LEADER 01508nam 2200349Ia 450 001 996385574203316 005 20200824132315.0 035 $a(CKB)4940000000079333 035 $a(EEBO)2240851793 035 $a(OCoLC)ocm12877600e 035 $a(OCoLC)12877600 035 $a(EXLCZ)994940000000079333 100 $a19851206d1664 uy | 101 0 $aeng 135 $aurbn||||a|bb| 200 10$aDon Juan Lamberto, or, A comical history of our late times$b[electronic resource] $ewherein the subtil contrivances, arch rogueries, and villainous treasons of the late notorious rebels, under several feigned names are jovially discovered, and to the very life displayed : in two parts /$fby Montelion, Knight of the Oracle, &c 205 $aThe third edition corrected. 210 $aLondon $cPrinted for Henry Marsh ...$d1664 215 $a[87] p. $cill. (woodcut) 300 $aAttributed also to John Phillips by Halkett and Laing, although DNB claims it to be "inferior to Phillips's acknowledged work, and ... doubtless from the pen of Thomas Flatman." cf. DNB XV, p. 1092. 300 $aReproduction of original in Huntington Library. 330 $aeebo-0113 700 $aFlatman$b Thomas$f1637-1688.$01003830 701 $aPhillips$b John$f1631-1706.$01004007 801 0$bEAA 801 1$bEAA 801 2$bm/c 801 2$bWaOLN 906 $aBOOK 912 $a996385574203316 996 $aDon Juan Lamberto: or, A comical history of our late times$92403740 997 $aUNISA LEADER 05236nam 2200649 450 001 9910830914103321 005 20230721003732.0 010 $a1-281-94021-6 010 $a9786611940218 010 $a0-470-99828-8 010 $a0-470-99829-6 035 $a(CKB)1000000000555964 035 $a(EBL)366781 035 $a(OCoLC)298943873 035 $a(SSID)ssj0000225573 035 $a(PQKBManifestationID)11208790 035 $a(PQKBTitleCode)TC0000225573 035 $a(PQKBWorkID)10233212 035 $a(PQKB)10176239 035 $a(MiAaPQ)EBC366781 035 $a(EXLCZ)991000000000555964 100 $a20160818h20082008 uy 0 101 0 $aeng 135 $aur|n|---||||| 181 $ctxt 182 $cc 183 $acr 200 12$aA practical approach to quantitative metal analysis of organic matrices /$fMartin C. Brennan 210 1$aWest Sussex, England :$cWiley,$d2008. 210 4$dİ2008 215 $a1 online resource (278 p.) 300 $aDescription based upon print version of record. 311 $a0-470-03197-2 320 $aIncludes bibliographical references and index. 327 $aA Practical Approach to Quantitative Metal Analysis of Organic Matrices; Contents; Preface; Biography; Acknowledgements; 1 A Practical Approach to Quantitative Metal Analysis of Organic Matrices Using ICP-OES; 1.1 Introduction and Basic Overview; 1.2 Schematic Representation of the Energies Generated by Atomic Spectroscopic Methods; 1.3 Excitation Energy (Quantum Theory and Atomic Spectra); 1.4 Ionisation Energy and Number of Excited Atoms; 1.5 Width of Atomic Lines; 1.5.1 Natural Broadening; 1.5.2 Doppler Broadening; 1.5.3 Lorentzian Broadening or Pressure Broadening 327 $a1.5.4 Holtsmark Broadening or Resonance Broadening1.5.5 Field Broadening or Stark Broadening; 1.5.6 Self-Absorption and Self-Reversal Broadening; 1.6 Brief Summary of Atomic Spectroscopic Techniques Used for Elemental Analysis; 1.6.1 The Atomic Absorption Spectrophotometer; 1.6.2 Atomic Fluorescence Spectroscopy; 1.6.3 Direct Current Plasma Optical Emission Spectrometry (DCP-OES); 1.6.4 Microwave Induced Plasma (MIP); 1.6.5 Glow Discharge Optical Emission Spectrometry (GD-OES); 1.6.6 Inductively Coupled Plasma Optical Emission Spectrometry (ICP-OES) 327 $a1.7 Summary: Applications of Atomic SpectroscopyReferences; 2 Instrumentations Associated with Atomic Spectroscopy; 2.1 Instrumentation; 2.2 Types of Plasma Sources; 2.2.1 Direct Current Plasma Atomic Emission Spectrograph; 2.2.2 Microwave Induced Plasma; 2.2.3 Optical Emission Spectroscopy; 2.3 Sample Introduction Systems; 2.3.1 Mechanical Transfer of Sample/Standards Using Peristaltic Pump, Pressure Valves, Motorised Syringes, etc.; 2.3.2 Nebulisers; 2.3.3 Brief Outline of Atomic Spectroscopy Hyphenated Systems; 2.4 Spray Chambers; 2.5 ICP-OES Torches; 2.6 Optics; 2.6.1 Grating Orders 327 $a2.7 Signal Detectors2.7.1 Photomultiplier Tubes; 2.7.2 Charge Coupled Devices; References; 3 Methodologies of Metal Analysis of Organic Matrices Using ICP-OES; 3.1 Sample Preparation Techniques and Methods of Analysis; 3.2 Defining Goals; 3.3 Steps in Chemical Analytical Protocol; 3.4 Sampling and its Importance; 3.5 Sample Preparation Methods; 3.5.1 Direct Analysis of Organic Solutions; 3.5.2 Sample Dissolution; 3.5.3 Chemical Extraction of Metals from Organic Matrices; 3.5.4 Dry Ashing without Retaining Aids; 3.5.5 Dry Ashing with Retaining Aids; 3.5.6 Acid Digestion Using Microwave Oven 327 $a3.5.7 Oxygen Bomb Flask Combustion (Low Pressure)3.5.8 High Pressure Oxygen Combustion; 3.5.9 Sample Preparation Using Fusion Methods; 3.5.10 Analysis Using Slurry Solution Method; 3.5.11 Sample Preparation Using Leaching Method; 3.5.12 Sample Preparation Using a UV Digester; 3.6 Non-Spectral Corrections Using ICP-OES; 3.6.1 Effect of Solvents on ICP-OES; 3.6.2 Effect of Viscosity on Signal Response; 3.6.3 Comparison of Nebulisation Efficiency of Solvents Using ICP-OES; 3.6.4 Choice of Carrier Liquid; 3.7 Methodology of Measurement; 3.7.1 Choice of Standard Materials 327 $a3.7.2 Quantitative Analysis Using Calibration Graph Method 330 $aThere has been significant expansion in the application of atomic spectrographic techniques in recent years, which has brought with it the need to provide more flexible methods to a wider range of samples, particularly non-aqueous samples. This book compares the traditional and improved methods in the analysis of non-aqueous samples for elemental analyses by atomic emission spectroscopic methods whilst describing procedures that will attempt to improve sample preparation methods. 606 $aAtomic emission spectroscopy 606 $aMetals$xAnalysis 606 $aChemistry, Organic 615 0$aAtomic emission spectroscopy. 615 0$aMetals$xAnalysis. 615 0$aChemistry, Organic. 676 $a543.52 676 $a543.6 700 $aBrennan$b Martin$f1943-$01682451 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910830914103321 996 $aA practical approach to quantitative metal analysis of organic matrices$94052574 997 $aUNINA