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Distillation control [[electronic resource] ] : an engineering perspective / / Cecil L. Smith
| Distillation control [[electronic resource] ] : an engineering perspective / / Cecil L. Smith |
| Autore | Smith Cecil L |
| Pubbl/distr/stampa | Hoboken, N.J., : John Wiley & Sons, c2012 |
| Descrizione fisica | 1 online resource (xi, 332 p. ) : ill |
| Disciplina | 660/.28425 |
| Soggetto topico | Distillation |
| ISBN |
1-5231-0986-6
1-118-25969-6 1-118-26005-8 1-280-59077-7 9786613620606 1-118-25968-8 |
| Classificazione | TEC009010 |
| Formato | Materiale a stampa  |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto | Machine generated contents note: Chapter 1. Principles 1.1 Separation Processes 1.2 Total Material Balance 1.3 Reflux and Boilup Ratios 1.4 Total Material Balance Around Condenser 1.5 Total Material Balance Around Reboiler 1.6 Component Material Balances 1.7 Energy and the Separation Factor 1.8 Multicomponent Distillation 1.9 Stage-by-Stage Separation Model 1.10 Formulation of the Control Problem 1.11 Tower Internals 1.12 Flooding 1.13 Tray Hydraulics 1.14 Inverse Response in Bottoms Level 1.15 Composition Dynamics Chapter 2. Composition Control 2.1 Product Specifications 2.2 Columns in Series 2.3 Composition Analyzers 2.4 Temperature 2.5 Distillate Composition Control, Constant Boilup 2.6 Distillate Composition Control, Constant Bottoms Flow 2.7 Operating Lines 2.8 Temperature Profiles 2.9 Feed Composition Disturbances 2.10 Bottoms Composition Control 2.11 Propagation of Variance in Level Control Configurations 2.12 Level Control in Direct Material Balance Configurations Chapter 3. Pressure Control and Condensers 3.1 Pressure Control 3.2 Once-Through Heat Transfer Processes 3.3 Water-Cooled Condensers 3.4 Flooded Condensers 3.5 Air-Cooled Condensers 3.6 Partial Condensers 3.7 Atmospheric Towers 3.8 Vacuum Towers 3.9 Floating Pressure / Pressure Minimization Chapter 4. Reboilers and Feed Preheaters 4.1 Types of Reboilers 4.2 Steam-Heated Reboilers 4.3 Hot Oil 4.4 Fired Heaters 4.5 Feed Preheater 4.6 Economizer Chapter 5. Applying Feedforward 5.1 Feed Flow and Composition 5.2 Internal Reflux Control 5.3 Extreme Feedforward 5.4 Feedforward for Bottoms Level 5.5 Feedforward for Column Pressure 5.6 Product Compositions Chapter 6. Unit Optimization 6.1 Energy and Separation 6.2 Optimization of a Column 6.3 Constraints in Distillation Columns 6.4 Control Configurations for Single Constraint 6.5 Control Configurations for Multiple Constraints Chapter 7. Double-End Composition Control 7.1 Defining the Problem. 7.2 Options for Composition Control 7.3 Relative Gain 7.4 Relative Gains from Open Loop Sensitivities 7.5 Relative Gains for Other Configurations 7.6 Ratios for Manipulated Variables 7.7 Effect of Operating Objectives 7.8 Model Predictive Control Chapter 8. Complex Towers 8.1 Heat Integration 8.2 Side Heater / Side Cooler 8.3 Sidestreams 8.4 Withdrawing a Liquid Sidestream 8.5 Withdrawing a vapor sidestream 8.6 Composition Control in Sidestream Towers. |
| Record Nr. | UNINA-9910814983903321 |
Smith Cecil L
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| Hoboken, N.J., : John Wiley & Sons, c2012 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
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Distillation control, optimization, and tuning : fundamentals and strategies / / Lanny Robbins
| Distillation control, optimization, and tuning : fundamentals and strategies / / Lanny Robbins |
| Autore | Robbins Lanny |
| Pubbl/distr/stampa | Boca Raton : , : CRC Press, , 2011 |
| Descrizione fisica | 1 online resource (144 p.) |
| Disciplina | 660/.28425 |
| Soggetto topico |
Distillation
Separation (Technology) |
| ISBN |
1-000-21862-7
0-429-10729-3 1-62870-490-X 1-4398-5800-4 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto | Front cover; Contents; The Author; Chapter 1. Introduction and Overview; Chapter 2. Distillation Control Variables; Chapter 3. Separation Power; Chapter 4. Distillate/Feed Material Balance Split; Chapter 5. Distillation Control Strategies; Chapter 6. Constraints; Chapter 7. Optimizing Product Quality Performance; Chapter 8. PID Feedback Control Loop; Chapter 9. Closed-Loop Tuning of Controllers; Chapter 10. Open-Loop Testing of Process Response; Appendix: Solutions to Chapter Exercises; Back cover |
| Record Nr. | UNINA-9910788255003321 |
|
Robbins Lanny
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| Boca Raton : , : CRC Press, , 2011 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Distillation control, optimization, and tuning : fundamentals and strategies / / Lanny Robbins
| Distillation control, optimization, and tuning : fundamentals and strategies / / Lanny Robbins |
