Info
- Utilizzare la checkbox di selezione a fianco di ciascun documento per attivare le funzionalità di stampa, invio email, download nei formati disponibili del (i) record.
Praxis der Hochleistungs-Flüssigchromatographie [[electronic resource] /] / Veronika R. Meyer
| Praxis der Hochleistungs-Flüssigchromatographie [[electronic resource] /] / Veronika R. Meyer |
| Autore | Meyer Veronika |
| Edizione | [9. Aufl.] |
| Pubbl/distr/stampa | Weinheim, : Wiley, 2004 |
| Descrizione fisica | 1 online resource (368 p.) |
| Disciplina |
543.0894
543.84 544.924 |
| Soggetto topico | Liquid chromatography |
| ISBN |
1-282-02134-6
9786612021343 3-527-62358-2 3-527-62359-0 |
| Formato | Materiale a stampa  |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | ger |
| Nota di contenuto |
Praxis der Hochleistungs- Flüssigchromatographie; Inhaltsverzeichnis; Vorwort; Vorwort zur neunten Auflage; 0 Wichtige und nützliche Gleichungen für die HPLC; 1 Einleitung; 1.1 HPLC: Eine leistungsfähige Trennmethode; 1.2 Ein erstes HPLC-Experiment; 1.3 Die flüssigchromatographischen Trennverfahren; 1.4 Die HPLC-Apparatur; 1.5 Sicherheit am HPLC-Arbeitsplatz; 1.6 Vergleich von Hochleistungs-Flüssigchromatographie und Gaschromatographie; 1.7 Druckeinheiten; 1.8 Längeneinheiten; 1.9 Wissenschaftliche Zeitschriften; 1.10 Empfehlenswerte Bücher; 2 Theoretische Grundlagen
2.1 Der chromatographische Prozess2.2 Bandenverbreiterung; 2.3 Das Chromatogramm und seine Aussage; 2.4 Graphische Darstellung von Peakpaaren mit verschiedener Auflösung; 2.5 Die Beeinflussung der Auflösung; 2.6 Totvolumina (extra-column-Volumina); 2.7 Tailing; 2.8 Peakkapazität und statistische Auflösungswahrscheinlichkeit; 2.9 Temperatureinflüsse in der HPLC; 2.10 Die Grenzen der HPLC; 3 Pumpen; 3.1 Allgemeines; 3.2 Die Kurzhub-Kolbenpumpe; 3.3 Unterhalt und Reparaturen; 3.4 Andere Pumpentypen; 4 Bereitstellung der Apparatur bis zur Probenaufgabe; 4.1 Auswahl der mobilen Phase 4.2 Vorbereitung der mobilen Phase4.3 Gradientensysteme; 4.4 Kapillarleitungen; 4.5 Fittings; 4.6 Probenaufgabesysteme; 4.7 Probelösung und Probevolumen; 5 Lösungsmitteleigenschaften; 5.1 Tabelle organischer Lösungsmittel; 5.2 Lösungsmittelselektivität; 5.3 Mischbarkeit; 5.4 Puffer; 5.5 Haltbarkeit von mobilen Phasen; 6 Detektoren; 6.1 Allgemeines; 6.2 UV-Detektoren; 6.3 Brechungsindex-Detektoren; 6.4 Fluoreszenz-Detektoren; 6.5 Elektrochemische Detektoren; 6.6 Lichtstreuungs-Detektoren; 6.7 Andere Detektoren; 6.8 Mehrfachdetektion; 6.9 Indirekte Detektion; 6.10 Kopplung mit Spektroskopie 7 Säulen und stationäre Phasen7.1 Säulen für die HPLC; 7.2 Vorsäulen; 7.3 Allgemeines über stationäre Phasen; 7.4 Silicagel; 7.5 Chemisch modifiziertes Silicagel; 7.6 Styrol-Divinylbenzol; 7.7 Einige weitere stationäre Phasen; 7.8 Vorsichtsmaßnahmen und Regeneration; 8 Das Testen von HPLC-Säulen; 8.1 Einfache Tests für HPLC-Säulen; 8.2 Bestimmung der Korngröße; 8.3 Bestimmung der Totzeit; 8.4 Das Testgemisch; 8.5 Dimensionslose Größen zur Charakterisierung von HPLC-Säulen; 8.6 Die van Deemter-Gleichung aus reduzierten Größen und ihre Nützlichkeit für die Säulendiagnose 8.7 Diffusionskoeffizienten9 Adsorptions-Chromatographie; 9.1 Was heißt Adsorption?; 9.2 Die eluotrope Reihe; 9.3 Selektivitätseigenschaften der mobilen Phase; 9.4 Wahl und Optimierung der mobilen Phase; 9.5 Anwendungsbeispiele; 10 Umkehrphasen-Chromatographie; 10.1 Prinzip; 10.2 Mobile Phasen in der Umkehrphasen-Chromatographie; 10.3 Selektivität und Stärke der mobilen Phase; 10.4 Stationäre Phasen; 10.5 Methodenentwicklung in der Umkehrphasen-Chromatographie; 10.6 Anwendungsbeispiele; 10.7 Hydrophobic-Interaction-Chromatographie; 11 Chromatographie mit chemisch gebundenen Phasen 11.1 Einführung |
