Solid-phase organic synthesis [[electronic resource] ] : concepts, strategies, and applications / / edited by Patrick H. Toy, Yulin Lam |
Edizione | [1st ed.] |
Pubbl/distr/stampa | Hoboken, NJ, : Wiley, 2012 |
Descrizione fisica | 1 online resource (562 p.) |
Disciplina | 547/.2 |
Altri autori (Persone) |
ToyPatrick H
LamYulin |
Soggetto topico |
Solid-phase synthesis
Organic compounds - Synthesis |
ISBN |
1-283-40957-7
9786613409577 1-118-14163-6 1-118-14164-4 1-118-14162-8 |
Classificazione | SCI013050 |
Formato | Materiale a stampa ![]() |
Livello bibliografico | Monografia |
Lingua di pubblicazione | eng |
Nota di contenuto |
SOLID-PHASE ORGANIC SYNTHESIS: Concepts, Strategies, and Applications; CONTENTS; Preface; Acknowledgments; Contributors; Part I: CONCEPTS AND STRATEGIES; 1 LINKER STRATEGIES IN MODERN SOLID-PHASE ORGANIC SYNTHESIS; 1.1 Introduction; 1.2 Classical Linker Strategies; 1.2.1 Acid and Base Cleavable Linker Units; 1.2.2 Cyclorelease Linker Units; 1.2.3 Traceless Linker Units; 1.2.4 Photolabile Linker Units; 1.2.5 Safety-Catch Linker Units; 1.3 Multifunctional Linker Strategies; 1.3.1 Nitrogen Linker Units; 1.3.1.1 Triazene Linker Units; 1.3.1.2 Hydrazone Linker Units
1.3.1.3 Benzotriazole Linker Units1.3.2 Sulfur Linker Units; 1.3.3 Phosphorus Linker Units; 1.3.4 Selenium and Tellurium Linker Units; 1.3.5 Silyl and Germyl Linker Units; 1.3.6 Boron and Stannane Linker Units; 1.3.7 Bismuth Linker Units; 1.3.8 Alkene Linker Units; 1.4 Conclusions; References; 2 COLORIMETRIC TEST FOR SOLID-PHASE ORGANIC SYNTHESIS; 2.1 Introduction; 2.2 Functional Group Tests; 2.2.1 Amine Groups; 2.2.1.1 Ninhydrin (Kaiser) Test; 2.2.1.2 TNBSA Test; 2.2.1.3 Bromophenol Blue Test; 2.2.1.4 Chloranil Test; 2.2.1.5 DABITC Test; 2.2.1.6 MGI Test; 2.2.1.7 Isatin Test 2.2.1.8 DESC Test2.2.1.9 NPIT Test; 2.2.1.10 NF31 Test; 2.2.1.11 Nondestructive NF31 Test; 2.2.1.12 Naphthol Test; 2.2.1.13 2-Amino-3-chloro-1,4-naphthoquinone Test; 2.2.2 Alcohols; 2.2.2.1 PNBP Test; 2.2.2.2 TCT-AliR and TCT-Fluorescein Test; 2.2.2.3 Diphenyldichlorosilane-Methyl Red Test; 2.2.2.4 9-Anthronylnitrile Test; 2.2.2.5 NMA Test; 2.2.2.6 Protecting Group NPB Test; 2.2.2.7 Methyl Red/DIC Test; 2.2.2.8 Other Methods; 2.2.3 Thiol Groups; 2.2.3.1 Ellman's Test; 2.2.3.2 Other Methods; 2.2.4 Halogen Groups; 2.2.4.1 Fluorescein Test; 2.2.4.2 Other Methods; 2.2.5 Carboxylic Acid Groups 2.2.5.1 Malachite Green Test2.2.5.2 PDAM Test; 2.2.6 Aldehyde and Ketone Groups; 2.2.6.1 Fluorescent Dansylhydrazine Test; 2.2.6.2 p-Anisaldehyde Test; 2.2.6.3 Purpald Test; 2.3 Conclusions; References; 3 PRACTICAL ASPECTS OF COMBINATORIAL SOLID-PHASE SYNTHESIS; 3.1 Introduction; 3.1.1 What Is Combinatorial Chemistry; 3.1.2 What Is Not Combinatorial Chemistry; 3.1.3 History of Combinatorial Chemistry: Breakthrough Discoveries That Shaped the Future of the Combinatorial Chemistry Field; 3.1.3.1 Solid-Phase Synthesis; 3.1.3.2 Pooling Strategy; 3.1.3.3 Parallel Synthesis 3.2 Strategies in Combinatorial Solid-Phase Synthesis3.2.1 Random Split-and-Pool Method; 3.2.1.1 One-Bead-One-Compound Concept; 3.2.1.2 Encoding Methods for the OBOC Technique; 3.2.1.3 Organized Mixtures; 3.2.2 Directed Split-and-Pool Method in Practice; 3.2.2.1 Formulation of Solid-Phase Supports for the Directed Split-and-Pool Technique; 3.2.2.2 Chemical History of the Resin Formulations; 3.3 Equipment and Instrumentation; 3.3.1 Manual Solid-Phase Synthesis; 3.3.2 Integrated Semiautomated Synthesis; 3.3.3 Fully Automated Synthesizers (Gone with the Wind); 3.3.4 Instruments for Sorting 3.4 Characterization and Purification |
