LEADER 01349nam 2200349 n 450 001 996384736303316 005 20221102113311.0 035 $a(CKB)4940000000070711 035 $a(EEBO)2240939369 035 $a(UnM)9928211400971 035 $a(UnM)99832976 035 $a(EXLCZ)994940000000070711 100 $a19951220d1682 uy | 101 0 $aeng 135 $aurbn||||a|bb| 200 14$aThe Holy Bible$b[electronic resource] $econtaining the old Testament and the New newly translated out of the original tongues and with the former translations diligently compared and revised by his Majesties speciall command Appointed to be read in churches 210 $aCambridge $cprinted by John Hayes printer to the Vniversitie$d1682 215 $a[1180+] p 300 $aThe title page is engraved. 300 $aSignatures: AČ B-2R 2S? 2T-3A 3B? 3C-3O 3P? a-o p?+. 300 $aWith an identical title page as the Huntington Library copy (smk 34129), but with a different setting of text. 300 $aCopy lacks New Testament. 300 $aReproduction of the original in the Guildhall Library, London. 330 $aeebo-0059 801 0$bCu-RivES 801 1$bCu-RivES 801 2$bCStRLIN 801 2$bWaOLN 906 $aBOOK 912 $a996384736303316 996 $aHoly Bible$9184530 997 $aUNISA LEADER 05724nam 22007454a 450 001 9911018781403321 005 20200520144314.0 010 $a9786611087890 010 $a9781281087898 010 $a1281087890 010 $a9783527609444 010 $a352760944X 010 $a9783527609307 010 $a352760930X 035 $a(CKB)1000000000327285 035 $a(EBL)481303 035 $a(SSID)ssj0000231057 035 $a(PQKBManifestationID)11194868 035 $a(PQKBTitleCode)TC0000231057 035 $a(PQKBWorkID)10198571 035 $a(PQKB)11053755 035 $a(MiAaPQ)EBC481303 035 $a(PPN)249608731 035 $a(OCoLC)86189676 035 $a(Perlego)2766849 035 $a(EXLCZ)991000000000327285 100 $a20070906d2007 uy 0 101 0 $aeng 135 $aur|n|---||||| 181 $ctxt 182 $cc 183 $acr 200 10$aQuality assurance in analytical chemistry $eapplications in environmental, food, and materials analysis, biotechnology, and medical engineering /$fWerner Funk, Vera Dammann, Gerhild Donnevert 205 $a2nd ed. 210 $aWeinheim $cWiley-VCH$dc2007 215 $a1 online resource (303 p.) 300 $aTranslated from the German. 311 08$a9783527311149 311 08$a3527311149 320 $aIncludes bibliographical references (p. 209-217) and index. 327 $aQuality Assurance in Analytical Chemistry; Contents; Preface to the Second Edition; Preface to the First Edition; List of Symbols; 0 Introduction; 0.1 General Differentiation of Analytical Processes; 0.2 Quality of Analytical Processes and Results; 0.3 The System of Analytical Quality Assurance; 0.4 The Four-Phase Model of Analytical Quality Assurance; 1 Phase I: Establishing a New Analytical Procedure; 1.1 Introduction; 1.1.1 Objectives of Phase I; 1.1.2 When Are Characteristic Data Obtained?; 1.1.3 The Progression of Phase I; 1.1.4 Results of Phase I; Statistical Data 327 $a1.2 Calibration of the Fundamental Analytical Procedure (Fundamental Calibration)1.2.1 Establishment of an Analytical Range; 1.2.2 Preparation of Standard Samples; 1.2.3 Determination of the Calibration Function and Process Data; 1.2.3.1 Process Data for the Linear Calibration Function; 1.2.3.2 Process Data for the Second-Order Calibration Function; 1.2.3.3 Calculating Analytical Results with the Aid of the Calibration Function; 1.2.4 Verification of the Fundamental Calibration; 1.2.4.1 Verification of Linearity; 1.2.4.2 Verification of Precision; 1.3 Analyses at Very Low Concentrations 327 $a1.3.1 Decision Limit [34, 120, 132]1.3.2 Determining the Minimum Detectable Value [34, 120]; 1.3.2.1 Minimum Detectable Value, Determined Using the Distribution of Blank Values; 1.3.2.2 Minimum Detectable Value, Obtained Using the Calibration Function; 1.3.3 Limit of Quantification [34]; 1.3.4 Quick Estimation; 1.3.5 Estimation of the Decision Limit and Limit of Quantification Using the S/N Ratio; 1.4 Validation of Individual Process Steps and Examination of Matrix Influences; 1.4.1 Systematic Errors; 1.4.1.1 Constant Systematic Errors, Additive Deviations 327 $a1.4.1.2 Proportional Systematic Errors, Multiplicative Deviations1.4.2 Establishment and Assessment of the Recovery Function; 1.4.2.1 Prerequisites for the Interpretation of the Recovery Function; 1.4.2.2 Testing for Systematic Errors; 1.4.3 Application of the Recovery Function; 1.4.3.1 Checking Individual Process Steps; 1.4.3.2 Determination of the Recovery Function to Prove the Influence of a Matrix; 1.5 Additional Statistical Methods; 1.6 Use of Internal Standards [50]; 1.6.1 Definition, Purpose; 1.6.2 Conditions and Limitations of the Use of Internal Standards; 1.6.3 Procedure 327 $a1.7 Preparing for Routine Analysis1.7.1 Examination of the Time Dependency of Measured Values; 1.7.1.1 Comparison of the "Within Batch" Standard Deviation (s(w)) with the "Between Batches" Standard Deviation (s(b)) [215]; 1.7.1.2 Determining the Need for Daily Adjustment of Analytical Equipment; 1.7.1.3 The Trend Test; 1.8 Summary of the Results of Phase I (Process Development): Documentation; 2 Phase II: An Analytical Process Becomes Routine; Preparative Quality Assurance; 2.1 Introduction; 2.1.1 Objective of Phase II; 2.1.2 Execution of Phase II; 2.1.3 Progression of Phase II 327 $a2.1.4 Results of Phase II 330 $aThis best-selling title both in German and English is now enhanced by a new chapter on the important topical subject of measurement uncertainty, plus a CD-ROM with interactive examples in the form of Excel-spreadsheets. These allow readers to gain an even better comprehension of the statistical procedures for quality assurance while also incorporating their own data.Following an introduction, the text goes on to elucidate the 4-phase model of analytical quality assurance: establishing a new analytical process, preparative quality assurance, routine quality assurance and external analytical 606 $aChemical laboratories$xQuality control 606 $aAnalytical chemistry$xQuality control 606 $aAnalytical chemistry$xTechnique 615 0$aChemical laboratories$xQuality control. 615 0$aAnalytical chemistry$xQuality control. 615 0$aAnalytical chemistry$xTechnique. 676 $a540 676 $a543.0685 700 $aFunk$b Werner$f1944-1996.$01841636 701 $aDammann$b Vera$01839961 701 $aDonnevert$b Gerhild$01839962 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9911018781403321 996 $aQuality assurance in analytical chemistry$94421452 997 $aUNINA