LEADER 05354nam 2200661Ia 450 001 996197603703316 005 20230422044830.0 010 $a1-281-76381-0 010 $a9786611763817 010 $a3-527-61176-2 010 $a3-527-61175-4 035 $a(CKB)1000000000376070 035 $a(EBL)482319 035 $a(OCoLC)261404611 035 $a(SSID)ssj0000240564 035 $a(PQKBManifestationID)11208765 035 $a(PQKBTitleCode)TC0000240564 035 $a(PQKBWorkID)10266188 035 $a(PQKB)10750800 035 $a(MiAaPQ)EBC482319 035 $a(iGPub)WILEYB0018691 035 $a(EXLCZ)991000000000376070 100 $a19980921d1999 uy 0 101 0 $aeng 135 $aur|n|---||||| 181 $ctxt 182 $cc 183 $acr 200 10$aSafety assessment for chemical processes$b[electronic resource] /$fJo?rg Steinbach 205 $a1st ed. 210 $aWeinheim ;$aNew York $cWiley-VCH$dc1999 215 $a1 online resource (321 p.) 300 $aDescription based upon print version of record. 311 $a3-527-28852-X 320 $aIncludes bibliographical references (p. [295]-299) and index. 327 $aSafety Assessment for Chemical Processes; Contents; 1 Basic Terminology in Loss Prevention; 1.1 General Safety Terms; 1.1.1 Hazard Potential and Expectable Damage; 1.1.2 Risk; 1.2 Basic Terminology for Plant/Process Operation; 2 Procedure for Process Safety Investigations; 2.1 Scope of Investigation in its Dependence on the Process Development Stage; 2.2 Definition of Significant Plant or Process Modifications; 2.3 Types of investigations Corresponding to the Life Cycle Progress; 3 Test Methods For The Thermal Stability Assessment Of Substances And Mixtures 327 $a3.1 Theoretical Considerations For Laboratory Processes3.2 Screening -Methods For kg-Scale Processes; 3.2.1 Difference Thermal Analysis (DTA) and Differential Scanning Calorimetry (DSC); 3.2.2 The Carius Tube Test; 3.2.3 The Miniautoclave Test; 3.2.4 Open Cup Measuring Techniques; 3.3 Further Basic Assessment Test Methods For kg-Scale Processes; 3.3.1 The Burning Test For Solids; 3.3.2 Test On The Ignitability Of Solids; 3.3.3 Flash-point of Liquids; 3.3.4 Ignition Temperature of Liquids; 3.4 Partial Testing for Explosion Risk; 3.5 Deflagration Testing 327 $a3.6 Assignment of Testing Methods to Process Unit Operations for the kg-Scale3.7 References to Other Problems and Test Methods; 4 Methods for the Investigation and Assessment of Chemical Reactions; 4.1 Reaction Engineering Fundamentals; 4.1.1 Stoichiometry and Extent of Reaction; 4.1.2 Reaction Rate; 4.1.3 Ideal Reactor Models; 4.1.4 Introduction of Characteristic Numbers; 4.1.5 Mass Balances of the Ideal Reactors; 4.1.6 Sample Solutions for Isothermal Operating Conditions; 4.1.7 The General Heat Balance of Cooled Ideal Reactors; 4.2 The Heat Explosion Theory 327 $a4.3 Investigation And Assessment Of Normal Operating Conditions4.3.1 The Safety Technical Assessment Of Normal Operating Conditions; 4.3.1.1 Safe Normal Operation Of The Cooled CSTR; 4.3.1.2 Safe Normal Operation of the Cooled PFTR; 4.3.1.3 Safe Normal Operation of Cooled Batch Reactors; 4.3.1.4 Safe Normal Operation of the Cooled Semibatch Reactor; 4.3.2 Special Problems In The Assessment Of Normal Operating Conditions; 4.3.2.1 Safe Normal Operation of Reactions Under Reflux; 4.3.2.2 Safe Normal Operation of Polymerization Reactions 327 $a4.3.3 Investigation Methods for the Characterization of Normal Operating Conditions4.3.3.1 Fundamentals of Thermokinetics; 4.3.3.2 Reaction Calorimetry; 4.3.3.3 Thermokinetic Evaluation of Reaction Calorimetric Measurements; 4.4 investigation And Assessment Of Upset Operating Conditions; 4.4.1 The Safety Technical Assessment Of The Process Design For Upset Operating Conditions; 4.4.1.1 Assessment Of The CSTR Under Upset Operating Conditions; 4.4.1.2 The Assessment Of The SBR Under Upset Operating Conditions; 4.4.1.3 The Assessment Of The BR Under Upset Operating Conditions 327 $a4.4.2 Methods For The Investigation Of Upset Operating Conditions 330 $aIn spite of the good safety records of chemical plants many people regard chemical production as dangerous because of a few major accidents that have occurred.A knowledge of at least the fundamentals of chemical safety technology is indispensable for chemists and engineers working in chemical industry. The increasingly stringent legal and administrative requirements can only be answered by more highly qualified employees.This book combines the author's experience of 15 years of research in the field of chemical safety and 10 years in the chemical industry. It provides newcomers 606 $aChemical plants$xSafety measures 606 $aChemical engineering$xSafety measures 606 $aHazardous substances$xSafety measures 615 0$aChemical plants$xSafety measures. 615 0$aChemical engineering$xSafety measures. 615 0$aHazardous substances$xSafety measures. 676 $a660.0684 676 $a660.2804 700 $aSteinbach$b Jo?rg$023101 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a996197603703316 996 $aSafety Assessment for Chemical Processes$9328227 997 $aUNISA