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Biblioteca

MARC Lista (tabellare)
Nature methods
Nature methods
Pubbl/distr/stampa New York, : Nature Pub. Group, 2004-
Disciplina 610
Soggetto topico Biology - Research
Biology - Methodology
Biologie - Recherche
Biologie - Méthodologie
Life Sciences
Soggetto genere / forma Periodicals.
Soggetto non controllato Biology - General
ISSN 1548-7105
Formato Materiale a stampa
Livello bibliografico Periodico
Lingua di pubblicazione eng
Record Nr. UNISA-996199819403316
New York, : Nature Pub. Group, 2004-
Materiale a stampa
Lo trovi qui: Univ. di Salerno
Opac: Controlla la disponibilità qui
Nature methods
Nature methods
Pubbl/distr/stampa New York, : Nature Pub. Group, 2004-
Disciplina 610
Soggetto topico Biology - Research
Biology - Methodology
Biologie - Recherche
Biologie - Méthodologie
Life Sciences
Soggetto genere / forma Periodicals.
Soggetto non controllato Biology - General
ISSN 1548-7105
Formato Materiale a stampa
Livello bibliografico Periodico
Lingua di pubblicazione eng
Record Nr. UNINA-9910143538903321
New York, : Nature Pub. Group, 2004-
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Nature protocols
Nature protocols
Pubbl/distr/stampa London, UK : , : Nature Pub. Group, , 2006-
Descrizione fisica 1 online resource
Disciplina 570.28
Soggetto topico Biology - Methodology
Chemistry - Methodology
Biology
Chemistry
Medical protocols
Clinical Laboratory Techniques
Biology - methods
Biomedical Research - methods
Naturwissenschaften
Soggetto genere / forma Periodical
Periodicals
Handbooks and manuals.
Zeitschrift
Online-Publikation
ISSN 1750-2799
Formato Materiale a stampa
Livello bibliografico Periodico
Lingua di pubblicazione eng
Altri titoli varianti Protocols
Record Nr. UNINA-9910144470103321
London, UK : , : Nature Pub. Group, , 2006-
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Scanning electron microscopy for the life sciences / / Heide Schatten [[electronic resource]]
Scanning electron microscopy for the life sciences / / Heide Schatten [[electronic resource]]
Autore Schatten Heide
Pubbl/distr/stampa Cambridge : , : Cambridge University Press, , 2013
Descrizione fisica 1 online resource (xi, 261 pages) : digital, PDF file(s)
Disciplina 570.28/25
Collana Advances in microscopy and microanalysis
Soggetto topico Biology - Methodology
Scanning electron microscopy
ISBN 1-107-23287-2
1-139-85343-0
1-139-01817-5
1-139-84549-7
1-139-83960-8
1-139-84198-X
1-139-84434-2
1-283-81251-7
1-139-84079-7
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto 1. The role of scanning electron microscopy in cell and molecular biology: SEM basics, past accomplishments and new frontiers / Heide Schatten -- 2. Corrosion casting technique / Jerzy Walocha, Jan A. Litwin and Adam J. Miodoński -- 3. Revealing the internal structure of cells in three dimensions with scanning electron microscopy / Sol Sepsenwol -- 4. Mitochondria form continuous intracellular network-structures visualized with high-resolution field-emission scanning electron microscopy / T. Naguro, H. Nakane and S. Inaga -- 5. Is the scanning mode the future of electron microscopy in cell biology? / Paul Walther, Christopher Schmid, Michaela Sailer, and Katherine Höhn -- 6. High resolution labeling for correlative microscopy / Ralph Albrecht, Daryl A. Meyer and O.E. Olorundare -- 7. The use of SEM to explore virus structure and trafficking / Jens M. Holl and Elizabeth R. Wright -- 8. High resolution scanning electron microscopy of the nuclear surface in Herpes Simplex Virus 1 infected cells / Peter Wild, Andres Kaech and Miriam S. Lucas -- 9. Scanning electron microscopy of chromosomes: structural and analytical investigations / Elizabeth Schroeder-Reiter and Gerhard Wanner -- 10. A method to visualize the microarchitecture of glycoprotein matrices with scanning electron microscopy / Giuseppe Familiari, Rosemarie Heyn, Luciano Petruzziello and Michela Relucenti -- 11. Scanning electron microscopy of cerebellar intrinsic circuits / Orlando J. Castejón -- 12. Application of in vivo cryotechnique to living animal organs examined by scanning electron microscopy / Shinichi Ohno, Nobuo Terada, Nobuhiko Ohno and Yasuhisa Fujii -- 13. SEM in dental research / Vladimir Dusevich, Jennifer R. Melander and J. David Eick -- 14. SEM, teeth and palaeoanthropology: the secret of ancient human diets / Alejandro Romero and Joaquín De Juan.
