Materials and man's needs [[electronic resource] ] : materials science and engineering; summary report |
Pubbl/distr/stampa | Washington, : National Academy of Sciences, 1974 |
Descrizione fisica | 1 online resource (247 p.) |
Disciplina | 620.1/1 |
Collana | Publication |
Soggetto topico |
Materials
Materials - Research |
ISBN |
1-280-24620-0
9786610246205 0-309-57403-X |
Formato | Materiale a stampa ![]() |
Livello bibliografico | Monografia |
Lingua di pubblicazione | eng |
Record Nr. | UNINA-9910826053703321 |
Washington, : National Academy of Sciences, 1974 | ||
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Lo trovi qui: Univ. Federico II | ||
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Materials and structures |
Pubbl/distr/stampa | London : , : E. & F.N. Spon, , 1992- |
Descrizione fisica | 1 online resource |
Disciplina | 620.1/1 |
Soggetto topico |
Dwellings - Remodeling
Materials - Testing Concrete - Testing Testing laboratories |
Soggetto genere / forma |
Handbooks and manuals.
Periodicals. |
Soggetto non controllato |
materialen
materials beton concrete fractals reologische eigenschappen rheological properties treksterkte tensile strength fysische eigenschappen physical properties engineering Physics (General) Mechanical and Electronic Engineering Fysica (algemeen) Werktuigbouwkunde en elektrotechniek |
ISSN | 1871-6873 |
Formato | Materiale a stampa ![]() |
Livello bibliografico | Periodico |
Lingua di pubblicazione | eng |
Record Nr. | UNINA-9910135464403321 |
London : , : E. & F.N. Spon, , 1992- | ||
![]() | ||
Lo trovi qui: Univ. Federico II | ||
|
Materials and structures |
Pubbl/distr/stampa | London : , : E. & F.N. Spon, , 1992- |
Descrizione fisica | 1 online resource |
Disciplina | 620.1/1 |
Soggetto topico |
Dwellings - Remodeling
Materials - Testing Concrete - Testing Testing laboratories |
Soggetto genere / forma |
Handbooks and manuals.
Periodicals. |
Soggetto non controllato |
materialen
materials beton concrete fractals reologische eigenschappen rheological properties treksterkte tensile strength fysische eigenschappen physical properties engineering Physics (General) Mechanical and Electronic Engineering Fysica (algemeen) Werktuigbouwkunde en elektrotechniek |
ISSN | 1871-6873 |
Formato | Materiale a stampa ![]() |
Livello bibliografico | Periodico |
Lingua di pubblicazione | eng |
Record Nr. | UNISA-996204168203316 |
London : , : E. & F.N. Spon, , 1992- | ||
![]() | ||
Lo trovi qui: Univ. di Salerno | ||
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Materials characterization [[electronic resource] ] : introduction to microscopic and spectroscopic methods / / Yang Leng |
Autore | Leng Y (Yang) |
Edizione | [2nd ed.] |
Pubbl/distr/stampa | Weinheim, : J. Wiley, c2013 |
Descrizione fisica | xiv, 376 p. : ill |
Disciplina | 620.1/1 |
Soggetto topico |
Materials - Analysis
Materials |
ISBN |
9783527670802
3527670807 9783527670772 |
Classificazione |
501.4
620.11 |
Formato | Materiale a stampa ![]() |
Livello bibliografico | Monografia |
Lingua di pubblicazione | eng |
Record Nr. | UNINA-9910796092403321 |
Leng Y (Yang)
![]() |
||
Weinheim, : J. Wiley, c2013 | ||
![]() | ||
Lo trovi qui: Univ. Federico II | ||
|