| Record Nr. | UNINA-9910830485403321 |
Meyer Veronika
|
||
| Weinheim, : Wiley, 2004 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Praxis der Hochleistungs-Flüssigchromatographie / / Veronika R. Meyer
| Praxis der Hochleistungs-Flüssigchromatographie / / Veronika R. Meyer |
| Autore | Meyer Veronika |
| Edizione | [9. Aufl.] |
| Pubbl/distr/stampa | Weinheim, : Wiley, 2004 |
| Descrizione fisica | 1 online resource (368 p.) |
| Disciplina |
543.0894
543.84 544.924 |
| Soggetto topico | Liquid chromatography |
| ISBN |
1-282-02134-6
9786612021343 3-527-62358-2 3-527-62359-0 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | ger |
| Nota di contenuto |
Praxis der Hochleistungs- Flüssigchromatographie; Inhaltsverzeichnis; Vorwort; Vorwort zur neunten Auflage; 0 Wichtige und nützliche Gleichungen für die HPLC; 1 Einleitung; 1.1 HPLC: Eine leistungsfähige Trennmethode; 1.2 Ein erstes HPLC-Experiment; 1.3 Die flüssigchromatographischen Trennverfahren; 1.4 Die HPLC-Apparatur; 1.5 Sicherheit am HPLC-Arbeitsplatz; 1.6 Vergleich von Hochleistungs-Flüssigchromatographie und Gaschromatographie; 1.7 Druckeinheiten; 1.8 Längeneinheiten; 1.9 Wissenschaftliche Zeitschriften; 1.10 Empfehlenswerte Bücher; 2 Theoretische Grundlagen
2.1 Der chromatographische Prozess2.2 Bandenverbreiterung; 2.3 Das Chromatogramm und seine Aussage; 2.4 Graphische Darstellung von Peakpaaren mit verschiedener Auflösung; 2.5 Die Beeinflussung der Auflösung; 2.6 Totvolumina (extra-column-Volumina); 2.7 Tailing; 2.8 Peakkapazität und statistische Auflösungswahrscheinlichkeit; 2.9 Temperatureinflüsse in der HPLC; 2.10 Die Grenzen der HPLC; 3 Pumpen; 3.1 Allgemeines; 3.2 Die Kurzhub-Kolbenpumpe; 3.3 Unterhalt und Reparaturen; 3.4 Andere Pumpentypen; 4 Bereitstellung der Apparatur bis zur Probenaufgabe; 4.1 Auswahl der mobilen Phase 4.2 Vorbereitung der mobilen Phase4.3 Gradientensysteme; 4.4 Kapillarleitungen; 4.5 Fittings; 4.6 Probenaufgabesysteme; 4.7 Probelösung und Probevolumen; 5 Lösungsmitteleigenschaften; 5.1 Tabelle organischer Lösungsmittel; 5.2 Lösungsmittelselektivität; 5.3 Mischbarkeit; 5.4 Puffer; 5.5 Haltbarkeit von mobilen Phasen; 6 Detektoren; 6.1 Allgemeines; 6.2 UV-Detektoren; 6.3 Brechungsindex-Detektoren; 6.4 Fluoreszenz-Detektoren; 6.5 Elektrochemische Detektoren; 6.6 Lichtstreuungs-Detektoren; 6.7 Andere Detektoren; 6.8 Mehrfachdetektion; 6.9 Indirekte Detektion; 6.10 Kopplung mit Spektroskopie 7 Säulen und stationäre Phasen7.1 Säulen für die HPLC; 7.2 Vorsäulen; 7.3 Allgemeines über stationäre Phasen; 7.4 Silicagel; 7.5 Chemisch modifiziertes Silicagel; 7.6 Styrol-Divinylbenzol; 7.7 Einige weitere stationäre Phasen; 7.8 Vorsichtsmaßnahmen und Regeneration; 8 Das Testen von HPLC-Säulen; 8.1 Einfache Tests für HPLC-Säulen; 8.2 Bestimmung der Korngröße; 8.3 Bestimmung der Totzeit; 8.4 Das Testgemisch; 8.5 Dimensionslose Größen zur Charakterisierung von HPLC-Säulen; 8.6 Die van Deemter-Gleichung aus reduzierten Größen und ihre Nützlichkeit für die Säulendiagnose 8.7 Diffusionskoeffizienten9 Adsorptions-Chromatographie; 9.1 Was heißt Adsorption?; 9.2 Die eluotrope Reihe; 9.3 Selektivitätseigenschaften der mobilen Phase; 9.4 Wahl und Optimierung der mobilen Phase; 9.5 Anwendungsbeispiele; 10 Umkehrphasen-Chromatographie; 10.1 Prinzip; 10.2 Mobile Phasen in der Umkehrphasen-Chromatographie; 10.3 Selektivität und Stärke der mobilen Phase; 10.4 Stationäre Phasen; 10.5 Methodenentwicklung in der Umkehrphasen-Chromatographie; 10.6 Anwendungsbeispiele; 10.7 Hydrophobic-Interaction-Chromatographie; 11 Chromatographie mit chemisch gebundenen Phasen 11.1 Einführung |
| Record Nr. | UNINA-9910840773803321 |
|
Meyer Veronika
|
||