Record Nr. UNINA-9910453005703321
Schatten Heide  
Cambridge : , : Cambridge University Press, , 2013
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Scanning electron microscopy for the life sciences / / Heide Schatten [[electronic resource]]
Scanning electron microscopy for the life sciences / / Heide Schatten [[electronic resource]]
Autore Schatten Heide
Pubbl/distr/stampa Cambridge : , : Cambridge University Press, , 2013
Descrizione fisica 1 online resource (xi, 261 pages) : digital, PDF file(s)
Disciplina 570.28/25
Collana Advances in microscopy and microanalysis
Soggetto topico Biology - Methodology
Scanning electron microscopy
ISBN 1-107-23287-2
1-139-85343-0
1-139-01817-5
1-139-84549-7
1-139-83960-8
1-139-84198-X
1-139-84434-2
1-283-81251-7
1-139-84079-7
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto 1. The role of scanning electron microscopy in cell and molecular biology: SEM basics, past accomplishments and new frontiers / Heide Schatten -- 2. Corrosion casting technique / Jerzy Walocha, Jan A. Litwin and Adam J. Miodoński -- 3. Revealing the internal structure of cells in three dimensions with scanning electron microscopy / Sol Sepsenwol -- 4. Mitochondria form continuous intracellular network-structures visualized with high-resolution field-emission scanning electron microscopy / T. Naguro, H. Nakane and S. Inaga -- 5. Is the scanning mode the future of electron microscopy in cell biology? / Paul Walther, Christopher Schmid, Michaela Sailer, and Katherine Höhn -- 6. High resolution labeling for correlative microscopy / Ralph Albrecht, Daryl A. Meyer and O.E. Olorundare -- 7. The use of SEM to explore virus structure and trafficking / Jens M. Holl and Elizabeth R. Wright -- 8. High resolution scanning electron microscopy of the nuclear surface in Herpes Simplex Virus 1 infected cells / Peter Wild, Andres Kaech and Miriam S. Lucas -- 9. Scanning electron microscopy of chromosomes: structural and analytical investigations / Elizabeth Schroeder-Reiter and Gerhard Wanner -- 10. A method to visualize the microarchitecture of glycoprotein matrices with scanning electron microscopy / Giuseppe Familiari, Rosemarie Heyn, Luciano Petruzziello and Michela Relucenti -- 11. Scanning electron microscopy of cerebellar intrinsic circuits / Orlando J. Castejón -- 12. Application of in vivo cryotechnique to living animal organs examined by scanning electron microscopy / Shinichi Ohno, Nobuo Terada, Nobuhiko Ohno and Yasuhisa Fujii -- 13. SEM in dental research / Vladimir Dusevich, Jennifer R. Melander and J. David Eick -- 14. SEM, teeth and palaeoanthropology: the secret of ancient human diets / Alejandro Romero and Joaquín De Juan.