Record Nr. | UNINA-9910817949103321 |
Hoboken, NJ, : Wiley, 2012 | ||
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Lo trovi qui: Univ. Federico II | ||
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Solid-phase palladium chemistry / / edited by Peter J.H. Scott |
Pubbl/distr/stampa | Hoboken, New Jersey : , : Wiley, , [2012] |
Descrizione fisica | 1 online resource (186 p.) |
Disciplina |
547.056362
547/.056362 |
Collana | Wiley series on solid-phase organic syntheses |
Soggetto topico |
Organopalladium compounds
Organic compounds - Synthesis Solid-phase synthesis |
ISBN |
1-280-77848-2
9786613688873 1-118-33670-4 1-118-33695-X 1-118-33669-0 |
Classificazione | SCI013050 |
Formato | Materiale a stampa ![]() |
Livello bibliografico | Monografia |
Lingua di pubblicazione | eng |
Nota di contenuto |
Solid-Phase Organic Syntheses; CONTENTS; Contributors; Preface; Abbreviations; PART I INTRODUCTION; 1. An Introduction to Solid-Phase Palladium Chemistry; PART II PALLADIUM-MEDIATED SPOS; 2. Pd-Catalyzed Solid-Phase Decoration of the2(1H)-Pyrazinone Scaffold; 3. One-Step Palladium- and Phenylsilane-ActivatedAmidation of Solid-Supported Ally Esters; 4. Solid-Phase Reactions of Polymer-BoundArenesulfonates with Aryl Grignard Reagents; 5. Fluorous Synthesis of 3-Aminoimidazo[1,2-a]-Pyridine/Pyrazine Library; 6. Resin-to-Resin Transfer Reactions (RRTR) viaSonogashira Coupling
PART III IMMOBILIZED CATALYSTS AND LIGANDS7. Polymer-supported Palladium Catalysts for Suzukiand Heck Reactions; 8. Solid-Phase Catalytic Activity of aPolymer-Supported Palladium Complex; 9. Polyaniline-immobilized Palladium forSuzuki-Miyaura Coupling Reaction in Water; 10. Synthesis of Polymer-SupportedAryldicyclohexylphosphine for an Efficient; 11. C-C or C-N Reactions Catalyzed byDiadamanthylphosphine Palladium-Based CatalystSupported on Dab-Dendrimers; PART IV PALLADIUM-MEDIATED MULTIFUNCTIONALCLEAVAGE; 12. Solid-Phase Reactions of Resin-Supported BoronicAcids 13. A Simple Diversity Linker Strategy Using ImmobilizedEnol Phosphonates as Electrophiles forSuzuki-Miyaura Reactions14. Heck Cleavage of Resin-bound Triazenes; 15. Pd-Mediated Cleavage fromTetrafluoroarylsulfonate Linker Units; 16. Palladium-Catalyzed Solid-Phase Synthesis ofAllylic Amines; 17. Palladium-Catalyzed Solid-Phase Synthesis of4-Methylene Pyrrolidines; Index |
Record Nr. | UNINA-9910141258703321 |
Hoboken, New Jersey : , : Wiley, , [2012] | ||
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Lo trovi qui: Univ. Federico II | ||
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Solid-phase palladium chemistry / / edited by Peter J.H. Scott |
Pubbl/distr/stampa | Hoboken, New Jersey : , : Wiley, , [2012] |
Descrizione fisica | 1 online resource (186 p.) |
Disciplina |
547.056362
547/.056362 |
Collana | Wiley series on solid-phase organic syntheses |
Soggetto topico |
Organopalladium compounds
Organic compounds - Synthesis Solid-phase synthesis |
ISBN |
1-280-77848-2
9786613688873 1-118-33670-4 1-118-33695-X 1-118-33669-0 |
Classificazione | SCI013050 |
Formato | Materiale a stampa ![]() |
Livello bibliografico | Monografia |
Lingua di pubblicazione | eng |
Nota di contenuto |
