, : Elsevier, 2011 |
| Descrizione fisica | 1 online resource (633 p.) |
| Disciplina | 543/.85 |
| Altri autori (Persone) |
PentonZelda
KitsonFulton G |
| Soggetto topico |
Gas chromatography
Mass spectrometry |
| ISBN |
1-283-17107-4
9786613171078 0-08-092015-2 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto | The fundamentals of GC/MS -- Introduction and history -- Gas chromatography -- The gc/ms interface -- Mass spectrometry instrumentation -- Mass spectral data interpretation -- Quantitation with GC/MS -- GC conditions, derivatization, and mass spectral interpretation -- Of specific compound types -- Acids -- Alcohols -- Aldehydes -- Amides -- Amines -- Amino acid -- Common contaminants -- Drugs and their metabolites -- Esters -- Ethers -- Fluorinated compounds -- Gases -- Glycols -- Halogenated compounds (other than fluorinated) -- Hydrocarbons -- Isocyanates -- Ketones -- Nitriles -- Nitroaromatics -- Nitrogen-containing heterocyclics -- Nucleosides (TMS derivatives) -- Pesticides -- Phenols -- Phosphorus compounds -- Plasticizers and other polymer additives (including phthalates) -- Prostaglandins (MO-TMS derivatives) -- Solvents and their impurities -- Steroids -- Sugars (monosaccharides) -- Sulfur compounds -- Appendices -- A definitions of terms related to gas chromatography -- B definitions of terms related to mass spectrometry -- C atomic masses and isotope abundances -- X+1 and x+2 values for ions containing atoms of C and H based on -- Isotope contributions -- E isotope peak patterns for ions containing atoms of Cl and/or Br -- F steps to follow in the determination of an elemental composition -- Based on isotope peak intensity ratios -- G derivatization in GC/MS -- H points of comparison of LC/MS vs GC/MS -- I list of available EI mass spectral databases -- J information required for reporting a GC/MS analysis -- K third-party software for use with GC/MS -- GC installation and maintenance -- Troubleshooting common GC problems -- N maintenance, operating tips, and troubleshooting for mass spectrometers -- O mixtures for determining mass spectral resolution -- P cross-index chart for GC stationary phases -- Q ions for determining unknown structures. |
| Record Nr. | UNINA-9910785586303321 |
|
Sparkman O. David (Orrin David), <1942->
|
||
| Boston, : Elsevier, 2011 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Gas chromatography and mass spectrometry : a practical guide / / O. David Sparkman, Zelda E. Penton, Fulton G. Kitson
| Gas chromatography and mass spectrometry : a practical guide / / O. David Sparkman, Zelda E. Penton, Fulton G. Kitson |
| Autore | Sparkman O. David (Orrin David), <1942-> |
| Edizione | [2nd ed.] |
| Pubbl/distr/stampa | Boston, : Elsevier, 2011 |
| Descrizione fisica | 1 online resource (633 p.) |
| Disciplina |
543/.85
543.85 |
| Altri autori (Persone) |
PentonZelda
KitsonFulton G |
| Soggetto topico |
Gas chromatography
Mass spectrometry |
| ISBN |
1-283-17107-4
9786613171078 0-08-092015-2 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto | The fundamentals of GC/MS -- Introduction and history -- Gas chromatography -- The gc/ms interface -- Mass spectrometry instrumentation -- Mass spectral data interpretation -- Quantitation with GC/MS -- GC conditions, derivatization, and mass spectral interpretation -- Of specific compound types -- Acids -- Alcohols -- Aldehydes -- Amides -- Amines -- Amino acid -- Common contaminants -- Drugs and their metabolites -- Esters -- Ethers -- Fluorinated compounds -- Gases -- Glycols -- Halogenated compounds (other than fluorinated) -- Hydrocarbons -- Isocyanates -- Ketones -- Nitriles -- Nitroaromatics -- Nitrogen-containing heterocyclics -- Nucleosides (TMS derivatives) -- Pesticides -- Phenols -- Phosphorus compounds -- Plasticizers and other polymer additives (including phthalates) -- Prostaglandins (MO-TMS derivatives) -- Solvents and their impurities -- Steroids -- Sugars (monosaccharides) -- Sulfur compounds -- Appendices -- A definitions of terms related to gas chromatography -- B definitions