| Autore | Robbins Lanny |
| Pubbl/distr/stampa | Boca Raton : , : CRC Press, , 2011 |
| Descrizione fisica | 1 online resource (144 p.) |
| Disciplina | 660/.28425 |
| Soggetto topico |
Distillation
Separation (Technology) |
| ISBN |
1-000-21862-7
0-429-10729-3 1-62870-490-X 1-4398-5800-4 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto | Front cover; Contents; The Author; Chapter 1. Introduction and Overview; Chapter 2. Distillation Control Variables; Chapter 3. Separation Power; Chapter 4. Distillate/Feed Material Balance Split; Chapter 5. Distillation Control Strategies; Chapter 6. Constraints; Chapter 7. Optimizing Product Quality Performance; Chapter 8. PID Feedback Control Loop; Chapter 9. Closed-Loop Tuning of Controllers; Chapter 10. Open-Loop Testing of Process Response; Appendix: Solutions to Chapter Exercises; Back cover |
| Record Nr. | UNINA-9910817571003321 |
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Robbins Lanny
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| Boca Raton : , : CRC Press, , 2011 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Distillation design and control using Aspen simulation / / William L. Luyben
| Distillation design and control using Aspen simulation / / William L. Luyben |
| Autore | Luyben William L. |
| Edizione | [Second edition.] |
| Pubbl/distr/stampa | Hoboken, New Jersey : , : AlChE : , : Wiley, , 2013 |
| Descrizione fisica | 1 online resource (742 p.) |
| Disciplina | 660/.28425 |
| Soggetto topico |
Distillation apparatus - Design and construction
Chemical process control - Simulation methods Petroleum - Refining |
| ISBN |
1-5231-1062-7
1-118-51019-4 1-118-51013-5 1-118-51009-7 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Cover; Title Page; Copyright; Dedication; Preface to the Second Edition; Preface to the First Edition; Chapter 1: Fundamentals of Vapor-Liquid-Equilibrium (VLE); 1.1 Vapor Pressure; 1.2 Binary VLE Phase Diagrams; 1.3 Physical Property Methods; 1.4 Relative Volatility; 1.5 Bubble Point Calculations; 1.6 Ternary Diagrams; 1.7 VLE Nonideality; 1.8 Residue Curves for Ternary Systems; 1.9 Distillation Boundaries; 1.10 Conclusions; Reference; Chapter 2: Analysis of Distillation Columns; 2.1 Design Degrees of Freedom; 2.2 Binary Mccabe-Thiele Method; 2.3 Approximate Multicomponent Methods
2.4 Conclusions Chapter 3: Setting Up a Steady-State Simulation; 3.1 Configuring a New Simulation; 3.2 Specifying Chemical Components and Physical Properties; 3.3 Specifying Stream Properties; 3.4 Specifying Parameters of Equipment; 3.5 Running the Simulation; 3.6 Using Design Spec/Vary Function; 3.7 Finding the Optimum Feed Tray and Minimum Conditions; 3.8 Column Sizing; 3.9 Conceptual Design; 3.10 Conclusions; Chapter 4: Distillation Economic Optimization; 4.1 Heuristic Optimization; 4.2 Economic Basis; 4.3 Results; 4.4 Operating Optimization; 4.5 Optimum Pressure for Vacuum Columns 4.6 Conclusions Chapter 5: More Complex Distillation Systems; 5.1 Extractive Distillation; 5.2 Ethanol Dehydration; 5.3 Pressure-Swing Azeotropic Distillation; 5.4 Heat-Integrated Columns; 5.5 Conclusions; Chapter 6: Steady-State Calculations for Control Structure Selection; 6.1 Control Structure Alternatives; 6.2 Feed Composition Sensitivity Analysis (ZSA); 6.3 Temperature Control Tray Selection; 6.4 Conclusions; Reference; Chapter 7: Converting From Steady-State to Dynamic Simulation; 7.1 Equipment Sizing; 7.2 Exporting to Aspen Dynamics; 7.3 Opening the Dynamic Simulation in Aspen Dynamics 7.4 Installing Basic Controllers 7.5 Installing Temperature and Composition Controllers; 7.6 Performance Evaluation; 7.7 Conclusions; Chapter 8: Control of More Complex Columns; 8.1 Extractive Distillation Process; 8.2 Columns with Partial Condensers; 8.3 Control of Heat-Integrated Distillation Columns; 8.4 Control of Azeotropic Columns/Decanter System; 8.5 Unusual Control Structure; 8.6 Conclusions; References; Chapter 9: Reactive Distillation; 9.1 Introduction; 9.2 Types of Reactive Distillation Systems; 9.3 Tame Process Basics; 9.4 Tame Reaction Kinetics and Vle 9.5 Plantwide Control Structure 9.6 Conclusions; References; Chapter 10: Control of Sidestream Columns; 10.1 Liquid Sidestream Column; 10.2 Vapor Sidestream Column; 10.3 Liquid Sidestream Column with Stripper; 10.4 Vapor Sidestream Column with Rectifier; 10.5 Sidestream Purge Column; 10.6 Conclusions; Chapter 11: Control of Petroleum Fractionators; 11.1 Petroleum Fractions; 11.2 Characterization Crude Oil; 11.3 Steady-State Design of Preflash Column; 11.4 Control of Preflash Column; 11.5 Steady-State Design of Pipestill; 11.6 Control of Pipestill; 11.7 Conclusions; References Chapter 12: Divided-Wall (Petlyuk) Columns |
| Record Nr. | UNINA-9910141607903321 |
|
Luyben William L.