Solid-Phase Organic Syntheses; CONTENTS; Contributors; Preface; Abbreviations; PART I INTRODUCTION; 1. An Introduction to Solid-Phase Palladium Chemistry; PART II PALLADIUM-MEDIATED SPOS; 2. Pd-Catalyzed Solid-Phase Decoration of the2(1H)-Pyrazinone Scaffold; 3. One-Step Palladium- and Phenylsilane-ActivatedAmidation of Solid-Supported Ally Esters; 4. Solid-Phase Reactions of Polymer-BoundArenesulfonates with Aryl Grignard Reagents; 5. Fluorous Synthesis of 3-Aminoimidazo[1,2-a]-Pyridine/Pyrazine Library; 6. Resin-to-Resin Transfer Reactions (RRTR) viaSonogashira Coupling
PART III IMMOBILIZED CATALYSTS AND LIGANDS7. Polymer-supported Palladium Catalysts for Suzukiand Heck Reactions; 8. Solid-Phase Catalytic Activity of aPolymer-Supported Palladium Complex; 9. Polyaniline-immobilized Palladium forSuzuki-Miyaura Coupling Reaction in Water; 10. Synthesis of Polymer-SupportedAryldicyclohexylphosphine for an Efficient; 11. C-C or C-N Reactions Catalyzed byDiadamanthylphosphine Palladium-Based CatalystSupported on Dab-Dendrimers; PART IV PALLADIUM-MEDIATED MULTIFUNCTIONALCLEAVAGE; 12. Solid-Phase Reactions of Resin-Supported BoronicAcids 13. A Simple Diversity Linker Strategy Using ImmobilizedEnol Phosphonates as Electrophiles forSuzuki-Miyaura Reactions14. Heck Cleavage of Resin-bound Triazenes; 15. Pd-Mediated Cleavage fromTetrafluoroarylsulfonate Linker Units; 16. Palladium-Catalyzed Solid-Phase Synthesis ofAllylic Amines; 17. Palladium-Catalyzed Solid-Phase Synthesis of4-Methylene Pyrrolidines; Index |
Record Nr. | UNINA-9910812850103321 |
Hoboken, New Jersey : , : Wiley, , [2012] | ||
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Lo trovi qui: Univ. Federico II | ||
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Structural glasses and supercooled liquids [[electronic resource] ] : theory, experiment, and applications / / edited By Peter G. Wolynes, Vassiliy Lubchenko |
Pubbl/distr/stampa | Hoboken, N.J., : Wiley, 2012 |
Descrizione fisica | 1 online resource (422 p.) |
Disciplina | 620.1/44 |
Altri autori (Persone) |
WolynesP. G (Peter G.)
LubchenkoVassiliy |
Soggetto topico | Glass - Analysis |
ISBN |
1-280-59253-2
9786613622365 1-118-20241-4 1-118-20247-3 1-118-20249-X |
Classificazione | SCI013050 |
Formato | Materiale a stampa ![]() |
Livello bibliografico | Monografia |
Lingua di pubblicazione | eng |
Nota di contenuto |
Structural Glasses and Supercooled Liquids: Theory, Experiment, and Applications; CONTENTS; Preface; Contributors; 1 Supercooled Liquid Dynamics: Advances and Challenges; 2 The Random First-Order Transition Theory of Glasses: A Critical Assessment; 3 Dielectric Spectroscopy of Glassy Dynamics; 4 Glasses and Replicas; 5 Glassiness in Uniformly Frustrated Systems; 6 Random First-Order Phase Transition Theory of the Structural Glass Transition; 7 Fragile Glass Formers: Evidence for a New Paradigm, and a New Relation to Strong Liquids; 8 Dynamics in the Crossover Region of Supercooled Liquids
9 Glassy Dynamics of Proteins10 Theories of Structural Glass Dynamics: Mosaics, Jamming, and All That; Index; Colour Plates |
Record Nr. | UNINA-9910141295203321 |
Hoboken, N.J., : Wiley, 2012 | ||
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Lo trovi qui: Univ. Federico II | ||
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Structural glasses and supercooled liquids [[electronic resource] ] : theory, experiment, and applications / / edited By Peter G. Wolynes, Vassiliy Lubchenko |
Pubbl/distr/stampa | Hoboken, N.J., : Wiley, 2012 |
Descrizione fisica | 1 online resource (422 p.) |
Disciplina | 620.1/44 |
Altri autori (Persone) |
WolynesP. G (Peter G.)
