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[null,"1.","Record Nr.",null,"UNINA9910144406903321"]
[null,null,"Autore",null,"Hübschmann Hans-Joachim"]
[null,null,"Titolo",null,"Handbook of GC/MS : fundamentals and applications / / Hans-Joachim Hübschmann"]
[null,null,"Pubbl/distr/stampa",null,"Weinheim, [Germany] : , : Wiley-VCH Verlag GmbH & Co. KGaA, , 2009"]
[{"$nulls":4},"©2009"]
[null,null,"ISBN",null,"1-282-02171-0"]
[{"$nulls":4},"9786612021718"]
[{"$nulls":4},"3-527-62521-6"]
[{"$nulls":4},"3-527-62522-4"]
[null,null,"Edizione",null,"[2nd ed.]"]
[null,null,"Descrizione fisica",null,"1 online resource (739 p.)"]
[null,null,"Disciplina",null,"543.85"]
[{"$nulls":4},"543/.85"]
[null,null,"Soggetti",null,"Gas chromatography"]
[{"$nulls":4},"Mass spectrometry"]
[null,null,"Lingua di pubblicazione",null,"Inglese"]
[null,null,"Formato",null,"Materiale a stampa"]
[null,null,null,"Livello bibliografico","Monografia"]
[null,null,null,"Note generali","Description based upon print version of record."]
[null,null,null,"Nota di bibliografia","Includes bibliographical references at the end of each chapters and index."]
[null,null,"Nota di contenuto",null,"Handbook of GC/MS; Foreword; Preface to the Second Edition; Preface to the First Edition; Contents; 1 Introduction; 2 Fundamentals; 2.1 Sample Preparation; 2.1.1 Solid Phase Extraction; 2.1.1.1 Solid Phase Microextraction; 2.1.2 Supercritical Fluid Extraction; 2.1.3 Pressurized Fluid Extraction; 2.1.4 Online Liquid Chromatography Clean-up; 2.1.5 Headspace Techniques; 2.1.5.1 Static Headspace Technique; 2.1.5.2 Dynamic Headspace Technique (Purge and Trap); 2.1.5.3 Headspace versus Purge and Trap; 2.1.6 Adsorptive Enrichment and Thermodesorption; 2.1.6.1 Sample Collection; 2.1.6.2 Calibration"]
[{"$nulls":4},"2.2.3.4 Cold Injection Systems2.2.3.5 Injection Volumes; 2.2.3.6 On-column Injection; 2.2.3.7 Cryofocusing; 2.2.4 Capillary Columns; 2.2.4.1 Sample Capacity; 2.2.4.2 Internal Diameter; 2.2.4.3 Film Thickness; 2.2.4.4 Column Length; 2.2.4.5 Adjusting the Carrier Gas Flow; 2.2.4.6 Properties of Stationary Phases; 2.2.5 Chromatography Parameters; 2.2.5.1 The Chromatogram and its Meaning; 2.2.5.2 Capacity Factor k ́; 2.2.5.3 Chromatographic Resolution; 2.2.5.4 Factors Affecting the Resolution; 2.2.5.5 Maximum Sample Capacity; 2.2.5.6 Peak Symmetry; 2.2.5.7 Optimisation of Flow"]
[{"$nulls":4},"2.2.6 Classical Detectors for GC/MS Systems2.2.6.1 FID; 2.2.6.2 NPD; "]
[{"$nulls":4},"2.2.6.3 ECD; 2.2.6.4 PID; 2.2.6.5 ELCD; 2.2.6.6 FPD; 2.2.6.7 PDD; 2.2.6.8 Connection of Classical Detectors Parallel to the Mass Spectrometer; 2.3 Mass Spectrometry; 2.3.1 Resolving Power and Resolution in Mass Spectrometry; 2.3.1.1 High Resolution; 2.3.1.2 Unit Mass Resolution; 2.3.1.3 High and Low Resolution in the Case of Dioxin Analysis; 2.3.2 Time-of-Flight Analyser; 2.3.3 Isotope Ratio Monitoring GC/MS; 2.3.4 Ionisation Procedures; 2.3.4.1 Electron Impact Ionisation; 2.3.4.2 Chemical Ionisation"]
[{"$nulls":4},"2.3.5 Measuring Techniques in GC/MS2.3.5.1 Detection of the Complete Spectrum (Full Scan); 2.3.5.2 Recording Individual Masses (SIM/MID); 2.3.5.3 High Resolution Accurate Mass MID Data Acquisition; 2.3.6 MS/MS -Tandem Mass Spectrometry; 2.3.7 Mass Calibration; 2.4 Special Aspects of GC/MS Coupling; 2.4.1 Vacuum Systems; 2.4.2 GC/MS Interface Solutions; 2.4.2.1 Open Split Coupling; 2.4.2.2 Direct Coupling; 2.4.2.3 Separator Techniques; References for Chapter 2; 3 Evaluation of GC/MS Analyses; 3.1 Display of Chromatograms; 3.1.1 Total Ion Current Chromatograms; 3.1.2 Mass Chromatograms"]
[{"$nulls":4},"3.2 Substance Identification"]
[null,null,null,"Sommario/riassunto","This is the first comprehensive reference work for GC/MS now in its second edition.It offers broad coverage, from sample preparation to the evaluation of MS-Data, including library searches. Fundamentals, techniques, and applications are described.A large part of the book is devoted to numerous examples for GC/MS-applications in environmental, food, pharmaceutical and clinical analysis. These proven examples come from the daily practice of various laboratories.The book also features a glossary of terms and a substance index that helps the reader to find information for his particul"]
[null,"2.","Record Nr.",null,"UNINA9910346691803321"]
[null,null,"Autore",null,"Belyakov Andrey"]
[null,null,"Titolo",null,"Microstructure and Mechanical Properties of Structural Metals and Alloys / Andrey Belyakov"]
[null,null,"Pubbl/distr/stampa",null,"MDPI - Multidisciplinary Digital Publishing Institute, 2019"]
[{"$nulls":4},"Basel, Switzerland : , : MDPI, , 2019"]
[null,null,"ISBN",null,"9783038975069"]
[{"$nulls":4},"3038975060"]
[null,null,"Descrizione fisica",null,"1 electronic resource (272 p.)"]
[null,null,"Soggetti",null,"Technology: general issues"]
[null,null,"Lingua di pubblicazione",null,"Inglese"]
[null,null,"Formato",null,"Materiale a stampa"]
[null,null,null,"Livello bibliografico","Monografia"]
[null,null,null,"Sommario/riassunto","The papers collected in this special issue clearly reflect the modern research trends in materials science. These fields of specific attention are high-Mn TWIP steels, high-Cr heat resistant steels, aluminum alloys, ultrafine grained materials including those developed by severe plastic deformation, and high-entropy alloys. The major portion of the collected papers is focused on the mechanisms of microstructure evolution and the mechanical properties of metallic materials subjected to various thermo-mechanical, deformation or heat treatments. Another large portion of the studies is aimed on the elaboration of alloying design of advanced steels and alloys. The changes in phase content, transformation and particle precipitation and their effect on the properties are also broadly presented in this collection, including the microstructure/property changes caused by irradiation."]