NMR spectroscopy [[electronic resource] ] : processing strategies / / Peter Bigler

• Autore: Bigler Peter
• Pubblicazione: Weinheim ; ; New York, : Wiley-VCH, c2000
• Edizione: 2nd updated ed.
• Descrizione fisica: 1 online resource (273 p.)
• Disciplina: 538.362; 543.0877
• Soggetto topico: Nuclear magnetic resonance spectroscopy - Data processing; Chemistry
• Note generali: Description based upon print version of record.
• Nota di bibliografia: Includes bibliographical references and index.
• Nota di contenuto: Spectroscopic Techniques: An Interactive Course; Table of Contents; 1 Introduction; 1.1 Scope and Audience; 1.2 Organisation; 1.3 Personal Qualifications; 1.4 Content; 1.5 Recommended Reading; 2 Your Personal "PC-NMR -Processing Station"; 2.1 Introduction; 2.2 Technical Requirements; 2.3 Software Tools; 2.3.1 General; 2.3.2 Installation of 1D WIN-NMR, 2D WIN-NMR and GETFILE; 2.3.3 Starting GETFILE, 1D WIN-NMR and 2D WIN-NMR; 2.4 Software- and Hardwareproblems; 2.5 NMR Data; 2.5.1 Samples; 2.5.2 Experiments; 2.5.3 Experimental Conditions; 2.5.4 Directory Structure ; 2.5.5 Copying the NMR Data from the CD to your Hard Disk2.5.6 Useful Options in the MS WINDOWS 95 Operating System; 2.6 Data Formats; 2.6.1 WINNMR Format; 2.6.2 UXNMR/XWINNMR Format; 2.6.3 DISNMR Format; 2.6.4 NMR Data Formats of other Manufacturers: Varian, JEOL, GE; 2.6.5 Other Formats: ASCII, JCAMP-DX; 2.7 Data Import and Export; 2.7.1 Network-Example; 2.7.2 Transfer and Conversion of NMR Data stored on Remote Computers; 2.7.2.1 UXNMR/XWINNMR-Format; 2.7.2.2 DISNMR-Format; 2.7.3 Decomposition of 2D Data Files; 2.8 References ; 3 Modern Homo- and Heteronuclear 1D and 2D NMR Experiments: A Short Overview3.1 Introduction; 3.2 The NMR Experiment; 3.3 1D Experiments; 3.3.1 1H Experiments; 3.3.1.1 1H One Pulse Experiment; 3.3.1.2 1H {1H} Selective Decoupling Experiment [3.1]; 3.3.1.3 1H {1H} Total Correlation Spectroscopy (TOCSY) Experiment [3.2]; 3.3.1.4 1H {1H} Nuclear Overhauser (NOE) Experiment [3.3]; 3.3.1.5 1H {1 H} Nuclear Overhauser Experiment in the Rotating Frame (ROE) [3.4]; 3.3.2 13C Experiments; 3.3.2.1 13C One-Pulse Experiment; 3.3.2.2 13C DEPT Experiment [3.5]; 3.3.2.3 13C JMOD (APT) Experiment [3.6,3.7] ; 3.3.2.4 13C T1 Inversion-Recovery Experiment [3.8,3.9]3.4 2D Experiments; 3.4.1 1H/1H Experiments [3.10,3.11]; 3.4.1.1 1H/1H COSY Experiment [3.10,3.11]; 3.4.1.2 1H/1H TOCSY Experiment [3.12,3.13]; 3.4.1.3 1H/1H NOESY and 1H/1H ROESY Experiments [3.14,3.15]; 3.4.1.4 1H/1H J -Resolved Spectroscopy Experiment [3.16]; 3.4.2 1H/13C Experiments; 3.4.2.1 1H/13C Shift Correlation Spectroscopy via 1JCH[3.17- 3.21]; 3.4.2.2 1H/13C Shift Correlation Spectroscopy via nJCH[3.22]; 3.4.2.3 1H/13C Shift Correlation Spectroscopy via 1JCH and 1H/1H TOCSY Transfer [3.23]; 3.5 Recommended Reading ; 4 How to Display and Plot 1D and 2D NMR Spectra4.1 Introduction; 4.2 Help Routines; 4.3 Application Windows for 1D WIN-NMR and 2D WIN-NMR; 4.4 File Handling; 4.5 Display of 1D Spectra with 1D WIN-NMR; 4.5.1 Buttons with 1D WIN-NMR [Spectrum]; 4.5.2 Additional Display Options with 1D WIN-NMR; 4.5.3 The Use of Scroll Bars, Keys and Function Keys with 1D WIN-NMR; 4.6 Basic Processing Steps with 1D Spectra; 4.6.1 Cali bration; 4.6.2 Peak Picking; 4.6.3 Integration; 4.6.4 Simple Spectral Analysis; 4.7 Plotting 1D Spectra; 4.7.1 Define Plot; 4.7.2 Page Layout ; 4.7.2.1 Page Layout Dialog Box in Normal 1D Display Mode
• Sommario/riassunto: Text for the series ""Spectroscopic Techniques"":Leading software designers and teachers of spectroscopy have pooled their expertise to devise a new series ""Spectroscopic Techniques: An Interactive Course"". User are able to gain a better understanding of a variety of spectroscopic techniques in these step-by-step guides.Let the experts show you new solutions to practiced problems using software provided on the interactive CD-ROM.
• Titolo autorizzato: NMR spectroscopy
• ISBN: 1-281-76414-0; 9786611764142; 3-527-61342-0; 3-527-61343-9
• Formato: Materiale a stampa
• Livello bibliografico: Monografia
• Lingua di pubblicazione: Inglese
• Record Nr.: 9910830100003321
• Lo trovi qui: Univ. Federico II
• Serie: Spectroscopic Techniques: An Interactive Course