LubchenkoVassiliy |
Soggetto topico | Glass - Analysis |
ISBN |
1-280-59253-2
9786613622365 1-118-20241-4 1-118-20247-3 1-118-20249-X |
Classificazione | SCI013050 |
Formato | Materiale a stampa ![]() |
Livello bibliografico | Monografia |
Lingua di pubblicazione | eng |
Nota di contenuto |
Structural Glasses and Supercooled Liquids: Theory, Experiment, and Applications; CONTENTS; Preface; Contributors; 1 Supercooled Liquid Dynamics: Advances and Challenges; 2 The Random First-Order Transition Theory of Glasses: A Critical Assessment; 3 Dielectric Spectroscopy of Glassy Dynamics; 4 Glasses and Replicas; 5 Glassiness in Uniformly Frustrated Systems; 6 Random First-Order Phase Transition Theory of the Structural Glass Transition; 7 Fragile Glass Formers: Evidence for a New Paradigm, and a New Relation to Strong Liquids; 8 Dynamics in the Crossover Region of Supercooled Liquids
9 Glassy Dynamics of Proteins10 Theories of Structural Glass Dynamics: Mosaics, Jamming, and All That; Index; Colour Plates |
Record Nr. | UNINA-9910824574403321 |
Hoboken, N.J., : Wiley, 2012 | ||
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Lo trovi qui: Univ. Federico II | ||
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Supercritical water [[electronic resource] ] : a green solvent : properties and uses / / Yizhak Marcus |
Autore | Marcus Y |
Edizione | [2nd ed.] |
Pubbl/distr/stampa | Hoboken, N.J., : Wiley, c2012 |
Descrizione fisica | 1 online resource (220 p.) |
Disciplina | 541/.3482 |
Soggetto topico |
Solvents
Green technology |
ISBN |
1-280-67881-X
9786613655745 1-118-31027-6 1-118-31025-X 1-118-31022-5 |
Classificazione | SCI013050 |
Formato | Materiale a stampa ![]() |
Livello bibliografico | Monografia |
Lingua di pubblicazione | eng |
Nota di contenuto | Machine generated contents note: PrefaceList of symbols1. Introduction1.1 Phase diagrams of single fluids1.2 The critical point1.3 Supercritical fluids as solvents1.4 Gaseous and liquid water1.5 Near-critical water1.6 Summary2. Bulk properties of SCW2.1 Equations of state2.2 Thermophysical properties2.3 Electrical and Optical Properties2.4 Transport Properties2.5 Ionic Dissociation of SCW2.6 Properties related to the solvent power of SCW2.7 Summary3. Molecular properties3.1 Structure of SCW obtained by diffraction3.2 Computer simulations of SCW3.3 Spectroscopic studies of SCW3.4 Extent of hydrogen bonding3.5 The dynamics of water molecules in SCW3.5 Summary4. SCW as a 'green' solvent4.1 Solutions of gases in SCW4.2 Solutions of organic substances in SCW4.3 Solutions of Salts and ions in SCW4.4 Binary mixtures of co-solvents with SCW4.5 Summary5. Applications of SCW5.1 Conversion of organic material to fuel5.2 SCWO: Total oxidation of obnoxious and hazardous materials5.3 Uses of SCW in organic synthesis5.4 Uses in powder technology of inorganic substances5.5 Geothermal aspects of SCW5.6 Application of SCW in nuclear reactors5.7 Corrosion problems with SCW5.8 Summary6. Indexes6.1 Author Index6.2 Subject Index. |
Record Nr. | UNINA-9910139697603321 |
Marcus Y
