Purification of laboratory chemicals [[electronic resource] /] / Wilfred L.F. Armarego, Christina Li Lin Chai

• Autore: Armarego W. L. F
• Pubblicazione: Amsterdam ; ; Boston, : Elsevier/Butterworth-Heinemann, c2009
• Edizione: 6th ed.
• Descrizione fisica: 1 online resource (761 p.)
• Disciplina: 542
• Soggetto topico: Chemicals - Purification
• Altri autori: ChaiChristina Li Lin
• Note generali: Description based upon print version of record.
• Nota di bibliografia: Includes bibliographical references and index.
• Nota di contenuto: Front Cover; Purification of Laboratory Chemicals; Copyright Page; CONTENTS; Preface to the Sixth Edition; Preface to the First Edition; Preface to the Second Edition; Preface to the Third Edition; Preface to the Fourth Edition; Preface to the Fifth Edition; CHAPTER 1. COMMON PHYSICAL TECHNIQUES USED IN PURIFICATION; INTRODUCTION; THE QUESTION OF PURITY; SAFETY PRECAUTIONS ASSOCIATED WITH THE PURIFICATION OF LABORATORY CHEMICALS; METHODS OF PURIFICATION OF REAGENTS AND SOLVENTS; TABLES; TABLE 1. SOME COMMON IMMISCIBLE OR SLIGHTLY MISCIBLE PAIRS OF SOLVENTS; FIGURE 1. NOMOGRAM ; TABLE 2A. PREDICTED EFFECT OF PRESSURE ON BOILING POINTTABLE 2B. PREDICTED EFFECT OF PRESSURE ON BOILING POINT; TABLE 3. HEATING BATHS; TABLE 4. WHATMAN FILTER PAPERS; TABLE 5. MICRO FILTERS; TABLE 6. COMMON SOLVENTS USED IN RECRYSTALLISATION; TABLE 7. PAIRS OF MISCIBLE SOLVENTS; TABLE 8. MATERIALS FOR COOLING BATHS; TABLE 9. LIQUIDS FOR STATIONARY PHASES IN GAS CHROMATOGRAPHY; TABLE 10. METHODS OF VISUALISATION OF TLC SPOTS; TABLE 11. GRADED ADSORBENTS AND SOLVENTS; TABLE 12. REPRESENTATIVE ION-EXCHANGE RESINS; TABLE 13. MODIFIED FIBROUS CELLULOSES FOR ION-EXCHANGE ; TABLE 14. BEAD FORM ION-EXCHANGE PACKAGINGSTABLE 15. LIQUIDS FOR DRYING PISTOLS; TABLE 16. VAPOUR PRESSURES (mm Hg) OF SATURATED AQUEOUS SOLUTIONS IN EQUILIBRIUM WITH SOLID SALTS; TABLE 17. DRYING AGENTS FOR CLASSES OF COMPOUNDS; TABLE 18. STATIC DRYING FOR SELECTED LIQUIDS (25°C); TABLE 19. AQUEOUS BUFFERS; TABLE 20. SOLUBILITY COEFFICIENTS OF AIR AT 1atm IN WATER; TABLE 21. SOLUBILITY COEFFICIENTS OF O2 AT 1atm IN WATER; TABLE 22. BUNSEN COEFFICIENTS (ß) OF GASES AT 1atm IN ORGANIC SOLVENTS AT 20°C; TABLE 23. OSTWALD COEFFICIENTS (l)/L OF O2 AT 1atm IN AQUEOUS SOLUTIONS AT 25°C ; TABLE 24. SOLUBILITIES OF HCl AND NH3 AT 760mm (g/100g OF SOLUTION)TABLE 25. BOILING POINTS OF SOME USEFUL GASES AT 760 mm; TABLE 26. PREFIXES FOR QUANTITIES; BIBLIOGRAPHY; CHAPTER 2. CHEMICAL METHODS USED IN PURIFICATION; GENERAL REMARKS; REMOVAL OF TRACES OF METALS FROM REAGENTS; USE OF METAL HYDRIDES; PURIFICATION via DERIVATIVES; GENERAL METHODS FOR THE PURIFICATION OF CLASSES OF COMPOUNDS; GENERAL PROCEDURES FOR THE PURIFICATION OF SOME CLASSES OF ORGANIC COMPOUNDS; BIBLIOGRAPHY; CHAPTER 3. THE FUTURE OF PURIFICATION; INTRODUCTION; ORGANOCATALYSIS; MICROWAVE TECHNOLOGIES ; SOLID PHASE SYNTHESISALTERNATIVE SOLVENTS; BIBLIOGRAPHY; CHAPTER 4. PURIFICATION OF ORGANIC CHEMICALS; INTRODUCTION; ALIPHATIC COMPOUNDS; ALICYCLIC COMPOUNDS; AROMATIC COMPOUNDS; HETEROCYCLIC COMPOUNDS; CHAPTER 5. PURIFICATION OF INORGANIC AND METAL-ORGANIC CHEMICALS (Including Organic compounds of B, Bi, P, Se, Si, and ammonium andmetal salts of organic acids); INTRODUCTION; INORGANIC COMPOUNDS; METAL-ORGANIC COMPOUNDS; CHAPTER 6. PURIFICATION OF BIOCHEMICALS AND RELATED PRODUCTS; INTRODUCTION; AMINO ACIDS and PEPTIDES; PROTEINS, ENZYMES, DNA and RNA; CAROTENOIDS; CARBOHYDRATES; STEROIDS ; MISCELLANEOUS COMPOUNDS
• Sommario/riassunto: A best seller since 1966, Purification of Laboratory Chemicals keeps engineers, scientists, chemists, biochemists and students up to date with the purification of the chemical reagents with which they work, the processes for their purification, and guides readerd on critical safety and hazards for the safe handling of chemicals and processes.The Sixth Edition is updated and provides expanded coverage of the latest chemical products and processing techniques, safety and hazards. The book has been reorganised and is now fully indexed by CAS Registry Numbers. Compounds are now grouped to
• Titolo autorizzato: Purification of laboratory chemicals
• ISBN: 1-282-28519-X; 9786612285196; 0-08-087824-5
• Formato: Materiale a stampa
• Livello bibliografico: Monografia
• Lingua di pubblicazione: Inglese
• Record Nr.: 9910777708503321
• Lo trovi qui: Univ. Federico II