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| Hoboken, New Jersey : , : AlChE : , : Wiley, , 2013 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Distillation design and control using Aspen simulation / / William L. Luyben
| Distillation design and control using Aspen simulation / / William L. Luyben |
| Autore | Luyben William L. |
| Edizione | [Second edition.] |
| Pubbl/distr/stampa | Hoboken, New Jersey : , : AlChE : , : Wiley, , 2013 |
| Descrizione fisica | 1 online resource (742 p.) |
| Disciplina | 660/.28425 |
| Soggetto topico |
Distillation apparatus - Design and construction
Chemical process control - Simulation methods Petroleum - Refining |
| ISBN |
1-5231-1062-7
1-118-51019-4 1-118-51013-5 1-118-51009-7 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Cover; Title Page; Copyright; Dedication; Preface to the Second Edition; Preface to the First Edition; Chapter 1: Fundamentals of Vapor-Liquid-Equilibrium (VLE); 1.1 Vapor Pressure; 1.2 Binary VLE Phase Diagrams; 1.3 Physical Property Methods; 1.4 Relative Volatility; 1.5 Bubble Point Calculations; 1.6 Ternary Diagrams; 1.7 VLE Nonideality; 1.8 Residue Curves for Ternary Systems; 1.9 Distillation Boundaries; 1.10 Conclusions; Reference; Chapter 2: Analysis of Distillation Columns; 2.1 Design Degrees of Freedom; 2.2 Binary Mccabe-Thiele Method; 2.3 Approximate Multicomponent Methods
2.4 Conclusions Chapter 3: Setting Up a Steady-State Simulation; 3.1 Configuring a New Simulation; 3.2 Specifying Chemical Components and Physical Properties; 3.3 Specifying Stream Properties; 3.4 Specifying Parameters of Equipment; 3.5 Running the Simulation; 3.6 Using Design Spec/Vary Function; 3.7 Finding the Optimum Feed Tray and Minimum Conditions; 3.8 Column Sizing; 3.9 Conceptual Design; 3.10 Conclusions; Chapter 4: Distillation Economic Optimization; 4.1 Heuristic Optimization; 4.2 Economic Basis; 4.3 Results; 4.4 Operating Optimization; 4.5 Optimum Pressure for Vacuum Columns 4.6 Conclusions Chapter 5: More Complex Distillation Systems; 5.1 Extractive Distillation; 5.2 Ethanol Dehydration; 5.3 Pressure-Swing Azeotropic Distillation; 5.4 Heat-Integrated Columns; 5.5 Conclusions; Chapter 6: Steady-State Calculations for Control Structure Selection; 6.1 Control Structure Alternatives; 6.2 Feed Composition Sensitivity Analysis (ZSA); 6.3 Temperature Control Tray Selection; 6.4 Conclusions; Reference; Chapter 7: Converting From Steady-State to Dynamic Simulation; 7.1 Equipment Sizing; 7.2 Exporting to Aspen Dynamics; 7.3 Opening the Dynamic Simulation in Aspen Dynamics 7.4 Installing Basic Controllers 7.5 Installing Temperature and Composition Controllers; 7.6 Performance Evaluation; 7.7 Conclusions; Chapter 8: Control of More Complex Columns; 8.1 Extractive Distillation Process; 8.2 Columns with Partial Condensers; 8.3 Control of Heat-Integrated Distillation Columns; 8.4 Control of Azeotropic Columns/Decanter System; 8.5 Unusual Control Structure; 8.6 Conclusions; References; Chapter 9: Reactive Distillation; 9.1 Introduction; 9.2 Types of Reactive Distillation Systems; 9.3 Tame Process Basics; 9.4 Tame Reaction Kinetics and Vle 9.5 Plantwide Control Structure 9.6 Conclusions; References; Chapter 10: Control of Sidestream Columns; 10.1 Liquid Sidestream Column; 10.2 Vapor Sidestream Column; 10.3 Liquid Sidestream Column with Stripper; 10.4 Vapor Sidestream Column with Rectifier; 10.5 Sidestream Purge Column; 10.6 Conclusions; Chapter 11: Control of Petroleum Fractionators; 11.1 Petroleum Fractions; 11.2 Characterization Crude Oil; 11.3 Steady-State Design of Preflash Column; 11.4 Control of Preflash Column; 11.5 Steady-State Design of Pipestill; 11.6 Control of Pipestill; 11.7 Conclusions; References Chapter 12: Divided-Wall (Petlyuk) Columns |
| Record Nr. | UNINA-9910808123303321 |
|
Luyben William L.
