LEADER 04855nam 22005655 450 001 9910958882403321 005 20250725091805.0 010 $a94-011-1324-6 024 7 $a10.1007/978-94-011-1324-3 035 $a(CKB)3400000000121728 035 $a(SSID)ssj0000933281 035 $a(PQKBManifestationID)11508105 035 $a(PQKBTitleCode)TC0000933281 035 $a(PQKBWorkID)10890862 035 $a(PQKB)10505826 035 $a(DE-He213)978-94-011-1324-3 035 $a(MiAaPQ)EBC3566196 035 $a(PPN)237956268 035 $a(EXLCZ)993400000000121728 100 $a20121227d1995 u| 0 101 0 $aeng 135 $aurnn#008mamaa 181 $ctxt 182 $cc 183 $acr 200 10$aThermal Methods of Analysis $ePrinciples, Applications and Problems /$fby P.J. Haines 205 $a1st ed. 1995. 210 1$aDordrecht :$cSpringer Netherlands :$cImprint: Springer,$d1995. 215 $a1 online resource (XII, 286 p.) 300 $aBibliographic Level Mode of Issuance: Monograph 311 08$a0-7514-0050-5 327 $a1 Introduction to thermal methods -- 1.1 Introduction -- 1.2 Historical development -- 1.3 Definitions -- 1.4 Computers and thermal methods -- 1.5 Factors affecting thermal analysis results -- 1.6 Simultaneous and complementary techniques -- 1.7 Problems -- References -- General Bibliography -- 2 Thermogravimetry -- 2.1 Introduction -- 2.2 Historical -- 2.3 Definition of thermogravimetry -- 2.4 Apparatus -- 2.5 Kinetics of reactions -- 2.6 Applications of thermogravimetry -- 2.7 Controlled rate thermogravimetry and Hi-Res? TGA -- 2.8 Problems -- References -- 3 Differential thermal analysis and differential scanning calorimetry -- 3.1 Introduction -- 3.2 Historical -- 3.3 Definitions -- 3.4 Apparatus -- 3.5 Theory of DTA and DSC -- 3.6 Heat flux DSC -- 3.7 Power-compensated DSC -- 3.8 Calibration -- 3.9 Applications -- 3.11 Problems -- References -- 4 Thermomechanical, dynamic mechanical and associated methods -- 4.1 Introduction -- 4.2 Definitions -- 4.3 Thermomechanical analysis -- 4.4 Dynamic mechanical analysis -- 4.5Dielectric thermal analysis -- 4.6 Thermally stimulated current analysis and relaxation map analysis -- 4.7 Problems -- References -- 5 Simultaneous techniques and product analysis -- 5.1 Introduction -- 5.2 Simultaneous thermal analysis -- 5.3 Evolved gas analysis -- 5.4 Detection and identification of evolved gases -- 5.5 Infrared and simultaneous TA-infrared -- 5.6 Infrared product analysis -- 5.7 Thermomicroscopy -- 5.8 X-ray methods -- 5.9 Electron microscopy and associated techniques -- 5.10 Conclusion -- 5.11 Less common thermal analysis techniques -- 5.12 Problems -- References -- 6 Problem solving and applications of thermal methods -- List of examples -- Problems/Solutions -- 6.1 Inorganic materials -- 6.2 Polymeric materials -- 6.3 Fine chemicals and pharmaceuticals -- 6.4 Other materials -- References -- Appendix: Solutions to problems in Chapters 1-5. 330 $aThe wide range of applications of thermal methods of analysis in measuring physical properties, studying chemical reactions and determining the thermal behaviour of samples is of interest to academics and to industry. These applications prompted the writing of this book, in the hope that the descriptions, explanations and examples given would be of help to the analyst and would stimulate the investigation of other thermal techniques. Thermal studies are a fascinating means of examining the samples and the problems brought to us by colleagues, students and clients. If time allows, watching crystals change on a hot-stage microscope, or measuring the properties and changes on a DSC or TG or any thermal instrument can be a rewarding activity, besides providing valuable analytical information. This book started from a series of lectures delivered at Kingston University and at meetings of the Thermal Methods Group of the United Kingdom. The collaboration and information supplied to all the contribu­ tors by colleagues and instrument manufacturers is most gratefully ack­ nowledged, as are the valuable contributions made at meetings of the International Confederation for Thermal Analysis and Calorimetry (ICT AC) and at the European Symposia on Thermal Analysis and Calorimetry (ESTAC). 606 $aAnalytical chemistry 606 $aChemistry 606 $aAnalytical Chemistry 606 $aChemistry 615 0$aAnalytical chemistry. 615 0$aChemistry. 615 14$aAnalytical Chemistry. 615 24$aChemistry. 676 $a543 700 $aHaines$b P.J$4aut$4http://id.loc.gov/vocabulary/relators/aut$0314643 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910958882403321 996 $aThermal methods of analysis$9192740 997 $aUNINA