Materials characterization : introduction to microscopic and spectroscopic methods / / Yang Leng |
Autore | Leng Y (Yang) |
Edizione | [2nd ed.] |
Pubbl/distr/stampa | Weinheim, : J. Wiley, c2013 |
Descrizione fisica | xiv, 376 p. : ill |
Disciplina | 620.1/1 |
Soggetto topico |
Materials - Analysis
Materials |
ISBN |
9783527670802
3527670807 9783527670772 |
Classificazione |
501.4
620.11 |
Formato | Materiale a stampa ![]() |
Livello bibliografico | Monografia |
Lingua di pubblicazione | eng |
Nota di contenuto |
Intro -- Materials Characterization -- Contents -- 1 Light Microscopy -- 1.1 Optical Principles -- 1.1.1 Image Formation -- 1.1.2 Resolution -- 1.1.2.1 Effective Magnification -- 1.1.2.2 Brightness and Contrast -- 1.1.3 Depth of Field -- 1.1.4 Aberrations -- 1.2 Instrumentation -- 1.2.1 Illumination System -- 1.2.2 Objective Lens and Eyepiece -- 1.2.2.1 Steps for Optimum Resolution -- 1.2.2.2 Steps to Improve Depth of Field -- 1.3 Specimen Preparation -- 1.3.1 Sectioning -- 1.3.1.1 Cutting -- 1.3.1.2 Microtomy -- 1.3.2 Mounting -- 1.3.3 Grinding and Polishing -- 1.3.3.1 Grinding -- 1.3.3.2 Polishing -- 1.3.4 Etching -- 1.4 Imaging Modes -- 1.4.1 Bright-Field and Dark-Field Imaging -- 1.4.2 Phase-Contrast Microscopy -- 1.4.3 Polarized-Light Microscopy -- 1.4.4 Nomarski Microscopy -- 1.4.5 Fluorescence Microscopy -- 1.5 Confocal Microscopy -- 1.5.1 Working Principles -- 1.5.2 Three-Dimensional Images -- References -- Further Reading -- 2 X-Ray Diffraction Methods -- 2.1 X-Ray Radiation -- 2.1.1 Generation of X-Rays -- 2.1.2 X-Ray Absorption -- 2.2 Theoretical Background of Diffraction -- 2.2.1 Diffraction Geometry -- 2.2.1.1 Bragg's Law -- 2.2.1.2 Reciprocal Lattice -- 2.2.1.3 Ewald Sphere -- 2.2.2 Diffraction Intensity -- 2.2.2.1 Structure Extinction -- 2.3 X-Ray Diffractometry -- 2.3.1 Instrumentation -- 2.3.1.1 System Aberrations -- 2.3.2 Samples and Data Acquisition -- 2.3.2.1 Sample Preparation -- 2.3.2.2 Acquisition and Treatment of Diffraction Data -- 2.3.3 Distortions of Diffraction Spectra -- 2.3.3.1 Preferential Orientation -- 2.3.3.2 Crystallite Size -- 2.3.3.3 Residual Stress -- 2.3.4 Applications -- 2.3.4.1 Crystal-Phase Identification -- 2.3.4.2 Quantitative Measurement -- 2.4 Wide-Angle X-Ray Diffraction and Scattering -- 2.4.1 Wide-Angle Diffraction -- 2.4.2 Wide-Angle Scattering -- References -- Further Reading.
3 Transmission Electron Microscopy -- 3.1 Instrumentation -- 3.1.1 Electron Sources -- 3.1.1.1 Thermionic Emission Gun -- 3.1.1.2 Field Emission Gun -- 3.1.2 Electromagnetic Lenses -- 3.1.3 Specimen Stage -- 3.2 Specimen Preparation -- 3.2.1 Prethinning -- 3.2.2 Final Thinning -- 3.2.2.1 Electrolytic Thinning -- 3.2.2.2 Ion Milling -- 3.2.2.3 Ultramicrotomy -- 3.3 Image Modes -- 3.3.1 Mass-Density Contrast -- 3.3.2 Diffraction Contrast -- 3.3.3 Phase Contrast -- 3.3.3.1 Theoretical Aspects -- 3.3.3.2 Two-Beam and Multiple-Beam Imaging -- 3.4 Selected-Area Diffraction (SAD) -- 3.4.1 Selected-Area Diffraction Characteristics -- 3.4.2 Single-Crystal Diffraction -- 3.4.2.1 Indexing a Cubic Crystal Pattern -- 3.4.2.2 Identification of Crystal Phases -- 3.4.3 Multicrystal Diffraction -- 3.4.4 Kikuchi Lines -- 3.5 Images of Crystal Defects -- 3.5.1 Wedge Fringe -- 3.5.2 Bending Contours -- 3.5.3 Dislocations -- References -- Further Reading -- 4 Scanning Electron Microscopy -- 4.1 Instrumentation -- 4.1.1 Optical Arrangement -- 4.1.2 Signal Detection -- 4.1.2.1 Detector -- 4.1.3 Probe Size and Current -- 4.2 Contrast Formation -- 4.2.1 Electron-Specimen Interactions -- 4.2.2 Topographic Contrast -- 4.2.3 Compositional Contrast -- 4.3 Operational Variables -- 4.3.1 Working Distance and Aperture Size -- 4.3.2 Acceleration Voltage and Probe Current -- 4.3.3 Astigmatism -- 4.4 Specimen Preparation -- 4.4.1 Preparation for Topographic Examination -- 4.4.1.1 Charging and Its Prevention -- 4.4.2 Preparation for Microcomposition Examination -- 4.4.3 Dehydration -- 4.5 Electron Backscatter Diffraction -- 4.5.1 EBSD Pattern Formation -- 4.5.2 EBSD Indexing and Its Automation -- 4.5.3 Applications of EBSD -- 4.6 Environmental SEM -- 4.6.1 ESEM Working Principle -- 4.6.2 Applications -- References -- Further Reading -- 5 Scanning Probe Microscopy -- 5.1 Instrumentation. 5.1.1 Probe and Scanner -- 5.1.2 Control and Vibration Isolation -- 5.2 Scanning Tunneling Microscopy -- 5.2.1 Tunneling Current -- 5.2.2 Probe Tips and Working Environments -- 5.2.3 Operational Modes -- 5.2.4 Typical Applications -- 5.3 Atomic Force Microscopy -- 5.3.1 Near-Field Forces -- 5.3.1.1 Short-Range Forces -- 5.3.1.2 van der Waals Forces -- 5.3.1.3 Electrostatic Forces -- 5.3.1.4 Capillary Forces -- 5.3.2 Force Sensors -- 5.3.3 Operational Modes -- 5.3.3.1 Static Contact Modes -- 5.3.3.2 Lateral Force Microscopy -- 5.3.3.3 Dynamic Operational Modes -- 5.3.4 Typical Applications -- 5.3.4.1 Static Mode -- 5.3.4.2 Dynamic Noncontact Mode -- 5.3.4.3 Tapping Mode -- 5.3.4.4 Force Modulation -- 5.4 Image Artifacts -- 5.4.1 Tip -- 5.4.2 Scanner -- 5.4.3 Vibration and Operation -- References -- Further Reading -- 6 X-Ray Spectroscopy for Elemental Analysis -- 6.1 Features of Characteristic X-Rays -- 6.1.1 Types of Characteristic X-Rays -- 6.1.1.1 Selection Rules -- 6.1.2 Comparison of K, L, and M Series -- 6.2 X-Ray Fluorescence Spectrometry -- 6.2.1 Wavelength Dispersive Spectroscopy -- 6.2.1.1 Analyzing Crystal -- 6.2.1.2 Wavelength Dispersive Spectra -- 6.2.2 Energy Dispersive Spectroscopy -- 6.2.2.1 Detector -- 6.2.2.2 Energy Dispersive Spectra -- 6.2.2.3 Advances in Energy Dispersive Spectroscopy -- 6.2.3 XRF Working Atmosphere and Sample Preparation -- 6.3 Energy Dispersive Spectroscopy in Electron Microscopes -- 6.3.1 Special Features -- 6.3.2 Scanning Modes -- 6.4 Qualitative and Quantitative Analysis -- 6.4.1 Qualitative Analysis -- 6.4.2 Quantitative Analysis -- 6.4.2.1 Quantitative Analysis by X-Ray Fluorescence -- 6.4.2.2 Fundamental Parameter Method -- 6.4.2.3 Quantitative Analysis in Electron Microscopy -- References -- Further Reading -- 7 Electron Spectroscopy for Surface Analysis -- 7.1 Basic Principles. 