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| Hoboken, New Jersey : , : AlChE : , : Wiley, , 2013 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Distillation design and control using Aspen simulation / / William L. Luyben
| Distillation design and control using Aspen simulation / / William L. Luyben |
| Autore | Luyben William L. |
| Pubbl/distr/stampa | Hoboken, New Jersey : , : Wiley-Interscience, , 2006 |
| Descrizione fisica | 1 online resource (361 p.) |
| Disciplina |
660.2842
660/.28425 |
| Soggetto topico |
Distillation apparatus - Design and construction
Chemical process control - Simulation methods |
| ISBN |
1-280-44809-1
9786610448098 0-470-36131-X 0-471-78525-3 1-61583-844-9 0-471-78524-5 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
DISTILLATION DESIGN AND CONTROL USING ASPENTM SIMULATION; CONTENTS; PREFACE; 1 FUNDAMENTALS OF VAPOR-LIQUID PHASE EQUILIBRIUM (VLE); 1.1 Vapor Pressure; 1.2 Binary VLE Phase Diagrams; 1.3 Physical Property Methods; 1.4 Relative Volatility; 1.5 Bubblepoint Calculations; 1.6 Ternary Diagrams; 1.7 VLE Nonideality; 1.8 Residue Curves for Ternary Systems; 1.9 Conclusion; 2 ANALYSIS OF DISTILLATION COLUMNS; 2.1 Design Degrees of Freedom; 2.2 Binary McCabe-Thiele Method; 2.3 Approximate Multicomponent Methods; 2.4 Analysis of Ternary Systems Using DISTIL; 2.5 Conclusion
3 SETTING UP A STEADY-STATE SIMULATION3.1 Configuring a New Simulation; 3.2 Specifying Chemical Components and Physical Properties; 3.3 Specifying Stream Properties; 3.4 Specifying Equipment Parameters; 3.5 Running the Simulation; 3.6 Using "Design Spec/Vary" Function; 3.7 Finding the Optimum Feed Tray and Minimum Conditions; 3.8 Column Sizing; 3.9 Conclusion; 4 DISTILLATION ECONOMIC OPTIMIZATION; 4.1 Heuristic Optimization; 4.2 Economic Basis; 4.3 Results; 4.4 Operating Optimization; 4.5 Conclusion; 5 MORE COMPLEX DISTILLATION SYSTEMS; 5.1 Methyl Acetate/Methanol/Water System 5.2 Ethanol Dehydration5.3 Heat-Integrated Columns; 5.4 Conclusion; 6 STEADY-STATE CALCULATIONS FOR CONTROL STRUCTURE SELECTION; 6.1 Summary of Methods; 6.2 Binary Propane/Isobutane System; 6.3 Ternary BTX System; 6.4 Multicomponent Hydrocarbon System; 6.5 Ternary Azeotropic System; 6.6 Conclusion; 7 CONVERTING FROM STEADY STATE TO DYNAMIC SIMULATION; 7.1 Equipment Sizing; 7.2 Exporting to Aspen Dynamics; 7.3 Opening the Dynamic Simulation in Aspen Dynamics; 7.4 Installing Basic Controllers; 7.5 Installing Temperature and Composition Controllers; 7.6 Performance Evaluation 7.7 Comparison with Economic Optimum Design7.8 Conclusion; 8 CONTROL OF MORE COMPLEX COLUMNS; 8.1 Methyl Acetate Column; 8.2 Columns with Partial Condensers; 8.3 Control of Heat-Integrated Distillation Columns; 8.4 Control of Azeotropic Columns/Decanter System; 8.5 Conclusion; 9 REACTIVE DISTILLATION; 9.1 Introduction; 9.2 Types of Reactive Distillation Systems; 9.3 TAME Process Basics; 9.4 TAME Reaction Kinetics and VLE; 9.5 Plantwide Control Structure; 9.6 Conclusion; 10 CONTROL OF SIDESTREAM COLUMNS; 10.1 Liquid Sidestream Column; 10.2 Vapor Sidestream Column 10.3 Liquid Sidestream Column with Stripper10.4 Vapor Sidestream Column with Rectifier; 10.5 Sidestream Purge Column; 10.6 Conclusion; 11 CONTROL OF PETROLEUM FRACTIONATORS; 11.1 Petroleum Fractions; 11.2 Characterization of Crude Oil; 11.3 Steady-State Design of PREFLASH Column; 11.4 Control of PREFLASH Column; 11.5 Steady-State Design of Pipestill; 11.6 Control of Pipestill; 11.7 Conclusion; INDEX |
| Record Nr. | UNISA-996202368903316 |
|
Luyben William L.
