Thermal ionization mass spectrometry (TIMS) : silicate digestion, separation, and measurement / / Akio Makishima

• Autore: Makishima Akio
• Pubblicazione: Weinheim, Germany : , : Wiley-VCH, , 2016; ©2016
• Descrizione fisica: 1 online resource (372 p.)
• Disciplina: 543.0873
• Soggetto topico: Mass spectrometry; Analytical geochemistry
• Note generali: Description based upon print version of record.
• Nota di bibliografia: Includes bibliographical references and index.
• Nota di contenuto: Cover; Title Page; Copyright; Dedication; Contents; Preface; Chapter 1 Analytical Geochemistry; 1.1 Overview of Analytical Geochemistry; 1.1.1 Major Element Geochemistry; 1.1.1.1 X-ray Fluorescence Spectrometer; 1.1.1.2 Loss on Ignition and Ferric/Ferrous Ratio of Iron; 1.1.2 Trace Element Geochemistry; 1.1.2.1 From REE Geochemistry to Trace Element Geochemistry; 1.1.2.2 Isotope Dilution Method (ID); 1.1.2.3 Error Magnification; 1.1.2.4 Isotope Dilution with Internal Standardization Method (ID-IS); 1.1.3 Determination of Mass Fractionation; 1.1.4 Age Dating; 1.1.4.1 Types of Radioactive Decay ; 1.1.4.2 Age Dating by Radioactive Isotopes 1.1.4.3 Extinct Nuclides; 1.1.4.4 An Isochron or a Mixing Line?; 1.1.4.5 A Single Zircon Dating; 1.1.4.6 Direct Single Zircon Analysis by TIMS; 1.1.5 Radiogenic Isotopes for Geochemical Tracers; 1.2 Element Synthesis in Stars; 1.2.1 Atom, Nucleus, Isotope, and Element; 1.2.2 Soon after the Big Bang; 1.2.3 Element Synthesis in Stars; 1.2.4 Element Syntheses in Other Processes; 1.2.4.1 The r-Process; 1.2.4.2 The p-Process; 1.2.4.3 The s-Process; 1.2.4.4 The x-Process; 1.2.4.5 Type Ia Supernova; 1.2.5 Other Types of Supernovae; 1.3 Errors ; 1.3.1 Average and Standard Deviation 1.3.2 Normal Population; 1.3.3 Standard Error; 1.3.4 ISO Suggestion; 1.3.5 Modified Savitzky-Golay Method; 1.3.6 Variance, Covariance, and Correlation Coefficient; 1.3.7 Weighted Average, Variance, and Covariance; 1.3.8 The Least-Squares Method; Chapter 2 Basics and Principles of Sample Digestion; 2.1 Clean Technologies, Powdering, and Weighing of Sample Powder; 2.1.1 Clean Room Technologies; 2.1.1.1 Clean Rooms; 2.1.1.2 Two Types of Clean Rooms; 2.1.1.3 Draft Chamber; 2.1.1.4 Clean Evaporator; 2.1.1.5 Protection to Acids; 2.1.1.6 Levels of Cleanness ; 2.1.1.7 Clean Benches and so on 2.1.2 Powdering of the Sample; 2.1.3 Weighing the Sample Powder; 2.2 Materials Used in Laboratory; 2.2.1 Glassware; 2.2.2 Plastics; 2.2.3 Water; 2.2.4 Azeotrope; 2.2.5 Physical and Chemical Properties of Acids; 2.2.5.1 Hydrofluoric Acid; 2.2.5.2 Hydrochloric Acid; 2.2.5.3 Hydrobromic Acid; 2.2.5.4 Nitric Acid; 2.2.5.5 Perchloric Acid; 2.2.6 Sub-Boiling Purification; 2.2.7 Alkali Reagents; 2.2.7.1 Ammonia Water; 2.2.7.2 TMSC®; 2.3 Characterization of Elements; 2.3.1 Characterization of Elements by Their Behavior in HF Solution ; 2.3.2 Characterization of Elements by Melting Temperature of Oxides 2.3.3 Characterization of Elements by Volatility of Fluorides and Chlorides; 2.4 Sample Digestion Techniques; 2.4.1 HF+HClO4 Digestion in Ambient Pressure (an ""Ultrasonic Method""); 2.4.2 HF Digestion in High Pressure and Temperature (a ""Bomb Method""); 2.4.3 Microwave Digestion Method; 2.4.4 Carius Tube Digestion for Os Separation; 2.4.5 HPA (High-Pressure Asher) Digestion Method; 2.4.6 Fusion; 2.4.6.1 Alkali Fusion; 2.4.6.2 Lithium Borate Fusion; 2.4.6.3 Sodium Peroxide Fusion; 2.4.6.4 V2O5 Fusion; 2.4.6.5 NiS Fire Assay ; 2.4.7 A Digestion Method Using NH4F
• Titolo autorizzato: Thermal ionization mass spectrometry (TIMS)
• ISBN: 3-527-69644-X; 3-527-69641-5; 3-527-69642-3
• Formato: Materiale a stampa
• Livello bibliografico: Monografia
• Lingua di pubblicazione: Inglese
• Record Nr.: 9910806942103321
• Lo trovi qui: Univ. Federico II