Record Nr. UNINA-9910779340903321
Schatten Heide  
Cambridge : , : Cambridge University Press, , 2013
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
Scanning electron microscopy for the life sciences / / Heide Schatten [[electronic resource]]
Scanning electron microscopy for the life sciences / / Heide Schatten [[electronic resource]]
Autore Schatten Heide
Pubbl/distr/stampa Cambridge : , : Cambridge University Press, , 2013
Descrizione fisica 1 online resource (xi, 261 pages) : digital, PDF file(s)
Disciplina 570.28/25
Collana Advances in microscopy and microanalysis
Soggetto topico Biology - Methodology
Scanning electron microscopy
ISBN 1-107-23287-2
1-139-85343-0
1-139-01817-5
1-139-84549-7
1-139-83960-8
1-139-84198-X
1-139-84434-2
1-283-81251-7
1-139-84079-7
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto 1. The role of scanning electron microscopy in cell and molecular biology: SEM basics, past accomplishments and new frontiers / Heide Schatten -- 2. Corrosion casting technique / Jerzy Walocha, Jan A. Litwin and Adam J. Miodoński -- 3. Revealing the internal structure of cells in three dimensions with scanning electron microscopy / Sol Sepsenwol -- 4. Mitochondria form continuous intracellular network-structures visualized with high-resolution field-emission scanning electron microscopy / T. Naguro, H. Nakane and S. Inaga -- 5. Is the scanning mode the future of electron microscopy in cell biology? / Paul Walther, Christopher Schmid, Michaela Sailer, and Katherine Höhn -- 6. High resolution labeling for correlative microscopy / Ralph Albrecht, Daryl A. Meyer and O.E. Olorundare -- 7. The use of SEM to explore virus structure and trafficking / Jens M. Holl and Elizabeth R. Wright -- 8. High resolution scanning electron microscopy of the nuclear surface in Herpes Simplex Virus 1 infected cells / Peter Wild, Andres Kaech and Miriam S. Lucas -- 9. Scanning electron microscopy of chromosomes: structural and analytical investigations / Elizabeth Schroeder-Reiter and Gerhard Wanner -- 10. A method to visualize the microarchitecture of glycoprotein matrices with scanning electron microscopy / Giuseppe Familiari, Rosemarie Heyn, Luciano Petruzziello and Michela Relucenti -- 11. Scanning electron microscopy of cerebellar intrinsic circuits / Orlando J. Castejón -- 12. Application of in vivo cryotechnique to living animal organs examined by scanning electron microscopy / Shinichi Ohno, Nobuo Terada, Nobuhiko Ohno and Yasuhisa Fujii -- 13. SEM in dental research / Vladimir Dusevich, Jennifer R. Melander and J. David Eick -- 14. SEM, teeth and palaeoanthropology: the secret of ancient human diets / Alejandro Romero and Joaquín De Juan.
Record Nr. UNINA-9910828651903321
Schatten Heide  
Cambridge : , : Cambridge University Press, , 2013
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
X-ray fluorescence in biological sciences : principles, instrumentation and applications / / edited by Vivek K. Singh, Jun Kawai and Durgesh K. Tripathi
X-ray fluorescence in biological sciences : principles, instrumentation and applications / / edited by Vivek K. Singh, Jun Kawai and Durgesh K. Tripathi
Pubbl/distr/stampa Hoboken, NJ : , : John Wiley & Sons, Inc., , [2022]
Descrizione fisica 1 online resource (685 pages)
Disciplina 543.08586
Soggetto topico Biology - Methodology
Chemical biology
X-ray spectroscopy
ISBN 1-119-64571-9
1-119-64558-1
9781119645580
9781119645665
9781119645542
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Cover -- Title Page -- Copyright Page -- Contents -- List of Contributors -- Preface -- Part I General Introduction -- Chapter 1 X-Ray Fluorescence and Comparison with Other Analytical Methods (AAS, ICP-AES, LA-ICP-MS, IC, LIBS, SEM-EDS, and XRD) -- 1.1 Introduction -- 1.2 Analytical Capabilities of XRF and Micro-XRF -- 1.2.1 Micro-XRF -- 1.3 Comparison with Other Analytical Methods -- 1.3.1 Overview -- 1.3.2 Inductively Coupled Plasma (ICP) Analysis -- 1.3.3 Inductively Coupled Plasma Atomic Emission Spectroscopy (ICP-AES) -- 1.3.4 Ion Chromatography (IC) -- 1.3.5 Laser-Induced Breakdown Spectroscopy (LIBS) -- 1.3.6 Proton-Induced X-Ray Emission (PIXE) -- 1.3.7 Scanning Electron Microscopy-Energy Dispersive X-Ray Spectroscopy (SEM-EDS) -- 1.4 Comparison of XRF and XRD -- 1.5 Comparison of XRF and Raman Spectroscopy -- 1.6 Conclusion and Prospects -- References -- Chapter 2 X-Ray Fluorescence for Multi-elemental Analysis of Vegetation Samples -- 2.1 Introduction -- 2.2 Features and Analytical Capabilities of XRF Configurations used in Vegetation Sample Analysis -- 2.3 General Sample Treatment Procedures used for Vegetation Sample Analysis using XRF Techniques -- 2.4 Applications of XRF in the Field of Vegetation Samples Analysis -- 2.4.1 Environmental Studies -- 2.4.2 Nutritional and Agronomic Studies -- 2.5 Concluding Remarks and Future Perspectives -- References -- Chapter 3 X-Ray Fluorescence Studies of Tea and Coffee -- 3.1 Introduction -- 3.2 The Equipment Used -- 3.3 Preparation of Samples for Analysis -- 3.4 Examples of Practical Applications of XRF for Tea Research -- 3.5 Examples of Practical Applications of XRF for Coffee Research -- 3.6 Determination of the Elemental Composition of Krasnodar Tea Samples by TXRF and WDXRF -- 3.6.1 Instrumentation -- 3.6.2 Suspension Preparation -- 3.6.3 Infusion Preparation -- 3.6.4 Acid Digestion.