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| Hoboken, New Jersey : , : Wiley-Interscience, , 2006 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. di Salerno | ||
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Reactive distillation [[electronic resource] ] : status and future directions / / Kai Sundmacher and Achim Kienle (eds.)
| Reactive distillation [[electronic resource] ] : status and future directions / / Kai Sundmacher and Achim Kienle (eds.) |
| Pubbl/distr/stampa | Weinheim, : Wiley-VCH, c2003 |
| Descrizione fisica | 1 online resource (309 p.) |
| Disciplina |
660
660.28425 660/.28425 |
| Altri autori (Persone) |
SundmacherKai
KienleAchim |
| Soggetto topico |
Distillation
Distillation apparatus - Design and construction Reactivity (Chemistry) - Industrial applications |
| Soggetto genere / forma | Electronic books. |
| ISBN |
1-280-55826-1
9786610558261 3-527-60626-2 3-527-60052-3 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Reactive Distillation Status and Future Directions; Contents; Preface; List of Contributors; Part I Industrial Applications; 1 Industrial Applications of Reactive Distillation; 1.1 Introduction; 1.2 Etherification: MTBE, ETBE, and TAME; 1.3 Dimerization, Oligomerization, and Condensation; 1.4 Esterification: Methyl Acetate and Other Esters; 1.5 Hydrolysis of Esters; 1.6 Hydration; 1.7 Hydrogenation/Hydrodesulfurization/Hydrocracking; 1.7.1 Benzene to Cyclohexane; 1.7.2 Selective Hydrogenation of C(4) Stream; 1.7.3 Hydrogenation of Pentadiene; 1.7.4 C(4) Acetylene Conversion
1.7.5 Hydrodesulfurization, Hydrodenitrogenation, and Hydrocracking1.7.6 Miscellaneous Hydrogenations; 1.8 Chlorination; 1.9 Acetalization/Ketalization; 1.10 Recovery and Purification of Chemicals; 1.11 Difficult Separations; 1.12 Chemical Heat Pumps; 1.13 RD with Supercritical Fluids; 1.14 Conclusions; 2 Reactive Distillation Process Development in the Chemical Process Industries; 2.1 Introduction; 2.2 Process Synthesis; 2.3 Process Design and Optimization; 2.4 Limitations of the Methods for Synthesis and Design: the Scale-Up Problem; 2.5 Choice of Equipment 2.6 Some Remarks on the Role of Catalysis2.7 Conclusions; 2.8 Acknowledgments; 2.9 Notation; 3 Application of Reactive Distillation and Strategies in Process Design; 3.1 Introduction; 3.2 Challenges in Process Design for Reactive Distillation; 3.2.1 Feasibility Analysis; 3.2.2 Catalyst and Hardware Selection; 3.2.3 Column Scale-Up; 3.3 MTBE Decomposition via Reactive Distillation; 3.3.1 Conceptual Design; 3.3.2 Model Development; 3.3.2.1 Catalyst Selection and Reaction Kinetics; 3.3.2.2 Phase Equilibrium Model; 3.3.2.3 Steady-State Simulation; 3.3.3 Lab-Scale Experiments 3.3.4 Pilot-Plant Experiments3.4 Conclusions; Part II Physicochemical Fundamentals; 4 Thermodynamics of Reactive Separations; 4.1 Introduction; 4.2 Process Models for Reactive Distillation; 4.2.1 Outline; 4.2.2 Case Study: Methyl Acetate; 4.3 Equilibrium Thermodynamics of Reacting Multiphase Mixtures; 4.4 Fluid Property Models for Reactive Distillation; 4.4.1 Outline; 4.4.2 Examples; 4.4.2.1 Hexyl Acetate: Sensitivity Analysis; 4.4.2.2 Methyl Acetate: Prediction of Polynary Vapor-Liquid Equilibria; 4.4.2.3 Butyl Acetate: Thermodynamic Consistency 4.4.2.4 Ethyl Acetate: Consequences of Inconsistency4.4.2.5 Formaldehyde + Water + Methanol: Intrinsically Reactive Complex Mixture; 4.5 Experimental Studies of Phase Equilibria in Reacting Systems; 4.5.1 Outline; 4.5.2 Reactive Vapor-Liquid Equilibria; 4.5.2.1 Batch Experiments; 4.5.2.2 Flow Experiments; 4.5.2.3 Recirculation Experiments; 4.6 Conclusions; 4.7 Acknowledgments; 4.8 Notation; 5 Importance of Reaction Kinetics for Catalytic Distillation Processes; 5.1 Introduction; 5.2 Reactive Ideal Binary Mixtures; 5.2.1 Reaction-Distillation Process with External Recycling 5.2.1.1 (,)-Analysis |
| Record Nr. | UNINA-9910146239603321 |
| Weinheim, : Wiley-VCH, c2003 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Reactive distillation [[electronic resource] ] : status and future directions / / Kai Sundmacher and Achim Kienle (eds.)