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Hoboken, N.J., : Wiley, c2012 | ||
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Lo trovi qui: Univ. Federico II | ||
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Supercritical water [[electronic resource] ] : a green solvent : properties and uses / / Yizhak Marcus |
Autore | Marcus Y |
Edizione | [2nd ed.] |
Pubbl/distr/stampa | Hoboken, N.J., : Wiley, c2012 |
Descrizione fisica | 1 online resource (220 p.) |
Disciplina | 541/.3482 |
Soggetto topico |
Solvents
Green technology |
ISBN |
1-280-67881-X
9786613655745 1-118-31027-6 1-118-31025-X 1-118-31022-5 |
Classificazione | SCI013050 |
Formato | Materiale a stampa ![]() |
Livello bibliografico | Monografia |
Lingua di pubblicazione | eng |
Nota di contenuto | Machine generated contents note: PrefaceList of symbols1. Introduction1.1 Phase diagrams of single fluids1.2 The critical point1.3 Supercritical fluids as solvents1.4 Gaseous and liquid water1.5 Near-critical water1.6 Summary2. Bulk properties of SCW2.1 Equations of state2.2 Thermophysical properties2.3 Electrical and Optical Properties2.4 Transport Properties2.5 Ionic Dissociation of SCW2.6 Properties related to the solvent power of SCW2.7 Summary3. Molecular properties3.1 Structure of SCW obtained by diffraction3.2 Computer simulations of SCW3.3 Spectroscopic studies of SCW3.4 Extent of hydrogen bonding3.5 The dynamics of water molecules in SCW3.5 Summary4. SCW as a 'green' solvent4.1 Solutions of gases in SCW4.2 Solutions of organic substances in SCW4.3 Solutions of Salts and ions in SCW4.4 Binary mixtures of co-solvents with SCW4.5 Summary5. Applications of SCW5.1 Conversion of organic material to fuel5.2 SCWO: Total oxidation of obnoxious and hazardous materials5.3 Uses of SCW in organic synthesis5.4 Uses in powder technology of inorganic substances5.5 Geothermal aspects of SCW5.6 Application of SCW in nuclear reactors5.7 Corrosion problems with SCW5.8 Summary6. Indexes6.1 Author Index6.2 Subject Index. |
Record Nr. | UNINA-9910822158803321 |
Marcus Y
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Hoboken, N.J., : Wiley, c2012 | ||
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Lo trovi qui: Univ. Federico II | ||
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Supramolecular photochemistry [[electronic resource] ] : controlling photochemical processes / / edited by V. Ramamurthy, Yoshihisa Inoue |
Pubbl/distr/stampa | Hoboken, N.J., : Wiley, 2011 |
Descrizione fisica | 1 online resource (637 p.) |
Disciplina | 541/.226 |
Altri autori (Persone) |
RamamurthyV
InoueYoshihisa <1949-> |
Soggetto topico |
Photochemistry
Supramolecular chemistry |
ISBN |
1-283-20398-7
9786613203984 1-118-09529-4 1-118-09530-8 1-118-09527-8 |
Classificazione | SCI013050 |
Formato | Materiale a stampa ![]() |
Livello bibliografico | Monografia |
Lingua di pubblicazione | eng |
Nota di contenuto |