3.6.5 Preparation of Samples for WDXRF -- 3.6.6 Results and Discussion -- 3.7 Interelement Effects and Procedures of their Accounting -- 3.8 Conclusion -- References -- Chapter 4 Total Reflection X-Ray Fluorescence and it's Suitability for Biological Samples -- 4.1 Introduction -- 4.2 Advantages and Limitations of conventional XRF for Elemental Determinations in Biological Systems -- 4.3 Factors Limiting the Application of XRF for Biological Sample Analysis -- 4.4 Modifying XRF to Make it Suitable for Elemental Determinations at Trace Levels: Total Reflection X-Ray Fluorescence (TXRF) Spectrometry -- 4.4.1 Principles of TXRF -- 4.4.2 Theoretical Considerations -- 4.4.3 TXRF Instrumentation for Trace Element Determination -- 4.4.4 Sample Preparation for TXRF Analysis -- 4.5 Suitability of TXRF for Elemental Analysis in Biological Samples -- References -- Chapter 5 Micro X-Ray Fluorescence and X-Ray Absorption near Edge Structure Analysis of Heavy Metals in Micro-organism -- 5.1 Introduction -- 5.2 Effects of Heavy Metals on Microbial Growth -- 5.3 Application of -XRF and XAS in Understanding the Cycling of Elements Driven by Micro-organism -- 5.4 Application of -XRF and XAS in Understanding the Transformation of Elements Driven by Micro-organisms -- 5.5 Application of -XRF and XAS in Understanding the Mechanism of Using Micro-organisms in Bioremediation -- 5.6 The Advantage of Using -XRF and XAS to Explore the Interaction Mechanism Between Micro-organisms and Heavy Metals -- References -- Chapter 6 Use of Energy Dispersive X-Ray Fluorescence for Clinical Diagnosis -- 6.1 Introduction -- 6.2 Determination of Arsenic Concentration in Human Scalp Hair for the Diagnosis of Arsenicosis Disease -- 6.2.1 Background -- 6.2.2 Role of EDXRF -- 6.2.3 Collection and Preparation of Hair Sample -- 6.2.4 Sample Preparation -- 6.2.5 Sample Analysis.
6.2.6 Accuracy and Precision of the Method -- 6.3 Determination of Lead Concentrations in Human Whole Blood Using EDXRF Technique with Special Emphasis on Evaluating Association of Blood Lead Levels with Autism Spectrum Disorders (ASD) -- 6.3.1 Background -- 6.3.2 Role of EDXRF in Diagnosis of Blood Lead Level -- 6.3.3 Collection of Blood Sample and Preparation -- 6.3.4 Preparation of Pellets from Powdered Sample -- 6.3.5 Sample Irradiation -- 6.3.6 Precision and Accuracy of the Result -- 6.4 Conclusion -- References -- Chapter 7 Preparation of Sample for X-Ray Fluorescence Analysis -- 7.1 Introduction -- 7.2 Solid Samples -- 7.2.1 Metallic Samples -- 7.3 Powder Samples -- 7.3.1 Grinding -- 7.3.2 Pelletizing -- 7.3.3 Fused Samples -- 7.4 Liquid Samples -- 7.5 Sample Preparation for Infinitely Thick and Intermediate Specimen -- 7.6 Sample Preparation of Animal Cells -- 7.7 Sample Preparation of Plant Section -- 7.8 Precautions During Sample Preparation and Handling -- 7.9 Conclusion and Future Directions -- References -- Part II Synchrotron Radiation XRF -- Chapter 8 Elemental Analysis Using Synchrotron Radiation X-Ray Fluorescence -- 8.1 Importance of Trace and Ultra-Trace Elemental Analysis -- 8.2 Various Methods for Trace Element Analysis -- 8.2.1 Atomic Absorption Spectroscopy (AAS) Method -- 8.2.2 Inductively Coupled Plasma Mass Spectrometry (ICP-MS) Method -- 8.2.3 Neutron Activation Analysis (NAA) Method -- 8.2.4 Accelerator Ion Beam Techniques -- 8.2.5 X-Ray Fluorescence (XRF) Method -- 8.2.6 Total Reflection X-Ray Fluorescence (TXRF) Method -- 8.3 Comparison of TXRF and EDXRF Geometries -- 8.4 Synchrotron Radiation -- 8.4.1 Selection of a Laboratory X-Ray Source for TXRF -- 8.5 Indus Synchrotron Radiation Facility -- 8.6 Microprobe X-Ray Fluorescence Beamline (BL-16) -- 8.6.1 Working Principles of a Double Crystal Monochromator (DCM) Optic.