| Weinheim, : Wiley, 2004 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Preparative enantioselective chromatography [[electronic resource] /] / edited by Geoffrey B Cox
| Preparative enantioselective chromatography [[electronic resource] /] / edited by Geoffrey B Cox |
| Edizione | [1st ed.] |
| Pubbl/distr/stampa | Ames, Iowa, : Blackwell Pub., 2005 |
| Descrizione fisica | 1 online resource (346 p.) |
| Disciplina |
543.089
543.84 543/.84 |
| Altri autori (Persone) | CoxGeoffrey J. <1952-> |
| Soggetto topico |
Liquid chromatography
Enantiomers - Separation |
| Soggetto genere / forma | Electronic books. |
| ISBN |
1-280-19691-2
9786610196913 0-470-98842-8 1-4051-4471-8 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Preparative Enantioselective Chromatography; Contents; Contributors; Preface; 1. Chiral chromatography in support of pharmaceutical process research; 1.1 Introduction; 1.2 A brief introduction to chirality; 1.3 Why chirality is important; 1.4 Accessing enantiopurity: a brief overview of approaches; 1.4.1 Enantiopure starting materials: the chiral pool; 1.4.2 Removable enantioenriched auxiliaries; 1.4.3 Enantioselective catalysis; 1.4.4 Resolution technologies: introduction; 1.4.5 Chromatographic productivity is the key metric for preparative chromatography
1.4.6 Stationary phases for preparative chiral chromatography1.4.7 Advantages of preparative chiral chromatography over other approaches for accessing enantiopure materials; 1.4.8 Simulated moving bed enantioseparation; 1.5 Green enantioseparation; 1.6 What is the appropriate role of preparative chromatography in organic synthesis?; 1.7 Fording the river at the easiest point: some observations on the appropriate placement of a chromatographic resolution within a chiral synthesis; 1.8 Origins of preparative chiral chromatography 1.9 Practical tips for preparative chromatographic enantioseparation1.10 Conclusion; 2. Introduction to preparative chromatography; 2.1 Introduction; 2.2 Adsorption isotherms; 2.2.1 The simple case - the Langmuir isotherm; 2.2.2 Other isotherms; 2.2.3 Competitive isotherms; 2.3 Kinetics; 2.4 Metrics for preparative operations; 2.4.1 Throughput; 2.4.2 Production rate; 2.4.3 Productivity; 2.4.4 Specific productivity; 2.4.5 Cost; 2.5 The influence of chromatographic parameters on preparative chromatography; 2.5.1 Effect of particle size on preparative performance; 2.5.2 Effects of pressure 2.5.3 Effects of column efficiency2.5.4 Effect of column length; 2.5.5 The effects of selectivity; 2.6 Economics of preparative separations; 2.6.1 Point of insertion of the chromatographic resolution in the synthetic route; 3 Chiral stationary phases for preparative enantioselective chromatography; 3.1 Summary; 3.2 Introduction; 3.3 Historical development of CSPs for preparative chromatography; 3.4 Preparative CSPs; 3.4.1 Classification of CSPs; 3.4.2 Polymeric phases; 3.4.3 Brush-type CSPs; 3.4.4 Chiral phases for ligand-exchange chromatography; 3.4.5 Imprinted phases 3.5 Chemical and physical properties of CSPs3.5.1 Loading capacity; 3.5.2 Chemical and physical stability; 3.5.3 Solubility of the chiral solute; 3.6 New and future developments in the field of preparative CSPs; 3.6.1 CSPs with improved loading capacity; 3.6.2 CSPs with improved selectivity; 3.6.3 Immobilised polysaccharide-based CSPs; 3.7 Conclusion; 4 Method development for preparative enantioselective chromatography; 4.1 Introduction; 4.2 Chiral stationary phases for enantioselective chromatography; 4.3 Screening and optimisation strategy for preparative chiral chromatography 4.3.1 Choice of the stationary phase |
| Record Nr. | UNINA-9910143298903321 |