7.1.1 X-Ray Photoelectron Spectroscopy -- 7.1.2 Auger Electron Spectroscopy -- 7.2 Instrumentation -- 7.2.1 Ultrahigh Vacuum System -- 7.2.2 Source Guns -- 7.2.2.1 X-Ray Gun -- 7.2.2.2 Electron Gun -- 7.2.2.3 Ion Gun -- 7.2.3 Electron Energy Analyzers -- 7.3 Characteristics of Electron Spectra -- 7.3.1 Photoelectron Spectra -- 7.3.2 Auger Electron Spectra -- 7.4 Qualitative and Quantitative Analysis -- 7.4.1 Qualitative Analysis -- 7.4.1.1 Peak Identification -- 7.4.1.2 Chemical Shifts -- 7.4.1.3 Problems with Insulating Materials -- 7.4.2 Quantitative Analysis -- 7.4.2.1 Peaks and Sensitivity Factors -- 7.4.3 Composition Depth Profiling -- References -- Further Reading -- 8 Secondary Ion Mass Spectrometry for Surface Analysis -- 8.1 Basic Principles -- 8.1.1 Secondary Ion Generation -- 8.1.2 Dynamic and Static SIMS -- 8.2 Instrumentation -- 8.2.1 Primary Ion System -- 8.2.1.1 Ion Sources -- 8.2.1.2 Wien Filter -- 8.2.2 Mass Analysis System -- 8.2.2.1 Magnetic Sector Analyzer -- 8.2.2.2 Quadrupole Mass Analyzer -- 8.2.2.3 Time-of-Flight Analyzer -- 8.3 Surface Structure Analysis -- 8.3.1 Experimental Aspects -- 8.3.1.1 Primary Ions -- 8.3.1.2 Flood Gun -- 8.3.1.3 Sample Handling -- 8.3.2 Spectrum Interpretation -- 8.3.2.1 Element Identification -- 8.4 SIMS Imaging -- 8.4.1 Generation of SIMS Images -- 8.4.2 Image Quality -- 8.5 SIMS Depth Profiling -- 8.5.1 Generation of Depth Profiles -- 8.5.2 Optimization of Depth Profiling -- 8.5.2.1 Primary Beam Energy -- 8.5.2.2 Incident Angle of Primary Beam -- 8.5.2.3 Analysis Area -- References -- 9 Vibrational Spectroscopy for Molecular Analysis -- 9.1 Theoretical Background -- 9.1.1 Electromagnetic Radiation -- 9.1.2 Origin of Molecular Vibrations -- 9.1.3 Principles of Vibrational Spectroscopy -- 9.1.3.1 Infrared Absorption -- 9.1.3.2 Raman Scattering -- 9.1.4 Normal Mode of Molecular Vibrations. 9.1.4.1 Number of Normal Vibration Modes -- 9.1.4.2 Classification of Normal Vibration Modes -- 9.1.5 Infrared and Raman Activity -- 9.1.5.1 Infrared Activity -- 9.1.5.2 Raman Activity -- 9.2 Fourier Transform Infrared Spectroscopy -- 9.2.1 Working Principles -- 9.2.2 Instrumentation -- 9.2.2.1 Infrared Light Source -- 9.2.2.2 Beamsplitter -- 9.2.2.3 Infrared Detector -- 9.2.2.4 Fourier Transform Infrared Spectra -- 9.2.3 Examination Techniques -- 9.2.3.1 Transmittance -- 9.2.3.2 Solid Sample Preparation -- 9.2.3.3 Liquid and Gas Sample Preparation -- 9.2.3.4 Reflectance -- 9.2.4 Fourier Transform Infrared Microspectroscopy -- 9.2.4.1 Instrumentation -- 9.2.4.2 Applications -- 9.3 Raman Microscopy -- 9.3.1 Instrumentation -- 9.3.1.1 Laser Source -- 9.3.1.2 Microscope System -- 9.3.1.3 Prefilters -- 9.3.1.4 Diffraction Grating -- 9.3.1.5 Detector -- 9.3.2 Fluorescence Problem -- 9.3.3 Raman Imaging -- 9.3.4 Applications -- 9.3.4.1 Phase Identification -- 9.3.4.2 Polymer Identification -- 9.3.4.3 Composition Determination -- 9.3.4.4 Determination of Residual Strain -- 9.3.4.5 Determination of Crystallographic Orientation -- 9.4 Interpretation of Vibrational Spectra -- 9.4.1 Qualitative Methods -- 9.4.1.1 Spectrum Comparison -- 9.4.1.2 Identifying Characteristic Bands -- 9.4.1.3 Band Intensities -- 9.4.2 Quantitative Methods -- 9.4.2.1 Quantitative Analysis of Infrared Spectra -- 9.4.2.2 Quantitative Analysis of Raman Spectra -- References -- Further Reading -- 10 Thermal Analysis -- 10.1 Common Characteristics -- 10.1.1 Thermal Events -- 10.1.1.1 Enthalpy Change -- 10.1.2 Instrumentation -- 10.1.3 Experimental Parameters -- 10.2 Differential Thermal Analysis and Differential Scanning Calorimetry -- 10.2.1 Working Principles -- 10.2.1.1 Differential Thermal Analysis -- 10.2.1.2 Differential Scanning Calorimetry. 10.2.1.3 Temperature-Modulated Differential Scanning Calorimetry. |