of terms related to mass spectrometry -- C atomic masses and isotope abundances -- X+1 and x+2 values for ions containing atoms of C and H based on -- Isotope contributions -- E isotope peak patterns for ions containing atoms of Cl and/or Br -- F steps to follow in the determination of an elemental composition -- Based on isotope peak intensity ratios -- G derivatization in GC/MS -- H points of comparison of LC/MS vs GC/MS -- I list of available EI mass spectral databases -- J information required for reporting a GC/MS analysis -- K third-party software for use with GC/MS -- GC installation and maintenance -- Troubleshooting common GC problems -- N maintenance, operating tips, and troubleshooting for mass spectrometers -- O mixtures for determining mass spectral resolution -- P cross-index chart for GC stationary phases -- Q ions for determining unknown structures. |
| Record Nr. | UNINA-9910827470903321 |
|
Sparkman O. David (Orrin David), <1942->
|
||
| Boston, : Elsevier, 2011 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
GC/MS : a practical user's guide / / Marvin C. McMaster
| GC/MS : a practical user's guide / / Marvin C. McMaster |
| Autore | McMaster Marvin C. |
| Edizione | [2nd ed.] |
| Pubbl/distr/stampa | Hoboken, New Jersey : , : Wiley-Interscience, , 2008 |
| Descrizione fisica | 1 online resource (194 p.) |
| Disciplina |
543
543.85 543/.85 |
| Soggetto topico |
Gas chromatography
Mass spectrometry |
| ISBN |
1-118-21005-0
1-281-20402-1 9786611204020 0-470-22835-0 0-470-22834-2 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto | Introduction -- Sample preparation and introduction -- The gas chromatograph -- The mass spectrometer -- Getting started in GC/MS -- Chromatographic methods development -- Mass spectrometer setup and operation -- Data processing and network interfacing -- System maintenance and troubleshooting -- GC/MS in the environmental laboratory -- GC/MS in forensics, toxicology, and space science -- An introduction to structural interpretation -- Ion trap GC/MS systems -- Other GC/MS systems -- An introduction to LC/MS -- Innovation in GC/MS. |
| Record Nr. | UNINA-9910145283803321 |
|
McMaster Marvin C.
|
||
| Hoboken, New Jersey : , : Wiley-Interscience, , 2008 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
GC/MS : a practical user's guide / / Marvin C. McMaster
| GC/MS : a practical user's guide / / Marvin C. McMaster |
| Autore | McMaster Marvin C. |
| Edizione | [2nd ed.] |
| Pubbl/distr/stampa | Hoboken, New Jersey : , : Wiley-Interscience, , 2008 |
| Descrizione fisica | 1 online resource (194 p.) |
| Disciplina |
543
543.85 543/.85 |
| Soggetto topico |
Gas chromatography
Mass spectrometry |
| ISBN |
1-118-21005-0
1-281-20402-1 9786611204020 0-470-22835-0 0-470-22834-2 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto | Introduction -- Sample preparation and introduction -- The gas chromatograph -- The mass spectrometer -- Getting started in GC/MS -- Chromatographic methods development -- Mass spectrometer setup and operation -- Data processing and network interfacing -- System maintenance and troubleshooting -- GC/MS in the environmental laboratory -- GC/MS in forensics, toxicology, and space science -- An introduction to structural interpretation -- Ion trap GC/MS systems -- Other GC/MS systems -- An introduction to LC/MS -- Innovation in GC/MS. |
| Record Nr. | UNINA-9910830358003321 |
|
McMaster Marvin C.
|
||
| Hoboken, New Jersey : , : Wiley-Interscience, , 2008 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
GC/MS assays for abused drugs in body fluids / / Rodger L. Foltz, Allison F. Fentiman, Jr., Ruth B. Foltz
| GC/MS assays for abused drugs in body fluids / / Rodger L. Foltz, Allison F. Fentiman, Jr., Ruth B. Foltz |
| Autore | Foltz Rodger L. |
| Pubbl/distr/stampa | Rockville, Maryland : , : Department of Health and Human Services, Public Health Service, Alcohol, Drug Abuse and Mental Health Administration, National Institute on Drug Abuse, Division on Research, , 1980 |