| Ames, Iowa, : Blackwell Pub., 2005 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Preparative enantioselective chromatography [[electronic resource] /] / edited by Geoffrey B Cox
| Preparative enantioselective chromatography [[electronic resource] /] / edited by Geoffrey B Cox |
| Edizione | [1st ed.] |
| Pubbl/distr/stampa | Ames, Iowa, : Blackwell Pub., 2005 |
| Descrizione fisica | 1 online resource (346 p.) |
| Disciplina |
543.089
543.84 543/.84 |
| Altri autori (Persone) | CoxGeoffrey J. <1952-> |
| Soggetto topico |
Liquid chromatography
Enantiomers - Separation |
| ISBN |
1-280-19691-2
9786610196913 0-470-98842-8 1-4051-4471-8 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Preparative Enantioselective Chromatography; Contents; Contributors; Preface; 1. Chiral chromatography in support of pharmaceutical process research; 1.1 Introduction; 1.2 A brief introduction to chirality; 1.3 Why chirality is important; 1.4 Accessing enantiopurity: a brief overview of approaches; 1.4.1 Enantiopure starting materials: the chiral pool; 1.4.2 Removable enantioenriched auxiliaries; 1.4.3 Enantioselective catalysis; 1.4.4 Resolution technologies: introduction; 1.4.5 Chromatographic productivity is the key metric for preparative chromatography
1.4.6 Stationary phases for preparative chiral chromatography1.4.7 Advantages of preparative chiral chromatography over other approaches for accessing enantiopure materials; 1.4.8 Simulated moving bed enantioseparation; 1.5 Green enantioseparation; 1.6 What is the appropriate role of preparative chromatography in organic synthesis?; 1.7 Fording the river at the easiest point: some observations on the appropriate placement of a chromatographic resolution within a chiral synthesis; 1.8 Origins of preparative chiral chromatography 1.9 Practical tips for preparative chromatographic enantioseparation1.10 Conclusion; 2. Introduction to preparative chromatography; 2.1 Introduction; 2.2 Adsorption isotherms; 2.2.1 The simple case - the Langmuir isotherm; 2.2.2 Other isotherms; 2.2.3 Competitive isotherms; 2.3 Kinetics; 2.4 Metrics for preparative operations; 2.4.1 Throughput; 2.4.2 Production rate; 2.4.3 Productivity; 2.4.4 Specific productivity; 2.4.5 Cost; 2.5 The influence of chromatographic parameters on preparative chromatography; 2.5.1 Effect of particle size on preparative performance; 2.5.2 Effects of pressure 2.5.3 Effects of column efficiency2.5.4 Effect of column length; 2.5.5 The effects of selectivity; 2.6 Economics of preparative separations; 2.6.1 Point of insertion of the chromatographic resolution in the synthetic route; 3 Chiral stationary phases for preparative enantioselective chromatography; 3.1 Summary; 3.2 Introduction; 3.3 Historical development of CSPs for preparative chromatography; 3.4 Preparative CSPs; 3.4.1 Classification of CSPs; 3.4.2 Polymeric phases; 3.4.3 Brush-type CSPs; 3.4.4 Chiral phases for ligand-exchange chromatography; 3.4.5 Imprinted phases 3.5 Chemical and physical properties of CSPs3.5.1 Loading capacity; 3.5.2 Chemical and physical stability; 3.5.3 Solubility of the chiral solute; 3.6 New and future developments in the field of preparative CSPs; 3.6.1 CSPs with improved loading capacity; 3.6.2 CSPs with improved selectivity; 3.6.3 Immobilised polysaccharide-based CSPs; 3.7 Conclusion; 4 Method development for preparative enantioselective chromatography; 4.1 Introduction; 4.2 Chiral stationary phases for enantioselective chromatography; 4.3 Screening and optimisation strategy for preparative chiral chromatography 4.3.1 Choice of the stationary phase |
| Record Nr. | UNISA-996214620903316 |
| Ames, Iowa, : Blackwell Pub., 2005 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. di Salerno | ||
| ||