Record Nr. | UNINA-9910822761803321 |
Leng Y (Yang)
![]() |
||
Weinheim, : J. Wiley, c2013 | ||
![]() | ||
Lo trovi qui: Univ. Federico II | ||
|
Materials characterization [[electronic resource] ] : introduction to microscopic and spectroscopic methods / / Yang Leng |
Autore | Leng Y (Yang) |
Pubbl/distr/stampa | Singapore ; ; Hoboken, NJ, : J. Wiley, c2008 |
Descrizione fisica | 1 online resource (351 p.) |
Disciplina |
620.1/1
620.11 620.1127 |
Soggetto topico |
Materials
Materials - Analysis |
ISBN |
9786612031403
0-470-82299-6 0-470-82300-3 |
Formato | Materiale a stampa ![]() |
Livello bibliografico | Monografia |
Lingua di pubblicazione | eng |
Nota di contenuto |
MATERIALS CHARACTERIZATION Introduction to Microscopic and Spectroscopic Methods; Contents; Preface; 1 Light Microscopy; 1.1 Optical Principles; 1.1.1 Image Formation; 1.1.2 Resolution; 1.1.3 Depth of Field; 1.1.4 Aberrations; 1.2 Instrumentation; 1.2.1 Illumination System; 1.2.2 Objective Lens and Eyepiece; 1.3 Specimen Preparation; 1.3.1 Sectioning; 1.3.2 Mounting; 1.3.3 Grinding and Polishing; 1.3.4 Etching; 1.4 Imaging Modes; 1.4.1 Bright-Field and Dark-Field Imaging; 1.4.2 Phase Contrast Microscopy; 1.4.3 Polarized Light Microscopy; 1.4.4 Nomarski Microscopy
1.4.5 Fluorescence Microscopy1.5 Confocal Microscopy; 1.5.1 Working Principles; 1.5.2 Three-Dimensional Images; References; Questions; 2 X-ray Diffraction Methods; 2.1 X-ray Radiation; 2.1.1 Generation of X-rays; 2.1.2 X-ray Absorption; 2.2 Theoretical Background of Diffraction; 2.2.1 Diffraction Geometry; 2.2.2 Diffraction Intensity; 2.3 X-ray Diffractometry; 2.3.1 Instrumentation; 2.3.2 Samples and Data Acquisition; 2.3.3 Distortions of Diffraction Spectra; 2.3.4 Applications; 2.4 Wide Angle X-ray Diffraction and Scattering; 2.4.1 Wide Angle Diffraction; 2.4.2 Wide Angle Scattering ReferencesQuestions; 3 Transmission Electron Microscopy; 3.1 Instrumentation; 3.1.1 Electron Sources; 3.1.2 Electromagnetic Lenses; 3.1.3 Specimen Stage; 3.2 Specimen Preparation; 3.2.1 Pre-Thinning; 3.2.2 Final Thinning; 3.3 Image Modes; 3.3.1 Mass-Density Contrast; 3.3.2 Diffraction Contrast; 3.3.3 Phase Contrast; 3.4 Selected Area Diffraction; 3.4.1 Selected Area Diffraction Characteristics; 3.4.2 Single-Crystal Diffraction; 3.4.3 Multi-Crystal Diffraction; 3.4.4 Kikuchi Lines; 3.5 Images of Crystal Defects; 3.5.1 Wedge Fringe; 3.5.2 Bending Contours; 3.5.3 Dislocations; References Questions4 Scanning Electron Microscopy; 4.1 Instrumentation; 4.1.1 Optical Arrangement; 4.1.2 Signal Detection; 4.1.3 Probe Size and Current; 4.2 Contrast Formation; 4.2.1 ElectronSpecimen Interactions; 4.2.2 Topographic Contrast; 4.2.3 Compositional Contrast; 4.3 Operational Variables; 4.3.1 Working Distance and Aperture Size; 4.3.2 Acceleration Voltage and Probe Current; 4.3.3 Astigmatism; 4.4 Specimen Preparation; 4.4.1 Preparation for Topographic Examination; 4.4.2 Preparation for Micro-Composition Examination; 4.4.3 Dehydration; References; Questions; 5 Scanning Probe Microscopy 5.1 Instrumentation5.1.1 Probe and Scanner; 5.1.2 Control and Vibration Isolation; 5.2 Scanning Tunneling Microscopy; 5.2.1 Tunneling