{"text_format":"2","workbook":"xls","n_sheets":1,"sheets":["report2"],"not_rendered":{"charts":0,"images":0,"macros":0,"external_links":1,"defined_names":2,"comments":0,"pivot_tables":0},"unopened":[],"bounds":{"document_bytes":16777216,"sheet_cells":100000,"run_cost":"one","rows_first":2000,"rows_last":500,"rows_between":2000,"halvings":0,"cell_chars":16384,"cell_head_chars":4096},"cells_cut":0,"cells_raw":0,"read":"whole","date_system":"1900","formulas":"cached_only"}

{"sheet":"report2","index":0,"n_rows":44,"n_cols":5,"rows_kept":44,"cut":false,"hidden":false,"merged":[[0,2,0,3],[0,4,0,5],[1,2,1,3],[1,4,1,5],[2,2,2,3],[2,4,2,5],[3,2,3,3],[4,2,4,3],[5,2,5,3],[6,2,6,3],[7,2,7,3],[9,2,9,3],[11,2,11,3],[12,2,12,3],[14,2,14,3],[14,4,14,5],[15,2,15,3],[15,4,15,5],[16,2,16,3],[16,4,16,5],[17,2,17,3],[18,2,18,3],[27,2,27,3],[28,2,28,3],[29,2,29,3],[30,2,30,3],[31,2,31,3],[32,2,32,3],[36,2,36,3]],"flags":["formulas_cached_only"]}
[null,"1.","Record Nr.",null,"UNINA990006701760403321"]
[null,null,"Autore",null,"Cataldi Madonna, Luigi"]
[null,null,"Titolo",null,"Il razionalismo di Nietzsche : filologia e teoria della conoscenza negli scritti giovanili / Luigi Cataldi Madonna"]
[null,null,"Pubbl/distr/stampa",null,"Napoli : Edizioni scientifiche italiane, 1983"]
[null,null,"Descrizione fisica",null,"244 p. ; 21 cm"]
[null,null,"Collana",null,"Poiesis ; 4"]
[null,null,"Disciplina",null,"193"]
[null,null,"Locazione",null,"FSPBC"]
[{"$nulls":4},"DDRC"]
[null,null,"Collocazione",null,"COLLEZ. 1351 (4)"]
[{"$nulls":4},"FIL-79"]
[null,null,"Lingua di pubblicazione",null,"Italiano"]
[null,null,"Formato",null,"Materiale a stampa"]
[null,null,null,"Livello bibliografico","Monografia"]
[null,"2.","Record Nr.",null,"UNINA9911019891103321"]
[null,null,"Autore",null,"Kolb Bruno"]
[null,null,"Titolo",null,"Static headspace-gas chromatography : theory and practice / / Bruno Kolb and Leslie S. Ettre"]
[null,null,"Pubbl/distr/stampa",null,"Hoboken, N.J., : Wiley, c2006"]
[null,null,"ISBN",null,"9786610448197"]
[{"$nulls":4},"9781280448195"]
[{"$nulls":4},"1280448199"]
[{"$nulls":4},"9780470325988"]
[{"$nulls":4},"0470325984"]
[{"$nulls":4},"9780471914587"]
[{"$nulls":4},"0471914584"]
[{"$nulls":4},"9780471914563"]
[{"$nulls":4},"0471914568"]
[null,null,"Edizione",null,"[2nd ed.]"]
[null,null,"Descrizione fisica",null,"1 online resource (377 p.)"]
[null,null,"Disciplina",null,"543/.85"]
[null,null,"Soggetti",null,"Gas chromatography"]
[null,null,"Lingua di pubblicazione",null,"Inglese"]
[null,null,"Formato",null,"Materiale a stampa"]
[null,null,null,"Livello bibliografico","Monografia"]
[null,null,null,"Note generali","Description based upon print version of record."]
[null,null,null,"Nota di bibliografia","Includes bibliographical references and index."]