SUPRAMOLECULAR PHOTOCHEMISTRY: Controlling Photochemical Processes; CONTENTS; PREFACE; CONTRIBUTORS; 1: DYNAMICS OF GUEST BINDING TO SUPRAMOLECULAR ASSEMBLIES; 2: TEMPLATING PHOTOREACTIONS IN SOLUTION; 3: COMPLEXATION OF FLUORESCENT DYES BY MACROCYCLIC HOSTS; 4: SUPRAMOLECULAR PHOTOCHIROGENESIS; 5: REAL-TIME CRYSTALLOGRAPHY OF PHOTOINDUCED PROCESSES IN SUPRAMOLECULAR FRAMEWORK SOLIDS; 6: BIMOLECULAR PHOTOREACTIONS IN THE CRYSTALLINE STATE; 7: STRUCTURAL ASPECTS AND TEMPLATION OF PHOTOCHEMISTRY IN SOLID-STATE SUPRAMOLECULAR SYSTEMS; 8: PHOTOCHROMISM OF MULTICOMPONENT DIARYLETHENE CRYSTALS
9: MANIPULATION OF ENERGY TRANSFER PROCESSES WITHIN THE CHANNELS OF L-ZEOLITE10: CONTROLLING PHOTOREACTIONS THROUGH NONCOVALENT INTERACTIONS WITHIN ZEOLITE NANOCAGES; 11: PHOTOCHEMICAL AND PHOTOPHYSICAL STUDIES OF AND IN BULK POLYMERS; 12: DELOCALIZATION AND MIGRATION OF EXCITATION ENERGY AND CHARGE IN SUPRAMOLECULAR SYSTEMS; 13: SUPRAMOLECULAR EFFECTS ON MECHANISMS OF PHOTOISOMERIZATION: HULA TWIST, BICYCLE PEDAL, AND ONE-BOND-FLIP; 14: PROTEIN-CONTROLLED ULTRAFAST PHOTOISOMERIZATION IN RHODOPSIN AND BACTERIORHODOPSIN; INDEX |
Record Nr. | UNINA-9910139633103321 |
Hoboken, N.J., : Wiley, 2011 | ||
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Lo trovi qui: Univ. Federico II | ||
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Supramolecular photochemistry [[electronic resource] ] : controlling photochemical processes / / edited by V. Ramamurthy, Yoshihisa Inoue |
Pubbl/distr/stampa | Hoboken, N.J., : Wiley, 2011 |
Descrizione fisica | 1 online resource (637 p.) |
Disciplina | 541/.226 |
Altri autori (Persone) |
RamamurthyV
InoueYoshihisa <1949-> |
Soggetto topico |
Photochemistry
Supramolecular chemistry |
ISBN |
1-283-20398-7
9786613203984 1-118-09529-4 1-118-09530-8 1-118-09527-8 |
Classificazione | SCI013050 |
Formato | Materiale a stampa ![]() |
Livello bibliografico | Monografia |
Lingua di pubblicazione | eng |
Nota di contenuto |
SUPRAMOLECULAR PHOTOCHEMISTRY: Controlling Photochemical Processes; CONTENTS; PREFACE; CONTRIBUTORS; 1: DYNAMICS OF GUEST BINDING TO SUPRAMOLECULAR ASSEMBLIES; 2: TEMPLATING PHOTOREACTIONS IN SOLUTION; 3: COMPLEXATION OF FLUORESCENT DYES BY MACROCYCLIC HOSTS; 4: SUPRAMOLECULAR PHOTOCHIROGENESIS; 5: REAL-TIME CRYSTALLOGRAPHY OF PHOTOINDUCED PROCESSES IN SUPRAMOLECULAR FRAMEWORK SOLIDS; 6: BIMOLECULAR PHOTOREACTIONS IN THE CRYSTALLINE STATE; 7: STRUCTURAL ASPECTS AND TEMPLATION OF PHOTOCHEMISTRY IN SOLID-STATE SUPRAMOLECULAR SYSTEMS; 8: PHOTOCHROMISM OF MULTICOMPONENT DIARYLETHENE CRYSTALS
9: MANIPULATION OF ENERGY TRANSFER PROCESSES WITHIN THE CHANNELS OF L-ZEOLITE10: CONTROLLING PHOTOREACTIONS THROUGH NONCOVALENT INTERACTIONS WITHIN ZEOLITE NANOCAGES; 11: PHOTOCHEMICAL AND PHOTOPHYSICAL STUDIES OF AND IN BULK POLYMERS; 12: DELOCALIZATION AND MIGRATION OF EXCITATION ENERGY AND CHARGE IN SUPRAMOLECULAR SYSTEMS; 13: SUPRAMOLECULAR EFFECTS ON MECHANISMS OF PHOTOISOMERIZATION: HULA TWIST, BICYCLE PEDAL, AND ONE-BOND-FLIP; 14: PROTEIN-CONTROLLED ULTRAFAST PHOTOISOMERIZATION IN RHODOPSIN AND BACTERIORHODOPSIN; INDEX |
Record Nr. | UNINA-9910818322103321 |
Hoboken, N.J., : Wiley, 2011 | ||
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Lo trovi qui: Univ. Federico II | ||
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