| Reactive distillation [[electronic resource] ] : status and future directions / / Kai Sundmacher and Achim Kienle (eds.) |
| Pubbl/distr/stampa | Weinheim, : Wiley-VCH, c2003 |
| Descrizione fisica | 1 online resource (309 p.) |
| Disciplina |
660
660.28425 660/.28425 |
| Altri autori (Persone) |
SundmacherKai
KienleAchim |
| Soggetto topico |
Distillation
Distillation apparatus - Design and construction Reactivity (Chemistry) - Industrial applications |
| ISBN |
1-280-55826-1
9786610558261 3-527-60626-2 3-527-60052-3 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Reactive Distillation Status and Future Directions; Contents; Preface; List of Contributors; Part I Industrial Applications; 1 Industrial Applications of Reactive Distillation; 1.1 Introduction; 1.2 Etherification: MTBE, ETBE, and TAME; 1.3 Dimerization, Oligomerization, and Condensation; 1.4 Esterification: Methyl Acetate and Other Esters; 1.5 Hydrolysis of Esters; 1.6 Hydration; 1.7 Hydrogenation/Hydrodesulfurization/Hydrocracking; 1.7.1 Benzene to Cyclohexane; 1.7.2 Selective Hydrogenation of C(4) Stream; 1.7.3 Hydrogenation of Pentadiene; 1.7.4 C(4) Acetylene Conversion
1.7.5 Hydrodesulfurization, Hydrodenitrogenation, and Hydrocracking1.7.6 Miscellaneous Hydrogenations; 1.8 Chlorination; 1.9 Acetalization/Ketalization; 1.10 Recovery and Purification of Chemicals; 1.11 Difficult Separations; 1.12 Chemical Heat Pumps; 1.13 RD with Supercritical Fluids; 1.14 Conclusions; 2 Reactive Distillation Process Development in the Chemical Process Industries; 2.1 Introduction; 2.2 Process Synthesis; 2.3 Process Design and Optimization; 2.4 Limitations of the Methods for Synthesis and Design: the Scale-Up Problem; 2.5 Choice of Equipment 2.6 Some Remarks on the Role of Catalysis2.7 Conclusions; 2.8 Acknowledgments; 2.9 Notation; 3 Application of Reactive Distillation and Strategies in Process Design; 3.1 Introduction; 3.2 Challenges in Process Design for Reactive Distillation; 3.2.1 Feasibility Analysis; 3.2.2 Catalyst and Hardware Selection; 3.2.3 Column Scale-Up; 3.3 MTBE Decomposition via Reactive Distillation; 3.3.1 Conceptual Design; 3.3.2 Model Development; 3.3.2.1 Catalyst Selection and Reaction Kinetics; 3.3.2.2 Phase Equilibrium Model; 3.3.2.3 Steady-State Simulation; 3.3.3 Lab-Scale Experiments 3.3.4 Pilot-Plant Experiments3.4 Conclusions; Part II Physicochemical Fundamentals; 4 Thermodynamics of Reactive Separations; 4.1 Introduction; 4.2 Process Models for Reactive Distillation; 4.2.1 Outline; 4.2.2 Case Study: Methyl Acetate; 4.3 Equilibrium Thermodynamics of Reacting Multiphase Mixtures; 4.4 Fluid Property Models for Reactive Distillation; 4.4.1 Outline; 4.4.2 Examples; 4.4.2.1 Hexyl Acetate: Sensitivity Analysis; 4.4.2.2 Methyl Acetate: Prediction of Polynary Vapor-Liquid Equilibria; 4.4.2.3 Butyl Acetate: Thermodynamic Consistency 4.4.2.4 Ethyl Acetate: Consequences of Inconsistency4.4.2.5 Formaldehyde + Water + Methanol: Intrinsically Reactive Complex Mixture; 4.5 Experimental Studies of Phase Equilibria in Reacting Systems; 4.5.1 Outline; 4.5.2 Reactive Vapor-Liquid Equilibria; 4.5.2.1 Batch Experiments; 4.5.2.2 Flow Experiments; 4.5.2.3 Recirculation Experiments; 4.6 Conclusions; 4.7 Acknowledgments; 4.8 Notation; 5 Importance of Reaction Kinetics for Catalytic Distillation Processes; 5.1 Introduction; 5.2 Reactive Ideal Binary Mixtures; 5.2.1 Reaction-Distillation Process with External Recycling 5.2.1.1 (,)-Analysis |
| Record Nr. | UNINA-9910830995803321 |
| Weinheim, : Wiley-VCH, c2003 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
Reactive distillation [[electronic resource] ] : status and future directions / / Kai Sundmacher and Achim Kienle (eds.)