Current; 5.2.2 Probe Tips and Working Environments; 5.2.3 Operational Modes; 5.2.4 Typical Applications; 5.3 Atomic Force Microscopy; 5.3.1 Near-Field Forces; 5.3.2 Force Sensors; 5.3.3 Operational Modes; 5.3.4 Typical Applications; 5.4 Image Artifacts; 5.4.1 Tip; 5.4.2 Scanner; 5.4.3 Vibration and Operation; References; Questions; 6 X-ray Spectroscopy for Elemental Analysis; 6.1 Features of Characteristic X-rays; 6.1.1 Types of Characteristic X-rays 6.1.2 Comparison ofK,L andM Series |
Record Nr. | UNINA-9910139934303321 |
Leng Y (Yang)
![]() |
||
Singapore ; ; Hoboken, NJ, : J. Wiley, c2008 | ||
![]() | ||
Lo trovi qui: Univ. Federico II | ||
|
Materials characterization [[electronic resource] ] : introduction to microscopic and spectroscopic methods / / Yang Leng |
Autore | Leng Y (Yang) |
Pubbl/distr/stampa | Singapore ; ; Hoboken, NJ, : J. Wiley, c2008 |
Descrizione fisica | 1 online resource (351 p.) |
Disciplina |
620.1/1
620.11 620.1127 |
Soggetto topico |
Materials
Materials - Analysis |
ISBN |
9786612031403
0-470-82299-6 0-470-82300-3 |
Formato | Materiale a stampa ![]() |
Livello bibliografico | Monografia |
Lingua di pubblicazione | eng |
Nota di contenuto |
MATERIALS CHARACTERIZATION Introduction to Microscopic and Spectroscopic Methods; Contents; Preface; 1 Light Microscopy; 1.1 Optical Principles; 1.1.1 Image Formation; 1.1.2 Resolution; 1.1.3 Depth of Field; 1.1.4 Aberrations; 1.2 Instrumentation; 1.2.1 Illumination System; 1.2.2 Objective Lens and Eyepiece; 1.3 Specimen Preparation; 1.3.1 Sectioning; 1.3.2 Mounting; 1.3.3 Grinding and Polishing; 1.3.4 Etching; 1.4 Imaging Modes; 1.4.1 Bright-Field and Dark-Field Imaging; 1.4.2 Phase Contrast Microscopy; 1.4.3 Polarized Light Microscopy; 1.4.4 Nomarski Microscopy
1.4.5 Fluorescence Microscopy1.5 Confocal Microscopy; 1.5.1 Working Principles; 1.5.2 Three-Dimensional Images; References; Questions; 2 X-ray Diffraction Methods; 2.1 X-ray Radiation; 2.1.1 Generation of X-rays; 2.1.2 X-ray Absorption; 2.2 Theoretical Background of Diffraction; 2.2.1 Diffraction Geometry; 2.2.2 Diffraction Intensity; 2.3 X-ray Diffractometry; 2.3.1 Instrumentation; 2.3.2 Samples and Data Acquisition; 2.3.3 Distortions of Diffraction Spectra; 2.3.4 Applications; 2.4 Wide Angle X-ray Diffraction and Scattering; 2.4.1 Wide Angle Diffraction; 2.4.2 Wide Angle Scattering ReferencesQuestions; 3 Transmission Electron Microscopy; 3.1 Instrumentation; 3.1.1 Electron Sources; 3.1.2 Electromagnetic Lenses; 3.1.3 Specimen Stage; 3.2 Specimen Preparation; 3.2.1 Pre-Thinning; 3.2.2 Final Thinning; 3.3 Image Modes; 3.3.1 Mass-Density Contrast; 3.3.2 Diffraction Contrast; 3.3.3 Phase Contrast; 3.4 Selected Area Diffraction; 3.4.1 Selected Area Diffraction Characteristics; 3.4.2 Single-Crystal Diffraction; 3.4.3 Multi-Crystal Diffraction; 3.4.4 Kikuchi Lines; 3.5 Images of Crystal Defects; 3.5.1 Wedge Fringe; 3.5.2 Bending Contours; 3.5.3 Dislocations; References Questions4 Scanning Electron Microscopy; 4.1 Instrumentation; 4.1.1 Optical Arrangement; 4.1.2 Signal Detection; 4.1.3 Probe Size and Current; 4.2 Contrast Formation; 4.2.1 ElectronSpecimen Interactions; 4.2.2 Topographic Contrast; 4.2.3 Compositional Contrast; 4.3 Operational Variables; 4.3.1 Working Distance and