[null,null,"Nota di contenuto",null,"Static Headspace-Gas Chromatography; Contents; Preface; Preface to the First Edition; List of Acronyms and Symbols; 1 General Introduction; 1.1 Principles of Headspace Analysis; 1.2 Types of Headspace Analysis; 1.2.1 Principles of Static HS-GC; 1.2.2 Principles of Dynamic HS-GC; 1.2.2.1 The Trap; 1.2.2.2 The Water Problem; 1.2.2.3 The Flow Problem; 1.2.2.4 The Time Problem; 1.2.2.5 Comparison of Static HS-GC with P&T; 1.3 The Evolution of the HS-GC Methods; 1.4 HS-GS Literature; 1.5 Regulatory Methods Utilizing (Static) HS-GC; References; 2 Theoretical Background of HS-GC and Its Applications"]
[{"$nulls":4},"2.1 Basic Theory of Headspace Analysis2.2 Basic Physicochemical Relationships; 2.3 Headspace Sensitivity; 2.3.1 Influence of Temperature on Vapor Pressure and Partition Coefficient; 2.3.1.1 Enhancement of Lower Boiling Compounds; 2.3.2 Influence of Temperature on Headspace Sensitivity for Compounds with Differing Partition Coefficients; 2.3.3 Influence of Sample Volume on Headspace Sensitivity for Compounds with Differing Partition Coefficients; 2.3.3.1 Sample-to-Sample Reproducibility; 2.3.4 Changing the Sample Matrix "]
[{"$nulls":4},"by Varying the Activity Coefficient; 2.4 Headspace Linearity"]
[{"$nulls":4},"2.5 Duplicate Analyses2.6 Multiple Headspace Extraction (MHE); 2.6.1 Principles of MHE; 2.6.2 Theoretical Background of MHE; 2.6.3 Simplified MHE Calculation; References; 3 The Technique of HS-GC; 3.1 Sample Vials; 3.1.1 Vial Types; 3.1.2 Selection of the Vial Volume; 3.1.3 Vial Cleaning; 3.1.4 Wall Adsorption Effects; 3.2 Caps; 3.2.1 Pressure on Caps; 3.2.2 Safety Closures; 3.3 Septa; 3.3.1 Septa Types; 3.3.2 Septum Blank; 3.3.3 Should a Septum Be Pierced Twice?; 3.3.3.1 Closed-Vial versus Open-Vial Sample Introduction Technique; 3.4 Thermostatting; 3.4.1 Influence of Temperature"]
[{"$nulls":4},"3.4.2 Working Modes3.5 The Fundamental Principles of Headspace Sampling Systems; 3.5.1 Systems Using Gas Syringes; 3.5.2 Solid Phase Microextraction (SPME); 3.5.2.1 Comparison of the Sensitivities in HS-SPME and Direct Static HS-GC; 3.5.3 Balanced Pressure Sampling Systems; 3.5.4 Pressure/Loop Systems; 3.5.5 Conditions for Pressurization Systems; 3.5.6 Volume of the Headspace Gas Sample; 3.5.6.1 Sample Volume with Gas Syringes; 3.5.6.2 Sample Volume with Loop Systems; 3.5.6.3 Sample Volume with the Balanced Pressure System; 3.6 Use of Open-Tubular (Capillary) Columns"]
[{"$nulls":4},"3.6.1 Properties of Open-Tubular Columns for Gas Samples3.6.2 Headspace Sampling with Split or Splitless Introduction; 3.6.3 Comparison of Split and Splitless Headspace Sampling; 3.6.4 Band Broadening During Sample Introduction; 3.6.5 Influence of Temperature on Band Broadening; 3.6.5.1 Conclusions; 3.6.6 The Combination of Different Columns and Detectors; 3.7 Enrichment Techniques in HS-GC; 3.7.1 Systems for Cryogenic Trapping; 3.7.1.1 Trapping by Cryogenic Condensation; 3.7.1.2 Trapping by Cryogenic Focusing; 3.7.1.3 Influence of Temperature on Cryogenic Focusing"]
[{"$nulls":4},"3.7.1.4 Comparison of the Various Techniques of Cryogenic Trapping"]
[null,null,null,"Sommario/riassunto","The only reference to provide both current and thorough coverage of this important analytical techniqueStatic headspace-gas chromatography (HS-GC) is an indispensable technique for analyzing volatile organic compounds, enabling the analyst to assay a variety of sample matrices while avoiding the costly and time-consuming preparation involved with traditional GC.Static Headspace-Gas Chromatography: Theory and Practice has long been the only reference to provide in-depth coverage of this method of analysis. The Second Edition has been thoroughly updated to reflect the most recent"]