Preparative enantioselective chromatography [[electronic resource] /] / edited by Geoffrey B Cox
| Preparative enantioselective chromatography [[electronic resource] /] / edited by Geoffrey B Cox |
| Edizione | [1st ed.] |
| Pubbl/distr/stampa | Ames, Iowa, : Blackwell Pub., 2005 |
| Descrizione fisica | 1 online resource (346 p.) |
| Disciplina |
543.089
543.84 543/.84 |
| Altri autori (Persone) | CoxGeoffrey J. <1952-> |
| Soggetto topico |
Liquid chromatography
Enantiomers - Separation |
| ISBN |
1-280-19691-2
9786610196913 0-470-98842-8 1-4051-4471-8 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Preparative Enantioselective Chromatography; Contents; Contributors; Preface; 1. Chiral chromatography in support of pharmaceutical process research; 1.1 Introduction; 1.2 A brief introduction to chirality; 1.3 Why chirality is important; 1.4 Accessing enantiopurity: a brief overview of approaches; 1.4.1 Enantiopure starting materials: the chiral pool; 1.4.2 Removable enantioenriched auxiliaries; 1.4.3 Enantioselective catalysis; 1.4.4 Resolution technologies: introduction; 1.4.5 Chromatographic productivity is the key metric for preparative chromatography
1.4.6 Stationary phases for preparative chiral chromatography1.4.7 Advantages of preparative chiral chromatography over other approaches for accessing enantiopure materials; 1.4.8 Simulated moving bed enantioseparation; 1.5 Green enantioseparation; 1.6 What is the appropriate role of preparative chromatography in organic synthesis?; 1.7 Fording the river at the easiest point: some observations on the appropriate placement of a chromatographic resolution within a chiral synthesis; 1.8 Origins of preparative chiral chromatography 1.9 Practical tips for preparative chromatographic enantioseparation1.10 Conclusion; 2. Introduction to preparative chromatography; 2.1 Introduction; 2.2 Adsorption isotherms; 2.2.1 The simple case - the Langmuir isotherm; 2.2.2 Other isotherms; 2.2.3 Competitive isotherms; 2.3 Kinetics; 2.4 Metrics for preparative operations; 2.4.1 Throughput; 2.4.2 Production rate; 2.4.3 Productivity; 2.4.4 Specific productivity; 2.4.5 Cost; 2.5 The influence of chromatographic parameters on preparative chromatography; 2.5.1 Effect of particle size on preparative performance; 2.5.2 Effects of pressure 2.5.3 Effects of column efficiency2.5.4 Effect of column length; 2.5.5 The effects of selectivity; 2.6 Economics of preparative separations; 2.6.1 Point of insertion of the chromatographic resolution in the synthetic route; 3 Chiral stationary phases for preparative enantioselective chromatography; 3.1 Summary; 3.2 Introduction; 3.3 Historical development of CSPs for preparative chromatography; 3.4 Preparative CSPs; 3.4.1 Classification of CSPs; 3.4.2 Polymeric phases; 3.4.3 Brush-type CSPs; 3.4.4 Chiral phases for ligand-exchange chromatography; 3.4.5 Imprinted phases 3.5 Chemical and physical properties of CSPs3.5.1 Loading capacity; 3.5.2 Chemical and physical stability; 3.5.3 Solubility of the chiral solute; 3.6 New and future developments in the field of preparative CSPs; 3.6.1 CSPs with improved loading capacity; 3.6.2 CSPs with improved selectivity; 3.6.3 Immobilised polysaccharide-based CSPs; 3.7 Conclusion; 4 Method development for preparative enantioselective chromatography; 4.1 Introduction; 4.2 Chiral stationary phases for enantioselective chromatography; 4.3 Screening and optimisation strategy for preparative chiral chromatography 4.3.1 Choice of the stationary phase |
| Record Nr. | UNINA-9910831095603321 |
| Ames, Iowa, : Blackwell Pub., 2005 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Preparative enantioselective chromatography [[electronic resource] /] / edited by Geoffrey B Cox