Aperture Size; 4.3.2 Acceleration Voltage and Probe Current; 4.3.3 Astigmatism; 4.4 Specimen Preparation; 4.4.1 Preparation for Topographic Examination; 4.4.2 Preparation for Micro-Composition Examination; 4.4.3 Dehydration; References; Questions; 5 Scanning Probe Microscopy 5.1 Instrumentation5.1.1 Probe and Scanner; 5.1.2 Control and Vibration Isolation; 5.2 Scanning Tunneling Microscopy; 5.2.1 Tunneling Current; 5.2.2 Probe Tips and Working Environments; 5.2.3 Operational Modes; 5.2.4 Typical Applications; 5.3 Atomic Force Microscopy; 5.3.1 Near-Field Forces; 5.3.2 Force Sensors; 5.3.3 Operational Modes; 5.3.4 Typical Applications; 5.4 Image Artifacts; 5.4.1 Tip; 5.4.2 Scanner; 5.4.3 Vibration and Operation; References; Questions; 6 X-ray Spectroscopy for Elemental Analysis; 6.1 Features of Characteristic X-rays; 6.1.1 Types of Characteristic X-rays 6.1.2 Comparison ofK,L andM Series |
Record Nr. | UNINA-9910830184903321 |
Leng Y (Yang)
![]() |
||
Singapore ; ; Hoboken, NJ, : J. Wiley, c2008 | ||
![]() | ||
Lo trovi qui: Univ. Federico II | ||
|
Materials characterization [[electronic resource] ] : introduction to microscopic and spectroscopic methods / / Yang Leng |
Autore | Leng Y (Yang) |
Pubbl/distr/stampa | Singapore ; ; Hoboken, NJ, : J. Wiley, c2008 |
Descrizione fisica | 1 online resource (351 p.) |
Disciplina |
620.1/1
620.11 620.1127 |
Soggetto topico |
Materials
Materials - Analysis |
ISBN |
9786612031403
0-470-82299-6 0-470-82300-3 |
Formato | Materiale a stampa ![]() |
Livello bibliografico | Monografia |
Lingua di pubblicazione | eng |
Nota di contenuto |
MATERIALS CHARACTERIZATION Introduction to Microscopic and Spectroscopic Methods; Contents; Preface; 1 Light Microscopy; 1.1 Optical Principles; 1.1.1 Image Formation; 1.1.2 Resolution; 1.1.3 Depth of Field; 1.1.4 Aberrations; 1.2 Instrumentation; 1.2.1 Illumination System; 1.2.2 Objective Lens and Eyepiece; 1.3 Specimen Preparation; 1.3.1 Sectioning; 1.3.2 Mounting; 1.3.3 Grinding and Polishing; 1.3.4 Etching; 1.4 Imaging Modes; 1.4.1 Bright-Field and Dark-Field Imaging; 1.4.2 Phase Contrast Microscopy; 1.4.3 Polarized Light Microscopy; 1.4.4 Nomarski Microscopy
1.4.5 Fluorescence Microscopy1.5 Confocal Microscopy; 1.5.1 Working Principles; 1.5.2 Three-Dimensional Images; References; Questions; 2 X-ray Diffraction Methods; 2.1 X-ray Radiation; 2.1.1 Generation of X-rays; 2.1.2 X-ray Absorption; 2.2 Theoretical Background of Diffraction; 2.2.1 Diffraction Geometry; 2.2.2 Diffraction Intensity; 2.3 X-ray Diffractometry; 2.3.1 Instrumentation; 2.3.2 Samples and Data Acquisition; 2.3.3 Distortions of Diffraction Spectra; 2.3.4 Applications; 2.4 Wide Angle X-ray Diffraction and Scattering; 2.4.1 Wide Angle Diffraction; 2.4.2 Wide Angle Scattering ReferencesQuestions; 3 Transmission Electron Microscopy; 3.1 Instrumentation; 3.1.1 Electron Sources; 3.1.2 Electromagnetic Lenses; 3.1.3 Specimen Stage; 3.2 Specimen Preparation; 3.2.1 Pre-Thinning; 3.2.2 Final Thinning; 3.3 Image Modes; 3.3.1 Mass-Density Contrast; 3.3.2 Diffraction Contrast; 3.3.3 Phase Contrast; 3.4 Selected Area Diffraction; 3.4.1 Selected Area Diffraction Characteristics; 3.4.2 Single-Crystal Diffraction; 3.4.3 Multi-Crystal Diffraction; 3.4.4 Kikuchi Lines; 3.5 Images