| Reactive distillation [[electronic resource] ] : status and future directions / / Kai Sundmacher and Achim Kienle (eds.) |
| Pubbl/distr/stampa | Weinheim, : Wiley-VCH, c2003 |
| Descrizione fisica | 1 online resource (309 p.) |
| Disciplina |
660
660.28425 660/.28425 |
| Altri autori (Persone) |
SundmacherKai
KienleAchim |
| Soggetto topico |
Distillation
Distillation apparatus - Design and construction Reactivity (Chemistry) - Industrial applications |
| ISBN |
1-280-55826-1
9786610558261 3-527-60626-2 3-527-60052-3 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
Reactive Distillation Status and Future Directions; Contents; Preface; List of Contributors; Part I Industrial Applications; 1 Industrial Applications of Reactive Distillation; 1.1 Introduction; 1.2 Etherification: MTBE, ETBE, and TAME; 1.3 Dimerization, Oligomerization, and Condensation; 1.4 Esterification: Methyl Acetate and Other Esters; 1.5 Hydrolysis of Esters; 1.6 Hydration; 1.7 Hydrogenation/Hydrodesulfurization/Hydrocracking; 1.7.1 Benzene to Cyclohexane; 1.7.2 Selective Hydrogenation of C(4) Stream; 1.7.3 Hydrogenation of Pentadiene; 1.7.4 C(4) Acetylene Conversion
1.7.5 Hydrodesulfurization, Hydrodenitrogenation, and Hydrocracking1.7.6 Miscellaneous Hydrogenations; 1.8 Chlorination; 1.9 Acetalization/Ketalization; 1.10 Recovery and Purification of Chemicals; 1.11 Difficult Separations; 1.12 Chemical Heat Pumps; 1.13 RD with Supercritical Fluids; 1.14 Conclusions; 2 Reactive Distillation Process Development in the Chemical Process Industries; 2.1 Introduction; 2.2 Process Synthesis; 2.3 Process Design and Optimization; 2.4 Limitations of the Methods for Synthesis and Design: the Scale-Up Problem; 2.5 Choice of Equipment 2.6 Some Remarks on the Role of Catalysis2.7 Conclusions; 2.8 Acknowledgments; 2.9 Notation; 3 Application of Reactive Distillation and Strategies in Process Design; 3.1 Introduction; 3.2 Challenges in Process Design for Reactive Distillation; 3.2.1 Feasibility Analysis; 3.2.2 Catalyst and Hardware Selection; 3.2.3 Column Scale-Up; 3.3 MTBE Decomposition via Reactive Distillation; 3.3.1 Conceptual Design; 3.3.2 Model Development; 3.3.2.1 Catalyst Selection and Reaction Kinetics; 3.3.2.2 Phase Equilibrium Model; 3.3.2.3 Steady-State Simulation; 3.3.3 Lab-Scale Experiments 3.3.4 Pilot-Plant Experiments3.4 Conclusions; Part II Physicochemical Fundamentals; 4 Thermodynamics of Reactive Separations; 4.1 Introduction; 4.2 Process Models for Reactive Distillation; 4.2.1 Outline; 4.2.2 Case Study: Methyl Acetate; 4.3 Equilibrium Thermodynamics of Reacting Multiphase Mixtures; 4.4 Fluid Property Models for Reactive Distillation; 4.4.1 Outline; 4.4.2 Examples; 4.4.2.1 Hexyl Acetate: Sensitivity Analysis; 4.4.2.2 Methyl Acetate: Prediction of Polynary Vapor-Liquid Equilibria; 4.4.2.3 Butyl Acetate: Thermodynamic Consistency 4.4.2.4 Ethyl Acetate: Consequences of Inconsistency4.4.2.5 Formaldehyde + Water + Methanol: Intrinsically Reactive Complex Mixture; 4.5 Experimental Studies of Phase Equilibria in Reacting Systems; 4.5.1 Outline; 4.5.2 Reactive Vapor-Liquid Equilibria; 4.5.2.1 Batch Experiments; 4.5.2.2 Flow Experiments; 4.5.2.3 Recirculation Experiments; 4.6 Conclusions; 4.7 Acknowledgments; 4.8 Notation; 5 Importance of Reaction Kinetics for Catalytic Distillation Processes; 5.1 Introduction; 5.2 Reactive Ideal Binary Mixtures; 5.2.1 Reaction-Distillation Process with External Recycling 5.2.1.1 (,)-Analysis |
| Record Nr. | UNINA-9910841154403321 |
| Weinheim, : Wiley-VCH, c2003 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
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Reactive distillation design and control [[electronic resource] /] / William L. Luyben, Cheng-Ching Yu