| Preparative enantioselective chromatography [[electronic resource] /] / edited by Geoffrey B Cox |
| Edizione | [1st ed.] |
| Pubbl/distr/stampa | Ames, Iowa, : Blackwell Pub., 2005 |
| Descrizione fisica | 1 online resource (346 p.) |
| Disciplina |
543.089
543.84 543/.84 |
| Altri autori (Persone) | CoxGeoffrey J. <1952-> |
| Soggetto topico |
Liquid chromatography
Enantiomers - Separation |
| ISBN |
1-280-19691-2
9786610196913 0-470-98842-8 1-4051-4471-8 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Preparative Enantioselective Chromatography; Contents; Contributors; Preface; 1. Chiral chromatography in support of pharmaceutical process research; 1.1 Introduction; 1.2 A brief introduction to chirality; 1.3 Why chirality is important; 1.4 Accessing enantiopurity: a brief overview of approaches; 1.4.1 Enantiopure starting materials: the chiral pool; 1.4.2 Removable enantioenriched auxiliaries; 1.4.3 Enantioselective catalysis; 1.4.4 Resolution technologies: introduction; 1.4.5 Chromatographic productivity is the key metric for preparative chromatography
1.4.6 Stationary phases for preparative chiral chromatography1.4.7 Advantages of preparative chiral chromatography over other approaches for accessing enantiopure materials; 1.4.8 Simulated moving bed enantioseparation; 1.5 Green enantioseparation; 1.6 What is the appropriate role of preparative chromatography in organic synthesis?; 1.7 Fording the river at the easiest point: some observations on the appropriate placement of a chromatographic resolution within a chiral synthesis; 1.8 Origins of preparative chiral chromatography 1.9 Practical tips for preparative chromatographic enantioseparation1.10 Conclusion; 2. Introduction to preparative chromatography; 2.1 Introduction; 2.2 Adsorption isotherms; 2.2.1 The simple case - the Langmuir isotherm; 2.2.2 Other isotherms; 2.2.3 Competitive isotherms; 2.3 Kinetics; 2.4 Metrics for preparative operations; 2.4.1 Throughput; 2.4.2 Production rate; 2.4.3 Productivity; 2.4.4 Specific productivity; 2.4.5 Cost; 2.5 The influence of chromatographic parameters on preparative chromatography; 2.5.1 Effect of particle size on preparative performance; 2.5.2 Effects of pressure 2.5.3 Effects of column efficiency2.5.4 Effect of column length; 2.5.5 The effects of selectivity; 2.6 Economics of preparative separations; 2.6.1 Point of insertion of the chromatographic resolution in the synthetic route; 3 Chiral stationary phases for preparative enantioselective chromatography; 3.1 Summary; 3.2 Introduction; 3.3 Historical development of CSPs for preparative chromatography; 3.4 Preparative CSPs; 3.4.1 Classification of CSPs; 3.4.2 Polymeric phases; 3.4.3 Brush-type CSPs; 3.4.4 Chiral phases for ligand-exchange chromatography; 3.4.5 Imprinted phases 3.5 Chemical and physical properties of CSPs3.5.1 Loading capacity; 3.5.2 Chemical and physical stability; 3.5.3 Solubility of the chiral solute; 3.6 New and future developments in the field of preparative CSPs; 3.6.1 CSPs with improved loading capacity; 3.6.2 CSPs with improved selectivity; 3.6.3 Immobilised polysaccharide-based CSPs; 3.7 Conclusion; 4 Method development for preparative enantioselective chromatography; 4.1 Introduction; 4.2 Chiral stationary phases for enantioselective chromatography; 4.3 Screening and optimisation strategy for preparative chiral chromatography 4.3.1 Choice of the stationary phase |
| Record Nr. | UNINA-9910841338203321 |
| Ames, Iowa, : Blackwell Pub., 2005 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Protein and peptide analysis by LC-MS [[electronic resource] ] : experimental strategies / / edited by Thomas Letzel
| Protein and peptide analysis by LC-MS [[electronic resource] ] : experimental strategies / / edited by Thomas Letzel |