of Crystal Defects; 3.5.1 Wedge Fringe; 3.5.2 Bending Contours; 3.5.3 Dislocations; References Questions4 Scanning Electron Microscopy; 4.1 Instrumentation; 4.1.1 Optical Arrangement; 4.1.2 Signal Detection; 4.1.3 Probe Size and Current; 4.2 Contrast Formation; 4.2.1 ElectronSpecimen Interactions; 4.2.2 Topographic Contrast; 4.2.3 Compositional Contrast; 4.3 Operational Variables; 4.3.1 Working Distance and Aperture Size; 4.3.2 Acceleration Voltage and Probe Current; 4.3.3 Astigmatism; 4.4 Specimen Preparation; 4.4.1 Preparation for Topographic Examination; 4.4.2 Preparation for Micro-Composition Examination; 4.4.3 Dehydration; References; Questions; 5 Scanning Probe Microscopy 5.1 Instrumentation5.1.1 Probe and Scanner; 5.1.2 Control and Vibration Isolation; 5.2 Scanning Tunneling Microscopy; 5.2.1 Tunneling Current; 5.2.2 Probe Tips and Working Environments; 5.2.3 Operational Modes; 5.2.4 Typical Applications; 5.3 Atomic Force Microscopy; 5.3.1 Near-Field Forces; 5.3.2 Force Sensors; 5.3.3 Operational Modes; 5.3.4 Typical Applications; 5.4 Image Artifacts; 5.4.1 Tip; 5.4.2 Scanner; 5.4.3 Vibration and Operation; References; Questions; 6 X-ray Spectroscopy for Elemental Analysis; 6.1 Features of Characteristic X-rays; 6.1.1 Types of Characteristic X-rays 6.1.2 Comparison ofK,L andM Series |
Record Nr. | UNINA-9910841618903321 |
Leng Y (Yang)
![]() |
||
Singapore ; ; Hoboken, NJ, : J. Wiley, c2008 | ||
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Lo trovi qui: Univ. Federico II | ||
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Materials in a new era [[electronic resource] ] : proceedings of the 1999 Solid State Sciences Committee Forum / / Solid State Sciences Committee, Board on Physics and Astronomy, Commission on Physical Sciences, Mathematics, and Applications, National Research Council |
Pubbl/distr/stampa | Washington, D.C., : National Academy Press, c1999 |
Descrizione fisica | 1 online resource (63 p.) |
Disciplina | 620.1/1 |
Collana | Compass series (Washington, D.C.) |
Soggetto topico |
Materials science
Materials - Research Solid state physics |
Soggetto genere / forma | Electronic books. |
ISBN | 0-309-51584-X |
Formato | Materiale a stampa ![]() |
Livello bibliografico | Monografia |
Lingua di pubblicazione | eng |
Record Nr. | UNINA-9910456158003321 |
Washington, D.C., : National Academy Press, c1999 | ||
![]() | ||
Lo trovi qui: Univ. Federico II | ||
|
Materials in a new era [[electronic resource] ] : proceedings of the 1999 Solid State Sciences Committee Forum / / Solid State Sciences Committee, Board on Physics and Astronomy, Commission on Physical Sciences, Mathematics, and Applications, National Research Council |
Pubbl/distr/stampa | Washington, D.C., : National Academy Press, c1999 |
Descrizione fisica | 1 online resource (63 p.) |
Disciplina | 620.1/1 |
Collana | Compass series (Washington, D.C.) |
Soggetto topico |
Materials science
Materials - Research Solid state physics |
ISBN |
0-309-17240-3
0-309-51584-X |
Formato | Materiale a stampa ![]() |
Livello bibliografico | Monografia |
Lingua di pubblicazione | eng |
Record Nr. | UNINA-9910778749803321 |
Washington, D.C., : National Academy Press, c1999 | ||
![]() | ||
Lo trovi qui: Univ. Federico II | ||
|