8.7 Experimental Facilities Available on the BL-16 -- 8.7.1 Normal EDXRF Measurements -- 8.7.2 Total Reflection X-Ray Fluorescence (TXRF) Measurements -- 8.7.3 Elemental Quantification -- 8.7.4 X-Ray Fluorescence Analysis of Nanostructures -- 8.7.5 Microfocus X-Ray Beam Mode -- 8.7.6 Micro-Fluorescence Mapping -- 8.7.7 Micro-XRF Mapping Analysis of Old Archeological Tile Samples -- 8.8 Discussion and Summary -- References -- Chapter 9 Synchrotron Radiation Based Micro X-Ray Fluorescence Spectroscopy of Plant Materials -- 9.1 Introduction -- 9.2 Instrumentation and Sample Preparation -- 9.3 Case Studies -- 9.3.1 Metal Tolerance Mechanisms in Hyperaccumulating Plants -- 9.3.2 Metal Toxicity and Tolerance in Plants and Fungi -- 9.3.3 Distribution of Mineral Nutrients and Potentially Toxic Elements in Grain -- 9.3.4 Investigation of Interactions between Plants and Engineered Nanomaterials -- Acknowledgements -- References -- Chapter 10 Micro X-Ray Fluorescence Analysis of Toxic Elements in Plants -- 10.1 Introduction -- 10.2 Advantages of XRF Technique for Plants Analysis -- 10.3 Preparation of Plant Samples for -XRF Analysis -- 10.4 The Case Studies of Synchrotron -XRF for Determination of Toxic Elements in Plants -- 10.4.1 Applications in Edible Plants -- 10.4.2 Applications in Accumulating Plants -- 10.4.3 Applications in Hyperaccumulator Plants -- 10.4.4 The Case Studies of Laboratory -XRF to Determine Elements in Waterlogged Oenanthe javanica DC -- 10.5 Conclusion and Outlook -- References -- Chapter 11 Micro X-Ray Fluorescence Studies of Earthworm (Benthonic Fauna) in Soils and Sediments -- 11.1 Introduction -- 11.2 Sample Preparation Methods -- 11.3 Earthworms and Soil Ecosystem -- 11.3.1 Case 1-Bioaccumulation of Arsenic (As) in Earthworms -- 11.3.2 Case 2-Silver(Ag) Nanoparticles Localization in Earthworms -- 11.4 Overview -- References.
Chapter 12 Synchronous Radiation X-Ray Fluorescence Analysis of Microelements in Biopsy Tissues -- 12.1 Introduction -- 12.2 Samples Preparation -- 12.3 Materials and Methods -- 12.4 SRXRF Measurements -- 12.5 SRXRF Biopsy Material of Living Organisms -- 12.5.1 The Elemental Composition of Derivatives of Human Epithelial Tissues -- 12.5.2 Dynamics of Derivatives of Epithelial Tissues, Human Hair and Nails -- 12.6 Study of Elemental Composition and Inter-Element Correlations in the Liver and Lungs of Animals with Food Obesity -- 12.7 Concluding Remarks -- References -- Part III Total Reflection XRF -- Chapter 13 Total Reflection X-Ray Fluorescence Analysis of some Biological Samples -- 13.1 Introduction -- 13.2 Trace Element Determinations in Marine Organisms by TXRF -- 13.3 Trace Element Determination in Blood Samples by TXRF -- 13.4 Analysis of Saliva and Oral Fluids by TXRF -- 13.5 TXRF Analysis of Hair Samples for Detection of Metal Poisoning and Other Forensic Applications -- 13.6 Kidney Stone Analysis by TXRF -- 13.7 Elemental Analysis of Cancerous and Normal Tissues by TXRF -- 13.8 TXRF Studies on Blood and Heart Tissues as Biomarkers of Radiation Dose -- 13.9 Urine Analysis by TXRF -- 13.10 Nail Analysis by TXRF -- 13.11 Analysis of Human Eye Lens and Aqueous Humor of Cataract Patients -- 13.12 Future Prospects for TXRF Analysis of Biological Samples -- References -- Chapter 14 Recent Developments in X-Ray Fluorescence for Characterization of Nano-Structured Materials -- 14.1 Principles of GIXRF Analysis -- 14.1.1 Methodology -- 14.1.2 Phenomenon of Reflection and Refraction inside a Thin Film Medium -- 14.1.3 Calculation of Electric Field Intensity and Fluorescence Intensity -- 14.2 A Few Case Studies -- 14.2.1 Characterization of Ti/Co Bilayer Structures -- 14.3 Various Computational Tools (CATGIXRF Paper).