| Descrizione fisica | 1 online resource (ix, 202 pages) : illustrations |
| Collana |
NIDA research monograph
DHHS publication |
| Soggetto topico |
Psychotropic drugs - United States - Analysis
Gas chromatography Mass spectrometry Volatile organic compounds - United States - Analysis Body fluids - Analysis Psychotropic drugs - Analysis |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Altri titoli varianti | Gas chromatography/mass spectrometry assays for abused drugs in body fluids |
| Record Nr. | UNINA-9910712095703321 |
GC/MS in clinical chemistry [[electronic resource] /] / Petra Gerhards ... [et al.] ; translated by G. Leach
| GC/MS in clinical chemistry [[electronic resource] /] / Petra Gerhards ... [et al.] ; translated by G. Leach |
| Pubbl/distr/stampa | Weinheim ; ; New York, : Wiley-VCH, c1999 |
| Descrizione fisica | 1 online resource (259 p.) |
| Disciplina |
616.07/56
616.0756 |
| Altri autori (Persone) | GerhardsPetra |
| Soggetto topico |
Clinical chemistry
Gas chromatography Mass spectrometry |
| Soggetto genere / forma | Electronic books. |
| ISBN |
1-281-75842-6
9786611758424 3-527-61404-4 3-527-61405-2 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
GC/MS in Clinical Chemistry; Contents; Part I Fundamental Principles of Analysis by Gas Chromatography and Mass Spectrometry; 1. Physical Theory and Equipment Design; 1.1 Adsorption; 1.2 Partition; 1.3 Design of a Gas Chromatography System; 2. Injection and Headspace Technique; 2.1 Injection; 2.1.1 Splitless Injection; 2.1.2 Split Injection; 2.1.3 Temperature-Programmed Injection; 2.1.4 On-Column Injection; 2.2 Headspace Technique; 2.2.1 Static Headspace; 2.2.2 Dynamic Headspace; 3. Columns and Carrier Gas; 3.1 Packed Columns; 3.2 Capillary Columns; 3.3 Stationary Phases; 3.4 Film Thickness
3.5 Carrier Gas4. GC Detectors and Mass Spectrometry; 4.1 Selectivity; 4.2 The Flame Ionization Detector (FID); 4.3 The Electron Capture Detector (ECD); 4.4 Mass Spectrometry; 4.4.1 Design and Function of a Quadrupole Mass Spectrometer; 4.4.2 Detection; 4.4.3 Sample Introduction - the GC/MS Interface; 4.4.4 The Total Ion Current (TIC); 4.4.5 Selected Ion Monitoring (SIM); 4.4.6 Data Processing; 5. Quantification; 5.1 Methods Based on Internal Standards; 5.2 Standard Addition; 5.3 External Calibration; 5.4 Quantification in the Split Mode; 5.5 Limits of Detection; References for Part I Part II Drug Screening6. Epidemiology of the Abuse of Drugs and Medicaments; 6.1 Introduction; 6.2 Specific Data and Trends; 6.2.1 Opiates/Opioids; 6.2.1.1 Heroin; 6.2.1.2 Codeine; 6.2.1.3 Dehydrocodeine (DHC); 6.2.1.4 Methadone; 6.2.1.5 Tramadol; 6.2.1.6 Tilidine; 6.2.1.7 Other Centrally Active Analgesics; 6.2.2 Peripheral Analgesics; 6.2.3 Benzodiazepines; 6.2.3.1 Diazepam; 6.2.3.2 Flunitrazepam; 6.2.3.3 Bromazepam; 6.2.4 Barbiturates; 6.2.5 Other Sedatives and Addictive Substances; 6.2.5.1 Chlormethiazole; 6.2.5.2 Antihistamines; 6.2.6 Amphetamines and Related Substances 6.2.6.1 Substances of the Drug Scene6.2.6.2 Psychoanaleptics and Antihypotonics; 6.2.6.3 Appetite Suppressants; 6.2.7 Designer Drugs; 6.2.8 Cannabis; 6.2.9 Cocaine; 6.2.10 Other Hallucinogens; 6.2.10.1 Lysergic Acid Diethylamide (LSD); 6.2.10.2 Other Indole Derivatives; 6.2.10.3 Mescalin; 6.2.10.4 Nutmeg; 6.2.10.5 Pipendine Denvatives; 6.2.10.6 Fly Agaric; 6.2.10.7 Biperiden; 6.2.11 Substances Taken by Sniffing; 7. Methods of Sample Preparation for Drug Analysis; 7.1 History of Sample Preparation; 7.2 The Principle of Solid Phase Extraction; 7.2.1 Practical Aspects 7.2.1.1 Sample Preparation for the Matrix Urine7.2.1.2 Sample Preparation for the Matrix Whole Blood; 7.3 Liquid-Liquid Extraction (LLE); 7.4 Comparison of SPE with LLE; 7.5 Quantitative Determination of Derivatized Drugs; 7.5.1 Introduction; 7.5.2 Determination of the Detection Limits; 7.5.3 Sample Preparation and Analysis of Real Samples; 8. Drug Screening from Urine by GC/MS; 8.1 General Aspects of Drug Screening from Urine; 8.1.1 Differentiation between Drug Screening and Other Screening Procedures; 8.1.2 Sample Material; 8.1.3 Possibilities for Manipulation of Samples 8.1.4 Immunological Methods of Analysis |
