LEADER 04810nam 2200661Ia 450 001 9910876533403321 005 20200520144314.0 010 $a1-282-68755-7 010 $a9786612687556 010 $a0-470-55292-1 010 $a0-470-55291-3 035 $a(CKB)2550000000005937 035 $a(EBL)477765 035 $a(OCoLC)501316329 035 $a(SSID)ssj0000340174 035 $a(PQKBManifestationID)11274422 035 $a(PQKBTitleCode)TC0000340174 035 $a(PQKBWorkID)10388006 035 $a(PQKB)10464756 035 $a(MiAaPQ)EBC477765 035 $a(PPN)156422425 035 $a(EXLCZ)992550000000005937 100 $a20090513d2010 uy 0 101 0 $aeng 135 $aur|n|---||||| 181 $ctxt 182 $cc 183 $acr 200 10$aMass spectrometry in grape and wine chemistry /$fRiccardo Flamini, Pietro Traldi 210 $aHoboken, NJ $cWiley$dc2010 215 $a1 online resource (365 p.) 225 1 $aWiley-Interscience series in mass spectrometry 300 $aDescription based upon print version of record. 311 $a0-470-39247-9 320 $aIncludes bibliographical references and index. 327 $aMASS SPECTROMETRY IN GRAPE AND WINE CHEMISTRY; CONTENTS; PREFACE; ACKNOWLEDGMENTS; Introduction; PART I MASS SPECTROMETRY; 1 Ionization Methods; 1.1 Electrospray Ionization; 1.1.1 The Taylor Cone; 1.1.2 Some Further Considerations; 1.1.3 Positive- and Negative-Ion Modes; 1.1.4 Micro- and Nano-LC/ESI/MS; 1.2 Atmospheric Pressure Chemical Ionization; 1.3 Atmospheric Pressure Photoionization; 1.4 Surface-Activated Chemical Ionization; 1.5 Matrix-Assisted Laser Desorption-Ionization; References; 2 Mass Analyzers and Accurate Mass Measurements; 2.1 Double-Focusing Mass Analyzers 327 $a2.2 Quadrupole Mass Filters2.3 Ion Traps; 2.3.1 Three-Dimensional Quadrupole Ion Traps; 2.3.2 Linear Ion Traps; 2.3.3 Digital Ion Trap; 2.3.4 Fourier Transform-Ion Cyclotron Resonance; 2.3.5 Orbitrap; 2.4 Time of Flight; References; 3 MS/MS Methodologies; 3.1 Triple Quadrupole; 3.1.1 Quadrupole Ion Traps; 3.1.2 Linear Ion Traps; 3.1.3 The MS/MS by a Digital Ion Trap; 3.1.4 The FT-MS (ICR and Orbitrap) for MS/MS Studies; 3.2 The Q-TOF; 3.3 The MALDI TOF-TOF; References; PART II APPLICATIONS OF MASS SPECTROMETRY IN GRAPE AND WINE CHEMISTRY 327 $a4 Grape Aroma Compounds: Terpenes, C(13)-Norisoprenoids, Benzene Compounds, and 3-Alkyl-2-Methoxypyrazines4.1 Introduction; 4.2 The SPE-GC/MS of Terpenes, Norisoprenoids, and Benzenoids; 4.2.1 Preparation of Grape Sample; 4.2.2 Analysis of Free Compounds; 4.2.3 Analysis of Glycoside Compounds; 4.2.4 Analysis of Compounds Formed by Acid Hydrolysis; 4.2.5 GC-MS; 4.3 The SPME-GC/MS of Methoxypyrazines in Juice and Wine; References; 5 Volatile and Aroma Compounds in Wines; 5.1 Higher Alcohols and Esters Formed from Yeasts; 5.1.1 Introduction 327 $a5.1.2 SPME-GC/MS Analysis of Higher Alcohols and Esters5.2 Volatile Sulfur Compounds in Wines; 5.2.1 Introduction; 5.2.2 The HS-SPME-GC/MS Analysis of Volatile Sulfur Compounds; 5.2.3 HS-SPME-GC/MS Analysis of 3-MH and 3-MHA; 5.2.4 Analysis of Wine Mercaptans by Synthesis of Pentafluorobenzyl Derivatives; 5.3 Carbonyl Compounds in Wines and Distillates; 5.3.1 Introduction; 5.3.2 The GC/MS Analysis of Wine Carbonyl Compounds by Synthesis of PFBOA Derivatives; 5.3.3 HS-SPME-GC/MS of PFBOA Derivatives; 5.4 Ethyl and Vinyl Phenols in Wines; 5.4.1 Introduction; 5.4.2 Analysis of Ethylphenols 327 $a8 Compounds Responsible for Wine Defects 330 $aA concise, up-to-date overview of the applications of mass spectrometry To be able to estimate the potentiality of grapes and how it may be transferred into wine is key to grasping enological chemistry. Nowadays, mass spectrometry is a crucial aspect in ensuring the production, the quality, and the safety of grape, wine, and grape derivative products. Mass Spectrometry in Grape and Wine Chemistry examines in depth the relationship between the high structural identification power of mass spectrometry techniques and the chemistry of grapes and wine. The text is divided into two parts. 410 0$aWiley-Interscience series on mass spectrometry. 606 $aWine and wine making$xAnalysis 606 $aWine and wine making$xChemistry 606 $aMass spectrometry 615 0$aWine and wine making$xAnalysis. 615 0$aWine and wine making$xChemistry. 615 0$aMass spectrometry. 676 $a663.200284 700 $aFlamini$b Riccardo$0512090 701 $aTraldi$b Pietro$f1948-$0512091 801 0$bMiAaPQ 801 1$bMiAaPQ 801 2$bMiAaPQ 906 $aBOOK 912 $a9910876533403321 996 $aMass spectrometry in grape and wine chemistry$9765014 997 $aUNINA