14.4 Structural Analysis of some Complex Nano-Structures.
Record Nr. UNINA-9910566697903321
Hoboken, NJ : , : John Wiley & Sons, Inc., , [2022]
Materiale a stampa
Lo trovi qui: Univ. Federico II
Opac: Controlla la disponibilità qui
X-ray fluorescence in biological sciences : principles, instrumentation and applications / / edited by Vivek K. Singh, Jun Kawai and Durgesh K. Tripathi
X-ray fluorescence in biological sciences : principles, instrumentation and applications / / edited by Vivek K. Singh, Jun Kawai and Durgesh K. Tripathi
Pubbl/distr/stampa Hoboken, NJ : , : John Wiley & Sons, Inc., , [2022]
Descrizione fisica 1 online resource (685 pages)
Disciplina 543.08586
Soggetto topico Biology - Methodology
Chemical biology
X-ray spectroscopy
ISBN 1-119-64571-9
1-119-64558-1
Formato Materiale a stampa
Livello bibliografico Monografia
Lingua di pubblicazione eng
Nota di contenuto Cover -- Title Page -- Copyright Page -- Contents -- List of Contributors -- Preface -- Part I General Introduction -- Chapter 1 X-Ray Fluorescence and Comparison with Other Analytical Methods (AAS, ICP-AES, LA-ICP-MS, IC, LIBS, SEM-EDS, and XRD) -- 1.1 Introduction -- 1.2 Analytical Capabilities of XRF and Micro-XRF -- 1.2.1 Micro-XRF -- 1.3 Comparison with Other Analytical Methods -- 1.3.1 Overview -- 1.3.2 Inductively Coupled Plasma (ICP) Analysis -- 1.3.3 Inductively Coupled Plasma Atomic Emission Spectroscopy (ICP-AES) -- 1.3.4 Ion Chromatography (IC) -- 1.3.5 Laser-Induced Breakdown Spectroscopy (LIBS) -- 1.3.6 Proton-Induced X-Ray Emission (PIXE) -- 1.3.7 Scanning Electron Microscopy-Energy Dispersive X-Ray Spectroscopy (SEM-EDS) -- 1.4 Comparison of XRF and XRD -- 1.5 Comparison of XRF and Raman Spectroscopy -- 1.6 Conclusion and Prospects -- References -- Chapter 2 X-Ray Fluorescence for Multi-elemental Analysis of Vegetation Samples -- 2.1 Introduction -- 2.2 Features and Analytical Capabilities of XRF Configurations used in Vegetation Sample Analysis -- 2.3 General Sample Treatment Procedures used for Vegetation Sample Analysis using XRF Techniques -- 2.4 Applications of XRF in the Field of Vegetation Samples Analysis -- 2.4.1 Environmental Studies -- 2.4.2 Nutritional and Agronomic Studies -- 2.5 Concluding Remarks and Future Perspectives -- References -- Chapter 3 X-Ray Fluorescence Studies of Tea and Coffee -- 3.1 Introduction -- 3.2 The Equipment Used -- 3.3 Preparation of Samples for Analysis -- 3.4 Examples of Practical Applications of XRF for Tea Research -- 3.5 Examples of Practical Applications of XRF for Coffee Research -- 3.6 Determination of the Elemental Composition of Krasnodar Tea Samples by TXRF and WDXRF -- 3.6.1 Instrumentation -- 3.6.2 Suspension Preparation -- 3.6.3 Infusion Preparation -- 3.6.4 Acid Digestion.