| Record Nr. | UNINA-9910144142803321 |
| Weinheim ; ; New York, : Wiley-VCH, c1999 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
GC/MS in clinical chemistry [[electronic resource] /] / Petra Gerhards ... [et al.] ; translated by G. Leach
| GC/MS in clinical chemistry [[electronic resource] /] / Petra Gerhards ... [et al.] ; translated by G. Leach |
| Pubbl/distr/stampa | Weinheim ; ; New York, : Wiley-VCH, c1999 |
| Descrizione fisica | 1 online resource (259 p.) |
| Disciplina |
616.07/56
616.0756 |
| Altri autori (Persone) | GerhardsPetra |
| Soggetto topico |
Clinical chemistry
Gas chromatography Mass spectrometry |
| ISBN |
1-281-75842-6
9786611758424 3-527-61404-4 3-527-61405-2 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
GC/MS in Clinical Chemistry; Contents; Part I Fundamental Principles of Analysis by Gas Chromatography and Mass Spectrometry; 1. Physical Theory and Equipment Design; 1.1 Adsorption; 1.2 Partition; 1.3 Design of a Gas Chromatography System; 2. Injection and Headspace Technique; 2.1 Injection; 2.1.1 Splitless Injection; 2.1.2 Split Injection; 2.1.3 Temperature-Programmed Injection; 2.1.4 On-Column Injection; 2.2 Headspace Technique; 2.2.1 Static Headspace; 2.2.2 Dynamic Headspace; 3. Columns and Carrier Gas; 3.1 Packed Columns; 3.2 Capillary Columns; 3.3 Stationary Phases; 3.4 Film Thickness
3.5 Carrier Gas4. GC Detectors and Mass Spectrometry; 4.1 Selectivity; 4.2 The Flame Ionization Detector (FID); 4.3 The Electron Capture Detector (ECD); 4.4 Mass Spectrometry; 4.4.1 Design and Function of a Quadrupole Mass Spectrometer; 4.4.2 Detection; 4.4.3 Sample Introduction - the GC/MS Interface; 4.4.4 The Total Ion Current (TIC); 4.4.5 Selected Ion Monitoring (SIM); 4.4.6 Data Processing; 5. Quantification; 5.1 Methods Based on Internal Standards; 5.2 Standard Addition; 5.3 External Calibration; 5.4 Quantification in the Split Mode; 5.5 Limits of Detection; References for Part I Part II Drug Screening6. Epidemiology of the Abuse of Drugs and Medicaments; 6.1 Introduction; 6.2 Specific Data and Trends; 6.2.1 Opiates/Opioids; 6.2.1.1 Heroin; 6.2.1.2 Codeine; 6.2.1.3 Dehydrocodeine (DHC); 6.2.1.4 Methadone; 6.2.1.5 Tramadol; 6.2.1.6 Tilidine; 6.2.1.7 Other Centrally Active Analgesics; 6.2.2 Peripheral Analgesics; 6.2.3 Benzodiazepines; 6.2.3.1 Diazepam; 6.2.3.2 Flunitrazepam; 6.2.3.3 Bromazepam; 6.2.4 Barbiturates; 6.2.5 Other Sedatives and Addictive Substances; 6.2.5.1 Chlormethiazole; 6.2.5.2 Antihistamines; 6.2.6 Amphetamines and Related Substances 6.2.6.1 Substances of the Drug Scene6.2.6.2 Psychoanaleptics and Antihypotonics; 6.2.6.3 Appetite Suppressants; 6.2.7 Designer Drugs; 6.2.8 Cannabis; 6.2.9 Cocaine; 6.2.10 Other Hallucinogens; 6.2.10.1 Lysergic Acid Diethylamide (LSD); 6.2.10.2 Other Indole Derivatives; 6.2.10.3 Mescalin; 6.2.10.4 Nutmeg; 6.2.10.5 Pipendine Denvatives; 6.2.10.6 Fly Agaric; 6.2.10.7 Biperiden; 6.2.11 Substances Taken by Sniffing; 7. Methods of Sample Preparation for Drug Analysis; 7.1 History of Sample Preparation; 7.2 The Principle of Solid Phase Extraction; 7.2.1 Practical Aspects 7.2.1.1 Sample Preparation for the Matrix Urine7.2.1.2 Sample Preparation for the Matrix Whole Blood; 7.3 Liquid-Liquid Extraction (LLE); 7.4 Comparison of SPE with LLE; 7.5 Quantitative Determination of Derivatized Drugs; 7.5.1 Introduction; 7.5.2 Determination of the Detection Limits; 7.5.3 Sample Preparation and Analysis of Real Samples; 8. Drug Screening from Urine by GC/MS; 8.1 General Aspects of Drug Screening from Urine; 8.1.1 Differentiation between Drug Screening and Other Screening Procedures; 8.1.2 Sample Material; 8.1.3 Possibilities for Manipulation of Samples 8.1.4 Immunological Methods of Analysis |
| Record Nr. | UNINA-9910830074703321 |
| Weinheim ; ; New York, : Wiley-VCH, c1999 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Soggetto topico
-
Mass spectrometry
(351)
- Mass Spectrometry (45)
- Gas chromatography (34)
- Drugs - Analysis (20)
- Liquid chromatography (20)