| Pubbl/distr/stampa | Cambridge, : RSC Pub., 2011 |
| Descrizione fisica | 1 online resource (195 p.) |
| Disciplina | 547.7 |
| Altri autori (Persone) | LetzelThomas <1970-> |
| Collana | RSC chromatography monographs |
| Soggetto topico |
Proteins - Analysis
Peptides - Analysis Liquid chromatography |
| Soggetto genere / forma | Electronic books. |
| ISBN | 1-84973-314-7 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto | i-iv.PDF.pdf; v-vi; vii-x; xi-xviii; xix-xx; 1-10; 11-25; 26-37; 38-55; 56-70; 71-86; 87-103; 104-122; 123-132; 133-141; 142-155; 156-167; 168-174 |
| Record Nr. | UNINA-9910457384103321 |
| Cambridge, : RSC Pub., 2011 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Protein and peptide analysis by LC-MS [[electronic resource] ] : experimental strategies / / edited by Thomas Letzel
| Protein and peptide analysis by LC-MS [[electronic resource] ] : experimental strategies / / edited by Thomas Letzel |
| Pubbl/distr/stampa | Cambridge, : RSC Pub., 2011 |
| Descrizione fisica | 1 online resource (195 p.) |
| Disciplina | 547.7 |
| Altri autori (Persone) | LetzelThomas <1970-> |
| Collana | RSC chromatography monographs |
| Soggetto topico |
Proteins - Analysis
Peptides - Analysis Liquid chromatography |
| ISBN | 1-84973-314-7 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto | i-iv.PDF.pdf; v-vi; vii-x; xi-xviii; xix-xx; 1-10; 11-25; 26-37; 38-55; 56-70; 71-86; 87-103; 104-122; 123-132; 133-141; 142-155; 156-167; 168-174 |
| Record Nr. | UNINA-9910781951703321 |
| Cambridge, : RSC Pub., 2011 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Protein and peptide analysis by LC-MS [[electronic resource] ] : experimental strategies / / edited by Thomas Letzel
| Protein and peptide analysis by LC-MS [[electronic resource] ] : experimental strategies / / edited by Thomas Letzel |
| Pubbl/distr/stampa | Cambridge, : RSC Pub., 2011 |
| Descrizione fisica | 1 online resource (195 p.) |
| Disciplina | 547.7 |
| Altri autori (Persone) | LetzelThomas <1970-> |
| Collana | RSC chromatography monographs |
| Soggetto topico |
Proteins - Analysis
Peptides - Analysis Liquid chromatography |
| ISBN | 1-84973-314-7 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto | i-iv.PDF.pdf; v-vi; vii-x; xi-xviii; xix-xx; 1-10; 11-25; 26-37; 38-55; 56-70; 71-86; 87-103; 104-122; 123-132; 133-141; 142-155; 156-167; 168-174 |
| Record Nr. | UNINA-9910822255303321 |
| Cambridge, : RSC Pub., 2011 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Proteomic biology using LC-MS [[electronic resource] ] : large scale analysis of cellular dynamics and function / / Nobuhiro Takahashi, Toshiaki Isobe
| Proteomic biology using LC-MS [[electronic resource] ] : large scale analysis of cellular dynamics and function / / Nobuhiro Takahashi, Toshiaki Isobe |
| Autore | Takahashi Nobuhiro |
| Pubbl/distr/stampa | Hoboken, N.J., : Wiley-Interscience, c2008 |
| Descrizione fisica | 1 online resource (275 p.) |
| Disciplina | 572/.6 |
| Altri autori (Persone) | IsobeToshiaki |
| Collana | Wiley-Interscience series in mass spectrometry |
| Soggetto topico |
Proteomics
Liquid chromatography Mass spectrometry |
| Soggetto genere / forma | Electronic books. |
| ISBN |
1-281-13467-8
9786611134679 0-470-14965-5 0-470-14964-7 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto | Overview of proteomics -- Proteomic tools for analysis of cellular dynamics -- Dynamics of functional cellular machinery : from statics to dynamics in proteomic biology. |
| Record Nr. | UNINA-9910144143903321 |
|
Takahashi Nobuhiro
|
||
| Hoboken, N.J., : Wiley-Interscience, c2008 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