3.6.5 Preparation of Samples for WDXRF -- 3.6.6 Results and Discussion -- 3.7 Interelement Effects and Procedures of their Accounting -- 3.8 Conclusion -- References -- Chapter 4 Total Reflection X-Ray Fluorescence and it's Suitability for Biological Samples -- 4.1 Introduction -- 4.2 Advantages and Limitations of conventional XRF for Elemental Determinations in Biological Systems -- 4.3 Factors Limiting the Application of XRF for Biological Sample Analysis -- 4.4 Modifying XRF to Make it Suitable for Elemental Determinations at Trace Levels: Total Reflection X-Ray Fluorescence (TXRF) Spectrometry -- 4.4.1 Principles of TXRF -- 4.4.2 Theoretical Considerations -- 4.4.3 TXRF Instrumentation for Trace Element Determination -- 4.4.4 Sample Preparation for TXRF Analysis -- 4.5 Suitability of TXRF for Elemental Analysis in Biological Samples -- References -- Chapter 5 Micro X-Ray Fluorescence and X-Ray Absorption near Edge Structure Analysis of Heavy Metals in Micro-organism -- 5.1 Introduction -- 5.2 Effects of Heavy Metals on Microbial Growth -- 5.3 Application of -XRF and XAS in Understanding the Cycling of Elements Driven by Micro-organism -- 5.4 Application of -XRF and XAS in Understanding the Transformation of Elements Driven by Micro-organisms -- 5.5 Application of -XRF and XAS in Understanding the Mechanism of Using Micro-organisms in Bioremediation -- 5.6 The Advantage of Using -XRF and XAS to Explore the Interaction Mechanism Between Micro-organisms and Heavy Metals -- References -- Chapter 6 Use of Energy Dispersive X-Ray Fluorescence for Clinical Diagnosis -- 6.1 Introduction -- 6.2 Determination of Arsenic Concentration in Human Scalp Hair for the Diagnosis of Arsenicosis Disease -- 6.2.1 Background -- 6.2.2 Role of EDXRF -- 6.2.3 Collection and Preparation of Hair Sample -- 6.2.4 Sample Preparation -- 6.2.5 Sample Analysis.
6.2.6 Accuracy and Precision of the Method -- 6.3 Determination of Lead Concentrations in Human Whole Blood Using EDXRF Technique with Special Emphasis on Evaluating Association of Blood Lead Levels with Autism Spectrum Disorders (ASD) -- 6.3.1 Background -- 6.3.2 Role of EDXRF in Diagnosis of Blood Lead Level -- 6.3.3 Collection of Blood Sample and Preparation -- 6.3.4 Preparation of Pellets from Powdered Sample -- 6.3.5 Sample Irradiation -- 6.3.6 Precision and Accuracy of the Result -- 6.4 Conclusion -- References -- Chapter 7 Preparation of Sample for X-Ray Fluorescence Analysis -- 7.1 Introduction -- 7.2 Solid Samples -- 7.2.1 Metallic Samples -- 7.3 Powder Samples -- 7.3.1 Grinding -- 7.3.2 Pelletizing -- 7.3.3 Fused Samples -- 7.4 Liquid Samples -- 7.5 Sample Preparation for Infinitely Thick and Intermediate Specimen -- 7.6 Sample Preparation of Animal Cells -- 7.7 Sample Preparation of Plant Section -- 7.8 Precautions During Sample Preparation and Handling -- 7.9 Conclusion and Future Directions -- References -- Part II Synchrotron Radiation XRF -- Chapter 8 Elemental Analysis Using Synchrotron Radiation X-Ray Fluorescence -- 8.1 Importance of Trace and Ultra-Trace Elemental Analysis -- 8.2 Various Methods for Trace Element Analysis -- 8.2.1 Atomic Absorption Spectroscopy (AAS) Method -- 8.2.2 Inductively Coupled Plasma Mass Spectrometry (ICP-MS) Method -- 8.2.3 Neutron Activation Analysis (NAA) Method -- 8.2.4 Accelerator Ion Beam Techniques -- 8.2.5 X-Ray Fluorescence (XRF) Method -- 8.2.6 Total Reflection X-Ray Fluorescence (TXRF) Method -- 8.3 Comparison of TXRF and EDXRF Geometries -- 8.4 Synchrotron Radiation -- 8.4.1 Selection of a Laboratory X-Ray Source for TXRF -- 8.5 Indus Synchrotron Radiation Facility -- 8.6 Microprobe X-Ray Fluorescence Beamline (BL-16) -- 8.6.1 Working Principles of a Double Crystal Monochromator (DCM) Optic.
