{"text_format":"2","workbook":"xls","n_sheets":1,"sheets":["report2"],"not_rendered":{"charts":0,"images":0,"macros":0,"external_links":1,"defined_names":1,"comments":0,"pivot_tables":0},"unopened":[],"bounds":{"document_bytes":16777216,"sheet_cells":100000,"run_cost":"one","rows_first":2000,"rows_last":500,"rows_between":2000,"halvings":0,"cell_chars":16384,"cell_head_chars":4096},"cells_cut":0,"cells_raw":0,"read":"whole","date_system":"1900","formulas":"cached_only"}

{"sheet":"report2","index":0,"n_rows":28,"n_cols":5,"rows_kept":28,"cut":false,"hidden":false,"merged":[[0,2,0,3],[0,4,0,5],[1,2,1,3],[1,4,1,5],[2,2,2,3],[2,4,2,5],[3,2,3,3],[5,2,5,3],[9,2,9,3],[10,2,10,3],[12,2,12,3],[15,2,15,3],[16,2,16,3],[20,2,20,3]],"flags":["formulas_cached_only"]}
[null,"1.","Record Nr.",null,"UNINA9910830914103321"]
[null,null,"Autore",null,"Brennan Martin <1943->"]
[null,null,"Titolo",null,"A practical approach to quantitative metal analysis of organic matrices / / Martin C. Brennan"]
[null,null,"Pubbl/distr/stampa",null,"West Sussex, England : , : Wiley, , 2008"]
[{"$nulls":4},"©2008"]
[null,null,"ISBN",null,"1-281-94021-6"]
[{"$nulls":4},"9786611940218"]
[{"$nulls":4},"0-470-99828-8"]
[{"$nulls":4},"0-470-99829-6"]
[null,null,"Descrizione fisica",null,"1 online resource (278 p.)"]
[null,null,"Disciplina",null,"543.52"]
[{"$nulls":4},"543.6"]
[null,null,"Soggetti",null,"Atomic emission spectroscopy"]
[{"$nulls":4},"Metals - Analysis"]
[{"$nulls":4},"Chemistry, Organic"]
[null,null,"Lingua di pubblicazione",null,"Inglese"]
[null,null,"Formato",null,"Materiale a stampa"]
[null,null,null,"Livello bibliografico","Monografia"]
[null,null,null,"Note generali","Description based upon print version of record."]
[null,null,null,"Nota di bibliografia","Includes bibliographical references and index."]
[null,null,"Nota di contenuto",null,"A Practical Approach to Quantitative Metal Analysis of Organic Matrices; Contents; Preface; Biography; Acknowledgements; 1 A Practical Approach to Quantitative Metal Analysis of Organic Matrices Using ICP-OES; 1.1 Introduction and Basic Overview; 1.2 Schematic Representation of the Energies Generated by Atomic Spectroscopic Methods; 1.3 Excitation Energy (Quantum Theory and Atomic Spectra); 1.4 Ionisation Energy and Number of Excited Atoms; 1.5 Width of Atomic Lines; 1.5.1 Natural Broadening; 1.5.2 Doppler Broadening; 1.5.3 Lorentzian Broadening or Pressure Broadening"]
[{"$nulls":4},"1.5.4 Holtsmark Broadening or Resonance Broadening1.5.5 Field Broadening or Stark Broadening; 1.5.6 Self-Absorption and Self-Reversal Broadening; 1.6 Brief Summary of Atomic Spectroscopic Techniques Used for Elemental Analysis; 1.6.1 The Atomic Absorption Spectrophotometer; 1.6.2 Atomic Fluorescence Spectroscopy; 1.6.3 Direct Current Plasma Optical Emission Spectrometry (DCP-OES); 1.6.4 Microwave Induced Plasma (MIP); 1.6.5 Glow Discharge Optical Emission Spectrometry (GD-OES); 1.6.6 Inductively Coupled Plasma Optical Emission Spectrometry (ICP-OES)"]
[{"$nulls":4},"1.7 Summary: Applications of Atomic SpectroscopyReferences; 2 "]
[{"$nulls":4},"Instrumentations Associated with Atomic Spectroscopy; 2.1 Instrumentation; 2.2 Types of Plasma Sources; 2.2.1 Direct Current Plasma Atomic Emission Spectrograph; 2.2.2 Microwave Induced Plasma; 2.2.3 Optical Emission Spectroscopy; 2.3 Sample Introduction Systems; 2.3.1 Mechanical Transfer of Sample/Standards Using Peristaltic Pump, Pressure Valves, Motorised Syringes, etc.; 2.3.2 Nebulisers; 2.3.3 Brief Outline of Atomic Spectroscopy Hyphenated Systems; 2.4 Spray Chambers; 2.5 ICP-OES Torches; 2.6 Optics; 2.6.1 Grating Orders"]
[{"$nulls":4},"2.7 Signal Detectors2.7.1 Photomultiplier Tubes; 2.7.2 Charge Coupled Devices; References; 3 Methodologies of Metal Analysis of Organic Matrices Using ICP-OES; 3.1 Sample Preparation Techniques and Methods of Analysis; 3.2 Defining Goals; 3.3 Steps in Chemical Analytical Protocol; 3.4 Sampling and its Importance; 3.5 Sample Preparation Methods; 3.5.1 Direct Analysis of Organic Solutions; 3.5.2 Sample Dissolution; 3.5.3 Chemical Extraction of Metals from Organic Matrices; 3.5.4 Dry Ashing without Retaining Aids; 3.5.5 Dry Ashing with Retaining Aids; 3.5.6 Acid Digestion Using Microwave Oven"]
[{"$nulls":4},"3.5.7 Oxygen Bomb Flask Combustion (Low Pressure)3.5.8 High Pressure Oxygen Combustion; 3.5.9 Sample Preparation Using Fusion Methods; 3.5.10 Analysis Using Slurry Solution Method; 3.5.11 Sample Preparation Using Leaching Method; 3.5.12 Sample Preparation Using a UV Digester; 3.6 Non-Spectral Corrections Using ICP-OES; 3.6.1 Effect of Solvents on ICP-OES; 3.6.2 Effect of Viscosity on Signal Response; 3.6.3 Comparison of Nebulisation Efficiency of Solvents Using ICP-OES; 3.6.4 Choice of Carrier Liquid; 3.7 Methodology of Measurement; 3.7.1 Choice of Standard Materials"]
[{"$nulls":4},"3.7.2 Quantitative Analysis Using Calibration Graph Method"]
[null,null,null,"Sommario/riassunto","There has been significant expansion in the application of atomic spectrographic techniques in recent years, which has brought with it the need to provide more flexible methods to a wider range of samples, particularly non-aqueous samples. This book compares the traditional and improved methods in the analysis of non-aqueous samples for elemental analyses by atomic emission spectroscopic methods whilst describing procedures that will attempt to improve sample preparation methods."]