| Reactive distillation design and control [[electronic resource] /] / William L. Luyben, Cheng-Ching Yu |
| Autore | Luyben William L |
| Pubbl/distr/stampa | Hoboken, NJ, : John Wiley, c2008 |
| Descrizione fisica | 1 online resource (598 p.) |
| Disciplina |
660
660.28425 660/.28425 |
| Altri autori (Persone) | YuCheng-Ching <1956-> |
| Soggetto topico |
Distillation apparatus - Design and construction
Chemical process control Distillation Reactivity (Chemistry) |
| ISBN |
1-282-11265-1
9786612112652 0-470-37774-7 0-470-37779-8 |
| Formato | Materiale a stampa |
| Livello bibliografico | Monografia |
| Lingua di pubblicazione | eng |
| Nota di contenuto |
REACTIVE DISTILLATION DESIGN AND CONTROL; CONTENTS; PREFACE; 1 INTRODUCTION; 1.1 History; 1.2 Basics of Reactive Distillation; 1.3 Neat Operation Versus Excess Reactant; 1.4 Limitations; 1.4.1 Temperature Mismatch; 1.4.2 Unfavorable Volatilities; 1.4.3 Slow Reaction Rates; 1.4.4 Other Restrictions; 1.5 Scope; 1.6 Computational Methods; 1.6.1 Matlab Programs for Steady-State Design; 1.6.2 Aspen Simulations; 1.7 Reference Materials; PART I STEADY-STATE DESIGN OF IDEAL QUATERNARY SYSTEM; 2 PARAMETER EFFECTS; 2.1 Effect of Holdup on Reactive Trays; 2.2 Effect of Number of Reactive Trays
2.3 Effect of Pressure2.4 Effect of Chemical Equilibrium Constant; 2.5 Effect of Relative Volatilities; 2.5.1 Constant Relative Volatilities; 2.5.2 Temperature-Dependent Relative Volatilities; 2.6 Effect of Number of Stripping and Rectifying Trays; 2.7 Effect of Reactant Feed Location; 2.7.1 Reactant A Feed Location (N(FA)); 2.7.2 Reactant B Feed Location (N(FB)); 2.8 Conclusion; 3 ECONOMIC COMPARISON OF REACTIVE DISTILLATION WITH A CONVENTIONAL PROCESS; 3.1 Conventional Multiunit Process; 3.1.1 Assumptions and Specifications; 3.1.2 Steady-State Design Procedure 3.1.3 Sizing and Economic Equations3.2 Reactive Distillation Design; 3.2.1 Assumptions and Specifications; 3.2.2 Steady-State Design Procedure; 3.3 Results for Different Chemical Equilibrium Constants; 3.3.1 Conventional Process; 3.3.2 Reactive Distillation Process; 3.3.3 Comparisons; 3.4 Results for Temperature-Dependent Relative Volatilities; 3.4.1 Relative Volatilities; 3.4.2 Optimum Steady-State Designs; 3.4.3 Real Chemical Systems; 3.5 Conclusion; 4 NEAT OPERATION VERSUS USING EXCESS REACTANT; 4.1 Introduction; 4.2 Neat Reactive Column; 4.3 Two-Column System with Excess B 4.3.1 20% Excess B Case4.3.2 10% Excess B Case; 4.4 Two-Column System with 20% Excess of A; 4.5 Economic Comparison; 4.6 Conclusion; PART II STEADY-STATE DESIGN OF OTHER IDEAL SYSTEMS; 5 TERNARY REACTIVE DISTILLATION SYSTEMS; 5.1 Ternary System Without Inerts; 5.1.1 Column Configuration; 5.1.2 Chemistry and Phase Equilibrium Parameters; 5.1.3 Design Parameters and Procedure; 5.1.4 Effect of Pressure; 5.1.5 Holdup on Reactive Trays; 5.1.6 Number of Reactive Trays; 5.1.7 Number of Stripping Trays; 5.2 Ternary System With Inerts; 5.2.1 Column Configuration 5.2.2 Chemistry and Phase Equilibrium Parameters5.2.3 Design Parameters and Procedure; 5.2.4 Effect of Pressure; 5.2.5 Control Tray Composition; 5.2.6 Reactive Tray Holdup; 5.2.7 Effect of Reflux; 5.2.8 Chemical Equilibrium Constant; 5.2.9 Feed Composition; 5.2.10 Number of Reactive Trays; 5.2.11 Number of Rectifying and Stripping Trays; 5.3 Conclusion; 6 TERNARY DECOMPOSITION REACTION; 6.1 Ternary Decomposition Reaction: Intermediate-Boiling Reactant; 6.1.1 Column Configuration; 6.1.2 Chemistry and Phase Equilibrium Parameters; 6.1.3 Design Parameters and Procedure 6.1.4 Holdup on Reactive Trays |
| Record Nr. | UNINA-9910145955003321 |
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Luyben William L
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| Hoboken, NJ, : John Wiley, c2008 | ||
| Materiale a stampa | ||
| Lo trovi qui: Univ. Federico II | ||
| ||