8.7 Experimental Facilities Available on the BL-16 -- 8.7.1 Normal EDXRF Measurements -- 8.7.2 Total Reflection X-Ray Fluorescence (TXRF) Measurements -- 8.7.3 Elemental Quantification -- 8.7.4 X-Ray Fluorescence Analysis of Nanostructures -- 8.7.5 Microfocus X-Ray Beam Mode -- 8.7.6 Micro-Fluorescence Mapping -- 8.7.7 Micro-XRF Mapping Analysis of Old Archeological Tile Samples -- 8.8 Discussion and Summary -- References -- Chapter 9 Synchrotron Radiation Based Micro X-Ray Fluorescence Spectroscopy of Plant Materials -- 9.1 Introduction -- 9.2 Instrumentation and Sample Preparation -- 9.3 Case Studies -- 9.3.1 Metal Tolerance Mechanisms in Hyperaccumulating Plants -- 9.3.2 Metal Toxicity and Tolerance in Plants and Fungi -- 9.3.3 Distribution of Mineral Nutrients and Potentially Toxic Elements in Grain -- 9.3.4 Investigation of Interactions between Plants and Engineered Nanomaterials -- Acknowledgements -- References -- Chapter 10 Micro X-Ray Fluorescence Analysis of Toxic Elements in Plants -- 10.1 Introduction -- 10.2 Advantages of XRF Technique for Plants Analysis -- 10.3 Preparation of Plant Samples for -XRF Analysis -- 10.4 The Case Studies of Synchrotron -XRF for Determination of Toxic Elements in Plants -- 10.4.1 Applications in Edible Plants -- 10.4.2 Applications in Accumulating Plants -- 10.4.3 Applications in Hyperaccumulator Plants -- 10.4.4 The Case Studies of Laboratory -XRF to Determine Elements in Waterlogged Oenanthe javanica DC -- 10.5 Conclusion and Outlook -- References -- Chapter 11 Micro X-Ray Fluorescence Studies of Earthworm (Benthonic Fauna) in Soils and Sediments -- 11.1 Introduction -- 11.2 Sample Preparation Methods -- 11.3 Earthworms and Soil Ecosystem -- 11.3.1 Case 1-Bioaccumulation of Arsenic (As) in Earthworms -- 11.3.2 Case 2-Silver(Ag) Nanoparticles Localization in Earthworms -- 11.4 Overview -- References.
Chapter 12 Synchronous Radiation X-Ray Fluorescence Analysis of Microelements in Biopsy Tissues -- 12.1 Introduction -- 12.2 Samples Preparation -- 12.3 Materials and Methods -- 12.4 SRXRF Measurements -- 12.5 SRXRF Biopsy Material of Living Organisms -- 12.5.1 The Elemental Composition of Derivatives of Human Epithelial Tissues -- 12.5.2 Dynamics of Derivatives of Epithelial Tissues, Human Hair and Nails -- 12.6 Study of Elemental Composition and Inter-Element Correlations in the Liver and Lungs of Animals with Food Obesity -- 12.7 Concluding Remarks -- References -- Part III Total Reflection XRF -- Chapter 13 Total Reflection X-Ray Fluorescence Analysis of some Biological Samples -- 13.1 Introduction -- 13.2 Trace Element Determinations in Marine Organisms by TXRF -- 13.3 Trace Element Determination in Blood Samples by TXRF -- 13.4 Analysis of Saliva and Oral Fluids by TXRF -- 13.5 TXRF Analysis of Hair Samples for Detection of Metal Poisoning and Other Forensic Applications -- 13.6 Kidney Stone Analysis by TXRF -- 13.7 Elemental Analysis of Cancerous and Normal Tissues by TXRF -- 13.8 TXRF Studies on Blood and Heart Tissues as Biomarkers of Radiation Dose -- 13.9 Urine Analysis by TXRF -- 13.10 Nail Analysis by TXRF -- 13.11 Analysis of Human Eye Lens and Aqueous Humor of Cataract Patients -- 13.12 Future Prospects for TXRF Analysis of Biological Samples -- References -- Chapter 14 Recent Developments in X-Ray Fluorescence for Characterization of Nano-Structured Materials -- 14.1 Principles of GIXRF Analysis -- 14.1.1 Methodology -- 14.1.2 Phenomenon of Reflection and Refraction inside a Thin Film Medium -- 14.1.3 Calculation of Electric Field Intensity and Fluorescence Intensity -- 14.2 A Few Case Studies -- 14.2.1 Characterization of Ti/Co Bilayer Structures -- 14.3 Various Computational Tools (CATGIXRF Paper).
14.4 Structural Analysis of some Complex Nano-Structures.
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Hoboken, NJ : , : John Wiley & Sons, Inc., , [2022]
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